CN106422408A - Multistage separation device for animal and plant raw materials as well as method and application thereof - Google Patents
Multistage separation device for animal and plant raw materials as well as method and application thereof Download PDFInfo
- Publication number
- CN106422408A CN106422408A CN201611017461.5A CN201611017461A CN106422408A CN 106422408 A CN106422408 A CN 106422408A CN 201611017461 A CN201611017461 A CN 201611017461A CN 106422408 A CN106422408 A CN 106422408A
- Authority
- CN
- China
- Prior art keywords
- solid
- segregation apparatuss
- liquid
- separating
- animal
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS OR COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings or cooking oils
- A23D9/02—Other edible oils or fats, e.g. shortenings or cooking oils characterised by the production or working-up
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/02—Pretreatment
- C11B1/04—Pretreatment of vegetable raw material
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/10—Production of fats or fatty oils from raw materials by extracting
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/001—Refining fats or fatty oils by a combination of two or more of the means hereafter
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/008—Refining fats or fatty oils by filtration, e.g. including ultra filtration, dialysis
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Microbiology (AREA)
- General Chemical & Material Sciences (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Extraction Or Liquid Replacement (AREA)
Abstract
The invention discloses a multistage separation device for animal and plant raw materials as well as a method and an application thereof, and belongs to the technical field of plant extraction. The multistage separation device comprises separating devices and a pulverizer (3), wherein each separating device comprises a leaching tank (1) and a solid-liquid separator (2); the leaching tank (1) is connected with the pulverizer (3) by virtue of a raw material conveying pipe (101); a discharge port of the leaching tank (1) is connected with a feed port pipeline of the solid-liquid separator (2) by virtue of a pump (4); a separated liquid outlet of the solid-liquid separator (2) is connected with a separated liquid output pipe (201); a solid material outlet of the solid-liquid separator (2) is connected with a first conveyor (5); a plurality of the separating device are arranged on the multistage separation device in a multistage mode from top to bottom along a solid material conveying direction. The multistage separation device for the animal and plant raw materials can pulverize the raw materials into powder for solid-liquid separation extraction, is high in extraction efficiency and yield, and can obviously increase the concentration of the obtained separated liquid, reduce the use level of a solvent, and reduce the production cost.
Description
Technical field
A kind of multi-stage separation device for animal-plant material and its method and purposes, belong to animals and plants extractive technique neck
Domain.
Background technology
Animal-plant material leaches and refers to using suitable solvent or method, from animal-plant material（All or certain part）
Middle extraction processes acquisition effective ingredient（Effective ingredient can be dissolved in solvent）.In existing industrial mass production, animal-plant material
How the extracting mode of middle effective ingredient, obtain sheet-shaped material using by dry for animal-plant material, tabletting, sheet-shaped material sprayed molten
Agent, obtains extracting solution, then carries out separation and purification（As extraction, distillation）.
Applicant finds under study for action, and existing extraction element has problems with：First, existing extraction element is effective
The yield of composition is low, extraction efficiency is low, and the effective ingredient in plant by the way of tabletting is difficult to leach in solvent, and sprays
The mode of leaching agent is difficult to fully extract, and gained extracts active ingredients are less efficient.Secondly, though existing extraction element employs
Solid-liquid separation technique, but there is no any help for the yield how improving effective ingredient.Again, it is found by the applicant that existing
The concentration of extraction element gained separating liquid is low, volume big, not only increased the cost of solvent, also add follow-up smart to separating liquid
System, the energy consumption concentrating.
Content of the invention
The technical problem to be solved in the present invention is：Overcome the deficiencies in the prior art, provide a kind of for animal-plant material
Multi-stage separation device and its method and purposes, the multi-stage separation device extraction efficiency that this is used for animal-plant material is high, high income, and
And the concentration of gained separating liquid can be significantly improved, reduce the consumption of solvent, reduce production cost.
