CN106430976A - Mutton fat matt white glaze for ceramic decoration and preparation method of white glaze - Google Patents
Mutton fat matt white glaze for ceramic decoration and preparation method of white glaze Download PDFInfo
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- CN106430976A CN106430976A CN201610794537.9A CN201610794537A CN106430976A CN 106430976 A CN106430976 A CN 106430976A CN 201610794537 A CN201610794537 A CN 201610794537A CN 106430976 A CN106430976 A CN 106430976A
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- glaze
- white glaze
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- seu ovis
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
- C03C8/20—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions containing titanium compounds; containing zirconium compounds
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Structural Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Glass Compositions (AREA)
Abstract
The invention discloses mutton fat matt white glaze for a ceramic decoration and a preparation method of the white glaze. The white glaze is prepared from, by mass percentage, 15-25% of feldspar powder, 10-17% of calcium carbonate, 5-7% of dolomite, 6-12% of talc, 3-8% of barium carbonate, 15-20% of zirconium silicate, 10-15% of zirconium white frit, 0-6% of zinc oxide, 5-7% of aluminum oxide and 0-12% of kaolin. The components are weighed according to the formula, fully mixed and added into a grinding tank, water with the weight 45-50% that of dry powder is added for grinding for 10-15 h, then glaze slurry obtained after ball milling is subjected to iron removal and screening, and the concentration is adjusted till the true specific gravity is 50-54 degrees. A ceramic product is coated with the white glaze in a spraying mode or a soaking mode or other decoration modes. After drying, the ceramic product enters a kiln to be oxidized and fired for 8-11 h at the temperature of 1200-1235 DEG C, and the ceramic product is taken out of the kiln after being naturally cooled. The prepared mutton fat matt white glaze has the advantages of being high in processing property, high in operability and not prone to cracking.
Description
Technical field
The present invention relates to a kind of Adeps caprae seu ovis dumb light white glaze for ceramic ornament and preparation method thereof.
Background technology
Existing white glaze, mainly based on white gloss bright glaze, mainly applies to white clouds soil ceramic whiteware and vast Building class pottery
Porcelain, its feature is mainly to rely on the relatively low fritted glaze of firing temperature to make, relatively costly, is burnt with high temperature for ceramic whiteware
The enamel of knot is simultaneously deposited, and typically imposes ground-coat enamel and brilliant white glaze for architectural pottery.Pottery field product is all the time due to by base substrate
The factor impacts such as water absorption rate is high, big, the base glaze coefficient of expansion of moisture expantion, singly apply a kind of white glaze fictile and occur that cracking etc. is multiple to ask
Topic becomes one piece of short slab in this field.
Content of the invention
It is an object of the invention to overcoming the shortcomings of above-mentioned fictile field prior art problem, one kind is provided to be used for ceramic
Adeps caprae seu ovis dumb light white glaze of ornament and preparation method thereof, this ceramic ornament dumb light Adeps caprae seu ovis white glaze has that processing performance is strong, operation
Property the strong, advantage that is not easily cracked.
For achieving the above object, the present invention employs the following technical solutions：
A kind of Adeps caprae seu ovis dumb light white glaze for ceramic ornament, its technical recipe is calculated by mass percentage, by following component
Constitute：Feldspar powder 15-25%, Calcium Carbonate 10-17%, dolomite 5-7%, Talcum 6-12%, brium carbonate 3-8%, Zirconium orthosilicate. 15-
20%th, zirconium white frit 10-15%, zinc oxide 0-6%, aluminium oxide 5-7%, Kaolin 0-12%.
Preferably, its technical recipe is calculated by mass percentage, is made up of following component：Feldspar powder 15-25%, Calcium Carbonate
10-17%, dolomite 5-7%, Talcum 6-12%, brium carbonate 3-8%, Zirconium orthosilicate. 15-20%, zirconium white frit 10-15%, oxidation
Zinc 3-5%, aluminium oxide 5-7%, Kaolin 3-9%.
