[go: up one dir, main page]

CN106525848A - Simple identification method of pig, cattle and sheep split leather - Google Patents

Simple identification method of pig, cattle and sheep split leather Download PDF

Info

Publication number
CN106525848A
CN106525848A CN201610938736.2A CN201610938736A CN106525848A CN 106525848 A CN106525848 A CN 106525848A CN 201610938736 A CN201610938736 A CN 201610938736A CN 106525848 A CN106525848 A CN 106525848A
Authority
CN
China
Prior art keywords
fiber bundles
length
cattle
sheep
pig
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201610938736.2A
Other languages
Chinese (zh)
Other versions
CN106525848B (en
Inventor
李成琴
李夏
李晓龙
王豪
黄武平
罗媛媛
蔡白雪
张莉
胡文炬
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Chongqing Academy of Metrology and Quality Inspection
Original Assignee
Chongqing Academy of Metrology and Quality Inspection
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chongqing Academy of Metrology and Quality Inspection filed Critical Chongqing Academy of Metrology and Quality Inspection
Priority to CN201610938736.2A priority Critical patent/CN106525848B/en
Publication of CN106525848A publication Critical patent/CN106525848A/en
Application granted granted Critical
Publication of CN106525848B publication Critical patent/CN106525848B/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/84Systems specially adapted for particular applications
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/84Systems specially adapted for particular applications
    • G01N2021/8444Fibrous material

Landscapes

  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Sampling And Sample Adjustment (AREA)
  • Treatment And Processing Of Natural Fur Or Leather (AREA)

Abstract

本发明提供一种猪牛羊剖层革材质简易鉴别方法,包括以下步骤:S1、在剖层革任意位置剪开一个口,将剪口的两端分别夹持在拉力机的上下夹具上,开启拉力机,将剖层革沿剪口撕裂,撕裂长度100毫米以上;S2、剪取裂口纤维组织试样条,该试样条所包含的纤维束长短分布较均匀并具有代表性;S3、将剪取的试样条置于显微镜下观察并拍摄显微图像,通过显微镜工作站软件测量纤维束的长度和粗细程度,并记录纤维束的形态特征;S4、将拍摄的显微图像、测量的纤维束长度和粗细程度以及记录的形态特征与预存的已知样品图谱进行对比,鉴别出试样为猪牛羊中的何种皮革。本发明使猪牛羊剖层革的鉴别更加简单有效,减少了因横截面性状特征不明显带来的鉴别困难。

The invention provides a simple method for identifying the material of pig, cattle and sheep split leather, which includes the following steps: S1. Cut a hole at any position of the split leather, clamp the two ends of the cut on the upper and lower clamps of the tension machine, and open Tensile machine, tear the split leather along the notch, and the tear length is more than 100 mm; S2, cut the fibrous tissue sample strip of the crack, and the fiber bundle length distribution contained in the sample strip is relatively uniform and representative; S3 1. Place the clipped sample strip under a microscope to observe and take a microscopic image, measure the length and thickness of the fiber bundle through the microscope workstation software, and record the morphological characteristics of the fiber bundle; S4. Take the microscopic image, measure The length and thickness of the fiber bundles and the recorded morphological characteristics are compared with the pre-stored known sample maps to identify what kind of leather the sample is from pigs, cattle and sheep. The invention makes the identification of the pig, cattle and sheep split leather more simple and effective, and reduces the identification difficulty caused by the inconspicuous cross-sectional properties.

Description

一种猪牛羊剖层革材质简易鉴别方法A simple method for identifying the material of pig, cattle and sheep split leather

技术领域technical field

本发明涉及皮革材质鉴别技术领域,具体涉及一种猪牛羊剖层革材质简易鉴别方法。The invention relates to the technical field of leather material identification, in particular to a simple identification method for pig, cattle and sheep split leather materials.

背景技术Background technique

目前,皮革材质鉴别的方法有多样,最简单有效的就是通过显微镜观察皮革粒面花纹。在申请号为201210288246.4的中国专利申请文件中,公开了一种皮革纤维结构的简易鉴别方法,其主要是通过显微镜观察横截面形态特征的方法来进行鉴别。但是,本发明的发明人经过研究发现,当试样为剖层革材质的时候,由于没有粒面花纹,如果仅从横截面上观察,加上横截面上没有乳头层特征,鉴别往往显得比较困难,特别是当试样为黑色时,显微镜下观察到的横截面为一片黑,特征更难分辨。At present, there are various methods for leather material identification, the simplest and most effective is to observe the leather grain pattern through a microscope. In the Chinese patent application document with application number 201210288246.4, a simple identification method of leather fiber structure is disclosed, which is mainly identified by observing the cross-sectional morphological characteristics through a microscope. However, the inventors of the present invention have found through research that when the sample is a split leather material, because there is no grain pattern, if only observing from the cross section, and there is no papillary layer feature on the cross section, the identification often appears to be more difficult. Difficult, especially when the sample is black, the cross-section observed under the microscope is black, and the features are more difficult to distinguish.

