[go: up one dir, main page]

CN106501155A - Rock core gas liquid two purpose permeability test device and reservoir damage evaluation method - Google Patents

Rock core gas liquid two purpose permeability test device and reservoir damage evaluation method Download PDF

Info

Publication number
CN106501155A
CN106501155A CN201611037818.6A CN201611037818A CN106501155A CN 106501155 A CN106501155 A CN 106501155A CN 201611037818 A CN201611037818 A CN 201611037818A CN 106501155 A CN106501155 A CN 106501155A
Authority
CN
China
Prior art keywords
gas
rock core
port
liquid
permeability
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201611037818.6A
Other languages
Chinese (zh)
Inventor
吕帅锋
李�瑞
刘露露
肖宇航
董庆祥
袁铭
吕凯
谷媛媛
李俊阳
刘少杰
粟冬梅
刘盼盼
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
China University of Geosciences
Original Assignee
China University of Geosciences
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by China University of Geosciences filed Critical China University of Geosciences
Priority to CN201611037818.6A priority Critical patent/CN106501155A/en
Publication of CN106501155A publication Critical patent/CN106501155A/en
Pending legal-status Critical Current

Links

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N15/00Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
    • G01N15/08Investigating permeability, pore-volume, or surface area of porous materials
    • G01N15/082Investigating permeability by forcing a fluid through a sample
    • G01N15/0826Investigating permeability by forcing a fluid through a sample and measuring fluid flow rate, i.e. permeation rate or pressure change

Landscapes

  • Chemical & Material Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Analytical Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Fluid Mechanics (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Sampling And Sample Adjustment (AREA)

Abstract

本发明属于油气开发室内模拟实验装置及评价技术领域,具体涉及一种岩心气液两用渗透率测试装置及储层伤害评价方法。该装置至少包括:气驱进样装置,其包括气驱进气模块和气驱进液模块;可视岩心夹持器,其包括进口端、出口端、第一塞体和第二塞体;以及与出气管道连通的气体流量计。该方法通过上述装置分别测出岩心的气体渗透率K1和污染伤害后的岩心气体渗透率K2,再进行渗透率恢复率和渗透率伤害率的计算。本发明所提供的技术方案能够同时测试岩心的气体渗透率和液体流动渗透率以及在工作液污染下岩心的渗透率恢复程度。该装置仿真性强,连接巧妙,结构简单,操作方便,稳定性高,坚固耐用。

The invention belongs to the technical field of simulation experiment devices and evaluations in oil and gas development chambers, and in particular relates to a rock core gas-liquid dual-purpose permeability testing device and a reservoir damage evaluation method. The device at least includes: a gas-drive sampling device, which includes a gas-drive inlet module and a gas-drive liquid inlet module; a visible core holder, which includes an inlet port, an outlet port, a first plug body, and a second plug body; and A gas flow meter connected to the gas outlet pipeline. In the method, the gas permeability K 1 of the rock core and the gas permeability K 2 of the rock core after pollution damage are respectively measured by the above-mentioned device, and then the permeability recovery rate and the permeability damage rate are calculated. The technical solution provided by the invention can simultaneously test the gas permeability and liquid flow permeability of the rock core and the recovery degree of the rock core permeability under working fluid pollution. The device has strong simulation, ingenious connection, simple structure, convenient operation, high stability and durability.

Description

岩心气液两用渗透率测试装置及储层伤害评价方法Core gas-liquid dual-purpose permeability testing device and reservoir damage evaluation method

技术领域technical field

本发明属于油气开发室内模拟实验装置及评价技术领域,具体涉及一种岩心气液两用渗透率测试装置及储层伤害评价方法。The invention belongs to the technical field of simulation experiment devices and evaluations in oil and gas development chambers, and in particular relates to a rock core gas-liquid dual-purpose permeability testing device and a reservoir damage evaluation method.

背景技术Background technique

在油气藏开发过程中,工作液(如钻井液、完井液、压裂液等)常常会对储层造成伤害,造成储层渗透率的降低,从而影响油气产量的提高。模拟工作液对储层的污染过程以及评价储层渗透率伤害程度对油气开采和储层保护具有一定的指导意义和借鉴意义。During the development of oil and gas reservoirs, working fluids (such as drilling fluids, completion fluids, fracturing fluids, etc.) often cause damage to the reservoir, resulting in a decrease in the permeability of the reservoir, thereby affecting the increase in oil and gas production. Simulating the pollution process of the working fluid to the reservoir and evaluating the degree of damage to the reservoir permeability have certain guiding and reference significance for oil and gas production and reservoir protection.

以往测试岩心渗透率实验装置基本是气体渗透率测试装置和液体流动渗透率测试装置,往往二者是分开的两套装置。对于同一个岩心,需要分别用两套装置测试,在取出和装入岩心的过程中,一方面造成了岩心的不可避免的损伤以及实验条件的改变,另一方面使得实验时间和成本大大增加。本装置能够使同一岩心在同一装置中分别测出气体渗透率和液体渗透率,进而评价岩心的渗透率伤害和恢复程度。In the past, the experimental devices for testing rock core permeability were basically gas permeability testing devices and liquid flow permeability testing devices, which were often two separate devices. For the same rock core, two sets of devices are required to test respectively. During the process of taking out and loading the rock core, on the one hand, the inevitable damage of the rock core and the change of the experimental conditions are caused, and on the other hand, the time and cost of the experiment are greatly increased. The device can respectively measure the gas permeability and liquid permeability of the same rock core in the same device, and then evaluate the permeability damage and recovery degree of the rock core.

中国专利申请CN201110368838公开了一种煤岩岩心气体渗透率测量装置,主要由高压气源模块、岩心夹持器模块、环压加载模块、数据计量模块、真空处理模块组成,通过针型阀相连,所述高压气源模块包括高压气瓶、减压阀、缓冲容器;所述岩心夹持器模块为岩心夹持器;所述环压加载模块为手摇泵;所述数据计量模块包括精密压力表和精密压力表、皂泡流量计;所述真空处理模块为真空泵。虽然该装置操作方便,测量数据重复性好,实验误差小,成本低,适用于煤岩岩心气体渗透率及等效液体渗透率测试领域,但是只能完成岩心气体渗透率这一种岩心渗透率的测量。中国专利申请201610134362.9公开了一种气水两相有效渗透率精确测定新装置及方法,该装置包括恒压气源、水恒速微量泵、压力表、夹持器缸、岩心、钢制圆柱体、橡皮套、水计量器和气计量器,所述恒压气源、压力表、夹持器缸、岩心、橡皮套、水计量器和气计量器依次连接。本发明还提供了一种气水两相有效渗透率精确测定新方法,虽然排除测试流体沿岩石样品侧表面与密封套之间间隙通过对测试结果造成的干扰,对通过岩心流体的流量计量更准确,渗透率计算结果更可靠,但其主要在提高精确度上,适用面依然有局限。Chinese patent application CN201110368838 discloses a coal rock core gas permeability measurement device, which is mainly composed of a high-pressure gas source module, a core holder module, a ring pressure loading module, a data metering module, and a vacuum processing module, which are connected through needle valves. The high-pressure gas source module includes a high-pressure gas cylinder, a pressure reducing valve, and a buffer container; the core holder module is a core holder; the ring pressure loading module is a hand pump; the data metering module includes a precision pressure table and precision pressure gauge, soap bubble flowmeter; the vacuum processing module is a vacuum pump. Although the device is easy to operate, has good repeatability of measurement data, small experimental error, and low cost, it is suitable for testing the gas permeability and equivalent liquid permeability of coal rock cores, but it can only complete the test of core gas permeability. Measurement. Chinese patent application 201610134362.9 discloses a new device and method for accurate measurement of gas-water two-phase effective permeability. The device includes a constant-pressure gas source, a water constant-speed micro pump, a pressure gauge, a holder cylinder, a rock core, and a steel cylinder , a rubber sleeve, a water gauge and a gas gauge, the constant pressure gas source, a pressure gauge, a holder cylinder, a rock core, a rubber sleeve, a water gauge and a gas gauge are connected in sequence. The present invention also provides a new method for accurately measuring the gas-water two-phase effective permeability, although the interference caused by the passage of the test fluid along the gap between the side surface of the rock sample and the sealing sleeve on the test result is eliminated, the measurement of the flow rate of the fluid passing through the core is more accurate Accurate, the permeability calculation results are more reliable, but it is mainly to improve the accuracy, and the application is still limited.