The preparation method of described Adeps caprae seu ovis dumb light white glaze：It is sufficiently mixed addition grinding pot after each component being weighed by formula
In, add the 45-50% moisture being equivalent to dry powder weight to be ground 10～15 hours, then the good glaze slip of ball milling is removed ferrum mistake
Sieve, concentration is adjusted to true specific gravity 50-54 degree, enters kiln using in spray or immersion or other decoration technique again on fictile after airing
The interior oxidation carrying out 8-11 hour with 1200 DEG C -1235 DEG C of temperature is burnt till, and goes out cellar for storing things after natural cooling, and prepared Adeps caprae seu ovis dumb light is white
Glaze.
Preferably, carry out testing graininess after the grinding 10-15 hour that adds water, testing graininess crosses 325 mesh sieves, and screen over-size is in 0.1-
0.3% enters next process (concentration of glaze slip of milled is adjusted to concentration is true specific gravity 50-54).
After technique scheme, the present invention, compared with background technology, has the advantage that：
1st, the Adeps caprae seu ovis dumb light white glaze being obtained, presents matte effect, and feel is fine and smooth, and silk just as silk slides jade to glaze paint again
Gentle texture, artistic value is high；
2nd, overcome potter's clay glaze to be obtained after repeatedly drawing and washing with local characteristic mineral, color development is unstable, and technique is single, color
Single, the single defect of decorative effect, and wash operation due to not drawing, the moisture of preparation process easily controllable it is easier to realize
The scale and rapid of preparation, workable；
3rd, effectively solve the problems, such as the shortcoming of fictile white artistic glaze, cost is more cheap, and the secondary work of no any poison
With safety coefficient is high；
4th, adopt compound prescription system more stable, firing range width, the suitability extensively, solves fictile well and sends out
The problem of raw cracking.
Its realize principle be：The present invention is prepared using half-feeding glaze mode, and formula adopts calcium and magnesium zirconium tri compound unglazed
System.When introducing calcium no photo etching single in formula, introducing consumption reaches glaze paint during 0.5Mol and matte effect then, mainly with calcium
Anhydrite crystalline phase exists, and separates out calcium crystalline solid；When in formula with Talcum introduce magnesium no photo etching, in glaze crystalline phase separate out species sum
Amount has a significant impact, and can jointly generate diopside crystallization with Calcium Carbonate, so that the crystal seed amount of crystals that changes also substantially is increased, its
Main with crystalline phases such as cordierite and pyroxenes and be present in glaze, make glaze paint have good matte effect；Zirconium orthosilicate. is one kindization
Learn stable performance and excellent opalizer also has milkiness effect, when Zirconium orthosilicate. is introduced into increase glaze whiteness in formula, also improve
The elastic modelling quantity of the firing temperature of glaze and glaze, reagentia is collectively forming with the crystallization of diopside crystalline phase together with calcium and magnesium simultaneously
The opaque white glaze of body.
In the melting process of calcium and magnesium flux in glaze with composition each in glaze react generation various crystalline phase while, also with
Fictile base substrate material reacts.Glaze is liquefied part billet surface, and penetrates into the combination increasing base glaze in the middle of base substrate
Performance, the intermediate layer being thusly-formed the reaction of base glaze is conducive to the combination of base glaze.In glaze, calcium and magnesium substantially reduces the expansion system of glaze
Number, the introducing of dolomite makes the glaze coefficient of expansion reduce firing range to broaden, cause glaze can perfect combination with fictile base substrate and
Do not occur glaze to split and moisture expantion after the problems such as.Because the elasticity that increased glaze of Zirconium orthosilicate. is thus solve pottery well in glaze
The problems such as there is cracking in product.
Specific embodiment
In order that the objects, technical solutions and advantages of the present invention become more apparent, with reference to embodiments, to the present invention
It is further elaborated.It should be appreciated that specific embodiment described herein, only in order to explain the present invention, is not used to
Limit the present invention.
In addition, except special instruction, percentage ratio of the present invention is mass percent.
Embodiment 1
A kind of Adeps caprae seu ovis dumb light white glaze for ceramic ornament, its technical recipe is calculated by mass percentage, by such as the following group
Divide and constitute：Feldspar powder 15%, Calcium Carbonate 17%, dolomite 5%, Talcum 12%, brium carbonate 8%, Zirconium orthosilicate. 15%, zirconium white frit
15%th, zinc oxide 5%, aluminium oxide 5%, Kaolin 3%.