发明内容Contents of the invention

针对现有技术存在的当试样为剖层革材质时鉴别比较困难的技术问题,本发明提供一种猪牛羊剖层革材质简易鉴别方法,该方法能够准确反映猪牛羊剖层革胶原纤维组织结构特征,使猪牛羊剖层革的鉴别更加简单有效,减少由于横截面性状特征不明显带来的鉴别困难。Aiming at the technical problem existing in the prior art that it is difficult to identify when the sample is made of split leather, the present invention provides a simple method for identifying the material of split leather of pigs, cattle and sheep, which can accurately reflect the collagen fibers of split leather of pigs, cattle and sheep. The characteristics of tissue structure make the identification of pig, cattle and sheep split leather more simple and effective, and reduce the difficulty of identification caused by the inconspicuous cross-sectional properties.

为了解决上述技术问题,本发明采用了如下的技术方案:In order to solve the problems of the technologies described above, the present invention adopts the following technical solutions:

一种猪牛羊剖层革材质简易鉴别方法,包括以下步骤:A simple method for identifying the material of pig, cattle and sheep split leather, comprising the following steps:

S1、在剖层革任意位置上剪开一个口,将剪口的两边端口分别夹持在拉力机的上下夹具上,开启拉力机,将剖层革沿剪口以200-300毫米/分钟的速度匀速撕裂,撕裂长度100毫米以上;S1. Cut a hole at any position of the split leather, clamp the ports on both sides of the notch on the upper and lower clamps of the tension machine, turn on the tension machine, and move the split leather along the notch at a rate of 200-300 mm/min. Uniform speed tearing, tearing length more than 100mm;

S2、剪取撕裂裂口纤维组织试样条,所述试样条的长度为40-60毫米,宽度为3-6毫米,且该试样条所包含的纤维束长短分布较均匀并具有代表性;S2. Cut the tear fibrous tissue sample strip, the length of the sample strip is 40-60 mm, the width is 3-6 mm, and the length distribution of the fiber bundles contained in the sample strip is relatively uniform and representative sex;

S3、将剪取的试样条置于显微镜下观察并拍摄显微图像,通过显微镜工作站AxioVision软件测量纤维束的长度和粗细程度,并记录纤维束的形态特征;S3. Place the cut sample strip under a microscope to observe and take a microscopic image, measure the length and thickness of the fiber bundle through the microscope workstation AxioVision software, and record the morphological characteristics of the fiber bundle;

S4、将拍摄的显微图像、测量的纤维束长度和粗细程度以及记录的纤维束形态特征与预存的已知样品图谱进行对比,鉴别出试样为猪牛羊中的何种皮革。S4. Comparing the photographed microscopic image, the measured length and thickness of the fiber bundles, and the recorded morphological features of the fiber bundles with the pre-stored known sample atlas, to identify which kind of leather the sample is from pigs, cattle and sheep.

进一步,步骤S2中,所述试样条所包含的纤维束长短分布较均匀并具有代表性是指:所剪取的试样条纤维束长短、疏密要与全部裂口纤维束情况一致,不能只剪取纤维束全部为长或短、疏或密的试样。Further, in step S2, the length distribution of the fiber bundles contained in the sample strip is relatively uniform and representative, which means that the length and density of the fiber bundles of the cut sample strip should be consistent with the conditions of all the cracked fiber bundles, and cannot Only cut the samples whose fiber bundles are all long or short, sparse or dense.

进一步,步骤S3中,所述显微镜为体视显微镜并带有标尺功能,放大倍数至少能在10-100倍之间无级调节。Further, in step S3, the microscope is a stereo microscope with a ruler function, and the magnification can be adjusted steplessly between at least 10-100 times.

进一步,步骤S3中,所述显微镜分别拍摄放大倍数为10倍和100倍的显微图像,所述显微镜工作站AxioVision软件分别测量10倍显微图像下纤维束的长度和100倍显微图像下纤维束的粗细程度,并在100倍显微图像下观察纤维束的形态特征。Further, in step S3, the microscope takes microscopic images with magnifications of 10 times and 100 times respectively, and the microscope workstation AxioVision software measures the length of the fiber bundle under the 10 times microscopic image and the fiber bundle under the 100 times microscopic image respectively. The thickness of the bundle, and observe the morphological characteristics of the fiber bundle under the 100 times microscopic image.

进一步,步骤S3中,所述纤维束的长度测量的是纤维束长短较均匀部分的长度,所述纤维束的粗细程度测量的是纤维束中部靠尖端部分的粗细程度。Further, in step S3, the length of the fiber bundle is measured as the length of the portion of the fiber bundle with a relatively uniform length, and the thickness of the fiber bundle is measured as the thickness of the middle part of the fiber bundle near the tip.

进一步,步骤S3中,所述纤维束的形态特征包括纤维束或呈束状或分散、或竖直或卷曲以及纤维束或圆或扁。Further, in step S3, the morphological characteristics of the fiber bundles include fiber bundles being bundled or scattered, vertical or curled, and fiber bundles being round or flat.

进一步,步骤S4中,所述预存的已知样品图谱为实验室采集的大量猪牛羊已知种类剖层革经过实验步骤后归纳总结的猪牛羊典型性代表显微图谱,该样品图谱包括显微图像和纤维束长度、粗细程度及形态特征的描述。Further, in step S4, the pre-stored known sample atlas is a typical representative microscopic atlas of pigs, cattle and sheep summarized and summarized after a large number of split leathers of known species of pigs, cattle and sheep collected in the laboratory, the sample atlas includes Microscopic images and descriptions of fiber bundle length, thickness, and morphological characteristics.