The technical solution adopted for the present invention to solve the technical problems is：This is used for the multiple stage separation dress of animal-plant material
Put it is characterised in that：Including segregation apparatuss and pulverizer, segregation apparatuss include batch extractor and solid-liquid separating machine, and batch extractor passes through
Feed line is connected with pulverizer, and batch extractor discharging opening is connected with solid-liquid separation machine inlet pipeline by pump, and solid-liquid divides
The discharge channel disembarked is connected with separating liquid outlet tube, and the solid material outlet of solid-liquid separating machine is connected with the first conveyer；
Segregation apparatuss are multiple, and multiple described segregation apparatuss are along material conveying direction admittedly, from top to bottom in multistage setting；Adjacent institute
In the segregation apparatuss stated：Higher level's segregation apparatuss are connected with the batch extractor of subordinate segregation apparatuss by the first conveyer；Adjacent institute
In the segregation apparatuss stated：The discharge channel of subordinate's segregation apparatuss passes through the batch extractor of separating liquid reverse stream pipe and higher level's segregation apparatuss
It is connected.
In each described segregation apparatus, it is provided with second conveyor, the solid material outlet of solid-liquid separating machine conveys by second
Machine is connected with batch extractor.
In adjacent described segregation apparatuss：The discharge channel of higher level's segregation apparatuss, by separating liquid outlet tube and subordinate
The batch extractor of segregation apparatuss is connected.
Described separating liquid reverse stream pipe is provided with feeding engine, and separating liquid outlet tube and separating liquid reverse stream pipe are equipped with control
Valve.
The grinding particle size of described pulverizer is Centimeter Level, grade, micron order or nanoscale.
Described pulverizer is wet crushing mill, and pulverizer is connected with solvent delivery pipe.
Described pulverizer is dry grinding machine, batch extractor is connected with solvent delivery pipe, feed line is provided with feeding
Machine.
Described solvent delivery pipe is provided with thermoregulator.
In multiple described segregation apparatuss, it is provided with solvent make-up pipe, solvent make-up pipe positioned at most end flash trapping stage device
It is connected with batch extractor.
This is used for the operational approach of the multi-stage separation device of animal-plant material it is characterised in that comprising the steps：
a）Raw material pulverizing is powder by pulverizer, dusty raw materials and solvent is pressed proportioning and adds batch extractor, in batch extractor
Mixing is leached；The material that batch extractor is discharged, enters solid-liquid separating machine by pump and separates；
b）During solid-liquid separating machine work：The detached separating liquid of solid-liquid separating machine is discharged from separating liquid outlet tube, separating liquid reverse stream pipe,
Gu material is discharged by the first conveyer；
c）During multiple segregation apparatuss work：The separating obtained solid material of solid-liquid separating machine of higher level's segregation apparatuss, by the first conveyer,
Deliver in the batch extractor of subordinate's segregation apparatuss, extract again；The separating obtained separating liquid of solid-liquid separating machine of subordinate's segregation apparatuss, leads to
Cross in the batch extractor that separating liquid reverse stream pipe delivers to higher level's segregation apparatuss, reuse.
The purposes of the multi-stage separation device of this animal-plant material it is characterised in that：Extract oils and fatss, Chinese medicine extract in oil plant
Extraction, spice extract the application that volatile oil or edible animals and plants raw material extract the oily aspect of extraction.
Present invention applicant is described as follows：
The design that batch extractor of the present invention is connected with pulverizer by feed line, crushing material is powder, is soaked
Carry then solid-liquid separation so that in raw material the yield of effective ingredient and leaching efficiency be significantly improved.Pulverizer can be by dynamic plant
Raw material is sufficiently pulverized, and raw material is put in batch extractor in the form of powdery, after pulverizing, material powder reaches pulverizer
Grinding particle size be Centimeter Level, grade, micron order or nanoscale（10 centimetres ~ 0.1 nanometer）, the pulverizing grain of preferred pulverizer
Spend for 3 centimetres ~ 0.1 micron, the grinding particle size of further preferred pulverizer is 5000 ~ 2 microns, under this grinding particle size, pulverize energy
Consumption is little, and solid-liquid separation efficiency is high；The grinding particle size of further preferred pulverizer is 600 ~ 5 microns, energy under this grinding particle size
Fully abolish the cell wall of most plants so that the effective ingredient in animal and plant cellss fully leaches, improves yield, and
Solid-liquid separation efficiency is higher, can obtain higher economic well-being of workers and staff.Pulverizer can be dry grinding machine or wet crushing mill, is wet crushing mill
During pulverizing, pulverizer pulverizing liquid is extraction solvent.