Its preparation method is：It is sufficiently mixed after each component being weighed by formula in addition grinding pot, add and be equivalent to dry powder
The 45-50% moisture of weight is ground 10 hours, and then by the good glaze slip of ball milling except ferrum sieves, concentration is adjusted to true specific gravity 50-
54 degree, enter again after airing in kiln with 1200 DEG C -1235 DEG C of temperature on fictile using in spray or immersion or other decoration technique
Spend the oxidation carrying out 8 hours to burn till, go out cellar for storing things, prepared Adeps caprae seu ovis dumb light white glaze after natural cooling.
The coarse dull surface of Adeps caprae seu ovis dumb light white glaze texture that the present embodiment obtains, tone Bulbus Allii Fistulosi, it is lined with beans white glaze bottom, and in glaze
There is piece stricture of vagina in small, broken bits；Make Adeps caprae seu ovis dumb light white glaze texture, elegant and tasteful is white, sketches the contours of as pretty as a flower texture, and effect is muddy
So sky one-tenth, the romantic charm of great natural white jade and luxurious, rich romance breath.
Embodiment 2
A kind of Adeps caprae seu ovis dumb light white glaze for ceramic ornament, its technical recipe is calculated by mass percentage, by such as the following group
Divide and constitute：Feldspar powder 20%, Calcium Carbonate 13.5%, dolomite 6%, Talcum 9%, brium carbonate 5.5%, Zirconium orthosilicate. 17.5%, zirconium
White frit 12.5%, zinc oxide 4%, aluminium oxide 6%, Kaolin 6%.
Its preparation method is：It is sufficiently mixed after each component being weighed by formula in addition grinding pot, add and be equivalent to dry powder
The 45-50% moisture of weight is ground 13 hours, and then by the good glaze slip of ball milling except ferrum sieves, concentration is adjusted to true specific gravity 50-
54 degree, enter again after airing in kiln with 1200 DEG C -1235 DEG C of temperature on fictile using in spray or immersion or other decoration technique
Spend the oxidation carrying out 9.5 hours to burn till, go out cellar for storing things, prepared Adeps caprae seu ovis dumb light white glaze after natural cooling.
The coarse dull surface of Adeps caprae seu ovis dumb light white glaze texture that the present embodiment obtains, tone Bulbus Allii Fistulosi, it is lined with beans white glaze bottom, and in glaze
There is piece stricture of vagina in small, broken bits；Make Adeps caprae seu ovis dumb light white glaze texture, elegant and tasteful is white, sketches the contours of as pretty as a flower texture, and effect is muddy
So sky one-tenth, the romantic charm of great natural white jade and luxurious, rich romance breath.
Embodiment 3
A kind of Adeps caprae seu ovis dumb light white glaze for ceramic ornament, its technical recipe is calculated by mass percentage, by such as the following group
Divide and constitute：Feldspar powder 25%, Calcium Carbonate 10%, dolomite 7%, Talcum 6%, brium carbonate 3%, Zirconium orthosilicate. 20%, zirconium white frit
10%th, zinc oxide 3%, aluminium oxide 7%, Kaolin 9%.
Its preparation method is：It is sufficiently mixed after each component being weighed by formula in addition grinding pot, add and be equivalent to dry powder
The 45-50% moisture of weight is ground 15 hours, and then by the good glaze slip of ball milling except ferrum sieves, concentration is adjusted to true specific gravity 50-
54 degree, enter again after airing in kiln with 1200 DEG C -1235 DEG C of temperature on fictile using in spray or immersion or other decoration technique
Spend the oxidation carrying out 11 hours to burn till, go out cellar for storing things, prepared Adeps caprae seu ovis dumb light white glaze after natural cooling.
The coarse dull surface of Adeps caprae seu ovis dumb light white glaze texture that the present embodiment obtains, tone Bulbus Allii Fistulosi, it is lined with beans white glaze bottom, and in glaze
There is piece stricture of vagina in small, broken bits；Make Adeps caprae seu ovis dumb light white glaze texture, elegant and tasteful is white, sketches the contours of as pretty as a flower texture, and effect is muddy
So sky one-tenth, the romantic charm of great natural white jade and luxurious, rich romance breath.
