CN106418688A - A preparation method of fragrance-releasing gel fiber filter stick - Google Patents
A preparation method of fragrance-releasing gel fiber filter stick Download PDFInfo
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- CN106418688A CN106418688A CN201610823103.7A CN201610823103A CN106418688A CN 106418688 A CN106418688 A CN 106418688A CN 201610823103 A CN201610823103 A CN 201610823103A CN 106418688 A CN106418688 A CN 106418688A
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- 239000000835 fiber Substances 0.000 title claims abstract description 172
- 230000003578 releasing effect Effects 0.000 title claims abstract description 124
- 238000002360 preparation method Methods 0.000 title claims abstract description 61
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- 238000002156 mixing Methods 0.000 claims abstract description 16
- 239000000499 gel Substances 0.000 claims description 151
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- UHVMMEOXYDMDKI-JKYCWFKZSA-L zinc;1-(5-cyanopyridin-2-yl)-3-[(1s,2s)-2-(6-fluoro-2-hydroxy-3-propanoylphenyl)cyclopropyl]urea;diacetate Chemical compound [Zn+2].CC([O-])=O.CC([O-])=O.CCC(=O)C1=CC=C(F)C([C@H]2[C@H](C2)NC(=O)NC=2N=CC(=CC=2)C#N)=C1O UHVMMEOXYDMDKI-JKYCWFKZSA-L 0.000 claims description 21
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims description 19
- 239000000661 sodium alginate Substances 0.000 claims description 19
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- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims 1
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- 238000005520 cutting process Methods 0.000 claims 1
- 125000003074 decanoyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C(*)=O 0.000 claims 1
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- 235000002637 Nicotiana tabacum Nutrition 0.000 description 7
- 239000002775 capsule Substances 0.000 description 7
- WWZKQHOCKIZLMA-UHFFFAOYSA-N Caprylic acid Natural products CCCCCCCC(O)=O WWZKQHOCKIZLMA-UHFFFAOYSA-N 0.000 description 6
- 239000005635 Caprylic acid (CAS 124-07-2) Substances 0.000 description 6
- 229960002446 octanoic acid Drugs 0.000 description 6
- 239000008213 purified water Substances 0.000 description 5
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- 244000298697 Actinidia deliciosa Species 0.000 description 4
- 235000009436 Actinidia deliciosa Nutrition 0.000 description 4
- 235000017166 Bambusa arundinacea Nutrition 0.000 description 4
- 235000017491 Bambusa tulda Nutrition 0.000 description 4
- 241001330002 Bambuseae Species 0.000 description 4
- 235000015334 Phyllostachys viridis Nutrition 0.000 description 4
- 229920006221 acetate fiber Polymers 0.000 description 4
- 239000011425 bamboo Substances 0.000 description 4
- 239000006185 dispersion Substances 0.000 description 3
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- 239000008187 granular material Substances 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 230000000391 smoking effect Effects 0.000 description 3
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
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- 235000009434 Actinidia chinensis Nutrition 0.000 description 1
- 239000005632 Capric acid (CAS 334-48-5) Substances 0.000 description 1
- 229920000049 Carbon (fiber) Polymers 0.000 description 1
- GHVNFZFCNZKVNT-UHFFFAOYSA-N Decanoic acid Natural products CCCCCCCCCC(O)=O GHVNFZFCNZKVNT-UHFFFAOYSA-N 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 240000006240 Linum usitatissimum Species 0.000 description 1
- 235000004431 Linum usitatissimum Nutrition 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 239000004917 carbon fiber Substances 0.000 description 1
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- 239000011248 coating agent Substances 0.000 description 1
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- 238000009826 distribution Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- -1 incense sticks Substances 0.000 description 1
- 230000005923 long-lasting effect Effects 0.000 description 1
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- 238000001935 peptisation Methods 0.000 description 1
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- 238000007711 solidification Methods 0.000 description 1
- 230000008023 solidification Effects 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
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- 230000001502 supplementing effect Effects 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
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Classifications
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/08—Use of materials for tobacco smoke filters of organic materials as carrier or major constituent
- A24D3/10—Use of materials for tobacco smoke filters of organic materials as carrier or major constituent of cellulose or cellulose derivatives
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/02—Manufacture of tobacco smoke filters
- A24D3/0204—Preliminary operations before the filter rod forming process, e.g. crimping, blooming
- A24D3/0212—Applying additives to filter materials
- A24D3/0225—Applying additives to filter materials with solid additives, e.g. incorporation of a granular product
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/14—Use of materials for tobacco smoke filters of organic materials as additive
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/005—Compositions containing perfumes; Compositions containing deodorants
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/03—Polysaccharides or derivatives thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/03—Polysaccharides or derivatives thereof
- D06M15/13—Alginic acid or derivatives thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/53—Polyethers
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/10—Animal fibres
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/40—Fibres of carbon
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Materials Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Disinfection, Sterilisation Or Deodorisation Of Air (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
- Fats And Perfumes (AREA)
Abstract
Description
【技术领域】【Technical field】
本发明属于烟草技术加工领域。更具体地，本发明涉及一种释香凝胶纤维滤棒的制备方法。The invention belongs to the technical field of tobacco processing. More specifically, the present invention relates to a method for preparing a fragrance-releasing gel fiber filter stick.
【背景技术】【Background technique】
随着卷烟加香工艺的日趋成熟，滤棒加香工艺成为卷烟生产企业的重点研究方向。同时，国家烟草总局一直坚持卷烟低焦油化趋势，对于烟草生产企业而言增香补香技术尤为关键。然而，卷烟烟丝段加香工艺又会受到卷烟在燃烧时产生高温的制约，这种高温会导致增香补香技术赋予的特征香味发生变化。因此，低温释香技术，即滤棒加香技术是目前克服高温增香技术缺陷的重要技术手段。With the maturity of the cigarette flavoring process, the filter stick flavoring process has become a key research direction for cigarette manufacturers. At the same time, the State Tobacco Administration has been adhering to the trend of low-tar cigarettes, and the technology of increasing flavor and supplementing flavor is particularly critical for tobacco manufacturers. However, the cigarette shredded tobacco flavoring process will be restricted by the high temperature generated when the cigarette is burned, and this high temperature will lead to changes in the characteristic fragrance given by the flavoring and flavoring technology. Therefore, the low-temperature aroma release technology, that is, the filter stick aroma technology is an important technical means to overcome the defects of the high-temperature aroma technology.
目前滤棒加香技术主要分为胶囊、香线、颗粒等。烟用胶囊释香技术目前已趋于成熟，但是其强度指标有待于提高，胶囊强度低，破裂漏香，导致胶囊滤棒成品率低；胶囊强度高导致释香困难；而且成本较高。颗粒释香和香线释香同时存在保香留香差的问题。同时胶囊载香的只能选择辛癸酸甘油酯的香精进行滴制。胶囊壁材遇水溶解是该技术的另一短板。At present, filter stick flavoring technology is mainly divided into capsules, incense sticks, granules and so on. The aroma release technology of cigarette capsules has become mature, but its strength index needs to be improved. The strength of the capsule is low, and the fragrance leaks due to rupture, resulting in a low yield of capsule filter rods; the high strength of the capsule makes it difficult to release aroma; and the cost is high. There is the problem of poor fragrance retention and fragrance retention in particle fragrance release and incense thread fragrance release. At the same time, capsules with fragrance can only choose the essence of caprylic acid glyceride for dripping. The dissolution of capsule wall material in water is another shortcoming of this technology.
CN 105595417公开了一种线状凝胶释香滤棒的制备方法。这种方法首先需要使用大量的凝胶，在卷烟滤棒段大约60℃的抽吸温度下凝胶不能完全溶化开，添加的增香物质释香就会不充分，导致香气量不足，而且要增加比较复杂的设备来实现凝胶在丝束上的喷射工艺。CN 105595417 discloses a method for preparing a linear gel fragrance-releasing filter stick. This method first requires the use of a large amount of gel. The gel cannot be completely melted at the smoking temperature of the cigarette filter rod section at about 60°C, and the added flavoring substances will not release enough flavor, resulting in insufficient aroma. More complex equipment is added to realize the spraying process of gel on the tow.