And applicant designs, and carries out solid-liquid separation using solid-liquid separating machine, solves the problems, such as filtration difficulty, solid-liquid divides
Disembark as decanter type, membrane filtration formula, filter-press type, net filtration formula, spiral squeezing type, vacuum type, swinging or centrifuge formula solid-liquid
Seperator.Preferably solid-liquid separating machine is that filter-press type solid-liquid separating machine, screw extruding type solid-liquid separator or centrifugal solid-liquid divide
Disembark.
For the first conveyer and second conveyor, the separating obtained solid material of solid-liquid separating machine（I.e. solid material）Using first
Conveyer and second conveyor are conveyed, the first conveyer and second conveyor are ribbon conveyer, screw conveyer or
Drag conveyor.
Compared with prior art, a kind of multi-stage separation device for animal-plant material of the present invention and its method and purposes
Had an advantageous effect in that：
1st, raw material pulverizing to powder can be carried out solid-liquid separation extraction by the multi-stage separation device that this is used for animal-plant material, tool
There are higher yield and leaching efficiency, and the concentration of gained separating liquid can be significantly improved, reduce the consumption of solvent, reduce life
Produce cost.
First, applicant is devised batch extractor and is connected with pulverizer by feed line, and pulverizer is by raw material pulverizing
For powder, the raw material of powder and solvent are directly fully contacted, and so that effective ingredient is fully leached in solvent so that effectively becoming
The yield dividing and leaching efficiency are significantly improved.Secondly, applicant devises batch extractor and is connected with solid-liquid separator, using solid
Material can be directly separated the solid material of separating liquid for liquid and solid-state by liquid/gas separator, and the response rate for separating liquid is high, point
In chaotropic, impurity is few.Again, applicant finds under study for action：Existing extraction element yield is low, still deposits in the raw material after extraction
Effective ingredient in high level.And, existing extraction element generally requires to put into substantial amounts of solvent, could normally run, and
And the volume of existing extraction element gained extracting solution is big, effective ingredient concentration is low, later separation, refined, need to disappear when concentrating
Consume higher energy consumption.Therefore, applicant devises multiple described segregation apparatuss along material conveying direction admittedly, from top to bottom in multistage
Setting, in adjacent described segregation apparatuss：Higher level's segregation apparatuss pass through the first conveyer, the batch extractor phase with subordinate's segregation apparatuss
Connect, designed with this and solid material after separation is repeatedly leached-separates, fully extract the effective ingredient in solid material.Finally, Shen
Ask someone to devise in adjacent described segregation apparatuss：The discharge channel of subordinate's segregation apparatuss passes through separating liquid reverse stream pipe, and upper
The batch extractor of level segregation apparatuss is connected so that the separating liquid adverse current of subordinate's segregation apparatuss gained low concentration inputs higher level and separates dress
In the batch extractor put, both supplemented the solvent in the batch extractor of higher level's segregation apparatuss, and can leach again again, reduce solvent use
Amount, the separating liquid that improve yield, finally obtain high concentration, and the separating liquid of high concentration is higher, also reduces subsequently refined, dense
Energy consumption during division chaotropic, in a disguised form reduces cost.
2nd, the multi-stage separation device that this is used for animal-plant material further increases leaching efficiency.First, applicant's design
Pulverizer is dry grinding machine or wet crushing mill, meets different pulverizing and requires, improve production efficiency.Secondly, applicant designs
Solvent delivery pipe with thermoregulator, can adjust the temperature of solvent, improve leaching efficiency.
3rd, this is used for the multi-stage separation device low cost of animal-plant material and applied widely.This is used for animal-plant material
Multi-stage separation device can be used in multiple fields, can be used in oil crop and carry oil（As the extracting bean oil from Semen sojae atricolor）, can
Extract for plant medicine raw material（As Ramulus Cinnamomi extracts volatile oil, ethyl acetate extraction Semen Cassiae extract, methanol as solvent
Extract the glycoside in Radix Ginseng）, can be used in plant perfume and carry oil（Extraction as volatile oil in Flos Rosae Rugosae, lavandula angustifolia）, can be used in
Edible animals and plants raw material extracts and leaches oil（As extracted carrot oil in Radix Dauci Sativae, extracting algal oil in Sargassum）.
Brief description
Fig. 1 is a kind of structural representation of multi-stage separation device for animal-plant material of embodiment 1.