发明内容Contents of the invention

为解决现有技术的不足,本发明提供了一种岩心气液两用渗透率测试装置及储层伤害评价方法。本发明所提供的技术方案能够同时测试岩心的气体渗透率和液体流动渗透率以及在工作液污染下岩心的渗透率恢复程度。该装置仿真性强,连接巧妙,结构简单,操作方便,稳定性高,坚固耐用。In order to solve the deficiencies of the prior art, the invention provides a rock core gas-liquid dual-purpose permeability testing device and a reservoir damage evaluation method. The technical solution provided by the invention can simultaneously test the gas permeability and liquid flow permeability of the rock core and the recovery degree of the rock core permeability under working fluid pollution. The device has strong simulation, ingenious connection, simple structure, convenient operation, high stability and durability.

本发明所提供的技术方案如下:The technical scheme provided by the present invention is as follows:

一种岩心气液两用渗透率测试装置,至少包括:A rock core gas-liquid dual-purpose permeability testing device, at least including:

气驱进样装置,所述气驱进样装置包括气驱进气模块和气驱进液模块;A gas drive sampling device, the gas drive sampling device includes a gas drive intake module and a gas drive liquid intake module;

可视岩心夹持器,所述可视岩心夹持器包括进口端和出口端,所述进口端设置有第一塞体,所述第一塞体设置有进气管道,所述出口端设置有第二塞体,所述第二塞体设置有出气管道,所述气驱进气模块和所述气驱进液模块分别连通所述进气管道;Visible core holder, the visible core holder includes an inlet end and an outlet end, the inlet end is provided with a first plug body, the first plug body is provided with an air inlet pipe, and the outlet end is provided with There is a second plug body, and the second plug body is provided with an air outlet pipe, and the air-drive air intake module and the air-drive liquid intake module are respectively connected to the air intake pipes;

以及与所述出气管道连通的气体流量计。And a gas flowmeter communicated with the gas outlet pipeline.

可视岩心夹持器具有透明的壳体,能够观测到液体流过岩心的现象,直观的反映岩心受污染过程。The visible core holder has a transparent shell, which can observe the phenomenon of liquid flowing through the core, and intuitively reflect the process of core contamination.

具体的:specific:

所述气驱进气模块包括依次连通的第一气源、储气罐和第一加热装置,所述第一加热装置连通所述进气管道;The gas drive intake module includes a first gas source, a gas storage tank, and a first heating device connected in sequence, and the first heating device communicates with the intake pipe;

所述气驱进液模块包括依次连通的第二气源、储液罐和第二加热装置,所述第二加热装置连通所述进气管道。The gas drive liquid intake module includes a second gas source, a liquid storage tank and a second heating device connected in sequence, and the second heating device communicates with the intake pipe.

进一步的,所述第一气源与所述第二气源为同一气源瓶;所述第一加热装置与所述第二加热装置为同一加热器。气源瓶提供氮气或者甲烷等气体,依据实验调整。Further, the first gas source and the second gas source are the same gas source bottle; the first heating device and the second heating device are the same heater. The gas source bottle provides gas such as nitrogen or methane, which is adjusted according to the experiment.

进一步的,在所述出气管道和所述气体流量计之间设置有集液瓶;Further, a liquid collecting bottle is arranged between the gas outlet pipeline and the gas flow meter;

在所述气体流量计的后端设置有气体收集瓶,所述气体收集瓶分别连通所述可视岩心夹持器和所述储气罐。A gas collection bottle is arranged at the rear end of the gas flow meter, and the gas collection bottle communicates with the visible core holder and the gas storage tank respectively.

进一步的,所述气驱进样装置还包括第一三通管路、第二三通管路、第三三通管路、第四三通管路、第五三通管路和第六三通管路,所述储气罐包括进气口和出气口,所述储液罐包括进液口和出液口,其中:Further, the gas drive sampling device also includes a first three-way pipeline, a second three-way pipeline, a third three-way pipeline, a fourth three-way pipeline, a fifth three-way pipeline and a sixth three-way pipeline. The gas storage tank includes an air inlet and an air outlet, and the liquid storage tank includes a liquid inlet and a liquid outlet, wherein:

所述第一三通管路的第一个端口连通所述气源瓶,所述第一三通管路的第二个端口连通所述可视岩心夹持器的加压端,所述第一三通管路的第三个端口分别连通所述进气口和所述进液口,;The first port of the first three-way pipeline communicates with the gas source bottle, the second port of the first three-way pipeline communicates with the pressurized end of the visible core holder, and the second A third port of the three-way pipeline communicates with the air inlet and the liquid inlet respectively;

所述第二三通管路的第一个端口连通所述出气口,所述第二三通管路的第二个端口连通所述第三三通管路的第一个端口;The first port of the second three-way pipeline communicates with the gas outlet, and the second port of the second three-way pipeline communicates with the first port of the third three-way pipeline;

所述第三三通管路的第二个端口连通所述储液罐的上端,所述第三三通管路的第三个端口连通所述第四三通管路的第一个端口;The second port of the third three-way pipeline communicates with the upper end of the liquid storage tank, and the third port of the third three-way pipeline communicates with the first port of the fourth three-way pipeline;

所述第四三通管路的第二个端口连通所述出液口,所述第四三通管路的第三个端口连通所述加热器,所述加热器连通所述可视岩心夹持器的进气管道;The second port of the fourth three-way pipeline communicates with the liquid outlet, the third port of the fourth three-way pipeline communicates with the heater, and the heater communicates with the visible core holder the intake pipe of the holder;

所述第五三通管路的第一个端口连通所述可视岩心夹持器的出气管道,所述第五三通管路的第二个端口连通所述集液瓶,所述第五三通管路的第三个端口连通所述气体流量计;The first port of the fifth three-way pipeline communicates with the gas outlet pipe of the visible core holder, the second port of the fifth three-way pipeline communicates with the liquid collection bottle, and the fifth The third port of the three-way pipeline communicates with the gas flow meter;

所述第六三通管路的第一个端口连通所述第二三通管路的第三个端口,所述第六三通管路的第二个端口连通所述可视岩心夹持器的卸压端,所述第六三通管路的第三个端口连通所述气体收集瓶。The first port of the sixth three-way pipeline communicates with the third port of the second three-way pipeline, and the second port of the sixth three-way pipeline communicates with the visible core holder The pressure relief end of the sixth three-way pipeline communicates with the gas collection bottle at the third port.

进一步的,所述第一三通管路的第二个端口连通有围压控制阀,所述围压控制阀连通所述可视岩心夹持器的加压端;Further, the second port of the first three-way pipeline is communicated with a confining pressure control valve, and the confining pressure control valve is communicated with the pressurized end of the visible core holder;

所述第一三通管路的第三个端口连通有进口压力控制阀,所述进口压力控制阀分别连通所述进气口和所述进液口;The third port of the first three-way pipeline is connected with an inlet pressure control valve, and the inlet pressure control valve is respectively connected with the air inlet and the liquid inlet;

所述第二三通管路的第三个端口连通有第一泄压阀,所述第一泄压阀连通所述第六三通管路的第一个端口;The third port of the second three-way pipeline is connected with a first pressure relief valve, and the first pressure relief valve is connected with the first port of the sixth three-way pipeline;

所述第六三通管路的第二个端口连通有第二泄压阀,所述第二泄压阀连通所述可视岩心夹持器的卸压端。The second port of the sixth three-way pipeline is communicated with a second pressure relief valve, and the second pressure relief valve is communicated with the pressure relief end of the visible core holder.

进一步的,在所述气源瓶和所述第一三通管路的第一个端口之间设置有第一气压表;Further, a first air pressure gauge is provided between the air source bottle and the first port of the first three-way pipeline;

在所述储气罐和所述储液罐的并联的进气端与所述进口压力控制阀之间设置有第二气压表;A second air pressure gauge is arranged between the parallel inlet ports of the air storage tank and the liquid storage tank and the inlet pressure control valve;

在所述围压控制阀和所述可视岩心夹持器的加压端之间设置有第三气压表。A third air pressure gauge is provided between the confining pressure control valve and the pressurized end of the visible core holder.