The above, the only present invention preferably specific embodiment, but protection scope of the present invention is not limited thereto,
Any those familiar with the art the invention discloses technical scope in, the change or replacement that can readily occur in,
All should be included within the scope of the present invention.Therefore, protection scope of the present invention should be with scope of the claims
It is defined.
Claims (4)
1. a kind of Adeps caprae seu ovis dumb light white glaze for ceramic ornament it is characterised in that：Its technical recipe is calculated by mass percentage, by
Following component is constituted：Feldspar powder 15-25%, Calcium Carbonate 10-17%, dolomite 5-7%, Talcum 6-12%, brium carbonate 3-8%,
Zirconium orthosilicate. 15-20%, zirconium white frit 10-15%, zinc oxide 0-6%, aluminium oxide 5-7%, Kaolin 0-12%.
2. a kind of Adeps caprae seu ovis dumb light white glaze for ceramic ornament it is characterised in that：Its technical recipe is calculated by mass percentage, by
Following component is constituted：Feldspar powder 15-25%, Calcium Carbonate 10-17%, dolomite 5-7%, Talcum 6-12%, brium carbonate 3-8%,
Zirconium orthosilicate. 15-20%, zirconium white frit 10-15%, zinc oxide 3-5%, aluminium oxide 5-7%, Kaolin 3-9%.
3. a kind of Adeps caprae seu ovis dumb light white glaze according to claim 1 and 2 preparation method it is characterised in that：Will be each by formula
Component is sufficiently mixed after weighing in addition grinding pot, adds the 45-50% moisture being equivalent to dry powder weight to be ground 10～15
Hour, then by the good glaze slip of ball milling except ferrum sieves, concentration is adjusted to true specific gravity 50-54 degree, using spray or immersion or other decoration
In maneuver on fictile, enter the oxidation in kiln, 8-11 hour being carried out with 1200 DEG C -1235 DEG C of temperature after airing again and burn till, warp
Cellar for storing things, prepared Adeps caprae seu ovis dumb light white glaze is gone out after natural cooling.
4. a kind of Adeps caprae seu ovis dumb light white glaze according to claim 3 preparation method it is characterised in that：Add water grinding 10-15
Carry out testing graininess, testing graininess crosses 325 mesh sieves, and screen over-size then enters next process (by milled in 0.1-0.3% after hour
Concentration of glaze slip be adjusted to concentration be true specific gravity 50-54).
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Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106830881A (en) * | 2017-04-06 | 2017-06-13 | 潮州市潮安区皓强瓷业有限公司 | The production method of domestic ceramics transmutation color glaze product |
| CN106986544A (en) * | 2017-05-04 | 2017-07-28 | 山东工业陶瓷研究设计院有限公司 | The insulator grey matt colour glaze in sea |
| CN107010997A (en) * | 2017-03-07 | 2017-08-04 | 陈宝坤 | A kind of surface has the manufacture craft and its base glaze used of the ceramic utensil of matt marble grain |
| CN108545939A (en) * | 2018-05-11 | 2018-09-18 | 河南城建学院 | A kind of purplish blue matt glaze and preparation method thereof, purplish blue Sub-shine glaze and preparation method thereof |
| CN109354405A (en) * | 2018-09-30 | 2019-02-19 | 湖南益嘉瓷业有限公司 | Dumb light streak glaze and preparation method thereof |
| CN109775985A (en) * | 2019-02-01 | 2019-05-21 | 美艺陶(福建)高新建材有限公司 | Sheen glaze, sheen vitreous brick and preparation method thereof |
| CN109928778A (en) * | 2019-04-24 | 2019-06-25 | 佛山市东鹏陶瓷有限公司 | A kind of antifouling glaze of dumb light and glaze slip preparation method, Ceramic Tiles and preparation method |
