CN106555344A - A kind of colouring method of polyester-cotton blend interweaving product large red - Google Patents
A kind of colouring method of polyester-cotton blend interweaving product large red Download PDFInfo
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- CN106555344A CN106555344A CN201611096210.0A CN201611096210A CN106555344A CN 106555344 A CN106555344 A CN 106555344A CN 201611096210 A CN201611096210 A CN 201611096210A CN 106555344 A CN106555344 A CN 106555344A
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- 229920000742 Cotton Polymers 0.000 title claims abstract description 58
- 239000000203 mixture Substances 0.000 title claims abstract description 34
- 238000000034 method Methods 0.000 title claims abstract description 28
- 238000004040 coloring Methods 0.000 title claims abstract description 15
- 239000000975 dye Substances 0.000 claims abstract description 69
- 238000004043 dyeing Methods 0.000 claims abstract description 57
- 239000003518 caustics Substances 0.000 claims abstract description 43
- 238000005406 washing Methods 0.000 claims abstract description 37
- 238000010186 staining Methods 0.000 claims abstract description 30
- 238000010792 warming Methods 0.000 claims abstract description 28
- 238000005554 pickling Methods 0.000 claims abstract description 22
- 239000000985 reactive dye Substances 0.000 claims abstract description 15
- 239000000344 soap Substances 0.000 claims abstract description 12
- 238000011210 chromatographic step Methods 0.000 claims abstract description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 71
- GHMLBKRAJCXXBS-UHFFFAOYSA-N resorcinol Chemical compound OC1=CC=CC(O)=C1 GHMLBKRAJCXXBS-UHFFFAOYSA-N 0.000 claims description 21
- 239000002253 acid Substances 0.000 claims description 13
- 238000006386 neutralization reaction Methods 0.000 claims description 13
- 241001584775 Tunga penetrans Species 0.000 claims description 12
- 239000003795 chemical substances by application Substances 0.000 claims description 10
- 238000004587 chromatography analysis Methods 0.000 claims description 7
- 238000003756 stirring Methods 0.000 claims description 5
- 238000010014 continuous dyeing Methods 0.000 claims description 2
- 238000009472 formulation Methods 0.000 claims description 2
- 239000006210 lotion Substances 0.000 claims description 2
- 239000000843 powder Substances 0.000 claims 1
- 239000000835 fiber Substances 0.000 abstract description 17
- 239000008187 granular material Substances 0.000 abstract description 3
- 230000009257 reactivity Effects 0.000 abstract description 3
- 241000219146 Gossypium Species 0.000 description 11
- 230000008859 change Effects 0.000 description 7
- 239000002351 wastewater Substances 0.000 description 7
- 230000000052 comparative effect Effects 0.000 description 6
- 239000004744 fabric Substances 0.000 description 5
- 238000004090 dissolution Methods 0.000 description 4
- 230000008569 process Effects 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 3
- 238000005728 strengthening Methods 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- 238000004140 cleaning Methods 0.000 description 2
- 238000004044 disperse dyeing Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 230000009467 reduction Effects 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000000274 adsorptive effect Effects 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000012769 bulk production Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 239000000986 disperse dye Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000005457 optimization Methods 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 238000012805 post-processing Methods 0.000 description 1
- 238000004045 reactive dyeing Methods 0.000 description 1
- 238000007634 remodeling Methods 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/38—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using reactive dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
- D06P1/67333—Salts or hydroxides
- D06P1/6735—Salts or hydroxides of alkaline or alkaline-earth metals with anions different from those provided for in D06P1/67341
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/82—Textiles which contain different kinds of fibres
- D06P3/8204—Textiles which contain different kinds of fibres fibres of different chemical nature
- D06P3/8223—Textiles which contain different kinds of fibres fibres of different chemical nature mixtures of fibres containing hydroxyl and ester groups
- D06P3/8228—Textiles which contain different kinds of fibres fibres of different chemical nature mixtures of fibres containing hydroxyl and ester groups using one kind of dye
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Coloring (AREA)
Abstract
A kind of colouring method of polyester-cotton blend interweaving product large red, belongs to polyester-cotton blend interweaving product staining technique field.Characterized in that, dyestuff is stirred in secondary cylinder in advance, is changed, without dye granule in chromatography step, dye vat is added, 60 DEG C of constant temperature dyeings is warming up to, is walked twice, Matrii Sulfas Exsiccatus 80g/L tri-, four roads are added in two times, ground caustic 20g/L, seven, eight roads are added in two times, continue 10 road of constant temperature dyeing, soap, washing, pickling, under roll out cylinder.The present invention improves the suction color of cotton fiber, realizes that depth is good, lifting force is high, dye dosage is few by selecting cotton fiber dyeing reactive dye, improves the reactivity of dyestuff and fiber, removes the loose colour of fiber surface, improves color fastness.