进一步的,在所述气源瓶和所述第一气压表之间设置有第一开关;Further, a first switch is provided between the air source bottle and the first air pressure gauge;

在所述储气罐和所述储液罐的并联的进气端和所述进气口之间设置有第二开关;A second switch is provided between the parallel air inlets of the air storage tank and the liquid storage tank and the air inlet;

在所述储气罐和所述储液罐的并联的进气端和所述进液口之间设置有第三开关;A third switch is provided between the parallel air inlets of the air storage tank and the liquid storage tank and the liquid inlet;

在所述出气口和所述第二三通管路的第一个端口之间设置有第四开关;A fourth switch is provided between the air outlet and the first port of the second three-way pipeline;

在连通所述储液罐的上端和所述第三三通管路的第二个端口的管路上设置有第五开关;A fifth switch is arranged on the pipeline connecting the upper end of the liquid storage tank and the second port of the third three-way pipeline;

在所述出液口和所述第四三通管路的第二个端口之间设置有第六开关;A sixth switch is provided between the liquid outlet and the second port of the fourth three-way pipeline;

在所述第五三通管路的第三个端口和所述气体流量计之间设置有第七开关;A seventh switch is provided between the third port of the fifth three-way pipeline and the gas flow meter;

在所述第五三通管路的第二个端口和所述集液瓶直接设置有第八开关;An eighth switch is directly arranged at the second port of the fifth three-way pipeline and the liquid collection bottle;

在所述第三三通管路的第三个端口和所述第四三通管路的第一个端口之间设置有第九开关。A ninth switch is provided between the third port of the third three-way line and the first port of the fourth three-way line.

需要说明的是,针对上述各三通管路,为了便于描述,将靠近气源一侧的端口描述为第一个端口,将远离气源一侧的端口描述为第三个端口,将第一个端口和第三个端口之间的端口描述为第二个端口。It should be noted that, for the above-mentioned three-way pipelines, for the convenience of description, the port on the side close to the gas source is described as the first port, the port on the side away from the gas source is described as the third port, and the first port Ports between the first port and the third port are described as second ports.

本发明还提供了一种储层伤害评价方法,包括以下步骤:The present invention also provides a reservoir damage evaluation method, comprising the following steps:

1)以权利要求7或8所述的岩心气液两用渗透率测试装置对岩心进行气体渗透率的测定,并计算岩心的气体渗透率,记为K11) carry out the mensuration of gas permeability to rock core with the described rock core gas-liquid dual-purpose permeability testing device of claim 7 or 8, and calculate the gas permeability of rock core, be denoted as K 1 ;

2)以权利要求7或8所述的岩心气液两用渗透率测试装置用测试岩心的液体渗透率的方法对岩心进行污染伤害;2) Carry out pollution damage to the rock core with the method for testing the liquid permeability of the rock core with the rock core gas-liquid dual-purpose permeability testing device described in claim 7 or 8;

3)以权利要求7或8所述的岩心气液两用渗透率测试装置对步骤2)污染伤害后的岩心进行气体渗透率的测定,并计算岩心的气体渗透率,记为K23) carry out the measurement of gas permeability to the rock core after step 2) pollution damage with the rock core gas-liquid dual-purpose permeability testing device described in claim 7 or 8, and calculate the gas permeability of rock core, be denoted as K 2 ;

4)计算K2/K1×100%,得到岩心的渗透率恢复率;计算(1-K2/K1)×100%,得到渗透率伤害率。4) Calculate K 2 /K 1 ×100% to obtain the core permeability recovery rate; calculate (1-K 2 /K 1 )×100% to obtain the permeability damage rate.

具体的,岩心的气体渗透率的测定方法包括以下步骤:Concrete, the measuring method of the gas permeability of rock core comprises the following steps:

1)关闭各开关、围压控制阀、进口压力控制阀和各泄压阀;1) Close all switches, confining pressure control valves, inlet pressure control valves and pressure relief valves;

2)在可视岩心夹持器中装入岩心,塞入第一塞体和第二塞体对岩心进行固定;2) Put the rock core in the visible rock core holder, insert the first plug body and the second plug body to fix the rock core;

3)打开第一开关,提供气压;3) Turn on the first switch to provide air pressure;

4)调节围压控制阀,给岩心施加围压;4) Adjust the confining pressure control valve to apply confining pressure to the rock core;

5)调节进口压力控制阀至固定压力,打开第二开关、第四开关、第九开关和第七开关,让实验气体通过岩心,调节加热器设定实验温度;5) Adjust the inlet pressure control valve to a fixed pressure, open the second switch, the fourth switch, the ninth switch and the seventh switch, let the experimental gas pass through the rock core, and adjust the heater to set the experimental temperature;

6)进口压力数值通过第二压力表5读取,出口压力为大气压,出口气体流量数值由气体流量计读取,岩心的长度和截面积测量得到,通过适合气体渗透率测试的修正达西公式计算出岩心的气体渗透率。6) The inlet pressure value is read by the second pressure gauge 5, the outlet pressure is atmospheric pressure, the outlet gas flow value is read by the gas flow meter, the length and cross-sectional area of the rock core are measured, and the modified Darcy formula suitable for the gas permeability test is obtained. Calculate the gas permeability of the core.

具体的,岩心的液体渗透率的测定方法包括以下步骤:Specifically, the measuring method of the liquid permeability of rock core comprises the following steps:

1)关闭各开关、围压控制阀、进口压力控制阀和各泄压阀;1) Close all switches, confining pressure control valves, inlet pressure control valves and pressure relief valves;

2)将待测液体装入储液罐,在可视岩心夹持器中装入岩心,塞入第一塞体和第二塞体对岩心进行固定;2) Put the liquid to be tested into the liquid storage tank, put the rock core into the visible rock core holder, insert the first plug body and the second plug body to fix the rock core;

3)打开第一开关,提供气压;3) Turn on the first switch to provide air pressure;

4)调节围压控制阀,对岩心施加围压;4) Adjust the confining pressure control valve to apply confining pressure to the rock core;

5)调节进口压力控制阀至固定压力,打开第三开关、第六开关和第八开关,让气体驱替待测液通过岩心,调节加热器设定实验温度;5) Adjust the inlet pressure control valve to a fixed pressure, open the third switch, the sixth switch and the eighth switch, let the gas displace the liquid to be tested to pass through the rock core, and adjust the heater to set the experimental temperature;

6)进口压力数值通过第二压力表5读取,出口压力为大气压,出口液体流量通过计时和集液瓶中液体体积计算得到,岩心的长度和截面积测量得到,通过达西渗流公式计算出岩心的液体渗透率。6) The inlet pressure value is read by the second pressure gauge 5, the outlet pressure is atmospheric pressure, the outlet liquid flow rate is calculated by timing and the liquid volume in the liquid collection bottle, the length and cross-sectional area of the rock core are measured, and it is calculated by the Darcy seepage formula Liquid permeability of the core.

相比较现有技术,本发明具有以下优点:Compared with the prior art, the present invention has the following advantages:

1、在同一装置条件下可以实现测试岩心气体渗透率和液体渗透率的目的,操作简单,节省实验时间,避免了两套仪器分开测试造成的岩心损坏。1. Under the same device conditions, the purpose of testing the gas permeability and liquid permeability of the rock core can be realized. The operation is simple, the experiment time is saved, and the core damage caused by the separate testing of the two sets of instruments is avoided.

2、本装置中岩心夹持器可视,能够观测到液体流过岩心的现象,直观的反映岩心受污染过程。2. The core holder in this device is visible, and the phenomenon of liquid flowing through the core can be observed, which directly reflects the process of the core being polluted.

3、具有加热恒温装置,能够实现在特定的温度条件下测试液体或者气体渗透率。3. It has a heating constant temperature device, which can realize the test of liquid or gas permeability under specific temperature conditions.