| CN111233435A (en) * | 2020-03-24 | 2020-06-05 | 德化县宏顺陶瓷有限公司 | Glazed ceramic product and preparation method thereof |
| CN111807704A (en) * | 2020-09-02 | 2020-10-23 | 佛山东鹏洁具股份有限公司 | Matte glaze applied to sanitary ceramics, sanitary ceramics applying matte glaze and preparation method of sanitary ceramics |
| CN113149437A (en) * | 2021-06-24 | 2021-07-23 | 广东欧文莱陶瓷有限公司 | High-hardness digital protective glaze |
| CN114507085A (en) * | 2022-01-14 | 2022-05-17 | 广东欧文莱陶瓷有限公司 | Rock plate with meteorite pitted surface and preparation method thereof |
| CN114716146A (en) * | 2022-04-15 | 2022-07-08 | 东莞市唯美陶瓷工业园有限公司 | High-white matte fine wear-resistant glaze, ceramic tile and preparation method thereof |
| CN116947470A (en) * | 2023-08-19 | 2023-10-27 | 福建德化瓷国文化股份有限公司 | Shaving pattern ceramic with imitation old and black cloud imprinting effects and preparation method thereof |
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| CN107010997A (en) * | 2017-03-07 | 2017-08-04 | 陈宝坤 | A kind of surface has the manufacture craft and its base glaze used of the ceramic utensil of matt marble grain |
| CN106830881A (en) * | 2017-04-06 | 2017-06-13 | 潮州市潮安区皓强瓷业有限公司 | The production method of domestic ceramics transmutation color glaze product |
| CN106986544A (en) * | 2017-05-04 | 2017-07-28 | 山东工业陶瓷研究设计院有限公司 | The insulator grey matt colour glaze in sea |
| CN108545939A (en) * | 2018-05-11 | 2018-09-18 | 河南城建学院 | A kind of purplish blue matt glaze and preparation method thereof, purplish blue Sub-shine glaze and preparation method thereof |
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| CN109775985A (en) * | 2019-02-01 | 2019-05-21 | 美艺陶(福建)高新建材有限公司 | Sheen glaze, sheen vitreous brick and preparation method thereof |
| CN109928778B (en) * | 2019-04-24 | 2021-11-30 | 佛山市东鹏陶瓷有限公司 | Matte antifouling glaze, glaze slurry preparation method, ceramic tile and preparation method |
| CN109928778A (en) * | 2019-04-24 | 2019-06-25 | 佛山市东鹏陶瓷有限公司 | A kind of antifouling glaze of dumb light and glaze slip preparation method, Ceramic Tiles and preparation method |
| CN111233435A (en) * | 2020-03-24 | 2020-06-05 | 德化县宏顺陶瓷有限公司 | Glazed ceramic product and preparation method thereof |
| CN111807704A (en) * | 2020-09-02 | 2020-10-23 | 佛山东鹏洁具股份有限公司 | Matte glaze applied to sanitary ceramics, sanitary ceramics applying matte glaze and preparation method of sanitary ceramics |
| CN111807704B (en) * | 2020-09-02 | 2021-04-13 | 佛山东鹏洁具股份有限公司 | Matte glaze applied to sanitary ceramics, sanitary ceramics applying matte glaze and preparation method of sanitary ceramics |
| CN113149437A (en) * | 2021-06-24 | 2021-07-23 | 广东欧文莱陶瓷有限公司 | High-hardness digital protective glaze |
| CN113149437B (en) * | 2021-06-24 | 2021-09-17 | 广东欧文莱陶瓷有限公司 | High-hardness digital protective glaze |
| CN114507085A (en) * | 2022-01-14 | 2022-05-17 | 广东欧文莱陶瓷有限公司 | Rock plate with meteorite pitted surface and preparation method thereof |
| CN114716146A (en) * | 2022-04-15 | 2022-07-08 | 东莞市唯美陶瓷工业园有限公司 | High-white matte fine wear-resistant glaze, ceramic tile and preparation method thereof |
| CN114716146B (en) * | 2022-04-15 | 2022-11-29 | 东莞市唯美陶瓷工业园有限公司 | High-white matte fine wear-resistant glaze, ceramic tile and preparation method thereof |
| CN116947470A (en) * | 2023-08-19 | 2023-10-27 | 福建德化瓷国文化股份有限公司 | Shaving pattern ceramic with imitation old and black cloud imprinting effects and preparation method thereof |
| CN116947470B (en) * | 2023-08-19 | 2024-03-19 | 福建德化瓷国文化股份有限公司 | Shaving pattern ceramic with imitation old and black cloud imprinting effects and preparation method thereof |
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