Fig. 2 is a kind of structural representation of multi-stage separation device for animal-plant material of embodiment 2.
Wherein：1st, batch extractor 101, feed line 102, solvent delivery pipe 103, thermoregulator 2, solid
Liquid separator 201, separating liquid outlet tube 202, separating liquid reverse stream pipe 3, pulverizer 301, feeder 4, pump 5,
First conveyer 6, second conveyor 7, control valve 8, feeding engine 9, solvent make-up pipe.
Specific embodiment
Fig. 1 is highly preferred embodiment of the present invention, and with reference to Fig. 1 ~ 2, the present invention is described further.
Embodiment 1
With reference to Fig. 1, this is used for the multi-stage separation device of animal-plant material, and including segregation apparatuss and pulverizer 3, segregation apparatuss include
Batch extractor 1 and solid-liquid separating machine 2, batch extractor 1 is connected with pulverizer 3 by feed line 101, and batch extractor 1 discharging opening leads to
Cross pump 4 to be connected with solid-liquid separating machine 2 charging aperture pipeline, the discharge channel of solid-liquid separating machine 2 is connected with separating liquid outlet tube
201, the solid material outlet of solid-liquid separating machine 2 is connected with the first conveyer 5；Segregation apparatuss are multiple, and multiple segregation apparatuss are expected along solid
Conveying direction, from top to bottom be in multistage setting；In adjacent segregation apparatuss：Higher level's segregation apparatuss pass through the first conveyer 5 and subordinate
The batch extractor 1 of segregation apparatuss is connected；The discharge channel of subordinate's segregation apparatuss is separated with higher level by separating liquid reverse stream pipe 202
The batch extractor 1 of device is connected.In multiple segregation apparatuss, it is provided with solvent make-up pipe 9, solvent positioned at most end flash trapping stage device
Supplement pipe 9 to be connected with batch extractor 1.
With reference to Fig. 1, the present embodiment, except including above structure, also includes following structure：Pulverizer 3 is wet crushing mill, powder
It is connected with solvent delivery pipe 102 on broken machine 3.Solvent delivery pipe 102 is provided with thermoregulator 103.
In each segregation apparatus, be provided with second conveyor 6, the solid material outlet of solid-liquid separating machine 2 by second conveyor 6 with
Batch extractor 1 is connected.Separating liquid reverse stream pipe 202 is provided with feeding engine 8, on separating liquid outlet tube 201 and separating liquid reverse stream pipe 202
It is equipped with control valve 7.Wherein, it is provided with mixing arrangement in batch extractor 1, mixing arrangement can adopt agitator or jet mixing, leaching
Go out tank periphery and be provided with heater it is also possible to be not provided with heater.The grinding particle size of pulverizer 3 is Centimeter Level, grade, micro-
Meter level or nanoscale.Solid-liquid separating machine 2 is capable of solid-liquid separation.
Annexation for separating liquid outlet tube 201 has multiple designs, can be designed as 1）：With reference to Fig. 2, adjacent separation
In device, the discharge channel of higher level's segregation apparatuss, by separating liquid outlet tube 201, batch extractor 1 phase with subordinate's segregation apparatuss
Connect, separating liquid can be sent in subordinate's segregation apparatuss batch extractor 1 by separating liquid outlet tube 201, extracts again.Or, can
To be designed as 2）With reference to Fig. 1：Separating liquid outlet tube 201 is not connected with the batch extractor 1 of subordinate segregation apparatuss, and separating liquid is exported
The separating liquid that pipe 201 is discharged sends to follow-up refining step.
There are multiple designs for the separating liquid outlet tube 201 on every flash trapping stage device, can be designed as 1）：Reference Fig. 1 ~
2, every flash trapping stage device is equipped with separating liquid outlet tube 201, in work process, unlatching first stage separation device and most end
Separating liquid outlet tube 201 on flash trapping stage device, the separating liquid outlet tube 201 on remaining segregation apparatus at different levels is in cut out shape
State.Or can be designed as 2）（It is not drawn on figure）：Only first stage separation device and most end flash trapping stage device is provided with point
Chaotropic outlet tube 201, is not provided with separating liquid outlet tube 201 in remaining segregation apparatus at different levels.By solvent make-up pipe 9 and separating liquid
Reverse stream pipe 202, all has the solvent make-up of abundance in the batch extractor 1 that ensure that segregation apparatuss at different levels.