4、实验气体为氮气,可以排放至空气,如果为甲烷等对环境不友好气体,则可以通过气体收集器收集实验气体。4. The experimental gas is nitrogen, which can be discharged into the air. If it is an unfriendly gas such as methane, the experimental gas can be collected by a gas collector.

附图说明Description of drawings

图1是本发明所提供的岩心气液两用渗透率测试装置的结构示意图。Fig. 1 is a schematic structural view of a rock core gas-liquid dual-purpose permeability testing device provided by the present invention.

附图1中,各标号所代表的结构列表如下:In accompanying drawing 1, the structural list represented by each label is as follows:

1、气源瓶,2、第一开关,3、第一气压表,4、进口压力控制阀,5、第二气压表,6、第二开关,7、储气罐,8、第四开关,9、第三开关,10、储液罐,11、第六开关,12、可视岩心夹持器,13、第一塞体,14、第二塞体,15、岩心,16、围压控制阀,17、第一三通管路,18、第三气压表,19、第七开关,20、第八开关,21、集液瓶,22、气体流量计,23、气体收集瓶,24、加热器,25、第一泄压阀,26、第五开关,27、第九开关,28、第二泄压阀。1. Air source bottle, 2. First switch, 3. First air pressure gauge, 4. Inlet pressure control valve, 5. Second air pressure gauge, 6. Second switch, 7. Air storage tank, 8. Fourth switch , 9, the third switch, 10, the liquid storage tank, 11, the sixth switch, 12, the visible core holder, 13, the first plug body, 14, the second plug body, 15, the rock core, 16, the confining pressure Control valve, 17, first three-way pipeline, 18, third air pressure gauge, 19, seventh switch, 20, eighth switch, 21, liquid collection bottle, 22, gas flow meter, 23, gas collection bottle, 24 , heater, 25, the first pressure relief valve, 26, the fifth switch, 27, the ninth switch, 28, the second pressure relief valve.

具体实施方式detailed description

以下对本发明的原理和特征进行描述,所举实施例只用于解释本发明,并非用于限定本发明的范围。The principles and features of the present invention are described below, and the examples given are only used to explain the present invention, and are not intended to limit the scope of the present invention.

在一个具体实施方式中,如图1所示,一种岩心气液两用渗透率测试装置,包括气驱进样装置、可视岩心夹持器12、集液瓶21、气体流量计22和气体收集瓶23。可视岩心夹持器12包括进口端和出口端,进口端设置有第一塞体13,第一塞体13设置有进气管道,出口端设置有第二塞体14,第二塞体14设置有出气管道。可视岩心夹持器12内设置岩心15。In a specific embodiment, as shown in Figure 1, a rock core gas-liquid dual-purpose permeability testing device includes a gas drive sampling device, a visible rock core holder 12, a liquid collection bottle 21, a gas flow meter 22 and Gas collection bottle 23. The visible core holder 12 includes an inlet end and an outlet end, the inlet end is provided with a first plug body 13, the first plug body 13 is provided with an air inlet pipe, the outlet end is provided with a second plug body 14, and the second plug body 14 An outlet pipe is provided. A rock core 15 is arranged in the visible rock core holder 12 .

气驱进样装置包括气源瓶1、第一开关2、第一气压表3、第一三通管路17、进口压力控制阀4、第二气压表5、第二开关6、储气罐7、第四开关8、第三开关9、储液罐10、第六开关11、第二三通管路、第三三通管路、第四三通管路、加热器24、第五开关26和第九开关27。The air-driven sampling device includes a gas source bottle 1, a first switch 2, a first air pressure gauge 3, a first three-way pipeline 17, an inlet pressure control valve 4, a second air pressure gauge 5, a second switch 6, and an air storage tank 7. Fourth switch 8, third switch 9, liquid storage tank 10, sixth switch 11, second three-way pipeline, third three-way pipeline, fourth three-way pipeline, heater 24, fifth switch 26 and the ninth switch 27.

气源瓶1、第一开关2、第一气压表3、第一三通管路17和进口压力控制阀4和依次设置。进口压力控制阀4分别连通有第二开关6和第三开关9。第二开关6连通储气罐7,储气罐7连通第四开关8,第四开关8连通第二三通管路的第一个端口。The gas source bottle 1, the first switch 2, the first air gauge 3, the first three-way pipeline 17 and the inlet pressure control valve 4 are arranged in sequence. The inlet pressure control valve 4 communicates with a second switch 6 and a third switch 9 respectively. The second switch 6 communicates with the gas storage tank 7 , the gas storage tank 7 communicates with the fourth switch 8 , and the fourth switch 8 communicates with the first port of the second three-way pipeline.

第三开关9连通储液罐10,储液罐10连通第六开关11,第六开关11连通第四三通管路的第二个端口。The third switch 9 communicates with the liquid storage tank 10 , the liquid storage tank 10 communicates with the sixth switch 11 , and the sixth switch 11 communicates with the second port of the fourth three-way pipeline.

另外,储液罐10的上端连通第五开关26,第五开关26连通第三三通管路的第二个端口。In addition, the upper end of the liquid storage tank 10 is connected to the fifth switch 26, and the fifth switch 26 is connected to the second port of the third three-way pipeline.

第二三通阀的第二个端口、第三三通的第一个端口、第三三通阀的第三个端口、第四三通阀的第三个端口、加热器24以及进口管道依次连通。The second port of the second three-way valve, the first port of the third three-way valve, the third port of the third three-way valve, the third port of the fourth three-way valve, the heater 24 and the inlet pipeline in turn connected.

进口管道连通第五三通管路的第一个端口,第五三通管路的第二个端口连通第八开关20,第八开关20连通集液瓶21。第五三通管路的第三个端口连通第七开关19,第七开关19连通气体流量计22。气体流量计22连通气体收集瓶23,气体收集瓶23连通第六三通管路的第三个端口。第六三通管路的第二个端口连通第二泄压阀28,第二泄压阀28连通可视岩心夹持器12的泄压端。第六三通管路的第一个端口连通第一泄压阀25,第一泄压阀25连通第二三通管路的第三个端口。第三三通管路的第三个端口和第四三通管路的第一个端口之间设置第九开关27。The inlet pipeline communicates with the first port of the fifth three-way pipeline, the second port of the fifth three-way pipeline communicates with the eighth switch 20 , and the eighth switch 20 communicates with the liquid collection bottle 21 . The third port of the fifth three-way pipeline is connected to the seventh switch 19 , and the seventh switch 19 is connected to the gas flow meter 22 . The gas flow meter 22 is connected to the gas collection bottle 23, and the gas collection bottle 23 is connected to the third port of the sixth three-way pipeline. The second port of the sixth three-way pipeline communicates with the second pressure relief valve 28 , and the second pressure relief valve 28 communicates with the pressure relief end of the visible core holder 12 . The first port of the sixth three-way pipeline communicates with the first pressure relief valve 25, and the first pressure relief valve 25 communicates with the third port of the second three-way pipeline. A ninth switch 27 is arranged between the third port of the third three-way pipeline and the first port of the fourth three-way pipeline.

第一开关和第一三通管路17之间设置第一气压表3。进口压力控制阀4之后设置第二气压表5。第一三通管路的17的第二个端口连接围压控制阀16,围压控制阀16和可视岩心夹持器12的加压端之间设置、第三气压表18。A first air pressure gauge 3 is arranged between the first switch and the first three-way pipeline 17 . A second air pressure gauge 5 is arranged after the inlet pressure control valve 4 . The second port of the first three-way pipeline 17 is connected to the confining pressure control valve 16, and a third air pressure gauge 18 is provided between the confining pressure control valve 16 and the pressurized end of the visible core holder 12.