针对现有技术缺陷，本发明人在总结现有技术的基础之上，通过大量实验研究与分析，终于完成了本发明。Aiming at the defects of the prior art, the inventor finally completed the present invention through a large amount of experimental research and analysis on the basis of summarizing the prior art.
【发明内容】【Content of invention】
[要解决的技术问题][Technical problem to be solved]
本发明的目的是提供一种释香凝胶纤维滤棒的制备方法。The purpose of the present invention is to provide a method for preparing a fragrance-releasing gel fiber filter stick.
[技术方案][Technical solutions]
本发明是通过下述技术方案实现的。The present invention is achieved through the following technical solutions.
本发明涉及一种释香凝胶纤维滤棒的制备方法。The invention relates to a method for preparing a fragrance-releasing gel fiber filter stick.
该制备方法的步骤如下：The steps of the preparation method are as follows:
A、混纺纤维粉制备A. Preparation of blended fiber powder
将混纺纤维线经过压切、粉碎、筛分与去杂质处理，得到混纺纤维粉；The blended fiber thread is processed by pressing, crushing, screening and removing impurities to obtain the blended fiber powder;
B、香液制备B. Fragrance preparation
使用纯净水或辛癸酸甘油酯溶剂与陈皮香料配制得到一种浓度为以重量计12～18％的香液；Purified water or caprylic acid glyceride solvent and tangerine peel fragrance are used to prepare a fragrance liquid with a concentration of 12-18% by weight;
C、释香凝胶制备C. Preparation of fragrance-releasing gel
让卡拉胶、聚乙二醇、海藻酸钠、琼脂与水按照重量比0.2～1.5：5～8：0.1～0.2：0.1～0.2：0.1～0.2混合配制得到一种凝胶液，然后往所述凝胶液中添加在步骤B得到的香液，搅拌混合均匀，得到所述的释香凝胶；Mix carrageenan, polyethylene glycol, sodium alginate, agar and water according to the weight ratio of 0.2-1.5:5-8:0.1-0.2:0.1-0.2:0.1-0.2 to prepare a gel solution, and then add it to the Add the fragrance liquid obtained in step B to the gel liquid, stir and mix evenly to obtain the fragrance-releasing gel;
D、浸泡D. Soak
在室温下，将步骤A得到的混纺纤维粉浸泡在步骤B得到的香液中，分离得到释香混纺纤维粉；At room temperature, soak the blended fiber powder obtained in step A in the fragrance solution obtained in step B, and separate to obtain the fragrance-releasing blended fiber powder;
E、混配E. Mixing
在温度40～60℃的条件下，将步骤D得到的释香混纺纤维粉与步骤C得到的释香凝胶按照重量比1.5～2.0：0.3～0.8搅拌混合，得到一种释香凝胶混纺纤维粉；Under the condition of temperature 40-60°C, stir and mix the fragrance-releasing blended fiber powder obtained in step D and the fragrance-releasing gel obtained in step C according to the weight ratio of 1.5-2.0:0.3-0.8 to obtain a fragrance-releasing gel blend fiber powder;
F、成型F. Forming
在滤棒成型机上，在烟枪前端将醋纤丝束均匀铺展，将步骤E得到的释香凝胶混纺纤维粉通过水浴辊均匀涂抹在整个醋纤丝束展开面上，经过烟枪成型，硬化，得到所述的释香凝胶混纺纤维滤棒。On the filter rod forming machine, the cellulose acetate tow is evenly spread at the front end of the bong, and the fragrance-releasing gel blended fiber powder obtained in step E is evenly spread on the entire unfolded surface of the cellulose acetate tow by a water bath roller, and formed by the bong. hardening to obtain the fragrance-releasing gel blended fiber filter stick.
根据本发明的另一种优选实施方式，在步骤A中，所述混纺纤维线粉的尺寸是0.2～1.2mm。According to another preferred embodiment of the present invention, in step A, the size of the blended fiber strand powder is 0.2-1.2mm.
根据本发明的另一种优选实施方式，在步骤B中，所述的陈皮香料用猕猴桃香料、竹叶香料或桂花香料代替。According to another preferred embodiment of the present invention, in step B, the orange peel flavor is replaced with kiwi fruit flavor, bamboo leaf flavor or sweet-scented osmanthus flavor.
根据本发明的另一种优选实施方式，在步骤C中，卡拉胶、聚乙二醇、海藻酸钠、琼脂与水在温度40～60℃的条件下搅拌混合0.3～1.0小时。According to another preferred embodiment of the present invention, in step C, carrageenan, polyethylene glycol, sodium alginate, agar and water are stirred and mixed at a temperature of 40-60° C. for 0.3-1.0 hour.
根据本发明的另一种优选实施方式，在步骤C中，所述凝胶液与所述香液的重量比是0.8～1.2：0.4～0.6。According to another preferred embodiment of the present invention, in step C, the weight ratio of the gel liquid to the fragrance liquid is 0.8-1.2:0.4-0.6.
根据本发明的另一种优选实施方式，在步骤D中，所述的混纺纤维粉在香液中浸泡0.5～1.0小时。According to another preferred embodiment of the present invention, in step D, the blended fiber powder is soaked in perfume liquid for 0.5-1.0 hour.
根据本发明的另一种优选实施方式，在步骤E中，所述的释香混纺纤维粉与释香凝胶搅拌混合0.5～1.0小时。According to another preferred embodiment of the present invention, in step E, the fragrance-releasing blended fiber powder is stirred and mixed with the fragrance-releasing gel for 0.5-1.0 hour.
根据本发明的另一种优选实施方式，在步骤F中，在整个醋纤丝束的展开面上,所述释香凝胶混纺纤维粉的量是每毫米滤棒为1.4～1.6mg。According to another preferred embodiment of the present invention, in step F, on the unfolded surface of the entire acetate tow, the amount of the fragrance-releasing gel blended fiber powder is 1.4-1.6 mg per millimeter of filter rod.
下面将更详细地描述本发明。The present invention will be described in more detail below.
本发明涉及一种释香凝胶纤维滤棒的制备方法。The invention relates to a method for preparing a fragrance-releasing gel fiber filter stick.
该制备方法的步骤如下：The steps of the preparation method are as follows:
A、混纺纤维粉制备A. Preparation of blended fiber powder
将混纺纤维线经过压切、粉碎、筛分与去杂质处理，得到混纺纤维粉；The blended fiber thread is processed by pressing, crushing, screening and removing impurities to obtain the blended fiber powder;
所述的混纺纤维是一种安全、强度高、韧性强，多空隙结构非常合适的载香基材。如果使用其他基材，例如粘结烘干的淀粉类植物颗粒，在浸泡载香过程中会导致颗粒松散、碎化，并且干燥后因强度问题不能满足本发明制备方法。The blended fiber is a safe, high-strength, tough and highly suitable fragrance-carrying base material with a multi-void structure. If other substrates are used, such as bonded and dried starchy plant granules, the granules will become loose and fragmented during the process of soaking and carrying incense, and the preparation method of the present invention cannot be satisfied due to the strength problem after drying.
本发明使用的混纺纤维线是成品混纺纤维线，例如亚麻与棉混纺线、蚕丝与棉混纺线、碳纤维与棉混纺线。它们都是目前市场上销售的产品，例如由无锡市天然纺织实业有限公司以商品名棉麻混纺线销售的棉麻混纺线，由东莞市粤雄纺织品有限公司以商品名蚕丝棉混纺线销售的蚕丝棉混纺线。The blended fiber thread used in the present invention is a finished blended fiber thread, such as flax and cotton blended thread, silk and cotton blended thread, carbon fiber and cotton blended thread. They are all products currently on the market. For example, the cotton and linen blended thread sold by Wuxi Natural Textile Industry Co., Ltd. under the trade name of cotton and linen blended thread, and the silk and cotton blended thread sold by Dongguan Yuexiong Textile Co., Ltd. Silk and cotton blended thread.