Description
Technical field
A kind of colouring method of polyester-cotton blend interweaving product large red, belongs to polyester-cotton blend interweaving product staining technique field.
Background technology
Wide cut polyester-cotton blend intertexture jacquard product large red, it is overflowing with enthusiasm, it is happy celebrating, it is mainly used in making wedding celebration series bed necessaries
External member, it is deep to be welcome by Market Consumer.
Polyester-cotton blend intertexture jacquard product, refers to that warp is polyster fibre, and parallel is pure cotton fiber, and two kinds of fiber interweavings are formed,
Conventional weave specification 100d × 32,s/2 173 × 60, warp are 100d draw textured yarn dty, and parallel is 32s combed cottons plying
Yarn.The big red colouring of polyester-cotton blend intertexture jacquard product, produces in dye jigger, contaminates polyster fibre using disperse dyes High Temperature High Pressure, is commonly called as
" bottoming " color, room temperature dye gigging Dyeing of Cotton Fabric with Reactive Dyes fiber, is commonly called as " chromatography ", be dispersed through/two one-bath two-step process of reactive dye completes.Work
Skill flow process is as follows：High Temperature High Pressure disperse dyeing, reduction cleaning, washing, normal temperature dyeing jigger reactive dyeing, washing, soap
Wash, pickling, last volume.
From bulk production produce reality Analysis of test results, High Temperature High Pressure disperse dyeing, Jing after reduction cleaning, polyster fibre
Preferably, the technical problem underlying for existing is cotton fiber poor color fastness to the color fastness of dyeing, especially washes staining fastness, Ke Huzhi
Amount requires 3 ~ 4 grades, and the fastness of product only has 2 ~ 3 grades sometimes, does not reach quality standard, constrains production development.
The content of the invention
The technical problem to be solved in the present invention is：Overcome the deficiencies in the prior art, there is provided a kind of to improve polyester-cotton blend interweaving product
The colouring method of large red.
The technical solution adopted for the present invention to solve the technical problems is：The dyeing side of the polyester-cotton blend interweaving product large red
Method, it is characterised in that dye formulation is：Dark red RGB1.45%owf ~ the 1.75%owf of Remazol, Remazol orange RGB0.225%owf ~
0.35%owf, Matrii Sulfas Exsiccatus 77g/L ~ 84g/L, ground caustic 17g/L ~ 22g/L, neutralization acid 2.7g/L ~ 3.4g/L；
Comprise the following steps：Dye jigger reactive dye chromatography, warm water are washed, are soaped, washing, pickling and last volume；
The concrete technology of wherein described dye jigger reactive dye chromatography step is：
1）Dyestuff obtains dye solution with 50 DEG C ~ 60 DEG C water dissolutioies in advance in secondary cylinder, staining bath temperature control at 57 DEG C ~ 64 DEG C,
Staining bath adds the 45% ~ 55% of dye solution total amount, stirs, and drives operation together；Add excess dye to drive to run one
Road；
2）3rd road adds the Matrii Sulfas Exsiccatus for accounting for Matrii Sulfas Exsiccatus total amount 45% ~ 55% to run together under 57 DEG C ~ 64 DEG C of constant temperature in staining bath,
4th road adds remaining Matrii Sulfas Exsiccatus operation together；
3）Staining bath temperature is kept in 57 DEG C ~ 64 DEG C two roads of constant temperature dyeing；
4）Continuously add in 7th road staining bath and account for the operation of 45% ~ 55% ground caustic of ground caustic total amount together, the 8th road adds remaining ground caustic
Operation is together；
5）Then continue ten road of continuous dyeing under constant temperature at 57 DEG C ~ 64 DEG C and complete dye jigger reactive dye chromatography step.