在上述装置中In the above device

气源瓶1,可为氮气或者甲烷等气体,根据实验需要而定;Gas source bottle 1 can be gas such as nitrogen or methane, depending on the needs of the experiment;

第一开关2,控制气源开关;The first switch 2 controls the air source switch;

第一气压表3,显示气源压力;The first air pressure gauge 3 shows the air source pressure;

进口压力控制阀4,控制进入储气罐7和储液罐10中的压力;The inlet pressure control valve 4 controls the pressure entering the gas storage tank 7 and the liquid storage tank 10;

第二气压表5,显示进入储气罐7和储液罐10中的压力;The second air gauge 5 shows the pressure entering the air storage tank 7 and the liquid storage tank 10;

第二开关6,安装在进口压力控制阀4和储气罐7之间管路上,控制储气罐7的压力;The second switch 6 is installed on the pipeline between the inlet pressure control valve 4 and the gas storage tank 7 to control the pressure of the gas storage tank 7;

储气罐7,里边气体即气源1中的气体;The gas storage tank 7, the gas inside is the gas in the gas source 1;

第四开关8,安装在储气罐7和夹持器第一塞体13之间管路上,控制储气罐气体的进口压力;The fourth switch 8 is installed on the pipeline between the gas storage tank 7 and the first plug body 13 of the holder to control the inlet pressure of the gas storage tank;

第三开关9,安装在进口压力控制阀4和储液罐10之间管路上,控制储液罐10的压力;The third switch 9 is installed on the pipeline between the inlet pressure control valve 4 and the liquid storage tank 10 to control the pressure of the liquid storage tank 10;

储液罐10,内装实验待测液,比如清水、钻井液等;Fluid storage tank 10, built-in experimental liquid to be tested, such as clear water, drilling fluid, etc.;

第六开关11,安装在储气罐10和夹持器第一塞体13之间管路上,控制储液罐气体的进口压力;The sixth switch 11 is installed on the pipeline between the gas storage tank 10 and the first plug body 13 of the holder to control the gas inlet pressure of the liquid storage tank;

可视岩心夹持器12,夹持器由刚性外壳和内部气囊构成,可以通过控制围压阀16使气体进入刚性外壳和气囊之间的密闭空间,从而施加围压以夹紧岩心,此夹持器为透明材料做成;Visible core holder 12, the holder is composed of a rigid shell and an internal air bag, the gas can enter the closed space between the rigid shell and the air bag by controlling the confining pressure valve 16, thereby exerting confining pressure to clamp the core, this clamp The holder is made of transparent material;

第一塞体13和第二塞体14,第一塞体13和第二塞体分别在夹持器12两端,可以插入夹持器从而固定岩心;The first plug body 13 and the second plug body 14, the first plug body 13 and the second plug body are respectively at both ends of the holder 12, and can be inserted into the holder to fix the rock core;

岩心15,装在夹持器中,为天然岩心或者人造岩心;The rock core 15 is contained in the holder and is a natural rock core or an artificial rock core;

围压控制阀16,通过调节围压控制阀从而调节岩心周向压力;The confining pressure control valve 16 is used to adjust the peripheral pressure of the rock core by adjusting the confining pressure control valve;

第一三通管路17,分别与气源钢瓶1、储气罐7/储液罐10、夹持器12相连,由气源钢瓶提供气体,通过进口压力控制阀4和围压控制阀18来调节输出压力大小;The first three-way pipeline 17 is respectively connected with the gas source steel cylinder 1, the gas storage tank 7/liquid storage tank 10, and the holder 12, and the gas is provided by the gas source steel cylinder through the inlet pressure control valve 4 and the confining pressure control valve 18 To adjust the output pressure;

第三气压表18,显示岩心围压大小;The third barometer 18 shows the size of the confining pressure of the rock core;

第七开关19,安装在第二塞体14和气体流量计22之间的管路上;The seventh switch 19 is installed on the pipeline between the second plug body 14 and the gas flow meter 22;

第八开关20,安装在第二塞体出液管路上,控制液体流出;The eighth switch 20 is installed on the liquid outlet pipeline of the second plug body to control the liquid outflow;

集液瓶21,收集流出的液体,可读出液体体积;The liquid collection bottle 21 collects the liquid flowing out, and the volume of the liquid can be read out;

气体流量计22,可读出气体通过时的流量;Gas flow meter 22, which can read the flow rate when the gas passes through;

气体收集器23,能够将从气体流量计通过的气体和储气罐中的气体收集起来;The gas collector 23 can collect the gas passing through the gas flow meter and the gas in the gas storage tank;

加热器24,装在连接第一塞体的管路上,为进入夹持器的气体/液体加热,可显示温度值;The heater 24 is installed on the pipeline connected to the first plug body to heat the gas/liquid entering the holder, and can display the temperature value;

第一泄压阀25,用于泄掉储气罐7和储液罐10中压力;The first pressure relief valve 25 is used to release the pressure in the gas storage tank 7 and the liquid storage tank 10;

第五开关26,装在连接储液罐10罐口和第一塞体的管路上;The fifth switch 26 is installed on the pipeline connecting the mouth of the liquid storage tank 10 and the first plug body;

第九开关装27在连接开关26和开关11的管路上;The ninth switch device 27 is on the pipeline connecting the switch 26 and the switch 11;

第二泄压阀28,用于泄掉夹持器围压。The second pressure relief valve 28 is used to release the confining pressure of the holder.

以上部件之间均为金属管路连接。The above components are connected by metal pipelines.

实施例Example

气体渗透率测试方法和步骤:Gas permeability test method and steps:

1实验开始前保证所有开关、控制阀和泄压阀关闭。1 Ensure that all switches, control valves and pressure relief valves are closed before the experiment starts.

2在可视岩心夹持器12中装入岩心,插入第一塞体13和第二塞体14固定之。2. Put the core in the visible core holder 12, insert the first plug body 13 and the second plug body 14 to fix it.

3打开第一开关2,提供气压。3. Turn on the first switch 2 to provide air pressure.

4调节围压控制阀16,给岩心施加一定围压。4. Adjust the confining pressure control valve 16 to apply a certain confining pressure to the rock core.

5调节进口压力控制阀4至固定压力,打开储气罐开关6、第四开关8、第九开关27和第七开关19,让实验气体通过岩心。调节加热器24设定实验温度。5 Adjust the inlet pressure control valve 4 to a fixed pressure, open the gas storage tank switch 6, the fourth switch 8, the ninth switch 27 and the seventh switch 19, and let the experimental gas pass through the rock core. Adjust the heater 24 to set the experimental temperature.

6进口压力数值通过第二气压表5读取,出口气体流量数值由气体流量计22读取,出口压力为大气压,岩心的长度和截面积可测,从而通过达西定律修正公式计算出岩心的气体渗透率。6. The inlet pressure value is read by the second barometer 5, and the outlet gas flow value is read by the gas flow meter 22. The outlet pressure is atmospheric pressure, and the length and cross-sectional area of the rock core can be measured, so that the rock core can be calculated by the modified formula of Darcy's law. gas permeability.

7实验完毕后,关闭第一开关2、第二开关6、第七开关19、第九开关27、进口压力控制阀4和围压控制阀16。打开泄压阀25排出储气罐7中的气体,之后关闭第四开关8和泄压阀25,打开泄压阀28泄掉夹持器12上的围压。7 After the experiment is completed, close the first switch 2, the second switch 6, the seventh switch 19, the ninth switch 27, the inlet pressure control valve 4 and the confining pressure control valve 16. Open the pressure relief valve 25 to discharge the gas in the gas storage tank 7, then close the fourth switch 8 and the pressure relief valve 25, and open the pressure relief valve 28 to release the confining pressure on the holder 12.

液体渗透率测试方法和步骤:Liquid permeability test method and steps:

1实验开始前保证所有开关、控制阀和泄压阀关闭。1 Ensure that all switches, control valves and pressure relief valves are closed before the experiment starts.

2将待测液体装入储液罐10;在可视岩心夹持器12中装入岩心,插入第一塞体13和第二塞体14固定之。2. Put the liquid to be tested into the liquid storage tank 10; put the core into the visible core holder 12, insert the first plug body 13 and the second plug body 14 to fix it.

3打开第一开关2,提供气压。3. Turn on the first switch 2 to provide air pressure.

4调节围压控制阀16,给岩心施加一定围压。4. Adjust the confining pressure control valve 16 to apply a certain confining pressure to the rock core.

5调节进口压力控制阀4至固定压力,打开储第三开关9、第六开关11和第八开关20,让气体驱替待测液通过岩心。调节加热器24设定实验温度。5. Adjust the inlet pressure control valve 4 to a fixed pressure, open the third switch 9, the sixth switch 11 and the eighth switch 20, and let the gas displace the liquid to be tested to pass through the core. Adjust the heater 24 to set the experimental temperature.