在本发明中，使用常规切刀将所述的混纺纤维线切成长为1.0～1.5cm的线段，这种线段再使用通常的粉碎机进行粉碎，用常规筛网筛分，收集纤维尺寸为0.2～1.2mm的线段，得到混纺纤维粉。同时，可以根据实际要求选择混纺纤维线的颜色。In the present invention, a conventional cutter is used to cut the blended fiber into 1.0-1.5 cm long segments, which are pulverized by a conventional pulverizer and sieved with a conventional sieve to collect fibers with a size of 0.2 cm. ~1.2mm line segment, to obtain blended fiber powder. At the same time, the color of the blended fiber thread can be selected according to actual requirements.
在本发明中，如果所述混纺纤维粉的尺寸小于0.2mm，则由于滤棒内部醋纤丝束存在间隙，纤维粉尺寸过小存在吸入人体肺部的安全隐患；如果所述混纺纤维粉的尺寸大于1.2mm，则在辊压过程中存在纤维交叉、重叠的情况，导致分布不均匀影响抽吸过程的释香量。因此，所述混纺纤维粉的尺寸为0.2～1.2mm是合理的。In the present invention, if the size of the blended fiber powder is less than 0.2mm, there is a gap in the acetate tow inside the filter rod, and the size of the fiber powder is too small to be inhaled into the lungs of the human body; if the size of the blended fiber powder is If the size is larger than 1.2mm, there will be crossing and overlapping of fibers during the rolling process, resulting in uneven distribution and affecting the amount of fragrance released during the smoking process. Therefore, it is reasonable for the size of the blended fiber powder to be 0.2-1.2 mm.
B、香液制备B. Fragrance preparation
使用纯净水或辛癸酸甘油酯溶剂与陈皮香料配制得到一种浓度为以重量计12～18％的香液；Purified water or caprylic acid glyceride solvent and tangerine peel fragrance are used to prepare a fragrance liquid with a concentration of 12-18% by weight;
根据本发明，根据实际需要，可以用猕猴桃香料、竹叶香料或桂花香料代替所述的陈皮香料。According to the present invention, according to actual needs, the tangerine peel flavor can be replaced with kiwi fruit flavor, bamboo leaf flavor or sweet-scented osmanthus flavor.
本发明使用的陈皮香料、猕猴桃香料、竹叶香料或桂花香料都是目前市场上销售的产品，例如由上海绿洲源香料有限公司以商品名陈皮香料销售的陈皮香料。Tangerine peel spices used in the present invention, kiwifruit spices, bamboo leaf spices or sweet-scented osmanthus spices are all products currently on the market, such as orange peel spices sold under the trade name orange peel spices by Shanghai Oasis Source Perfume Co., Ltd.
在本发明中，如果香液的浓度小于12％，则影响陈皮香不足，抽吸不明显；如果香液的浓度高于18％，则会因为陈皮香气量过大，影响整体烟气的协调性。因此，香液浓度为12～18％是合适的。In the present invention, if the concentration of the fragrance liquid is less than 12%, the fragrance of the tangerine peel will be insufficient, and the suction will not be obvious; if the concentration of the fragrance liquid is higher than 18%, the fragrance of the tangerine peel will be too large, which will affect the coordination of the overall smoke. sex. Therefore, the concentration of fragrance liquid is 12-18% is suitable.
C、释香凝胶制备C. Preparation of fragrance-releasing gel
让卡拉胶、聚乙二醇、海藻酸钠、琼脂与水按照重量比0.2～1.5：5～8：0.1～0.2：0.1～0.2：0.1～0.2混合配制得到一种凝胶液，然后往所述凝胶液中添加在步骤B得到的香液，搅拌混合均匀，得到所述的释香凝胶；Mix carrageenan, polyethylene glycol, sodium alginate, agar and water according to the weight ratio of 0.2-1.5:5-8:0.1-0.2:0.1-0.2:0.1-0.2 to prepare a gel solution, and then add it to the Add the fragrance liquid obtained in step B to the gel liquid, stir and mix evenly to obtain the fragrance-releasing gel;
在本发明中，卡拉胶在制备凝胶液中的主要作用是作为一种增稠剂，调节凝胶液的流动性，同时它具有一定的粘结效果。In the present invention, the main function of the carrageenan in preparing the gel solution is as a thickener to regulate the fluidity of the gel solution, and it has a certain binding effect at the same time.
聚乙二醇在制备凝胶液中的主要作用是作为一种固液态转换物质，聚乙二醇可以在低于40℃时为固态，高于40℃时溶化为液态，液态释香，固态锁香。The main function of polyethylene glycol in the preparation of gel solution is as a solid-liquid conversion substance. Polyethylene glycol can be solid when it is lower than 40 ° C, and melts into liquid when it is higher than 40 ° C. The liquid releases fragrance and solid Lock incense.
海藻酸钠在制备凝胶液中的主要作用是分散剂，将混合的混纺纤维粉均匀地分散在凝胶液中。The main role of sodium alginate in the preparation of the gel solution is as a dispersant, which disperses the mixed blended fiber powder evenly in the gel solution.
琼脂在制备凝胶液中的主要作用是调节凝胶固态强度和凝固速度。The main function of agar in the preparation of gel solution is to adjust the solid strength and solidification speed of the gel.
在本发明中，其它组分用量在所述的范围内时，如果卡拉胶的用量小于0.2，则凝胶液流动性太好，醋纤高速进入烟枪口时，会影响纤维颗粒粉的均匀分散；如果卡拉胶的用量大于1.5，则凝胶液在粘结过程中粘度过大，影响辊在醋纤面涂布效果；因此，卡拉胶的用量为0.2～1.5是合适的。In the present invention, when the consumption of other components is within the stated range, if the consumption of carrageenan is less than 0.2, the fluidity of the gel liquid is too good, and when the acetate fiber enters the mouth of the bong at a high speed, the uniformity of the fiber particle powder will be affected. Dispersion; if the amount of carrageenan is greater than 1.5, the viscosity of the gel solution will be too high during the bonding process, which will affect the coating effect of the roller on the acetate fiber surface; therefore, the amount of carrageenan is 0.2-1.5 is appropriate.
其它组分用量在所述的范围内时，如果聚乙二醇的用量小于5，则液态状态转换为固态的效果差，不利于凝胶液固态锁香；如果聚乙二醇的用量大于8，则卷烟温度滤嘴温度40～60℃不能充分由固态转化为液态；因此，聚乙二醇的用量为5～8是恰当的。When the amount of other components is within the stated range, if the amount of polyethylene glycol is less than 5, the effect of converting the liquid state into a solid state is poor, which is not conducive to the solid-state locking of the gel liquid; if the amount of polyethylene glycol is greater than 8 , the cigarette temperature and filter tip temperature of 40-60°C cannot fully transform from solid to liquid; therefore, the dosage of polyethylene glycol is 5-8 is appropriate.
其它组分用量在所述的范围内时，如果海藻酸钠的用量小于0.1，则混纺纤维颗粒粉在凝胶液中会产生沉淀，不能均匀分散，影响辊在涂布过程中出现不均匀现象；如果海藻酸钠的用量大于0.2，则由于凝胶液过于黏稠，不利于混纺纤维粉分散的均匀性；因此，海藻酸钠的用量为0.1～0.2是可行的。When the amount of other components is within the stated range, if the amount of sodium alginate is less than 0.1, the blended fiber particle powder will precipitate in the gel liquid and cannot be uniformly dispersed, which will affect the unevenness of the roller during the coating process. ; If the amount of sodium alginate is greater than 0.2, the gel solution is too viscous, which is not conducive to the uniformity of dispersion of the blended fiber powder; therefore, the amount of sodium alginate is 0.1 to 0.2 is feasible.