The fastness of the cotton fiber dyeing in polyester-cotton blend interweaving product is poor, and main cause one is that the suction color of cotton fiber is poor, to dye
The adsorptive value of material is low；Two is that dye dosage is big, and color depth, dyestuff are close to saturation in the absorption of cotton fiber, the fixation rate with fiber
It is low, loose colour weight；Three is dyeing, post processing is soaped, and effect is poor, and the loose colour of fiber surface is removed and totally do not caused.For affecting product
The above-mentioned factor of color fastness, the present invention pass through the control of dyeing step and process conditions, and dyestuff is abundant in secondary cylinder in advance
Stir, change, without dye granule, add staining bath, constant temperature dyeing after intensification to walk twice, three, four roads add Matrii Sulfas Exsiccatus point two
Secondary addition, seven, eight road ground caustics are added in two times, are continued constant temperature dyeing 10 road, are soaped, and are washed, pickling, under roll out cylinder.Improve
The suction color of cotton fiber, from the good Remazol RGB reactive dye of cotton fiber depth, dyestuff lifting force is high, consumption is few, reduces
Dye dosage, improves the reactivity of dyestuff and fiber, reduces the loose colour of fiber surface, so as to improve color fastness.
Described warm water-washing step is under the conditions of 57 DEG C ~ 64 DEG C to wash twice.Carry out in dye jigger reactive dye chromatography
Specific warm water is washed and is conducive to strengthening color fastness, and keeps the soft of polyester-cotton blend interweaving product.
Described soaps to be warming up to after 92 DEG C ~ 96 DEG C after adding 2.7g/L ~ 3.4g/L soaping agents in water lotion, operation three
Road.Specifically soaped in dye jigger reactive dye chromatography and be conducive to strengthening color fastness, and further removed fiber surface
Loose colour, makes polyester-cotton blend interweaving product colour stable.
Described water-washing step repeats two roads, adds water and be warming up to add water and being warming up to draining after 87 DEG C ~ 93 DEG C washings
Draining after 77 DEG C ~ 82 DEG C washings together；Finally add water and be warming up to 57 DEG C ~ 64 DEG C washings together.In dye jigger reactive dye chromatography
The multiple washing for carrying out specific cooling extent is conducive to strengthening color fastness, and the further loose colour of removal fiber surface, makes to wash
Cotton interweaving product colour stable.
Described pickling is addition neutralization acid 2.7g/L ~ 3.4g/L in 20 DEG C ~ 30 DEG C water, runs three roads.Live in dye jigger
Property dyestuff chromatography carry out specific cold water pickling be conducive to strengthen color fastness, and further remove fiber surface loose colour, make to wash
Cotton interweaving product colour stable.
Operation 1）Described in staining bath temperature control at 60 DEG C, staining bath adds the 50% of dye solution total amount, stirs 10 minutes
Operation is driven afterwards together, and second adds excess dye to drive operation together.
Operation 2）Described in staining bath in add Matrii Sulfas Exsiccatus when temperature be 60 DEG C, add total amount 50% Matrii Sulfas Exsiccatus operation
Together, add remaining Matrii Sulfas Exsiccatus operation together.
Operation 4）Described in staining bath in add the operation of 50% ground caustic together, add remaining ground caustic operation together.
Optimization to each operation process conditions, can make to adjust the suction color of cotton fiber in the present invention and reach optimal shape
State, using minimum dye dosage, completes the dyeing of highest color fastness.
Owf is the abbreviation of " On Weight the fabric ", refers to concentration on the basis of fabric weight, opposed fabric weight
The percentage ratio of amount.G/L is concentration unit, shows the grams that feeds intake in every liter of water.Matrii Sulfas Exsiccatus, ground caustic are technical grade, and market has
Sell；Soaping agent Si Nuofu SN-45, Wuxi De Guan Chemical Co., Ltd.s；Neutralization acid, Ha Gen Chemical Co., Ltd.s.