Embodiment 2
With reference to Fig. 2, the present embodiment is distinguished as with embodiment 1：Pulverizer 3 is dry grinding machine, batch extractor 1 is connected with solvent defeated
Send pipe 102, feed line 101 is provided with feeder 301.Solvent delivery pipe 102 is provided with thermoregulator 103.
The work process that this is used for the multi-stage separation device of animal-plant material is as follows：
a）Raw material pulverizing is powder by pulverizer 3, to improve effective ingredient yield and leaching efficiency in batch extractor 1；To pulverize
Dusty raw materials afterwards and solvent are pressed proportioning and are added batch extractor 1, and mixing in batch extractor 1 is leached；The material that batch extractor 1 is discharged,
Enter solid-liquid separating machine 2 by pump 4 to separate；
b）The detached separating liquid of solid-liquid separating machine 2 is discharged from separating liquid outlet tube 201, separating liquid reverse stream pipe 202, Gu material is by the
One conveyer 5, second conveyor 6 are discharged；
c）During multiple segregation apparatuss work, along material conveying direction admittedly, from top to bottom in multistage setting, the solid-liquid of higher level's segregation apparatuss
The separating obtained solid material of seperator 2, by the first conveyer 5, delivers in the batch extractor 1 of subordinate's segregation apparatuss, extracts again.Subordinate
The separating obtained separating liquid of solid-liquid separating machine 2 of segregation apparatuss（Concentration is relatively low）, higher level is delivered to by separating liquid reverse stream pipe 202 and separates
In the batch extractor 1 of device, extracting again, thus improving the concentration of every grade of segregation apparatuss gained separating liquid, reducing solvent load；
In addition, in every grade of segregation apparatuss：The separating obtained solid material of solid-liquid separating machine 2 is it is also possible to deliver to this level by second conveyor 6
In the batch extractor 1 of segregation apparatuss, circulation extraction；
During multiple segregation apparatuss work, the separating liquid outlet tube on a unlatching first stage separation device and most end flash trapping stage device
201, separating liquid outlet tube 201 valve closing of remaining segregation apparatus at different levels；By solvent make-up pipe 9 supplementing solvent and separating liquid
Reverse stream pipe 202, the liquid make-up in batch extractors 1 at different levels.
The above, be only presently preferred embodiments of the present invention, is not the restriction that the present invention is made with other forms, appoints
What those skilled in the art possibly also with the disclosure above technology contents changed or be modified as equivalent variations etc.
Effect embodiment.But every without departing from technical solution of the present invention content, according to the present invention technical spirit to above example institute
Any simple modification, equivalent variations and the remodeling made, still falls within the protection domain of technical solution of the present invention.
Claims (10)
1. a kind of multi-stage separation device for animal-plant material it is characterised in that：Including segregation apparatuss and pulverizer（3）, point
Include batch extractor from device（1）And solid-liquid separating machine（2）, batch extractor（1）By feed line（101）With pulverizer（3）Phase
Connect, batch extractor（1）Discharging opening passes through pump（4）With solid-liquid separating machine（2）Charging aperture pipeline connects, solid-liquid separating machine（2）Point
Chaotropic outlet is connected with separating liquid outlet tube（201）, solid-liquid separating machine（2）The outlet of solid material be connected with the first conveyer（5）；
Segregation apparatuss are multiple, and multiple described segregation apparatuss are along material conveying direction admittedly, from top to bottom in multistage setting；Adjacent institute
In the segregation apparatuss stated：Higher level's segregation apparatuss pass through the first conveyer（5）Batch extractor with subordinate's segregation apparatuss（1）It is connected；
In adjacent described segregation apparatuss：The discharge channel of subordinate's segregation apparatuss passes through separating liquid reverse stream pipe（202）Separate with higher level
The batch extractor of device（1）It is connected.
2. a kind of multi-stage separation device for animal-plant material according to claim 1 it is characterised in that：Described in each
Segregation apparatuss in, be provided with second conveyor（6）, solid-liquid separating machine（2）The outlet of solid material pass through second conveyor（6）With leaching
Tank（1）It is connected.