进一步,所述预存的已知样品图谱中,猪皮纤维束长2-10毫米,牛皮纤维束长2-10毫米,羊皮纤维束长0-6毫米;猪皮纤维束粗20-40微米,牛皮纤维束粗70-130微米,羊皮纤维束粗30-70微米;猪皮纤维束形态特征以束状形式存在,稍扁很细很直,牛皮纤维束形态特征以束状形式存在,较圆较直,羊皮纤维束形态特征以分散形式存在,稍扁略卷曲。Further, in the pre-stored known sample spectrum, the pigskin fiber bundles are 2-10 mm long, the cowhide fiber bundles are 2-10 mm long, and the sheepskin fiber bundles are 0-6 mm long; the pigskin fiber bundles are 20-40 microns thick, Cowhide fiber bundles are 70-130 microns thick, and sheepskin fiber bundles are 30-70 microns thick; pigskin fiber bundles are in the form of bundles, slightly flat, thin and straight, and cowhide fiber bundles are in bundles, relatively round Relatively straight, sheepskin fiber bundles exist in scattered form, slightly flattened and slightly curled.

与现有技术相比,本发明提供的猪牛羊剖层革材质简易鉴别方法,先在剖层革任意位置上剪开一个口并沿剪口撕裂,接着在撕裂裂口剪取纤维组织试样条,然后将试样条置于显微镜下观察并拍摄显微图像,并通过显微镜工作站软件测量纤维束的长度和粗细程度,同时记录纤维束的形态特征,最后将检测到的试样数据与预存的已知样品图谱进行对比,鉴别出试样为猪牛羊中的何种皮革。本发明开辟了猪牛羊剖层革材质鉴别的新方法,克服了猪牛羊剖层革仅从横截面观察鉴别方法中形态特征差异不明显,黑色甚至观察不到形态特征的缺点,能够准确反映猪牛羊剖层革胶原纤维组织结构特征;通过具体测量纤维束的长度和粗细程度,将试验过程数据化,使试验更具操作性;另外,猪牛羊剖层革纤维束的长度、粗细程度及形态特征差异较明显,因而能够准确的进行材质鉴别,鉴别更加简单有效。Compared with the prior art, the invention provides a simple method for identifying the material of the split leather of pigs, cattle and sheep. First, a hole is cut at any position of the split leather and torn along the cut, and then the fibrous tissue is cut at the tear gap. Then place the sample strip under a microscope to observe and take microscopic images, and measure the length and thickness of the fiber bundles through the microscope workstation software, and record the morphological characteristics of the fiber bundles, and finally the detected sample data Compared with the pre-stored known sample spectrum, it is identified which kind of leather the sample is from pigs, cattle and sheep. The invention opens up a new method for identifying the material of pig, cattle, and sheep split leather, overcomes the shortcomings of pig, cattle, and sheep split leather that are only observed from the cross-section in the identification method that the difference in morphological characteristics is not obvious, black or even no morphological characteristics can be observed, and can accurately Reflect the structural characteristics of collagen fibers in pig, cattle and sheep split leather; by measuring the length and thickness of fiber bundles, the test process is digitized to make the test more operable; in addition, the length of pig, cattle and sheep split leather fiber bundles, The difference in thickness and morphological characteristics is obvious, so the material identification can be accurately carried out, and the identification is simpler and more effective.

附图说明Description of drawings

图1是本发明实施例提供的试样条结构示意图。Fig. 1 is a schematic structural diagram of a sample strip provided by an embodiment of the present invention.

图2是本发明实施例提供的显微镜放大倍数为10倍时观察到的裂口纤维结构示意图。Fig. 2 is a schematic diagram of the fibrous structure of the split observed when the microscope magnification is 10 times provided by the embodiment of the present invention.

图3是是本发明实施例提供的显微镜放大倍数为100倍时观察到的裂口纤维结构示意图。Fig. 3 is a schematic diagram of the fibrous structure of the slit observed when the magnification of the microscope provided by the embodiment of the present invention is 100 times.

具体实施方式detailed description

为了使本发明实现的技术手段、创作特征、达成目的与功效易于明白了解,下面结合具体图示,进一步阐述本发明。In order to make the technical means, creative features, goals and effects achieved by the present invention easy to understand, the present invention will be further described below in conjunction with specific illustrations.

在本发明的描述中,需要理解的是,术语“纵向”、“径向”、“长度”、“宽度”、“厚度”、“上”、“下”、“前”、“后”、“左”、“右”、“竖直”、“水平”、“顶”、“底”、“内”、“外”等指示的方位或位置关系为基于附图所示的方位或位置关系,仅是为了便于描述本发明和简化描述,而不是指示或暗示所指的装置或元件必须具有特定的方位、以特定的方位构造和操作,因此不能理解为对本发明的限制。在本发明的描述中,除非另有说明,“多个”的含义是两个或两个以上。In describing the present invention, it is to be understood that the terms "longitudinal", "radial", "length", "width", "thickness", "upper", "lower", "front", "rear", The orientation or positional relationship indicated by "left", "right", "vertical", "horizontal", "top", "bottom", "inner", "outer", etc. is based on the orientation or positional relationship shown in the drawings , is only for the convenience of describing the present invention and simplifying the description, but does not indicate or imply that the referred device or element must have a specific orientation, be constructed and operated in a specific orientation, and thus should not be construed as limiting the present invention. In the description of the present invention, unless otherwise specified, "plurality" means two or more.