In view of soaping fastness, the lifting force of dyestuff, the dyeing rate of dyestuff and curve, the factor of the compatibility of dyestuff,
Preferably, cotton fiber dyeing is from the special dark color reactive dye of warm type in moral Sida Company, the dark red RGB of Remazol, Remazol orange
RGB。
Compared with prior art, the beneficial effect that a kind of colouring method of polyester-cotton blend interweaving product large red of the invention has
It is really：Problem of the present invention for the fastness difference of the cotton fiber dyeing in polyester-cotton blend interweaving product, by dyeing step and work
The control of skill condition, dyestuff are stirred in secondary cylinder in advance, are changed, and without dye granule, add staining bath, constant temperature after intensification
Dyeing, walks twice, and three, four roads add Matrii Sulfas Exsiccatus to add in two times, and seven, eight road ground caustics are added in two times, continue constant temperature dyeing 10
Road, soaps, washing, pickling, under roll out cylinder.The suction color of cotton fiber is improve, cotton fiber dyeing reactive dye are have adjusted, dye is deep
Property good, lifting force is high, dye dosage is few, reduce dye dosage, improve the reactivity of dyestuff and fiber, remove fiber surface
Loose colour, improves color fastness.
Specific embodiment
With reference to specific embodiment, the present invention will be further described, and embodiment 1 is highly preferred embodiment of the present invention, under
The present invention will be further described in face.Wherein, embodiment 1 ~ 3 and polyester-cotton blend jacquard fabric weave specification is used by comparative example 1 ~ 3
100d × 32,s/2 173 × 60, warp are polyster fibre, and parallel is cotton fiber.
Embodiment 1
Ty6629 polyester-cotton blend jacquard weaves are produced in the present embodiment bright red, 100d × 32s/2 combed cottons 173 × 60；
Its method is as follows：
Formula：The dark red RGB1.45%owf of Remazol, Remazol orange RGB0.225%owf, Matrii Sulfas Exsiccatus 80g/L, ground caustic 20g/L, in
With sour 3g/L
1）Plus dyestuff：Staining bath temperature 60 C, dyestuff use 50-60 DEG C of water dissolution in advance in secondary cylinder, are sufficiently stirred for 10 minutes, add
50%, drive operation together；Remaining 50% dyestuff is added, operation is driven together；
2）Plus Matrii Sulfas Exsiccatus：60 DEG C of constant temperature dyeings add the operation of 50% Matrii Sulfas Exsiccatus together, add remaining 50% Matrii Sulfas Exsiccatus operation together；
3）Constant temperature dyeing：60 DEG C of two roads of constant temperature dyeing；
4）Plus ground caustic：Add the operation of 50% ground caustic together, add remaining 50% ground caustic operation together；
5）Constant temperature dyeing：60 DEG C continue ten road of constant temperature dyeing；
6）Warm water is washed：60 DEG C of washing twice；
7）Soap：Plus 3g/L soaping agent SN-45, heat up 95 DEG C, run three roads, waste water of draining；
8）Hot water wash：Add water and be warming up to 90 DEG C and one change for one, wash two roads, drain；
9）Warm water is washed：Add water and be warming up to 80 DEG C of washings and drain together；Add water and be warming up to 60 DEG C of washings and drain together；
10）Pickling:Cold water adds neutralization acid 3g/L, runs three roads；
11）Last volume after pickling.
Embodiment 2
Ty6922 polyester-cotton blend jacquard weaves are produced in the present embodiment bright red, 100d × 32s/2 combed cottons 173 × 60
Its method is as follows：
Formula：The dark red RGB1.5%owf of Remazol, Remazol orange RGB0.25%owf, Matrii Sulfas Exsiccatus 79g/L, ground caustic 19g/L, neutralization
Sour 3.2g/L
1）Plus dyestuff：62 DEG C of staining bath temperature, dyestuff are sufficiently stirred for 10 minutes in advance in secondary cylinder with 58 DEG C of water dissolutioies, are added
48%, drive operation together；Remaining 52% dyestuff is added, operation is driven together；
2）Plus Matrii Sulfas Exsiccatus：62 DEG C of constant temperature dyeings add the operation of 52% Matrii Sulfas Exsiccatus together, add remaining 48% Matrii Sulfas Exsiccatus operation together；
3）Constant temperature dyeing：59 DEG C of two roads of constant temperature dyeing；
4）Plus ground caustic：Add the operation of 48% ground caustic together, add remaining 52% ground caustic operation together；
5）Constant temperature dyeing：62 DEG C continue ten road of constant temperature dyeing；
6）Warm water is washed：58 DEG C of washing twice；
7）Soap：Plus 2.9g/L soaping agent SN-45, heat up 94 DEG C, run three roads, waste water of draining；
8）Hot water wash：Add water and be warming up to 92 DEG C and one change for one, wash two roads, drain；
9）Warm water is washed：Add water and be warming up to 79 DEG C of washings and drain together；Add water and be warming up to 62 DEG C of washings and drain together；
10）Pickling:Cold water adds neutralization acid 3.2g/L, runs three roads；
11）Last volume after pickling.