其它组分用量在所述的范围内时，如果琼脂的用量小于0.1，则凝胶液由液态转换为固态时过程缓慢，凝胶液固态效果强度不够，影响锁香；如果琼脂的用量大于0.2，则滤棒中的固态凝胶在温度60℃时溶化效果不好，会出现溶化不充分，产生絮状物，影响释香效果；因此，琼脂的用量为0.1～0.2是合理的。When the amount of other components is within the stated range, if the amount of agar is less than 0.1, the process of the gel liquid being converted from a liquid state to a solid state is slow, and the solid effect of the gel liquid is not strong enough, which will affect the fragrance lock; if the amount of agar is greater than 0.2 , the solid gel in the filter rod does not melt well at a temperature of 60°C, and there will be insufficient melting, resulting in flocs and affecting the fragrance release effect; therefore, the amount of agar used is 0.1 to 0.2 is reasonable.
优选地，卡拉胶、聚乙二醇、海藻酸钠与琼脂的重量比是0.4～1.2：5.8～7.2：0.12～0.18：0.12～0.18。Preferably, the weight ratio of carrageenan, polyethylene glycol, sodium alginate and agar is 0.4-1.2:5.8-7.2:0.12-0.18:0.12-0.18.
更优选地，卡拉胶、聚乙二醇、海藻酸钠与琼脂的重量比是0.6～0.8：6.2～6.8：0.14～0.16：0.14～0.16。More preferably, the weight ratio of carrageenan, polyethylene glycol, sodium alginate and agar is 0.6-0.8:6.2-6.8:0.14-0.16:0.14-0.16.
优选地，卡拉胶、聚乙二醇、海藻酸钠、琼脂与水在温度40～60℃的条件下搅拌混合0.3～1.0小时。Preferably, the carrageenan, polyethylene glycol, sodium alginate, agar and water are stirred and mixed at a temperature of 40-60° C. for 0.3-1.0 hour.
在本发明中，所述凝胶液与所述香液的重量比是0.8～1.2：0.4～0.6。如果凝胶液与香液的重量比超过这个范围，将对释香凝胶的性能产生不良影响，例如凝胶液和香液重量比为0.7:0.3，凝胶中含有的香液量不足，凝胶溶化后释香量不充分，如果凝胶液和香液重量比为1.2:0.7，则凝胶液中香液添加过量，凝胶溶化后释香量过大，影响整体烟气的协调性。In the present invention, the weight ratio of the gel liquid to the fragrance liquid is 0.8-1.2:0.4-0.6. If the weight ratio of the gel liquid and the fragrance liquid exceeds this range, it will have an adverse effect on the performance of the fragrance-releasing gel. The amount of fragrance released after peptization is insufficient. If the weight ratio of gel liquid and fragrance liquid is 1.2:0.7, the amount of fragrance liquid in the gel liquid will be added too much, and the amount of fragrance released after gel melting will be too large, which will affect the coordination of the overall smoke.
D、浸泡D. Soak
在室温下，将步骤A得到的混纺纤维粉浸泡在步骤B得到的香液中，分离得到释香混纺纤维粉；At room temperature, soak the blended fiber powder obtained in step A in the fragrance solution obtained in step B, and separate to obtain the fragrance-releasing blended fiber powder;
在这个步骤中浸泡的主要目的是让香液渗透到混纺纤维粉中，使混纺纤维粉具有香液所含香料的香味。The main purpose of soaking in this step is to allow the fragrance liquid to penetrate into the blended fiber powder, so that the blended fiber powder has the fragrance of the spices contained in the fragrance liquid.
所述的混纺纤维粉在香液中浸泡时间为0.5～1.0小时。时间太短或太长很显然都是不利的。The soaking time of the blended fiber powder in the perfume liquid is 0.5-1.0 hour. Too short or too long is obviously not good.
E、混配E. Mixing
在温度40～60℃的条件下，将步骤D得到的释香混纺纤维粉与步骤C得到的释香凝胶按照重量比1.5～2.0：0.3～0.8搅拌混合，得到一种释香凝胶混纺纤维粉；Under the condition of temperature 40-60°C, stir and mix the fragrance-releasing blended fiber powder obtained in step D and the fragrance-releasing gel obtained in step C according to the weight ratio of 1.5-2.0:0.3-0.8 to obtain a fragrance-releasing gel blend fiber powder;
根据本发明，释香混纺纤维粉与释香凝胶搅拌混合的主要目的是在展开的醋纤表面能均匀的分散并粘结，防止醋纤快速进入烟枪口时混纺纤维粉聚集或掉落，影响分散均匀性。According to the present invention, the main purpose of stirring and mixing the fragrance-releasing blended fiber powder and the fragrance-releasing gel is to disperse and bond evenly on the surface of the unfolded acetate fiber, so as to prevent the blended fiber powder from gathering or falling off when the acetate fiber quickly enters the mouth of the bong , affecting the dispersion uniformity.
在这个步骤中，所述的释香混纺纤维粉与释香凝胶在温度40～60℃的条件下搅拌混合0.5～1.0小时。In this step, the fragrance-releasing blended fiber powder and the fragrance-releasing gel are stirred and mixed for 0.5-1.0 hour at a temperature of 40-60°C.
搅拌混合时的温度是很重要的。如果温度低于40℃，则卡拉胶、琼脂溶解不充分，有絮状物存在，混合不均匀；如果温度高于60℃，则因滤棒在卷烟抽吸状态下温度低于60℃，影响凝胶液及混纺纤维粉的释香；因此，搅拌混合时的温度为40～60℃是恰当的。The temperature at which the mixture is stirred is important. If the temperature is lower than 40°C, the dissolution of carrageenan and agar is insufficient, flocs exist, and the mixing is uneven; Fragrance release of gel liquid and blended fiber powder; therefore, it is appropriate to stir and mix at a temperature of 40-60°C.
F、成型F. Forming
在滤棒成型机上，在烟枪前端将醋纤丝束均匀铺展，将步骤E得到的释香凝胶混纺纤维粉通过水浴辊均匀涂抹在整个醋纤丝束展开面上，经过烟枪成型，硬化，得到所述的释香凝胶混纺纤维滤棒。On the filter rod forming machine, the cellulose acetate tow is evenly spread at the front end of the bong, and the fragrance-releasing gel blended fiber powder obtained in step E is evenly spread on the entire unfolded surface of the cellulose acetate tow by a water bath roller, and formed by the bong. hardening to obtain the fragrance-releasing gel blended fiber filter stick.
本发明使用的滤棒成型机是烟草加工技术领域里通常使用的设备，例如由沈飞烟机厂以商品名纤维滤棒成型机销售的ZL22A型滤棒成型机。The filter rod forming machine used in the present invention is equipment commonly used in the field of tobacco processing technology, such as the ZL22A filter rod forming machine sold by Shenfei Tobacco Machine Factory under the trade name fiber filter rod forming machine.
根据本发明，在整个醋纤丝束的展开面上,所述释香凝胶混纺纤维粉的量是每毫米滤棒为1.4～1.6mg。According to the present invention, the amount of the fragrance-releasing gel blended fiber powder is 1.4-1.6 mg per millimeter of the filter rod on the unfolded surface of the entire cellulose acetate tow.
如果超过这个量的范围都是不可取的，因为释香凝胶混纺纤维粉的添加量小于1.4mg/mm滤棒，滤棒加香量不足，释香效果差，如果添加量大于1.6mg/mm则因加香过量，影响烟气的协调性。If the amount exceeds this range, it is not advisable, because the addition amount of the fragrance-releasing gel blended fiber powder is less than 1.4mg/mm filter rod, the amount of fragrance added to the filter rod is insufficient, and the fragrance release effect is poor. If the addition amount is greater than 1.6mg/mm mm is due to excessive flavoring, which affects the coordination of the smoke.