6进口压力数值通过第二气压表5读取,出口液体流量通过计时和集液瓶21中液体体积计算得到,出口压力为大气压,岩心的长度和截面积可测,从而通过达西渗流公式计算出岩心的液体渗透率。6. The inlet pressure value is read by the second barometer 5, the outlet liquid flow rate is calculated by timing and the liquid volume in the liquid collection bottle 21, the outlet pressure is atmospheric pressure, and the length and cross-sectional area of the rock core can be measured, so it can be calculated by the Darcy seepage formula The fluid permeability of the core.

7实验完毕后,关闭第一开关2、第三开关9、第六开关11、开关20、进口压力控制阀4和围压控制阀16。打开泄压阀25和第五开关26排出储液罐10中的气体,之后关闭第五开关26和泄压阀25,打开泄压阀28卸掉夹持器12中的围压。最后将储液罐中剩余待测液体倒出。7 After the experiment is completed, close the first switch 2, the third switch 9, the sixth switch 11, the switch 20, the inlet pressure control valve 4 and the confining pressure control valve 16. Open the pressure relief valve 25 and the fifth switch 26 to discharge the gas in the liquid storage tank 10, then close the fifth switch 26 and the pressure relief valve 25, and open the pressure relief valve 28 to release the confining pressure in the holder 12. Finally pour out the remaining liquid to be tested in the liquid storage tank.

岩心渗透率伤害实验:Core permeability damage experiment:

1测得岩心的气体渗透率K1。1 Measure the gas permeability K1 of the core.

2通过测试岩心液体渗透率的方法用待测液对岩心进行污染伤害。2. Contaminate and damage the core with the liquid to be tested by testing the permeability of the core liquid.

3再次测得岩心的气体渗透率K2。3 Measure the gas permeability K2 of the core again.

4岩心的渗透率恢复率为K2/K1×100%,渗透率伤害率为(1-K2/K1)×100%。4 The permeability recovery rate of the core is K 2 /K 1 ×100%, and the permeability damage rate is (1-K 2 /K 1 )×100%.

以上所述仅为本发明的较佳实施例,并不用以限制本发明,凡在本发明的精神和原则之内,所作的任何修改、等同替换、改进等,均应包含在本发明的保护范围之内。The above descriptions are only preferred embodiments of the present invention, and are not intended to limit the present invention. Any modifications, equivalent replacements, improvements, etc. made within the spirit and principles of the present invention shall be included in the protection of the present invention. within range.

Claims (10)

1. a kind of rock core gas liquid two purpose permeability test device, it is characterised in that at least include:
Gas drive sampling device, the gas drive sampling device include gas drive air inlet module and gas drive feed liquor module;
Visual core holding unit (12), described visual core holding unit (12) include that entrance point and the port of export, the entrance point set The first cock body (13) is equipped with, the first cock body (13) are provided with admission line, and the port of export is provided with the second cock body (14), Second cock body (14) are provided with outlet pipe, and the gas drive air inlet module and the gas drive feed liquor module are respectively communicated with described Admission line;
And the gas flowmeter (22) connected with the outlet pipe.
2. rock core gas liquid two purpose permeability test device according to claim 1, it is characterised in that:
The gas drive air inlet module includes the first source of the gas, air accumulator (7) and the first heater being sequentially communicated, and described first adds Thermal connects the admission line;
The gas drive feed liquor module includes the second source of the gas, fluid reservoir (10) and the secondary heating mechanism being sequentially communicated, described second Heater connects the admission line.
3. rock core gas liquid two purpose permeability test device according to claim 2, it is characterised in that:First source of the gas with Second source of the gas is same gas source bottle (1);The first heater is same heater with the secondary heating mechanism (24).
4. rock core gas liquid two purpose permeability test device according to claim 3, it is characterised in that:
Liquid-collecting bottle (21) is provided between the outlet pipe and the gas flowmeter (22);
Gas flowmeter (22) are also connected with gas collection bottle (23), and gas collection bottle (23) are also respectively communicated with described Visual core holding unit (12) and the air accumulator (7).
5. rock core gas liquid two purpose permeability test device according to claim 4, it is characterised in that:The gas drive sample introduction dress Put With the 6th triplate line, described air accumulator (7) include that air inlet and gas outlet, described fluid reservoir (10) include inlet and go out liquid Mouthful, wherein:
The a port of the first triplate line (17) connects gas source bottle (1), the first triplate line (17) Second port connects the live end of visual core holding unit (12), the 3rd port of the first triplate line (17) The air inlet and the inlet is respectively communicated with,;
The a port of second triplate line connects the gas outlet, and second port of second triplate line connects Lead to a port of the 3rd triplate line;
Second port of the 3rd triplate line connects the upper end of fluid reservoir (10), and the of the 3rd triplate line Three ports connect a port of the 4th triplate line;
Second port of the 4th triplate line connects the liquid outlet, and the 3rd port of the 4th triplate line connects Lead to heater (24), described heater (24) connect the admission line of visual core holding unit (12);
The outlet pipe of a port connection visual core holding unit (12) of the 5th triplate line, the described 5th Second port of triplate line connects liquid-collecting bottle (21), and the 3rd port of the 5th triplate line connects the gas Flowmeter body (22);
The a port of the 6th triplate line connects the 3rd port of second triplate line, the 6th threeway Second port of pipeline connects the pressure side of unloading of visual core holding unit (12), the 3rd end of the 6th triplate line Mouth connects gas collection bottle (23).
6. rock core gas liquid two purpose permeability test device according to claim 5, it is characterised in that:
Second port of the first triplate line (17) is communicated with confined pressure control valve (16), and described confined pressure control valve (16) connect Lead to the live end of visual core holding unit (12);
3rd port of the first triplate line (17) is communicated with inlet-pressure force control valve (4), the inlet pressure control Valve (4) is respectively communicated with the air inlet and the inlet;
3rd port of second triplate line is communicated with the first relief valve (25), and described first relief valve (25) connect institute State a port of the 6th triplate line;
Second port of the 6th triplate line is communicated with the second relief valve (28), and described second relief valve (28) connect institute That states visual core holding unit (12) unloads pressure side.
7. rock core gas liquid two purpose permeability test device according to claim 6, it is characterised in that:
The first air gauge (3) is provided between a port of the gas source bottle (1) and first triplate line (17);
Between the inlet end of the parallel connection of the air accumulator (7) and the fluid reservoir (10) and inlet-pressure force control valve (4) It is provided with the second air gauge (5);
The 3rd air gauge is provided between the live end of the confined pressure control valve (16) and the visual core holding unit (12) (18).
8. rock core gas liquid two purpose permeability test device according to claim 7, it is characterised in that:
First switch (2) is provided between the gas source bottle (1) and first air gauge (3);
Second is provided between the inlet end and the air inlet of the parallel connection of the air accumulator (7) and the fluid reservoir (10) to open Close (6);
The 3rd is provided between the inlet end and the inlet of the parallel connection of the air accumulator (7) and the fluid reservoir (10) to open Close (9);
The 4th switch (8) is provided between a port of the gas outlet and second triplate line;
The is provided with the pipeline of second port of the upper end and the 3rd triplate line for connecting fluid reservoir (10) Five switches (26);
The 6th switch (11) is provided between second port of the liquid outlet and the 4th triplate line;
The 7th switch (19) is provided between the 3rd port of the 5th triplate line and the gas flowmeter (22);
The 8th switch (20) is provided directly with second port of the 5th triplate line and the liquid-collecting bottle (21);
Is provided between the 3rd port of the 3rd triplate line and a port of the 4th triplate line Nine switches (27).
9. a kind of reservoir damage evaluation method, it is characterised in that comprise the following steps:
1) measure of gas permeability is carried out to rock core with the rock core gas liquid two purpose permeability test device described in claim 8, And the gas permeability of rock core is calculated, it is designated as K1
2) in the method for the Test Liquid Permeability of Core of the rock core gas liquid two purpose permeability test device testing rock core described in claim 8 Pollution damage is carried out to rock core;
3) with the rock core gas liquid two purpose permeability test device described in claim 8 to step 2) rock core after pollution damage carries out The measure of gas permeability, and the gas permeability of rock core is calculated, it is designated as K2
4) K is calculated2/K1× 100%, obtain the resume permeability rate of rock core;Calculate (1-K2/K1) × 100%, obtains permeability wound Evil rate.
10. reservoir damage evaluation method according to claim 9, it is characterised in that:
The assay method of the gas permeability of rock core is comprised the following steps:
1) each switch, confined pressure control valve (16), inlet-pressure force control valve (4) and each relief valve are closed;
2) load rock core in visual core holding unit (12), filling in the first cock body (13) and the second cock body (14) is carried out to rock core Fixed;
3) first switch (2) is opened, there is provided air pressure;
4) confined pressure control valve (16) is adjusted, applies confined pressure to rock core;
5) inlet-pressure force control valve (4) is adjusted to fixation pressure, open second switch (6), the 4th switch (8), the 9th switch (27) and the 7th switch (19), allow experimental gas by rock core, adjust heater (24) and set experimental temperature;
6) inlet pressure numerical value is read by second pressure table 5, and outlet pressure is atmospheric pressure, and exit gas flow number is by gas Flowmeter (22) reads, and the length of rock core and sectional area measurement are obtained, public by the correction darcy for being suitable for measuring gas permebility Formula calculates the gas permeability of rock core;
The assay method of the Test Liquid Permeability of Core of rock core is comprised the following steps:
1) each switch, confined pressure control valve (16), inlet-pressure force control valve (4) and each relief valve are closed;
2) testing liquid is loaded fluid reservoir (10), loads rock core in visual core holding unit (12), fill in the first cock body (13) and the second cock body (14) is fixed to rock core;
3) first switch (2) is opened, there is provided air pressure;
4) confined pressure control valve (16) is adjusted, confined pressure is applied to rock core;
5) inlet-pressure force control valve (4) is adjusted to fixation pressure, open the 3rd switch (9), the 6th switch (11) and the 8th switch (20) gas displacement prepare liquid, is allowed by rock core, adjust heater (24) and set experimental temperature;
6) inlet pressure numerical value is read by second pressure table 5, and outlet pressure is atmospheric pressure, liquid flow exit by timing and In liquid-collecting bottle (21), liquid volume is calculated and is obtained, and the length of rock core and sectional area measurement are obtained, and are calculated by darcy flow formula Go out the Test Liquid Permeability of Core of rock core.
CN201611037818.6A 2016-11-23 2016-11-23 Rock core gas liquid two purpose permeability test device and reservoir damage evaluation method Pending CN106501155A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201611037818.6A CN106501155A (en) 2016-11-23 2016-11-23 Rock core gas liquid two purpose permeability test device and reservoir damage evaluation method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201611037818.6A CN106501155A (en) 2016-11-23 2016-11-23 Rock core gas liquid two purpose permeability test device and reservoir damage evaluation method