Embodiment 3
Ty6820 polyester-cotton blend jacquard weaves are produced in the present embodiment bright red, 100d × 32s/2 combed cottons 173 × 60
Its method is as follows：
Formula：The dark red RGB1.45%owf of Remazol, Remazol orange RGB0.225%owf, Matrii Sulfas Exsiccatus 77g/L, ground caustic 22g/L, in
With sour 2.7g/L
1）Plus dyestuff：64 DEG C of staining bath temperature, dyestuff are sufficiently stirred for 8 minutes in advance in secondary cylinder with 50 DEG C of water dissolutioies, add 45%,
Operation drive together；Remaining 55% dyestuff is added, operation is driven together；
2）Plus Matrii Sulfas Exsiccatus：57 DEG C of constant temperature dyeings add the operation of 55% Matrii Sulfas Exsiccatus together, add remaining 45% Matrii Sulfas Exsiccatus operation together；
3）Constant temperature dyeing：64 DEG C of two roads of constant temperature dyeing；
4）Plus ground caustic：Add the operation of 55% ground caustic together, add remaining 45% ground caustic operation together；
5）Constant temperature dyeing：57 DEG C continue ten road of constant temperature dyeing；
6）Warm water is washed：64 DEG C of washing twice；
7）Soap：Plus 3.4g/L soaping agent SN-45, heat up 96 DEG C, run three roads, waste water of draining；
8）Hot water wash：Add water and be warming up to 87 DEG C and one change for one, wash two roads, drain；
9）Warm water is washed：Add water and be warming up to 82 DEG C of washings and drain together；Add water and be warming up to 57 DEG C of washings and drain together；
10）Pickling:Cold water adds neutralization acid 2.7g/L, runs three roads；
11）Last volume after pickling.
Embodiment 4
Ty6922 polyester-cotton blend jacquard weaves are produced in the present embodiment bright red, 100d × 32s/2 combed cottons 173 × 60
Its method is as follows：
Formula：The dark red RGB1.75%owf of Remazol, Remazol orange RGB0.35%owf, Matrii Sulfas Exsiccatus 84g/L, ground caustic 17g/L, in
With sour 3.4g/L
1）Plus dyestuff：57 DEG C of staining bath temperature, dyestuff are sufficiently stirred for 12 minutes in advance in secondary cylinder with 60 DEG C of water dissolutioies, are added
55%, drive operation together；Remaining 45% dyestuff is added, operation is driven together；
2）Plus Matrii Sulfas Exsiccatus：64 DEG C of constant temperature dyeings add the operation of 55% Matrii Sulfas Exsiccatus together, add remaining 45% Matrii Sulfas Exsiccatus operation together；
3）Constant temperature dyeing：57 DEG C of two roads of constant temperature dyeing；
4）Plus ground caustic：Add the operation of 45% ground caustic together, add remaining 55% ground caustic operation together；
5）Constant temperature dyeing：64 DEG C continue ten road of constant temperature dyeing；
6）Warm water is washed：57 DEG C of washing twice；
7）Soap：Plus 2.7g/L soaping agent SN-45, heat up 92 DEG C, run three roads, waste water of draining；
8）Hot water wash：Add water and be warming up to 93 DEG C and one change for one, wash two roads, drain；
9）Warm water is washed：Add water and be warming up to 77 DEG C of washings and drain together；Add water and be warming up to 64 DEG C of washings and drain together；
10）Pickling:Cold water adds neutralization acid 3.4g/L, runs three roads；
11）Last volume after pickling.