本发明制备得到一种在温度40～60℃下热溶解为液态，并释放香味的释香凝胶混纺纤维滤棒。在室温下滤棒内部纤维颗粒因为包裹在凝胶内部，呈固体状，香气保存持久。当卷烟烟丝燃烧、外加抽吸时，主流烟气温度约40～60℃会经过滤棒进入口腔，此时滤棒内凝胶纤维会由固态转化为液态，释香纤维颗粒与包裹其外层的凝胶层分离，释香纤维释放出香气，达到增香、补香的效果。本发明释香凝胶混纺纤维滤棒能够长久持香，同时也解决了稳定均匀释香的这个技术问题。The invention prepares a fragrance-releasing gel blended fiber filter stick which can be thermally dissolved into a liquid state at a temperature of 40-60° C. and release fragrance. At room temperature, the fiber particles inside the filter stick are solid because they are wrapped in the gel, and the aroma is preserved for a long time. When cigarette shredded tobacco is burned and smoked, the mainstream smoke temperature is about 40-60°C and enters the mouth through the filter rod. At this time, the gel fiber in the filter rod will change from solid to liquid state, and the fragrance-releasing fiber particles will wrap its outer layer. The gel layer of the product is separated, and the fragrance-releasing fiber releases the fragrance to achieve the effect of increasing fragrance and replenishing fragrance. The fragrance-releasing gel blended fiber filter stick of the present invention can hold fragrance for a long time, and also solves the technical problem of stable and uniform fragrance release.
[有益效果][beneficial effect]
本发明的有益效果是：与现有技术相比，本发明释香凝胶混纺纤维滤棒释香效果稳定，持香久。在抽吸过程中，由于凝胶用量低，凝胶易于溶化，方便纤维颗粒释香，效果稳定，同时整个抽吸过程释香均匀。The beneficial effects of the invention are: compared with the prior art, the fragrance-releasing gel blended fiber filter stick of the invention has a stable fragrance-releasing effect and a long-lasting fragrance. During the inhalation process, due to the low amount of gel, the gel is easy to dissolve, which is convenient for the fiber particles to release the fragrance, the effect is stable, and the fragrance is released evenly during the entire inhalation process.
【附图说明】【Description of drawings】
【具体实施方式】【detailed description】
通过下述实施例将能够更好地理解本发明。The present invention will be better understood by the following examples.
实施例1：制备本发明释香凝胶纤维滤棒Embodiment 1: Preparation of fragrance-releasing gel fiber filter stick of the present invention
该实施例的实施步骤如下：The implementation steps of this embodiment are as follows:
A、混纺纤维粉制备A. Preparation of blended fiber powder
将混纺纤维线经过压切为1.0cm的线段、粉碎、筛分，收集纤维尺寸为0.2mm的线段，除去杂质，得到混纺纤维粉；The blended fiber thread is cut into a line segment of 1.0 cm, crushed, and sieved, and the line segment with a fiber size of 0.2 mm is collected to remove impurities to obtain a blended fiber powder;
B、香液制备B. Fragrance preparation
使用辛癸酸甘油酯溶剂与陈皮香料配制得到一种浓度为以重量计15％的香液；A fragrance liquid with a concentration of 15% by weight is prepared by using caprylic acid glyceride solvent and orange peel fragrance;
C、释香凝胶制备C. Preparation of fragrance-releasing gel
让卡拉胶、聚乙二醇、海藻酸钠、琼脂与水按照重量比0.4：6.2：0.1：0.1：0.1混合配制得到一种凝胶液，然后按照凝胶液与香液的重量比0.8：0.5，往所述凝胶液中添加在步骤B得到的香液，搅拌混合均匀，得到所述的释香凝胶；Mix carrageenan, polyethylene glycol, sodium alginate, agar and water according to the weight ratio of 0.4:6.2:0.1:0.1:0.1 to prepare a gel solution, and then according to the weight ratio of the gel solution to the perfume solution 0.8: 0.5, add the fragrance liquid obtained in step B to the gel liquid, stir and mix evenly to obtain the fragrance releasing gel;
D、浸泡D. Soak
在室温下，将步骤A得到的混纺纤维粉在步骤B得到的香液中浸泡0.5小时，分离得到释香混纺纤维粉；At room temperature, soak the blended fiber powder obtained in step A in the fragrance liquid obtained in step B for 0.5 hour, and separate to obtain the fragrance-releasing blended fiber powder;
E、混配E. Mixing
在温度40℃的条件下，将步骤D得到的释香混纺纤维粉与步骤C得到的释香凝胶按照重量比1.5：0.4搅拌混合0.6小时，得到一种释香凝胶混纺纤维粉；At a temperature of 40°C, the fragrance-releasing blended fiber powder obtained in step D and the fragrance-releasing gel obtained in step C were stirred and mixed for 0.6 hours at a weight ratio of 1.5:0.4 to obtain a fragrance-releasing gel blended fiber powder;
F、成型F. Forming
在滤棒成型机上，在烟枪前端将醋纤丝束均匀铺展，将步骤E得到的释香凝胶混纺纤维粉通过水浴辊均匀涂抹在整个醋纤丝束展开面上，达到每毫米滤棒为1.4mg，经过烟枪成型，硬化，得到所述的释香凝胶混纺纤维滤棒。On the filter rod forming machine, the cellulose acetate tow is evenly spread at the front end of the bong, and the fragrance-releasing gel blended fiber powder obtained in step E is evenly spread on the entire unfolded surface of the cellulose acetate tow by a water bath roller, reaching It is 1.4 mg, and is molded and hardened through a pipe to obtain the described fragrance-releasing gel blended fiber filter stick.
实施例2：制备本发明释香凝胶纤维滤棒Embodiment 2: Preparation of fragrance-releasing gel fiber filter stick of the present invention
该实施例的实施步骤如下：The implementation steps of this embodiment are as follows:
A、混纺纤维粉制备A. Preparation of blended fiber powder
将混纺纤维线经过压切为1.2cm的线段、粉碎、筛分，收集纤维尺寸为0.4mm的线段，除去杂质，得到混纺纤维粉；The blended fiber thread is cut into a 1.2cm line segment, pulverized and sieved, and the line segment with a fiber size of 0.4mm is collected, and impurities are removed to obtain a blended fiber powder;
B、香液制备B. Fragrance preparation
使用辛癸酸甘油酯溶剂与猕猴桃香料配制得到一种浓度为以重量计12％的香液；Using caprylic capric acid glyceride solvent and kiwi flavor to prepare a fragrance liquid with a concentration of 12% by weight;
C、释香凝胶制备C. Preparation of fragrance-releasing gel
让卡拉胶、聚乙二醇、海藻酸钠、琼脂与水按照重量比1.2：6.8：0.2：0.1：0.2混合配制得到一种凝胶液，然后按照凝胶液与香液的重量比1.2：0.4，往所述凝胶液中添加在步骤B得到的香液，搅拌混合均匀，得到所述的释香凝胶；Mix carrageenan, polyethylene glycol, sodium alginate, agar and water according to the weight ratio of 1.2:6.8:0.2:0.1:0.2 to prepare a gel solution, and then according to the weight ratio of the gel solution to the perfume solution 1.2: 0.4, add the fragrance liquid obtained in step B to the gel liquid, stir and mix evenly to obtain the fragrance-releasing gel;
D、浸泡D. Soak
在室温下，将步骤A得到的混纺纤维粉在步骤B得到的香液中浸泡1.0小时，分离得到释香混纺纤维粉；At room temperature, soak the blended fiber powder obtained in step A in the fragrance liquid obtained in step B for 1.0 hour, and separate to obtain the fragrance-releasing blended fiber powder;
E、混配E. Mixing
在温度60℃的条件下，将步骤D得到的释香混纺纤维粉与步骤C得到的释香凝胶按照重量比1.8：0.6搅拌混合0.8小时，得到一种释香凝胶混纺纤维粉；At a temperature of 60°C, the fragrance-releasing blended fiber powder obtained in step D and the fragrance-releasing gel obtained in step C were stirred and mixed for 0.8 hours at a weight ratio of 1.8:0.6 to obtain a fragrance-releasing gel blended fiber powder;
F、成型F. Molding
在滤棒成型机上，在烟枪前端将醋纤丝束均匀铺展，将步骤E得到的释香凝胶混纺纤维粉通过水浴辊均匀涂抹在整个醋纤丝束展开面上，达到每毫米滤棒为1.6mg，经过烟枪成型，硬化，得到所述的释香凝胶混纺纤维滤棒。On the filter rod forming machine, the cellulose acetate tow is evenly spread at the front end of the bong, and the fragrance-releasing gel blended fiber powder obtained in step E is evenly spread on the entire unfolded surface of the cellulose acetate tow by a water bath roller, reaching It is 1.6 mg, and is molded and hardened through a pipe to obtain the described fragrance-releasing gel blended fiber filter stick.