Publications (1)

Publication Number Publication Date
CN106501155A true CN106501155A (en) 2017-03-15

Family

ID=58327685

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201611037818.6A Pending CN106501155A (en) 2016-11-23 2016-11-23 Rock core gas liquid two purpose permeability test device and reservoir damage evaluation method

Country Status (1)

Country Link
CN (1) CN106501155A (en)

Cited By (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107014731A (en) * 2017-03-29 2017-08-04 东北大学 A kind of hypotonic rock gas-liquid two drives pressure pulse decay infiltration experiment device and method
CN107144671A (en) * 2017-06-23 2017-09-08 中国电建集团贵阳勘测设计研究院有限公司 Shale gas-water lock effect evaluation device and method under high pressure condition
CN107525754A (en) * 2017-08-21 2017-12-29 浙江海洋大学 Storage tank reservoir area terrace antiseepage formula soil osmotic coefficient investigating method
CN108956385A (en) * 2018-06-13 2018-12-07 中国石油大学(北京) A kind of experimental system and its experimental method of gas diffusion migration
CN108982214A (en) * 2018-07-11 2018-12-11 中国电建集团华东勘测设计研究院有限公司 Brittle rock degree of injury test method and rock permeability coefficient testing device
CN109459362A (en) * 2017-09-06 2019-03-12 中国石油化工股份有限公司 The integrated testing device and method of high temperature and pressure Water-rock interaction and gas permeability
CN109490173A (en) * 2018-09-20 2019-03-19 南华大学 Uranium tailings pond uranium tailings and lower sleeping rock-soil layer permeability test device and test method
CN109632557A (en) * 2019-01-22 2019-04-16 中国矿业大学 A kind of gas-liquid two-phase saturation coal petrography sample experimental provision and saturation degree test method
CN110320343A (en) * 2019-07-08 2019-10-11 中国石油大学(华东) A kind of reservoir damage test device taken out convenient for rock core
CN110441207A (en) * 2019-08-06 2019-11-12 天津大学 A kind of gas/liquid two-phase test macro of porous material seepage coefficient
CN110501273A (en) * 2019-08-14 2019-11-26 中国地质大学(武汉) A device and method for studying the penetration law of drilling and completion fluid along the formation around the well
CN111024561A (en) * 2019-12-12 2020-04-17 中国石油化工股份有限公司 Experimental device and method for evaluating damage of solid particles in reinjection water to reservoir
CN111735751A (en) * 2020-08-07 2020-10-02 中国海洋石油集团有限公司 A dual-measurement device and method for hydrate core permeability
CN112858130A (en) * 2019-11-27 2021-05-28 中国石油天然气股份有限公司 Device and method for measuring damage rate of temporary plugging agent to reservoir permeability
CN112924361A (en) * 2021-02-22 2021-06-08 绍兴文理学院 Rock gas permeation detects uses permeability survey device
CN114383992A (en) * 2022-01-07 2022-04-22 核工业湖州勘测规划设计研究院股份有限公司 Sparse material gas permeability measuring device and method
CN115791560A (en) * 2022-11-28 2023-03-14 西安石油大学 A method for simulating Darcy seepage experiment of rock core and calibrating permeability parameters
CN116148071A (en) * 2021-11-23 2023-05-23 中国石油天然气股份有限公司 System and method for evaluating damage of fracturing fluid of tight oil shale reservoir

Citations (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN201546718U (en) * 2009-11-04 2010-08-11 湖北创联石油科技有限公司 High-pressure high-temperature dynamic fluid loss instrument
CN102011578A (en) * 2010-09-08 2011-04-13 中国海洋石油总公司 Oil reservoir sand production simulation sand filling experiment device
CN201874565U (en) * 2010-11-26 2011-06-22 中国石油大港油田勘探开发研究院 Core permeability damage flow test device
CN202092935U (en) * 2011-06-09 2011-12-28 青岛石大石仪科技有限责任公司 Core gripper capable of viewing core cracks
CN202882901U (en) * 2012-09-28 2013-04-17 中国石油化工股份有限公司 Experimental device for evaluating damage of rock core
CN103234971A (en) * 2013-04-23 2013-08-07 西南石油大学 Acidic etching instrument and operation method thereof
CN203164111U (en) * 2013-04-23 2013-08-28 西南石油大学 Holder and holder-based acidizing etching instrument
CN203758883U (en) * 2014-03-19 2014-08-06 中国海洋石油总公司 Device for experimentally evaluating pollution of high-temperature high-pressure steam to rock core
CN104316548A (en) * 2014-11-19 2015-01-28 中国石油大学(华东) Core holding unit based on Zeiss MCT-400 CT scanning and application thereof
CN104792683A (en) * 2015-04-20 2015-07-22 中国海洋石油总公司 Device and method for evaluating damage degree of working solution to tight reservoir
CN105527379A (en) * 2016-01-04 2016-04-27 中国石油大学(北京) Three-hole rock core kettle and ultra-low-permeability reservoir fluid damage evaluation test apparatus and method
CN206192840U (en) * 2016-11-23 2017-05-24 中国地质大学(武汉) Dual -purpose permeability testing arrangement of rock core gas -liquid