Comparative example 1
Ty6629 polyester-cotton blend jacquard weaves are produced in the present embodiment bright red, 100d × 32s/2 combed cottons 173 × 60；
Its method is as follows：
Formula：The dark red RGB1.45%owf of Remazol, Remazol orange RGB0.225%owf, Matrii Sulfas Exsiccatus 80g/L, ground caustic 20g/L, in
With sour 3g/L
1）Plus dyestuff：Staining bath temperature 60 C, dyestuff use 50-60 DEG C of water dissolution in advance in secondary cylinder, are sufficiently stirred for 10 minutes, add
All, drive to run two roads；
2）Plus Matrii Sulfas Exsiccatus：60 DEG C of constant temperature dyeings add whole Matrii Sulfas Exsiccatus to run two roads；
3）Constant temperature dyeing：60 DEG C of two roads of constant temperature dyeing；
4）Plus ground caustic：Whole ground caustics are added to run two roads；
5）Constant temperature dyeing：60 DEG C continue ten road of constant temperature dyeing；
6）Warm water is washed：60 DEG C of washing twice；
7）Soap：Plus 3g/L soaping agent SN-45, heat up 95 DEG C, run three roads, waste water of draining；
8）Hot water wash：Add water and be warming up to 90 DEG C and one change for one, wash two roads, drain；
9）Warm water is washed：Add water and be warming up to 80 DEG C of washings and drain together；Add water and be warming up to 60 DEG C of washings and drain together；
10）Pickling:Cold water adds neutralization acid 3g/L, runs three roads；
11）Last volume after pickling.
Comparative example 2
Ty6629 polyester-cotton blend jacquard weaves are produced in the present embodiment bright red, 100d × 32s/2 combed cottons 173 × 60；
Its method is as follows：
Formula：The dark red RGB1.45%owf of Remazol, Remazol orange RGB0.225%owf, Matrii Sulfas Exsiccatus 80g/L, ground caustic 20g/L, in
With sour 3g/L
1）Plus dyestuff：80 material of staining bath temperature uses 50-60 DEG C of water dissolution in advance in secondary cylinder, is sufficiently stirred for 10 minutes, adds 50%,
Operation drive together；Remaining 50% dyestuff is added, operation is driven together；
2）Plus Matrii Sulfas Exsiccatus：80 temperature dyeing add the operation of 50% Matrii Sulfas Exsiccatus together, add remaining 50% Matrii Sulfas Exsiccatus operation together；
3）Constant temperature dyeing：80 two roads of temperature dyeing；
4）Plus ground caustic：Add the operation of 50% ground caustic together, add remaining 50% ground caustic operation together；
5）Constant temperature dyeing：80 continuous ten roads of constant temperature dyeing；
6）Warm water is washed：80 wash twice；
7）Soap：Plus 3g/L soaping agent SN-45, heat up 95 DEG C, run three roads, waste water of draining；
8）Hot water wash：Add water and be warming up to 90 DEG C and one change for one, wash two roads, drain；
9）Warm water is washed：Add water and be warming up to 80 DEG C of washings and drain together；Add water and be warming up to 60 DEG C of washings and drain together；
10）Pickling:Cold water adds neutralization acid 3g/L, runs three roads；
11）Last volume after pickling.
Comparative example 3
Ty6629 polyester-cotton blend jacquard weaves are produced in the present embodiment bright red, 100d × 32s/2 combed cottons 173 × 60；
Its method is as follows：
Formula：The dark red RGB1.45%owf of Remazol, Remazol orange RGB0.225%owf, Matrii Sulfas Exsiccatus 80g/L, ground caustic 20g/L, in
With sour 3g/L
1）Plus dyestuff：Staining bath temperature 60 C, dyestuff use 50-60 DEG C of water dissolution in advance in secondary cylinder, are sufficiently stirred for 10 minutes, add
50%, drive operation together；Remaining 50% dyestuff is added, operation is driven together；
2）Plus Matrii Sulfas Exsiccatus：60 DEG C of constant temperature dyeings add the operation of 50% Matrii Sulfas Exsiccatus together, add remaining 50% Matrii Sulfas Exsiccatus operation together；
3）Constant temperature dyeing：60 DEG C of two roads of constant temperature dyeing；
4）Plus ground caustic：Add the operation of 50% ground caustic together, add remaining 50% ground caustic operation together；
5）Constant temperature dyeing：60 DEG C continue ten road of constant temperature dyeing；
6）Warm water is washed：60 DEG C of washing twice；
7）Soap：Plus 3g/L soaping agent SN-45, heat up 95 DEG C, run three roads, waste water of draining；
8）Warm water is washed：Add water be warming up to 80 DEG C washing four roads drain；
9）Pickling：Cold water adds neutralization acid 3g/L, runs three roads；
10）Last volume after pickling.