实施例3：制备本发明释香凝胶纤维滤棒Embodiment 3: Preparation of fragrance-releasing gel fiber filter stick of the present invention
该实施例的实施步骤如下：The implementation steps of this embodiment are as follows:
A、混纺纤维粉制备A. Preparation of blended fiber powder
将混纺纤维线经过压切为1.5cm的线段、粉碎、筛分，收集纤维尺寸为0.8mm的线段，除去杂质，得到混纺纤维粉；The blended fiber thread is cut into a 1.5cm line segment, pulverized, sieved, and the line segment with a fiber size of 0.8mm is collected, and impurities are removed to obtain a blended fiber powder;
B、香液制备B. Fragrance preparation
使用辛癸酸甘油酯溶剂与竹叶香料配制得到一种浓度为以重量计18％的香液；A fragrance liquid with a concentration of 18% by weight is prepared by using caprylic capric acid glyceride solvent and bamboo leaf spice;
C、释香凝胶制备C. Preparation of fragrance-releasing gel
让卡拉胶、聚乙二醇、海藻酸钠、琼脂与水按照重量比0.2：5：0.1：0.2：0.1混合配制得到一种凝胶液，然后按照凝胶液与香液的重量比1.0：0.6，往所述凝胶液中添加在步骤B得到的香液，搅拌混合均匀，得到所述的释香凝胶；Mix carrageenan, polyethylene glycol, sodium alginate, agar and water according to the weight ratio of 0.2:5:0.1:0.2:0.1 to prepare a gel solution, and then according to the weight ratio of the gel solution to the perfume solution 1.0: 0.6, add the fragrance liquid obtained in step B to the gel liquid, stir and mix evenly to obtain the fragrance releasing gel;
D、浸泡D. Soak
在室温下，将步骤A得到的混纺纤维粉在步骤B得到的香液中浸泡0.6小时，分离得到释香混纺纤维粉；At room temperature, soak the blended fiber powder obtained in step A in the fragrance liquid obtained in step B for 0.6 hours, and separate to obtain the fragrance-releasing blended fiber powder;
E、混配E. Mixing
在温度50℃的条件下，将步骤D得到的释香混纺纤维粉与步骤C得到的释香凝胶按照重量比2.0：0.3搅拌混合0.5小时，得到一种释香凝胶混纺纤维粉；At a temperature of 50°C, the fragrance-releasing blended fiber powder obtained in step D and the fragrance-releasing gel obtained in step C were stirred and mixed for 0.5 hours at a weight ratio of 2.0:0.3 to obtain a fragrance-releasing gel blended fiber powder;
F、成型F. Forming
在滤棒成型机上，在烟枪前端将醋纤丝束均匀铺展，将步骤E得到的释香凝胶混纺纤维粉通过水浴辊均匀涂抹在整个醋纤丝束展开面上，达到每毫米滤棒为1.5mg，经过烟枪成型，硬化，得到所述的释香凝胶混纺纤维滤棒。On the filter rod forming machine, the cellulose acetate tow is evenly spread at the front end of the bong, and the fragrance-releasing gel blended fiber powder obtained in step E is evenly spread on the entire unfolded surface of the cellulose acetate tow by a water bath roller, reaching It is 1.5 mg, and is molded and hardened through a pipe to obtain the described fragrance-releasing gel blended fiber filter stick.
实施例4：制备本发明释香凝胶纤维滤棒Embodiment 4: Preparation of fragrance-releasing gel fiber filter stick of the present invention
该实施例的实施步骤如下：The implementation steps of this embodiment are as follows:
A、混纺纤维粉制备A. Preparation of blended fiber powder
将混纺纤维线经过压切为1.4cm的线段、粉碎、筛分，收集纤维尺寸为1.2mm的线段，除去杂质，得到混纺纤维粉；The blended fiber thread is cut into a line segment of 1.4 cm, pulverized and sieved, and the line segment with a fiber size of 1.2 mm is collected to remove impurities to obtain a blended fiber powder;
B、香液制备B. Fragrance preparation
使用辛癸酸甘油酯溶剂与桂花香料配制得到一种浓度为以重量计14％的香液；Use caprylic acid glyceride solvent and sweet-scented osmanthus fragrance to prepare a kind of concentration and be the fragrance liquid of 14% by weight;
C、释香凝胶制备C. Preparation of fragrance-releasing gel
让卡拉胶、聚乙二醇、海藻酸钠、琼脂与水按照重量比1.5：8：0.2：0.2：0.1混合配制得到一种凝胶液，然后按照凝胶液与香液的重量比0.8：0.5，往所述凝胶液中添加在步骤B得到的香液，搅拌混合均匀，得到所述的释香凝胶；Mix carrageenan, polyethylene glycol, sodium alginate, agar and water according to the weight ratio of 1.5:8:0.2:0.2:0.1 to prepare a gel solution, and then according to the weight ratio of gel solution and perfume solution 0.8: 0.5, add the fragrance liquid obtained in step B to the gel liquid, stir and mix evenly to obtain the fragrance releasing gel;
D、浸泡D. Soak
在室温下，将步骤A得到的混纺纤维粉在步骤B得到的香液中浸泡0.8小时，分离得到释香混纺纤维粉；At room temperature, soak the blended fiber powder obtained in step A in the fragrance liquid obtained in step B for 0.8 hours, and separate to obtain the fragrance-releasing blended fiber powder;
E、混配E. Mixing
在温度45℃的条件下，将步骤D得到的释香混纺纤维粉与步骤C得到的释香凝胶按照重量比1.6：0.8搅拌混合1.0小时，得到一种释香凝胶混纺纤维粉；At a temperature of 45°C, the fragrance-releasing blended fiber powder obtained in step D and the fragrance-releasing gel obtained in step C were stirred and mixed for 1.0 hour at a weight ratio of 1.6:0.8 to obtain a fragrance-releasing gel blended fiber powder;
F、成型F. Forming
在滤棒成型机上，在烟枪前端将醋纤丝束均匀铺展，将步骤E得到的释香凝胶混纺纤维粉通过水浴辊均匀涂抹在整个醋纤丝束展开面上，达到每毫米滤棒为1.4mg，经过烟枪成型，硬化，得到所述的释香凝胶混纺纤维滤棒。On the filter rod forming machine, the cellulose acetate tow is evenly spread at the front end of the bong, and the fragrance-releasing gel blended fiber powder obtained in step E is evenly spread on the entire unfolded surface of the cellulose acetate tow by a water bath roller, reaching It is 1.4 mg, and is molded and hardened through a pipe to obtain the described fragrance-releasing gel blended fiber filter stick.