在本发明的描述中,需要说明的是,除非另有明确的规定和限定,术语“安装”、“相连”、“连接”应做广义理解,例如,可以是固定连接,也可以是可拆卸连接,或一体地连接;可以是机械连接,也可以是电连接;可以是直接相连,也可以通过中间媒介间接相连,可以是两个元件内部的连通。对于本领域的普通技术人员而言,可以具体情况理解上述术语在本发明中的具体含义。In the description of the present invention, it should be noted that unless otherwise specified and limited, the terms "installation", "connection" and "connection" should be understood in a broad sense, for example, it can be a fixed connection or a detachable connection. Connected, or integrally connected; it can be mechanically connected or electrically connected; it can be directly connected or indirectly connected through an intermediary, and it can be the internal communication of two components. Those of ordinary skill in the art can understand the specific meanings of the above terms in the present invention in specific situations.

本发明提供一种猪牛羊剖层革材质简易鉴别方法,包括以下步骤:The invention provides a simple method for identifying the material of pig, cattle and sheep split leather, which comprises the following steps:

S1、在剖层革任意位置上用剪刀剪开一个口,将剪口的两边端口分别夹持在拉力机的上下夹具上,开启拉力机,将剖层革沿剪口以200-300毫米/分钟的速度匀速撕裂,为了获得均匀和具有代表性的试样,撕裂长度100毫米以上。S1. Cut a hole with scissors at any position of the split leather, clamp the ports on both sides of the notch on the upper and lower clamps of the tension machine, turn on the tension machine, and cut the split leather along the notch at a distance of 200-300mm/ It is torn at a constant speed of 1 minute. In order to obtain a uniform and representative sample, the tear length should be more than 100 mm.

S2、将裂口纤维捋整齐,剪取撕裂裂口纤维组织试样条,请参考图1所示,所述试样条的长度为40-60毫米,宽度为3-6毫米,在剪取裂口纤维组织时注意观察裂口纤维长短、疏密整体情况,使剪取的该试样条所包含的纤维束长短疏密分布较均匀并具有代表性,由此可得到稳定均匀的裂口纤维,即让所剪取的试样条纤维束长短、疏密要与全部裂口纤维束情况一致,不能只剪取纤维束全部为长或短、疏或密的试样,因为那样的试样不具有代表性;其中,剪取的所述试样条的长度为40-60毫米,宽度为3-6毫米,由此可以更好地方便后续显微图像的采集和合理使用。S2. Squeeze the fibers of the rip neatly, and cut the fibrous tissue sample strip of the tear rip, as shown in Fig. 1, the length of the sample bar is 40-60 mm, and the width is 3-6 mm. Pay attention to observe the overall situation of the length and density of the fibrous fibers in the fibrous tissue, so that the distribution of the length and density of the fiber bundles contained in the cut sample strip is relatively uniform and representative, thus obtaining stable and uniform fibrous fibers, that is, let The length and density of the fiber bundles of the cut sample strips should be consistent with the condition of all the cracked fiber bundles. It is not possible to just cut samples with all the fiber bundles being long or short, sparse or dense, because such samples are not representative. Wherein, the length of the cut sample strip is 40-60 millimeters, and the width is 3-6 millimeters, which can better facilitate the collection and rational use of subsequent microscopic images.

S3、将剪取的试样条置于显微镜下观察并拍摄显微图像,通过显微镜工作站AxioVision软件测量纤维束的长度和粗细程度,并记录纤维束的形态特征;作为具体实施例,所述显微镜为体视显微镜并带有标尺功能,在观察过程中能调节试样的观察位置,放大倍数至少能在10-100倍之间无级调节,且显微镜系统能拍摄显微图像,通过工作站AxioVision软件能测量显微图像上任意两点之间的真实距离,从而测量出纤维束的长度和粗细程度。S3. Place the clipped sample strip under a microscope to observe and take a microscopic image, measure the length and thickness of the fiber bundle through the microscope workstation AxioVision software, and record the morphological characteristics of the fiber bundle; as a specific embodiment, the microscope It is a stereo microscope with a ruler function, which can adjust the observation position of the sample during the observation process, and the magnification can be adjusted steplessly between at least 10-100 times, and the microscope system can take microscopic images, through the workstation AxioVision software It can measure the real distance between any two points on the microscopic image, so as to measure the length and thickness of the fiber bundle.