Performance test is tested
Fastness to rubbing is tested with reference to standard GB/T/T3920 ~ 2008, and washing color fastness reference standard GB/T/
T5713 ~ 1997 are tested, and fastness to perspiration is tested with reference to standard GB/T/T3922 ~ 1995, fastness to soaping reference
Tested standard GB/T/T3921 ~ 2008.
The color fastness test result of 1 embodiment 1 ~ 3 of table and comparative example 1 ~ 3
。
Can be seen that by table 1, the fastness to rubbing of embodiment 1 ~ 3, washing color fastness, fastness to perspiration and resistance to jail of soaping
The indexs such as degree, are compared with comparative example 1 ~ 3, will be higher by 0.5 ~ 1 grade, with preferable color fastness.3 ~ 4 grades represent test results circle in
Between 3 grades and 4 grades, 3 ~ 4 grades are considered as and are higher by 0.5 grade than 3 grades, and 2 ~ 3 grades in the same manner.
The above, is only presently preferred embodiments of the present invention, is not the restriction for making other forms to the present invention, is appointed
What those skilled in the art possibly also with the disclosure above technology contents changed or be modified as equivalent variations etc.
Effect embodiment.But it is every without departing from technical solution of the present invention content, according to the technical spirit of the present invention to above example institute
Any simple modification, equivalent variations and the remodeling made, still falls within the protection domain of technical solution of the present invention.
Claims (8)
1. a kind of colouring method of polyester-cotton blend interweaving product large red, it is characterised in that dye formulation is：Remazol is dark red
RGB1.45%owf ~ 1.75%owf, Remazol orange RGB0.225%owf ~ 0.35%owf, Matrii Sulfas Exsiccatus 77g/L ~ 84g/L, ground caustic 17g/
L ~ 22g/L, neutralization acid 2.7g/L ~ 3.4g/L；
Comprise the following steps：Dye jigger reactive dye chromatography, warm water are washed, are soaped, washing, pickling and last volume；
The concrete operation of wherein described dye jigger reactive dye chromatography step is：
1）Dyestuff obtains dye solution with 50 DEG C ~ 60 DEG C water dissolutioies in advance in secondary cylinder, staining bath temperature control at 57 DEG C ~ 64 DEG C,
Staining bath adds the 45% ~ 55% of dye solution total amount, stirs, and drives operation together；Add excess dye to drive to run one
Road；
2）3rd road adds the Matrii Sulfas Exsiccatus for accounting for Matrii Sulfas Exsiccatus total amount 45% ~ 55% to run together under 57 DEG C ~ 64 DEG C of constant temperature in staining bath,
4th road adds remaining Matrii Sulfas Exsiccatus operation together；
3）Staining bath temperature is kept in 57 DEG C ~ 64 DEG C two roads of constant temperature dyeing；
4）Continuously add in 7th road staining bath and account for the operation of 45% ~ 55% ground caustic of ground caustic total amount together, the 8th road adds remaining ground caustic
Operation is together；
5）Then continue ten road of continuous dyeing under constant temperature at 57 DEG C ~ 64 DEG C and complete dye jigger reactive dye chromatography step.
2. the colouring method of a kind of polyester-cotton blend interweaving product large red according to claim 1, it is characterised in that：Described temperature
Water-washing step is under the conditions of 57 DEG C ~ 64 DEG C to wash twice.
3. the colouring method of a kind of polyester-cotton blend interweaving product large red according to claim 1, it is characterised in that：Described soap
Wash to be warming up to after 92 DEG C ~ 96 DEG C after 2.7g/L ~ 3.4g/L soaping agents being added in water lotion, run three roads.
4. the colouring method of a kind of polyester-cotton blend interweaving product large red according to claim 1, it is characterised in that：Described water
Step is washed to add water and being warming up to draining after 87 DEG C ~ 93 DEG C washings, repeats two roads, added water and be warming up to 77 DEG C ~ 82 DEG C washings one
Draining behind road；Finally add water and be warming up to 57 DEG C ~ 64 DEG C washings together.
5. the colouring method of a kind of polyester-cotton blend interweaving product large red according to claim 1, it is characterised in that：Described acid
Wash as neutralization acid 2.7g/L ~ 3.4g/L is added in 20 DEG C ~ 30 DEG C water, run three roads.