实施例5：制备本发明释香凝胶纤维滤棒Embodiment 5: Preparation of fragrance-releasing gel fiber filter stick of the present invention
该实施例的实施步骤如下：The implementation steps of this embodiment are as follows:
A、混纺纤维粉制备A. Preparation of blended fiber powder
将混纺纤维线经过压切为1.1cm的线段、粉碎、筛分，收集纤维尺寸为1.0mm的线段，除去杂质，得到混纺纤维粉；The blended fiber thread is cut into a line segment of 1.1 cm, pulverized, and sieved, and the line segment with a fiber size of 1.0 mm is collected, and impurities are removed to obtain a blended fiber powder;
B、香液制备B. Fragrance preparation
使用纯净水与陈皮香料配制得到一种浓度为以重量计14％的香液；Purified water and tangerine peel spices are used to prepare a fragrance liquid with a concentration of 14% by weight;
C、释香凝胶制备C. Preparation of fragrance-releasing gel
让卡拉胶、聚乙二醇、海藻酸钠、琼脂与水按照重量比0.6：5.8：0.1：0.2：0.1混合配制得到一种凝胶液，然后按照凝胶液与香液的重量比1.2：0.4，往所述凝胶液中添加在步骤B得到的香液，搅拌混合均匀，得到所述的释香凝胶；Mix carrageenan, polyethylene glycol, sodium alginate, agar and water according to the weight ratio of 0.6:5.8:0.1:0.2:0.1 to prepare a gel solution, and then according to the weight ratio of the gel solution to the perfume solution 1.2: 0.4, add the fragrance liquid obtained in step B to the gel liquid, stir and mix evenly to obtain the fragrance-releasing gel;
D、浸泡D. Soak
在室温下，将步骤A得到的混纺纤维粉在步骤B得到的香液中浸泡0.9小时，分离得到释香混纺纤维粉；At room temperature, soak the blended fiber powder obtained in step A in the fragrance liquid obtained in step B for 0.9 hours, and separate to obtain the fragrance-releasing blended fiber powder;
E、混配E. Mixing
在温度55℃的条件下，将步骤D得到的释香混纺纤维粉与步骤C得到的释香凝胶按照重量比1.8：0.4搅拌混合0.9小时，得到一种释香凝胶混纺纤维粉；At a temperature of 55°C, the fragrance-releasing blended fiber powder obtained in step D and the fragrance-releasing gel obtained in step C were stirred and mixed for 0.9 hours at a weight ratio of 1.8:0.4 to obtain a fragrance-releasing gel blended fiber powder;
F、成型F. Forming
在滤棒成型机上，在烟枪前端将醋纤丝束均匀铺展，将步骤E得到的释香凝胶混纺纤维粉通过水浴辊均匀涂抹在整个醋纤丝束展开面上，达到每毫米滤棒为1.6mg，经过烟枪成型，硬化，得到所述的释香凝胶混纺纤维滤棒。On the filter rod forming machine, the cellulose acetate tow is evenly spread at the front end of the bong, and the fragrance-releasing gel blended fiber powder obtained in step E is evenly spread on the entire unfolded surface of the cellulose acetate tow by a water bath roller, reaching It is 1.6 mg, and is molded and hardened through a pipe to obtain the described fragrance-releasing gel blended fiber filter stick.
实施例6：制备本发明释香凝胶纤维滤棒Embodiment 6: Preparation of fragrance-releasing gel fiber filter stick of the present invention
该实施例的实施步骤如下：The implementation steps of this embodiment are as follows:
A、混纺纤维粉制备A. Preparation of blended fiber powder
将混纺纤维线经过压切为1.3cm的线段、粉碎、筛分，收集纤维尺寸为0.6mm的线段，除去杂质，得到混纺纤维粉；The blended fiber thread is cut into a line segment of 1.3 cm, crushed and sieved, and the line segment with a fiber size of 0.6 mm is collected to remove impurities to obtain a blended fiber powder;
B、香液制备B. Fragrance preparation
使用辛癸酸甘油酯溶剂与桂花香料配制得到一种浓度为以重量计15％的香液；A fragrance liquid with a concentration of 15% by weight is prepared by using caprylic acid glyceride solvent and sweet-scented osmanthus fragrance;
C、释香凝胶制备C. Preparation of fragrance-releasing gel
让卡拉胶、聚乙二醇、海藻酸钠、琼脂与水按照重量比0.8：7.2：0.2：0.2混合配制得到一种凝胶液，然后按照凝胶液与香液的重量比1.0：0.6，往所述凝胶液中添加在步骤B得到的香液，搅拌混合均匀，得到所述的释香凝胶；Mix carrageenan, polyethylene glycol, sodium alginate, agar and water according to the weight ratio of 0.8:7.2:0.2:0.2 to prepare a gel solution, and then according to the weight ratio of gel solution and perfume solution 1.0:0.6, Add the fragrance liquid obtained in step B to the gel liquid, stir and mix evenly to obtain the fragrance-releasing gel;
D、浸泡D. Soak
在室温下，将步骤A得到的混纺纤维粉在步骤B得到的香液中浸泡0.8小时，分离得到释香混纺纤维粉；At room temperature, soak the blended fiber powder obtained in step A in the fragrance liquid obtained in step B for 0.8 hours, and separate to obtain the fragrance-releasing blended fiber powder;
E、混配E. Mixing
在温度50℃的条件下，将步骤D得到的释香混纺纤维粉与步骤C得到的释香凝胶按照重量比1.6：0.6搅拌混合0.8小时，得到一种释香凝胶混纺纤维粉；At a temperature of 50°C, the fragrance-releasing blended fiber powder obtained in step D and the fragrance-releasing gel obtained in step C were stirred and mixed for 0.8 hours at a weight ratio of 1.6:0.6 to obtain a fragrance-releasing gel blended fiber powder;
F、成型F. Forming
在滤棒成型机上，在烟枪前端将醋纤丝束均匀铺展，将步骤E得到的释香凝胶混纺纤维粉通过水浴辊均匀涂抹在整个醋纤丝束展开面上，达到每毫米滤棒为1.5mg，经过烟枪成型，硬化，得到所述的释香凝胶混纺纤维滤棒。On the filter rod forming machine, the cellulose acetate tow is evenly spread at the front end of the bong, and the fragrance-releasing gel blended fiber powder obtained in step E is evenly spread on the entire unfolded surface of the cellulose acetate tow by a water bath roller, reaching It is 1.5 mg, and is molded and hardened through a pipe to obtain the described fragrance-releasing gel blended fiber filter stick.