作为一种实施方式,打开显微镜,将放大倍数调到10倍,将试样条置于所述显微镜下,并调整试样条位置和显微镜的焦距,使显微镜能清晰的观察到完整的裂口纤维束(根部到尖部),利用显微镜拍摄显微图像,并利用显微镜工作站软件测量纤维束长短较均匀部分的长度,从而得到纤维束的长度,如图2所示,可知纤维束的长度大体为5-6毫米,且在图2中,由于右侧数字太小,左边圆圈内为右侧数字处放大效果;接着将显微镜的放大倍数调到100倍,按照前面相同的操作,将试样条置于所述显微镜下,并调整试样条位置和显微镜的焦距,使显微镜能清晰的观察到纤维束中部靠尖端部分,利用显微镜拍摄显微图像,并选择纤维束中部靠尖端部分粗细较均匀的部分测量纤维束的粗细程度,并记录纤维束的形态特征,该纤维束的形态特征包括纤维束或呈束状或分散、或竖直或卷曲以及纤维束或圆或扁。参考图3所示可知,纤维束的粗细程度大体为20-30微米,且由于左侧数字太小,右边圆圈内为左侧数字处放大效果;且由图3可见,纤维束呈束状、稍扁、又细又直。As an embodiment, turn on the microscope, adjust the magnification to 10 times, place the sample strip under the microscope, and adjust the position of the sample strip and the focal length of the microscope so that the microscope can clearly observe the complete split fiber bundle (root to tip), use a microscope to take microscopic images, and use the microscope workstation software to measure the length of the fiber bundle with a relatively uniform length, so as to obtain the length of the fiber bundle, as shown in Figure 2, it can be known that the length of the fiber bundle is roughly 5-6 mm, and in Figure 2, because the number on the right is too small, the circle on the left is the magnification effect of the number on the right; then adjust the magnification of the microscope to 100 times, and follow the same operation as before to place the sample strip Place it under the microscope, and adjust the position of the sample strip and the focal length of the microscope, so that the microscope can clearly observe the middle part of the fiber bundle near the tip, use the microscope to take microscopic images, and select the middle part of the fiber bundle near the tip to be more uniform in thickness The part measures the thickness of the fiber bundles, and records the morphological characteristics of the fiber bundles. The morphological characteristics of the fiber bundles include fiber bundles or bundles or scattered, or vertical or curled, and fiber bundles are round or flat. Referring to Figure 3, it can be seen that the thickness of the fiber bundle is generally 20-30 microns, and because the number on the left is too small, the circle on the right is the enlarged effect of the number on the left; and it can be seen from Figure 3 that the fiber bundle is in the form of a bundle, Slightly flat, thin and straight.

S4、将拍摄的显微图像、测量的纤维束长度和粗细程度以及记录的纤维束形态特征与预存的已知样品图谱进行对比,鉴别出试样为猪牛羊中的何种皮革,即根据显微图像、纤维束长短、粗细程度和形态特征与已知的样品图谱比较,确定出试样种类。其中,所述预存的样品图谱为实验室采集的大量猪牛羊已知种类剖层革经过本实验步骤后归纳总结的猪牛羊典型性代表显微图谱,该样品图谱包括显微图像和纤维束长度、粗细程度及形态特征的描述,以电子信息的方式进行存储,方便查阅,同时可将该样品图谱制成多套进行保存。作为具体实施例,所述预存的已知样品图谱中,猪皮纤维束长2-10毫米,牛皮纤维束长2-10毫米,羊皮纤维束长0-6毫米;猪皮纤维束粗20-40微米,牛皮纤维束粗70-130微米,羊皮纤维束粗30-70微米;猪皮纤维束形态特征绝大多数以束状形式存在,稍扁很细很直,牛皮纤维束形态特征大多以束状形式存在,较圆较直,羊皮纤维束形态特征多以分散形式存在,稍扁略卷曲。至此,结合前述的图2和图3可知,试样裂口纤维束的长度为5-6毫米,纤维束的粗为20-30微米,且纤维束呈束状、稍扁、又细又直,据此与预存的样品图谱对比,鉴别出试样为猪类皮革,即猪剖层革。S4. Compare the photographed microscopic image, the measured fiber bundle length and thickness, and the recorded fiber bundle morphological characteristics with the pre-stored known sample atlas to identify what kind of leather the sample is from pigs, cattle and sheep, that is, according to Compare the microscopic image, fiber bundle length, thickness and morphological characteristics with the known sample spectrum to determine the type of sample. Wherein, the pre-stored sample atlas is a typical representative microscopic atlas of pigs, cattle and sheep summarized and summarized after a large number of known types of split leather of pigs, cattle and sheep collected in the laboratory, the sample atlas includes microscopic images and fiber The description of beam length, thickness and morphological characteristics is stored in the form of electronic information, which is convenient for reference. At the same time, the sample map can be made into multiple sets for storage. As a specific example, in the pre-stored known sample atlas, the pigskin fiber bundles are 2-10 mm long, the cowhide fiber bundles are 2-10 mm long, and the sheepskin fiber bundles are 0-6 mm long; the pigskin fiber bundles are 20-10 mm thick. 40 microns, cowhide fiber bundles are 70-130 microns thick, sheepskin fiber bundles are 30-70 microns thick; pigskin fiber bundles are mostly in the form of bundles, slightly flat, thin and straight, and cowhide fiber bundles are mostly in the form of It exists in the form of fascicles, which are rounder and straighter. The morphological characteristics of sheepskin fiber bundles are mostly in dispersed forms, slightly flat and curly. So far, in conjunction with the aforementioned Figures 2 and 3, it can be seen that the length of the fiber bundles in the sample crack is 5-6 mm, the thickness of the fiber bundles is 20-30 microns, and the fiber bundles are in the form of bundles, slightly flat, thin and straight, Based on the comparison with the pre-stored sample spectrum, the sample was identified as pig leather, that is, pig split leather.