Patent Citations (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN201546718U (en) * 2009-11-04 2010-08-11 湖北创联石油科技有限公司 High-pressure high-temperature dynamic fluid loss instrument
CN102011578A (en) * 2010-09-08 2011-04-13 中国海洋石油总公司 Oil reservoir sand production simulation sand filling experiment device
CN201874565U (en) * 2010-11-26 2011-06-22 中国石油大港油田勘探开发研究院 Core permeability damage flow test device
CN202092935U (en) * 2011-06-09 2011-12-28 青岛石大石仪科技有限责任公司 Core gripper capable of viewing core cracks
CN202882901U (en) * 2012-09-28 2013-04-17 中国石油化工股份有限公司 Experimental device for evaluating damage of rock core
CN103234971A (en) * 2013-04-23 2013-08-07 西南石油大学 Acidic etching instrument and operation method thereof
CN203164111U (en) * 2013-04-23 2013-08-28 西南石油大学 Holder and holder-based acidizing etching instrument
CN203758883U (en) * 2014-03-19 2014-08-06 中国海洋石油总公司 Device for experimentally evaluating pollution of high-temperature high-pressure steam to rock core
CN104316548A (en) * 2014-11-19 2015-01-28 中国石油大学(华东) Core holding unit based on Zeiss MCT-400 CT scanning and application thereof
CN104792683A (en) * 2015-04-20 2015-07-22 中国海洋石油总公司 Device and method for evaluating damage degree of working solution to tight reservoir
CN105527379A (en) * 2016-01-04 2016-04-27 中国石油大学(北京) Three-hole rock core kettle and ultra-low-permeability reservoir fluid damage evaluation test apparatus and method
CN206192840U (en) * 2016-11-23 2017-05-24 中国地质大学(武汉) Dual -purpose permeability testing arrangement of rock core gas -liquid

Cited By (26)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107014731B (en) * 2017-03-29 2019-06-25 东北大学 A kind of drive of hypotonic rock gas-liquid two pressure pulse decaying permeability test method
CN107014731A (en) * 2017-03-29 2017-08-04 东北大学 A kind of hypotonic rock gas-liquid two drives pressure pulse decay infiltration experiment device and method
CN107144671A (en) * 2017-06-23 2017-09-08 中国电建集团贵阳勘测设计研究院有限公司 Shale gas-water lock effect evaluation device and method under high pressure condition
CN107144671B (en) * 2017-06-23 2022-04-19 中国电建集团贵阳勘测设计研究院有限公司 Shale gas-water lock effect evaluation device and method under high pressure condition
CN107525754A (en) * 2017-08-21 2017-12-29 浙江海洋大学 Storage tank reservoir area terrace antiseepage formula soil osmotic coefficient investigating method
CN109459362A (en) * 2017-09-06 2019-03-12 中国石油化工股份有限公司 The integrated testing device and method of high temperature and pressure Water-rock interaction and gas permeability
CN108956385B (en) * 2018-06-13 2020-11-06 中国石油大学(北京) An experimental system for gas diffusion and transport and its experimental method
CN108956385A (en) * 2018-06-13 2018-12-07 中国石油大学(北京) A kind of experimental system and its experimental method of gas diffusion migration
CN108982214A (en) * 2018-07-11 2018-12-11 中国电建集团华东勘测设计研究院有限公司 Brittle rock degree of injury test method and rock permeability coefficient testing device
CN108982214B (en) * 2018-07-11 2024-09-03 中国电建集团华东勘测设计研究院有限公司 Brittle rock damage degree testing method and rock permeability coefficient testing device
CN109490173A (en) * 2018-09-20 2019-03-19 南华大学 Uranium tailings pond uranium tailings and lower sleeping rock-soil layer permeability test device and test method
CN109490173B (en) * 2018-09-20 2021-01-05 南华大学 Uranium tailing pond uranium tailings and permeability testing device and testing method for lower lying rock-soil layer
CN109632557B (en) * 2019-01-22 2021-11-16 中国矿业大学 Gas-liquid two-phase saturated coal rock sample experimental device and saturation testing method
CN109632557A (en) * 2019-01-22 2019-04-16 中国矿业大学 A kind of gas-liquid two-phase saturation coal petrography sample experimental provision and saturation degree test method
CN110320343A (en) * 2019-07-08 2019-10-11 中国石油大学(华东) A kind of reservoir damage test device taken out convenient for rock core
CN110441207A (en) * 2019-08-06 2019-11-12 天津大学 A kind of gas/liquid two-phase test macro of porous material seepage coefficient
CN110501273A (en) * 2019-08-14 2019-11-26 中国地质大学(武汉) A device and method for studying the penetration law of drilling and completion fluid along the formation around the well
CN110501273B (en) * 2019-08-14 2024-04-16 中国地质大学(武汉) Device and method for researching penetration rule of drilling and completion fluid along well periphery stratum
CN112858130A (en) * 2019-11-27 2021-05-28 中国石油天然气股份有限公司 Device and method for measuring damage rate of temporary plugging agent to reservoir permeability
CN111024561A (en) * 2019-12-12 2020-04-17 中国石油化工股份有限公司 Experimental device and method for evaluating damage of solid particles in reinjection water to reservoir
CN111735751A (en) * 2020-08-07 2020-10-02 中国海洋石油集团有限公司 A dual-measurement device and method for hydrate core permeability
CN112924361A (en) * 2021-02-22 2021-06-08 绍兴文理学院 Rock gas permeation detects uses permeability survey device
CN112924361B (en) * 2021-02-22 2022-10-11 绍兴文理学院 A permeability measuring device for rock gas permeability detection
CN116148071A (en) * 2021-11-23 2023-05-23 中国石油天然气股份有限公司 System and method for evaluating damage of fracturing fluid of tight oil shale reservoir
CN114383992A (en) * 2022-01-07 2022-04-22 核工业湖州勘测规划设计研究院股份有限公司 Sparse material gas permeability measuring device and method
CN115791560A (en) * 2022-11-28 2023-03-14 西安石油大学 A method for simulating Darcy seepage experiment of rock core and calibrating permeability parameters

Similar Documents

Publication Publication Date Title
CN106501155A (en) Rock core gas liquid two purpose permeability test device and reservoir damage evaluation method
CN201532351U (en) A device for testing rock gas permeability coefficient by variable volume pressure pulse method
CN208171813U (en) A kind of multi-functional permeability test device
CN107764718A (en) Fractured shale gas-water phases flowing fracture condudtiviy evaluating apparatus and method
CN108088778B (en) A rock material permeability, porosity testing device
CN105606517A (en) Instrument for measuring relative permeability of low permeability reservoir using nuclear magnetic resonance
CN206192840U (en) Dual -purpose permeability testing arrangement of rock core gas -liquid
CN106644605B (en) Device and method for collecting bubble gas in geothermal water
CN204458305U (en) A kind of detection facility of Double-liquid mud-injection pump
CN108488630A (en) Experimental device for measuring leakage characteristic of gas pipeline and measuring method thereof
CN102865899B (en) Method and device for in-situ measurement of fluid volume during high temperature and high pressure core displacement
CN204575498U (en) A kind of perm-plug method device measuring flow in low permeability core
CN104880385A (en) System and method for testing rheological properties of carbon dioxide anhydrous fracturing fluid
CN108088768B (en) Experiment system and experiment method for tubule rheometer
CN208283230U (en) It is a kind of for measuring the device of compact rock core air water two-phase relative permeability
CN103149137A (en) Constant-pressure steady-state gas permeability measuring instrument
CN107328452A (en) A kind of device and its operating method for determining irregular seal cavity volume
CN209182187U (en) A kind of CO2Displacement test device
CN207019739U (en) A kind of device for determining irregular seal cavity volume
CN106383077A (en) Device for producing bound water
CN207832632U (en) The reasonable mining speed simulator of coal bed gas straight well single-phase flow
CN101393104B (en) Surface tension tester and method
CN104599582B (en) A kind of oil depot oil transferring examines and determine experiment device for teaching
CN204807158U (en) Flow measuring device for rock core displacement experiment
CN204405498U (en) Rock core perm-plug method device under a kind of simulated formation pressure condition

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication
RJ01 Rejection of invention patent application after publication

Application publication date: 20170315