6. the colouring method of a kind of polyester-cotton blend interweaving product large red according to claim 1, it is characterised in that：Operation 1）In
At 60 DEG C, staining bath adds the 50% of dye solution total amount, stirring that operation is driven after 10 minutes together to described staining bath temperature control,
Second adds excess dye to drive operation together.
7. the colouring method of a kind of polyester-cotton blend interweaving product large red according to claim 1, it is characterised in that：Operation 2）In
Add temperature during Matrii Sulfas Exsiccatus to be 60 DEG C in described staining bath, add the Matrii Sulfas Exsiccatus operation of total amount 50% together, add remaining unit
Bright powder operation is together.
8. the colouring method of a kind of polyester-cotton blend interweaving product large red according to claim 1, it is characterised in that：Operation 4）In
The operation of 50% ground caustic is added in described staining bath together, remaining ground caustic operation is added together.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107326595A (en) * | 2017-06-27 | 2017-11-07 | 南通金仕达超微阻燃材料有限公司 | The production method of the high pure cotton large red extra width woven fabric of wet rubbing fastness |
| CN107419568A (en) * | 2017-06-21 | 2017-12-01 | 淄博大染坊丝绸集团有限公司 | A kind of wedding celebration fabric repaiies color method |
| CN109023641A (en) * | 2018-08-01 | 2018-12-18 | 淄博大染坊丝绸集团有限公司 | A kind of production method of special dark dacron interweaved fabric |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101260621A (en) * | 2008-04-15 | 2008-09-10 | 达利(中国)有限公司 | Process for cotton reactive dye applying in silk broadcloth dying |
| CN102558904A (en) * | 2010-12-07 | 2012-07-11 | 佛山市宇丰染料有限公司 | Low-alkali reactive dye and its dyeing method |
| CN105040488A (en) * | 2015-06-02 | 2015-11-11 | 江苏金太阳纺织科技有限公司 | Fabric dyeing technology of viscose containing chitin |
-
2016
- 2016-12-02 CN CN201611096210.0A patent/CN106555344A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101260621A (en) * | 2008-04-15 | 2008-09-10 | 达利(中国)有限公司 | Process for cotton reactive dye applying in silk broadcloth dying |
| CN102558904A (en) * | 2010-12-07 | 2012-07-11 | 佛山市宇丰染料有限公司 | Low-alkali reactive dye and its dyeing method |
| CN105040488A (en) * | 2015-06-02 | 2015-11-11 | 江苏金太阳纺织科技有限公司 | Fabric dyeing technology of viscose containing chitin |
Non-Patent Citations (6)
| Title |
|---|
| 上海印染工业公司: "《染色》", 31 December 1981, 纺织工业出版社 * |
| 冒亚红 等: "《染色工艺与质量控制》", 31 August 2014, 中国纺织出版社 * |
| 尹耐冬 等: "《国外纺织染料助剂使用指南2009-2010》", 30 November 2008 * |
| 沈志平 等: "《染整技术（染色分册）》", 31 December 2014, 中国纺织出版社 * |
| 钱建栋: "《染色打样技术》", 30 September 2014, 东华大学出版社 * |
| 陆锦昌 等: "《丝绸染整手册 第二版》", 31 December 1995, 中国纺织出版社 * |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107419568A (en) * | 2017-06-21 | 2017-12-01 | 淄博大染坊丝绸集团有限公司 | A kind of wedding celebration fabric repaiies color method |
| CN107419568B (en) * | 2017-06-21 | 2019-09-17 | 淄博大染坊丝绸集团有限公司 | A kind of wedding celebration fabric repairs color method |
| CN107326595A (en) * | 2017-06-27 | 2017-11-07 | 南通金仕达超微阻燃材料有限公司 | The production method of the high pure cotton large red extra width woven fabric of wet rubbing fastness |
| CN109023641A (en) * | 2018-08-01 | 2018-12-18 | 淄博大染坊丝绸集团有限公司 | A kind of production method of special dark dacron interweaved fabric |
| CN109023641B (en) * | 2018-08-01 | 2020-03-31 | 淄博大染坊丝绸集团有限公司 | Production method of ultra-deep color polyester interwoven fabric |
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