与现有技术相比,本发明提供的猪牛羊剖层革材质简易鉴别方法,先在剖层革任意位置上剪开一个口并沿剪口撕裂,接着在撕裂裂口剪取纤维组织试样条,然后将试样条置于显微镜下观察并拍摄显微图像,并通过显微镜工作站软件测量纤维束的长度和粗细程度,同时记录纤维束的形态特征,最后将检测到的试样数据与预存的已知样品图谱进行对比,鉴别出试样为猪牛羊中的何种皮革。本发明开辟了猪牛羊剖层革材质鉴别的新方法,克服了猪牛羊剖层革仅从横截面观察鉴别方法中形态特征差异不明显,黑色甚至观察不到形态特征的缺点,能够准确反映猪牛羊剖层革胶原纤维组织结构特征;通过具体测量纤维束的长度和粗细程度,将试验过程数据化,使试验更具操作性;另外,猪牛羊剖层革纤维束的长度、粗细程度及形态特征差异较明显,因而能够准确的进行材质鉴别,鉴别更加简单有效。Compared with the prior art, the invention provides a simple method for identifying the material of the split leather of pigs, cattle and sheep. First, a hole is cut at any position of the split leather and torn along the cut, and then the fibrous tissue is cut at the tear gap. Then place the sample strip under a microscope to observe and take microscopic images, and measure the length and thickness of the fiber bundles through the microscope workstation software, and record the morphological characteristics of the fiber bundles, and finally the detected sample data Compared with the pre-stored known sample spectrum, it is identified which kind of leather the sample is from pigs, cattle and sheep. The invention opens up a new method for identifying the material of pig, cattle, and sheep split leather, overcomes the shortcomings of pig, cattle, and sheep split leather that are only observed from the cross-section in the identification method that the difference in morphological characteristics is not obvious, black or even no morphological characteristics can be observed, and can accurately Reflect the structural characteristics of collagen fibers in pig, cattle and sheep split leather; by measuring the length and thickness of fiber bundles, the test process is digitized to make the test more operable; in addition, the length of pig, cattle and sheep split leather fiber bundles, The difference in thickness and morphological characteristics is obvious, so the material identification can be accurately carried out, and the identification is simpler and more effective.

最后说明的是,以上实施例仅用以说明本发明的技术方案而非限制,尽管参照较佳实施例对本发明进行了详细说明,本领域的普通技术人员应当理解,可以对本发明的技术方案进行修改或者等同替换,而不脱离本发明技术方案的宗旨和范围,其均应涵盖在本发明的权利要求范围当中。Finally, it is noted that the above embodiments are only used to illustrate the technical solutions of the present invention without limitation. Although the present invention has been described in detail with reference to the preferred embodiments, those of ordinary skill in the art should understand that the technical solutions of the present invention can be carried out Modifications or equivalent replacements without departing from the spirit and scope of the technical solution of the present invention shall be covered by the claims of the present invention.

Claims (8)