3. a kind of multi-stage separation device for animal-plant material according to claim 1 it is characterised in that：Adjacent described
Segregation apparatuss in：The discharge channel of higher level's segregation apparatuss, by separating liquid outlet tube（201）Leaching with subordinate's segregation apparatuss
Go out tank（1）It is connected.
4. a kind of multi-stage separation device for animal-plant material according to claim 1 it is characterised in that：Described divides
Chaotropic reverse stream pipe（202）It is provided with feeding engine（8）, separating liquid outlet tube（201）With separating liquid reverse stream pipe（202）On be equipped with control
Valve processed（7）.
5. a kind of multi-stage separation device for animal-plant material according to claim 1 it is characterised in that：Described powder
Broken machine（3）Grinding particle size be Centimeter Level, grade, micron order or nanoscale.
6. a kind of multi-stage separation device for animal-plant material according to claim 1 it is characterised in that：Described powder
Broken machine（3）For wet crushing mill, pulverizer（3）On be connected with solvent delivery pipe（102）；Or, described pulverizer（3）For dry powder
Broken machine, batch extractor（1）On be connected with solvent delivery pipe（102）, feed line（101）It is provided with feeder（301）.
7. a kind of multi-stage separation device for animal-plant material according to claim 6 it is characterised in that：Described is molten
Agent delivery pipe（102）It is provided with thermoregulator（103）.
8. a kind of multi-stage separation device for animal-plant material according to claim 1 it is characterised in that：Multiple described
Segregation apparatuss in, be provided with solvent make-up pipe positioned at most end flash trapping stage device（9）, solvent make-up pipe（9）With batch extractor（1）
It is connected.
9. a kind of operational approach of the multi-stage separation device for animal-plant material described in claim 1 is it is characterised in that wrap
Include following steps：
a）Pulverizer（3）Raw material pulverizing is powder, dusty raw materials and solvent is pressed proportioning and adds batch extractor（1）, in leaching
Go out tank（1）Middle mixing is leached；Batch extractor（1）The material discharged, by pump（4）Enter solid-liquid separating machine（2）Separate；
b）Solid-liquid separating machine（2）During work：Solid-liquid separating machine（2）Detached separating liquid is from separating liquid outlet tube（201）, separating liquid
Reverse stream pipe（202）Discharge, Gu material passes through the first conveyer（5）Discharge；
c）During multiple segregation apparatuss work：The solid-liquid separating machine of higher level's segregation apparatuss（2）Separating obtained solid material, conveys by first
Machine（5）, deliver to the batch extractor of subordinate's segregation apparatuss（1）In, extract again；The solid-liquid separating machine of subordinate's segregation apparatuss（2）Separate
Gained separating liquid, by separating liquid reverse stream pipe（202）Deliver to the batch extractor of higher level's segregation apparatuss（1）In, reuse.
10. a kind of multi-stage separation device for animal-plant material described in claim 1 purposes it is characterised in that：In oil
Material extraction oils and fatss, the extraction of Chinese medicine extract, spice extraction volatile oil or edible animals and plants raw material extract answering of the oily aspect of extraction
With.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610883153 | 2016-10-10 | ||
| CN2016108831534 | 2016-10-10 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106422408A true CN106422408A (en) | 2017-02-22 |
Family
ID=58220893
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611017461.5A Pending CN106422408A (en) | 2016-10-10 | 2016-11-19 | Multistage separation device for animal and plant raw materials as well as method and application thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106422408A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106883932A (en) * | 2017-04-17 | 2017-06-23 | 福建鑫绿林产品开发有限公司 | A kind of low energy consumption high yield pulp1 obtains the production method and production line of fir essential oil |
| WO2019041887A1 (en) * | 2017-08-31 | 2019-03-07 | 山东江天生物科技有限公司 | High-performance extraction device |
| CN110215734A (en) * | 2019-06-17 | 2019-09-10 | 安徽紫山农业科技有限公司 | A kind of extract equipment and its extracting method of biological medicine |
| CN112870762A (en) * | 2021-01-20 | 2021-06-01 | 福建蔓丝源生物科技有限公司 | A multistage extraction and separation system for animal and plant raw materials |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0084554A1 (en) * | 1981-07-31 | 1983-08-03 | Mittex Ag | Extraction method. |