实施例7：制备本发明释香凝胶纤维滤棒Embodiment 7: Preparation of fragrance-releasing gel fiber filter stick of the present invention
该实施例的实施步骤如下：The implementation steps of this embodiment are as follows:
A、混纺纤维粉制备A. Preparation of blended fiber powder
将混纺纤维线经过压切为1.5cm的线段、粉碎、筛分，收集纤维尺寸为0.2mm的线段，除去杂质，得到混纺纤维粉；The blended fiber thread is cut into a 1.5cm line segment, pulverized and sieved, and the line segment with a fiber size of 0.2mm is collected to remove impurities to obtain a blended fiber powder;
B、香液制备B. Fragrance preparation
使用纯净水或辛癸酸甘油酯溶剂与陈皮香料、猕猴桃香料、竹叶香料或桂花香料配制得到一种浓度为以重量计12％的香液；Purified water or caprylic glyceride solvent is used to prepare a fragrance liquid with a concentration of 12% by weight;
C、释香凝胶制备C. Preparation of fragrance-releasing gel
让卡拉胶、聚乙二醇、海藻酸钠、琼脂与水按照重量比1.5：5.8：0.2：0.1混合配制得到一种凝胶液，然后按照凝胶液与香液的重量比1.2：0.6，往所述凝胶液中添加在步骤B得到的香液，搅拌混合均匀，得到所述的释香凝胶；Mix carrageenan, polyethylene glycol, sodium alginate, agar and water according to the weight ratio of 1.5:5.8:0.2:0.1 to prepare a gel solution, and then according to the weight ratio of gel solution and perfume solution 1.2:0.6, Add the fragrance liquid obtained in step B to the gel liquid, stir and mix evenly to obtain the fragrance-releasing gel;
D、浸泡D. Soak
在室温下，将步骤A得到的混纺纤维粉在步骤B得到的香液中浸泡0.8小时，分离得到释香混纺纤维粉；At room temperature, soak the blended fiber powder obtained in step A in the fragrance liquid obtained in step B for 0.8 hours, and separate to obtain the fragrance-releasing blended fiber powder;
E、混配E. Mixing
在温度55℃的条件下，将步骤D得到的释香混纺纤维粉与步骤C得到的释香凝胶按照重量比1.6：0.4搅拌混合0.8小时，得到一种释香凝胶混纺纤维粉；At a temperature of 55°C, the fragrance-releasing blended fiber powder obtained in step D and the fragrance-releasing gel obtained in step C were stirred and mixed for 0.8 hours at a weight ratio of 1.6:0.4 to obtain a fragrance-releasing gel blended fiber powder;
F、成型F. Forming
在滤棒成型机上，在烟枪前端将醋纤丝束均匀铺展，将步骤E得到的释香凝胶混纺纤维粉通过水浴辊均匀涂抹在整个醋纤丝束展开面上，达到每毫米滤棒为1.5mg，经过烟枪成型，硬化，得到所述的释香凝胶混纺纤维滤棒。On the filter rod forming machine, the cellulose acetate tow is evenly spread at the front end of the bong, and the fragrance-releasing gel blended fiber powder obtained in step E is evenly spread on the entire unfolded surface of the cellulose acetate tow by a water bath roller, reaching It is 1.5 mg, and is molded and hardened through a pipe to obtain the described fragrance-releasing gel blended fiber filter stick.
实施例8：制备本发明释香凝胶纤维滤棒Embodiment 8: Preparation of the fragrance-releasing gel fiber filter stick of the present invention
该实施例的实施步骤如下：The implementation steps of this embodiment are as follows:
A、混纺纤维粉制备A. Preparation of blended fiber powder
将混纺纤维线经过压切为1.0cm的线段、粉碎、筛分，收集纤维尺寸为1.2mm的线段，除去杂质，得到混纺纤维粉；The blended fiber thread is cut into a 1.0 cm line segment, pulverized, and sieved, and the line segment with a fiber size of 1.2 mm is collected, and impurities are removed to obtain a blended fiber powder;
B、香液制备B. Fragrance preparation
使用纯净水或辛癸酸甘油酯溶剂与陈皮香料、猕猴桃香料、竹叶香料或桂花香料配制得到一种浓度为以重量计18％的香液；Purified water or caprylic glyceride solvent is used to prepare a fragrance liquid with a concentration of 18% by weight;
C、释香凝胶制备C. Preparation of fragrance-releasing gel
让卡拉胶、聚乙二醇、海藻酸钠、琼脂与水按照重量比1.2：5：0.2：0.1混合配制得到一种凝胶液，然后按照凝胶液与香液的重量比1.0：0.5，往所述凝胶液中添加在步骤B得到的香液，搅拌混合均匀，得到所述的释香凝胶；Mix carrageenan, polyethylene glycol, sodium alginate, agar and water according to the weight ratio of 1.2:5:0.2:0.1 to prepare a gel solution, and then according to the weight ratio of gel solution and perfume solution 1.0:0.5, Add the fragrance liquid obtained in step B to the gel liquid, stir and mix evenly to obtain the fragrance-releasing gel;
D、浸泡D. Soak
在室温下，将步骤A得到的混纺纤维粉在步骤B得到的香液中浸泡1.0小时，分离得到释香混纺纤维粉；At room temperature, soak the blended fiber powder obtained in step A in the fragrance liquid obtained in step B for 1.0 hour, and separate to obtain the fragrance-releasing blended fiber powder;
E、混配E. Mixing
在温度50℃的条件下，将步骤D得到的释香混纺纤维粉与步骤C得到的释香凝胶按照重量比1.7：0.5搅拌混合0.8小时，得到一种释香凝胶混纺纤维粉；At a temperature of 50°C, the fragrance-releasing blended fiber powder obtained in step D and the fragrance-releasing gel obtained in step C were stirred and mixed for 0.8 hours at a weight ratio of 1.7:0.5 to obtain a fragrance-releasing gel blended fiber powder;
F、成型F. Forming
在滤棒成型机上，在烟枪前端将醋纤丝束均匀铺展，将步骤E得到的释香凝胶混纺纤维粉通过水浴辊均匀涂抹在整个醋纤丝束展开面上，达到每毫米滤棒为1.4mg，经过烟枪成型，硬化，得到所述的释香凝胶混纺纤维滤棒。On the filter rod forming machine, the cellulose acetate tow is evenly spread at the front end of the bong, and the fragrance-releasing gel blended fiber powder obtained in step E is evenly spread on the entire unfolded surface of the cellulose acetate tow by a water bath roller, reaching It is 1.4 mg, and is molded and hardened through a pipe to obtain the described fragrance-releasing gel blended fiber filter stick.
试验实施例1：卷烟样品对比评价Test Example 1: Comparative Evaluation of Cigarette Samples
现有技术加香滤棒对照样品制备如下：The prior art scented filter stick contrast sample is prepared as follows:
按照滤棒长度1.5mg/mm标准，广州香龙公司以商品名陈皮香精用辛癸酸甘油酯配制成浓度为以重量计15％的香液，采用混纺纤维线浸泡方式制得加释香线。然后添加到红塔山1956的滤棒中制得对照卷烟样品。According to the standard of 1.5 mg/mm filter rod length, Guangzhou Xianglong Co., Ltd. used capricin capric acid glyceride as the trade name to prepare a fragrance liquid with a concentration of 15% by weight, and made the added release fragrance thread by soaking the blended fiber thread . Then add it to the filter stick of Hongtashan 1956 to make the control cigarette sample.
本发明释香凝胶混纺纤维滤棒的制备：The preparation of the fragrance-releasing gel blended fiber filter stick of the present invention:
按照滤棒长度1.5mg/mm标准，将实施例1中制备释香凝胶混纺纤维滤棒进行四分切，取其中一段替换掉对照样品红塔山1956卷烟滤棒，这样每支卷烟的25mg/支。According to the filter stick length 1.5mg/mm standard, the fragrance-releasing gel blended fiber filter stick prepared in embodiment 1 is cut into quarters, and one of them is taken to replace the filter stick of the control sample Hongtashan 1956 cigarette, so that the 25mg/stick of each cigarette .
这些样品在恒温恒湿箱中在温度20℃与相对湿度60％的条件下平衡24h，然后每次间隔48h就按照GB 5606.4—2005《卷烟感官技术要求》的标准方法进行评吸，确定抽吸效果。评吸结果列于表1中。These samples were equilibrated for 24 hours in a constant temperature and humidity chamber under the conditions of a temperature of 20°C and a relative humidity of 60%, and then evaluated and smoked according to the standard method of GB 5606.4-2005 "Sensory Technical Requirements for Cigarettes" at an interval of 48 hours each time to determine the quality of the smoke. Effect. The evaluation results are listed in Table 1.
表1：试验样品的评吸结果Table 1: Evaluation results of test samples
表1评吸结果表明，与现有技术相比，本发明释香凝胶混纺纤维滤棒香气释放均匀，香味持续时间长，抽吸过程中能保持卷烟抽吸过程释香一致性，满足生产企业的技术要求和消费者的感官享受。The smoking evaluation results in Table 1 show that compared with the prior art, the fragrance-releasing gel blended fiber filter stick of the present invention releases fragrance evenly, and the fragrance lasts for a long time. The technical requirements of enterprises and the sensory enjoyment of consumers.
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