1.一种猪牛羊剖层革材质简易鉴别方法,其特征在于,包括以下步骤:1. A simple and easy identification method for pig, cattle and sheep split leather materials, characterized in that it comprises the following steps: S1、在剖层革任意位置上剪开一个口,将剪口的两边端口分别夹持在拉力机的上下夹具上,开启拉力机,将剖层革沿剪口以200-300毫米/分钟的速度匀速撕裂,撕裂长度100毫米以上;S1. Cut a hole at any position of the split leather, clamp the ports on both sides of the notch on the upper and lower clamps of the tension machine, turn on the tension machine, and move the split leather along the notch at a rate of 200-300 mm/min. Uniform speed tearing, tearing length more than 100mm; S2、剪取撕裂裂口纤维组织试样条,所述试样条的长度为40-60毫米,宽度为3-6毫米,且该试样条所包含的纤维束长短分布较均匀并具有代表性;S2. Cut the tear fibrous tissue sample strip, the length of the sample strip is 40-60 mm, the width is 3-6 mm, and the length distribution of the fiber bundles contained in the sample strip is relatively uniform and representative sex; S3、将剪取的试样条置于显微镜下观察并拍摄显微图像,通过显微镜工作站AxioVision软件测量纤维束的长度和粗细程度,并记录纤维束的形态特征;S3. Place the cut sample strip under a microscope to observe and take a microscopic image, measure the length and thickness of the fiber bundle through the microscope workstation AxioVision software, and record the morphological characteristics of the fiber bundle; S4、将拍摄的显微图像、测量的纤维束长度和粗细程度以及记录的纤维束形态特征与预存的已知样品图谱进行对比,鉴别出试样为猪牛羊中的何种皮革。S4. Comparing the photographed microscopic image, the measured length and thickness of the fiber bundles, and the recorded morphological features of the fiber bundles with the pre-stored known sample atlas, to identify which kind of leather the sample is from pigs, cattle and sheep. 2.根据权利要求1所述的猪牛羊剖层革材质简易鉴别方法,其特征在于,步骤S2中,所述试样条所包含的纤维束长短分布较均匀并具有代表性是指:所剪取的试样条纤维束长短、疏密要与全部裂口纤维束情况一致,不能只剪取纤维束全部为长或短、疏或密的试样。2. The simple method for identifying the material of pig, cattle and sheep split leather according to claim 1, characterized in that, in step S2, the length distribution of the fiber bundles contained in the sample strip is relatively uniform and representative means: The length and density of the fiber bundles of the cut sample strips should be consistent with the conditions of all the cracked fiber bundles, and it is not possible to just cut samples with all the fiber bundles being long or short, sparse or dense. 3.根据权利要求1所述的猪牛羊剖层革材质简易鉴别方法,其特征在于,步骤S3中,所述显微镜为体视显微镜并带有标尺功能,放大倍数至少能在10-100倍之间无级调节。3. The simple identification method for pig, cattle and sheep split leather material according to claim 1, characterized in that, in step S3, the microscope is a stereo microscope with a ruler function, and the magnification can be at least 10-100 times Stepless adjustment between. 4.根据权利要求1所述的猪牛羊剖层革材质简易鉴别方法,其特征在于,步骤S3中,所述显微镜分别拍摄放大倍数为10倍和100倍的显微图像,所述显微镜工作站AxioVision软件分别测量10倍显微图像下纤维束的长度和100倍显微图像下纤维束的粗细程度,并在100倍显微图像下观察纤维束的形态特征。4. The simple identification method for pig, cattle and sheep split leather material according to claim 1, characterized in that in step S3, the microscope takes microscopic images with magnifications of 10 times and 100 times respectively, and the microscope workstation AxioVision software measured the length of the fiber bundles under the 10X microscopic image and the thickness of the fiber bundles under the 100X microscopic image, and observed the morphological characteristics of the fiber bundles under the 100X microscopic image. 5.根据权利要求1所述的猪牛羊剖层革材质简易鉴别方法,其特征在于,步骤S3中,所述纤维束的长度测量的是纤维束长短较均匀部分的长度,所述纤维束的粗细程度测量的是纤维束中部靠尖端部分的粗细程度。5. The simple method for identifying the material of pig, cattle and sheep split leather according to claim 1, characterized in that, in step S3, the length of the fiber bundle is measured as the length of the part where the length of the fiber bundle is relatively uniform, and the length of the fiber bundle is The thickness of the fiber bundle measures the thickness of the middle part of the fiber bundle near the tip. 6.根据权利要求1所述的猪牛羊剖层革材质简易鉴别方法,其特征在于,步骤S3中,所述纤维束的形态特征包括纤维束或呈束状或分散、或竖直或卷曲以及纤维束或圆或扁。6. The simple method for identifying the material of pig, cattle and sheep split leather according to claim 1, characterized in that, in step S3, the morphological characteristics of the fiber bundles include fiber bundles or being bundled or scattered, or vertical or curled And fiber bundles are either round or flat. 7.根据权利要求1所述的猪牛羊剖层革材质简易鉴别方法,其特征在于,步骤S4中,所述预存的已知样品图谱为实验室采集的大量猪牛羊已知种类剖层革经过实验步骤后归纳总结的猪牛羊典型性代表显微图谱,该样品图谱包括显微图像和纤维束长度、粗细程度及形态特征的描述。7. The method for simple identification of pig, cattle and sheep split leather materials according to claim 1, characterized in that, in step S4, the pre-stored known sample atlas is a large number of known species of pigs, cattle and sheep split layers collected in the laboratory Typical representative micrographs of pigs, cattle and sheep summarized after the experimental procedures of leather, which include microscopic images and descriptions of fiber bundle length, thickness and morphological characteristics. 8.根据权利要求7所述的猪牛羊剖层革材质简易鉴别方法,其特征在于,所述预存的已知样品图谱中,猪皮纤维束长2-10毫米,牛皮纤维束长2-10毫米,羊皮纤维束长0-6毫米;猪皮纤维束粗20-40微米,牛皮纤维束粗70-130微米,羊皮纤维束粗30-70微米;猪皮纤维束形态特征以束状形式存在,稍扁很细很直,牛皮纤维束形态特征以束状形式存在,较圆较直,羊皮纤维束形态特征以分散形式存在,稍扁略卷曲。8. The simple and easy identification method of pig, cattle and sheep split leather material according to claim 7, characterized in that, in the known sample collections stored in advance, the length of pigskin fiber bundles is 2-10 mm, and the length of cowhide fiber bundles is 2-10 mm. 10 mm, sheepskin fiber bundles are 0-6 mm long; pigskin fiber bundles are 20-40 microns thick, cowhide fiber bundles are 70-130 microns thick, sheepskin fiber bundles are 30-70 microns thick; pigskin fiber bundles are characterized by bundles Existence, slightly flat, very thin and straight, the morphological characteristics of cowhide fiber bundles exist in the form of bundles, which are rounder and straighter, and the morphological characteristics of sheepskin fiber bundles exist in a dispersed form, slightly flat and slightly curly.
CN201610938736.2A 2016-10-31 2016-10-31 A simple method for identifying the material of pig, cattle and sheep split leather Expired - Fee Related CN106525848B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610938736.2A CN106525848B (en) 2016-10-31 2016-10-31 A simple method for identifying the material of pig, cattle and sheep split leather

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610938736.2A CN106525848B (en) 2016-10-31 2016-10-31 A simple method for identifying the material of pig, cattle and sheep split leather

Publications (2)

Publication Number Publication Date
CN106525848A true CN106525848A (en) 2017-03-22
CN106525848B CN106525848B (en) 2019-04-23