| CN1768891A (en) * | 2004-11-05 | 2006-05-10 | 济南倍力粉技术工程有限公司 | Extraction method and equipment of Chinese medicinal active component |
| CN104922930A (en) * | 2014-08-10 | 2015-09-23 | 王选明 | Two-stage rhododendron simsii planch extraction equipment |
| CN206184037U (en) * | 2016-10-10 | 2017-05-24 | 王芹 | A multistage separation device for animal and plant materials |
-
2016
- 2016-11-19 CN CN201611017461.5A patent/CN106422408A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0084554A1 (en) * | 1981-07-31 | 1983-08-03 | Mittex Ag | Extraction method. |
| CN1768891A (en) * | 2004-11-05 | 2006-05-10 | 济南倍力粉技术工程有限公司 | Extraction method and equipment of Chinese medicinal active component |
| CN104922930A (en) * | 2014-08-10 | 2015-09-23 | 王选明 | Two-stage rhododendron simsii planch extraction equipment |
| CN206184037U (en) * | 2016-10-10 | 2017-05-24 | 王芹 | A multistage separation device for animal and plant materials |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106883932A (en) * | 2017-04-17 | 2017-06-23 | 福建鑫绿林产品开发有限公司 | A kind of low energy consumption high yield pulp1 obtains the production method and production line of fir essential oil |
| CN106883932B (en) * | 2017-04-17 | 2023-03-10 | 福建鑫绿林产品开发有限公司 | Production method and production line for obtaining cedar essential oil with low energy consumption and high yield |
| WO2019041887A1 (en) * | 2017-08-31 | 2019-03-07 | 山东江天生物科技有限公司 | High-performance extraction device |
| CN110215734A (en) * | 2019-06-17 | 2019-09-10 | 安徽紫山农业科技有限公司 | A kind of extract equipment and its extracting method of biological medicine |
| CN110215734B (en) * | 2019-06-17 | 2021-11-23 | 安徽紫山农业科技有限公司 | Extraction equipment and extraction method of biological medicine |
| CN112870762A (en) * | 2021-01-20 | 2021-06-01 | 福建蔓丝源生物科技有限公司 | A multistage extraction and separation system for animal and plant raw materials |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN106422408A (en) | Multistage separation device for animal and plant raw materials as well as method and application thereof | |
| CN106362434A (en) | Multistage extraction unit for animal and plant raw materials, and method and application thereof | |
| CN206543604U (en) | A kind of radix glycyrrhizae extracts processing pulverizer | |
| CN206184037U (en) | A multistage separation device for animal and plant materials | |
| CN208098394U (en) | The combination centrifugal device of a small amount of fine particle impurity in a kind of separation liquid | |
| CN110237560B (en) | Continuous extraction device of traditional Chinese medicine for pharmacy | |
| CN108741078A (en) | The processing method for preparing the method and linseed of flaxseed gum, flax lignan, flax dietary fiber and flax protein powder | |
| CN106492501A (en) | A kind of single-stage segregation apparatuss and its method and purposes for animal-plant material | |
| CN214130382U (en) | Acanthopanax senticosus dispersion extraction element | |
| CN206334386U (en) | A kind of adverse current extraction element for animal-plant material | |
| CN206184036U (en) | A single -stage separator for animal and plant materials | |
| CN206184038U (en) | A multistage elution device for animal and plant materials | |
| CN106512471A (en) | Multi-stage elution device for animal and plant raw materials and purpose of device | |
| CN206334387U (en) | A kind of single-stage washing device for animal-plant material | |
| CN206184035U (en) | A multistage extraction element for animal and plant materials | |
| CN203829698U (en) | Natural plant effective constituent atomizing and extracting device | |
| CN219824100U (en) | Device of high-efficient extraction glossy ganoderma spore oil | |
| CN206334385U (en) | A kind of single-stage leaching device for animal-plant material | |
| CN111631956B (en) | Processing equipment and processing method of antibacterial liquid | |
| CN106334338A (en) | Single-stage elution device for animal and plant raw materials and method and application thereof | |
| CN206081745U (en) | Continuous leaching equipment | |
| CN205761570U (en) | Folium Eucommiae device for finely crushing | |
| CN205516613U (en) | Novel crude drug draws percolation tank | |
| CN109206528A (en) | A kind of fructus lycii functional component high-performance bio extracting method | |
| CN112870762A (en) | A multistage extraction and separation system for animal and plant raw materials |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20170222 |