Family

ID=58293283

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610938736.2A Expired - Fee Related CN106525848B (en) 2016-10-31 2016-10-31 A simple method for identifying the material of pig, cattle and sheep split leather

Country Status (1)

Country Link
CN (1) CN106525848B (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107463962A (en) * 2017-08-08 2017-12-12 张天君 A kind of method and system of micro- artificial intelligence identification suitcase
CN108254375A (en) * 2017-12-29 2018-07-06 广州检验检测认证集团有限公司 A kind of method for differentiating ox leather and buffalo leather

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4414250A1 (en) * 1994-01-04 1995-08-03 Jose Alba Fernandez Document holder with additional section for containing credit cards, identity card, etc.
CN202119686U (en) * 2011-06-02 2012-01-18 昆山阿基里斯人造皮有限公司 Seam fatigue testing machine
CN102725627A (en) * 2010-01-18 2012-10-10 沃尔斯多夫皮革施密特有限责任两合公司 Test device for determining the quality of leather
CN102809563A (en) * 2012-08-14 2012-12-05 广州市质量监督检测研究院 Simple identification method for leather fiber structure
CN105842431A (en) * 2016-03-17 2016-08-10 广州狮岭皮革皮具产业研究中心有限公司 Leather quality detection method

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4414250A1 (en) * 1994-01-04 1995-08-03 Jose Alba Fernandez Document holder with additional section for containing credit cards, identity card, etc.
CN102725627A (en) * 2010-01-18 2012-10-10 沃尔斯多夫皮革施密特有限责任两合公司 Test device for determining the quality of leather
CN202119686U (en) * 2011-06-02 2012-01-18 昆山阿基里斯人造皮有限公司 Seam fatigue testing machine
CN102809563A (en) * 2012-08-14 2012-12-05 广州市质量监督检测研究院 Simple identification method for leather fiber structure
CN105842431A (en) * 2016-03-17 2016-08-10 广州狮岭皮革皮具产业研究中心有限公司 Leather quality detection method

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
严关炳: "《皮革品痕迹检验》", 31 July 2007 *

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107463962A (en) * 2017-08-08 2017-12-12 张天君 A kind of method and system of micro- artificial intelligence identification suitcase
CN107463962B (en) * 2017-08-08 2020-06-02 张天君 Method and system for identifying leather bag through microscopic artificial intelligence
CN108254375A (en) * 2017-12-29 2018-07-06 广州检验检测认证集团有限公司 A kind of method for differentiating ox leather and buffalo leather

Also Published As

Publication number Publication date
CN106525848B (en) 2019-04-23

Similar Documents

Publication Publication Date Title
Bancelin et al. Ex vivo multiscale quantitation of skin biomechanics in wild-type and genetically-modified mice using multiphoton microscopy
Bachmann et al. Flexural stiffness of feather shafts: geometry rules over material properties
Mane et al. Validation of immunoexpression of tenascin-C in oral precancerous and cancerous tissues using ImageJ analysis with novel immunohistochemistry profiler plugin: An immunohistochemical quantitative analysis
Ragazzi et al. Ex vivo (fluorescence) confocal microscopy in surgical pathology: state of the art
CN106525848A (en) Simple identification method of pig, cattle and sheep split leather
Shein-Idelson et al. Large-scale mapping of cortical synaptic projections with extracellular electrode arrays
Dickson et al. Fluorescence imaging of cambial zones to study wood formation in Pinus radiata D. Don.
WO2002035207A2 (en) Method and system for analyzing cells
US20180040120A1 (en) Methods for quantitative assessment of mononuclear cells in muscle tissue sections
CN102967497B (en) Position observation in plant leaf blade micromechanism and the method that blade is processed
CN108230387A (en) A kind of method and device of fibrous septum characteristic quantification
DE102006038335A1 (en) Analysis of cell for diagnosing cancer, comprises introducing cells on carrier, coloring the cells by first coloring means, creating and storing first digital image of the colored cells, and treating the cells with second coloring means
Yildirim et al. Quantitative differentiation of normal and scarred tissues using second‐harmonic generation microscopy
Karlsson et al. Tissue microarray validation: a methodologic study with special reference to lung cancer
CN108198170B (en) A kind of identification method and device of fiber interval
CN105699312A (en) Method for identifying material of leather product
CN109978849A (en) Baseline cell determination method, device and readable medium based on digital pathological images
Jedrych et al. Expression of p75 neurotrophin receptor in desmoplastic trichoepithelioma, infiltrative basal cell carcinoma, and microcystic adnexal carcinoma
DE102005017515A1 (en) Wind tunnel reading analyzing device, for determining aerodynamic characteristics of aircraft, has processor performing automatic identification of flow unit in recorded image during wind tunnel reading, where image of flow unit is recorded
WO2019175082A1 (en) In-vitro method for determining a cell type of a white blood cell without labeling
Rogers et al. A method of sampling blood from Australian freshwater turtles
Wood et al. An ultrastructural and morphometric analysis of an in vivo contact guidance system
Rush et al. Detection of microinvasion in vulvar and cervical intraepithelial neoplasia using double immunostaining for cytokeratin and basement membrane components
Richena et al. Simultaneous morphological analysis of large numbers of hair cross sections as a tool for investigation of population‐level trends
Oztan et al. Biologically-driven cell-graphs for breast tissue grading

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20190423