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CN106396519A - Thin-thickness graphite sheet manufacturing and extracting device - Google Patents

Thin-thickness graphite sheet manufacturing and extracting device Download PDF

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Publication number
CN106396519A
CN106396519A CN201610772759.0A CN201610772759A CN106396519A CN 106396519 A CN106396519 A CN 106396519A CN 201610772759 A CN201610772759 A CN 201610772759A CN 106396519 A CN106396519 A CN 106396519A
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CN
China
Prior art keywords
blade
graphite
main shaft
preparation vessel
lever arm
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Application number
CN201610772759.0A
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Chinese (zh)
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CN106396519B (en
Inventor
沈宇栋
徐胜利
董圆柱
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Wuxi Dongheng New Energy Technology Co Ltd
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Wuxi Dongheng New Energy Technology Co Ltd
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Priority to CN201610772759.0A priority Critical patent/CN106396519B/en
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    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B28/00Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B26/00Compositions of mortars, concrete or artificial stone, containing only organic binders, e.g. polymer or resin concrete

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Carbon And Carbon Compounds (AREA)

Abstract

The invention discloses a thin-thickness graphite sheet manufacturing and extracting device which comprises a preparation tank, wherein the preparation tank is of a circular tank structure; a thinning device comprises a main shaft and is arranged in the preparation tank, two movable arms are arranged for connecting the main shaft, are respectively hinged to the main shaft and relatively move, a blade is arranged at the end part of each of the movable arms, and a graphite dust outlet and a bonding agent outlet are formed in each of the blades; an absorbing device is arranged on each of the blades, a dust suction device is arranged on the inner side wall, close to the bottom part, of the preparation tank, and a heating layer is arranged at the bottom of the preparation tank. Compared with the prior art, the thin-thickness graphite material manufacturing and extracting device disclosed by the invention has the benefits that through the relative rotation of the two movable arms, the blades are driven to lay a graphite solution in the preparation tank, and the graphite solution is pressed downwards to obtain a thin-thickness graphite sheet; the absorbing devices can be extracted after the graphite sheet is formed, so that the graphite sheet is not damaged; the heating layer can accelerate the formation of the graphite solution.

Description

A kind of graphite material minimal thickness manchining feature device
Technical field
The present invention relates to a kind of material manufacturing apparatus, particularly a kind of graphite material minimal thickness manchining feature device, belong to New material preparation field.
Background technology
In recent years, flourish with scientific and technological, the service behaviour of electronic product is constantly elevated, and electronic product Size also less and less, and the raising of the operating rate with electronic product and efficiency, this also means that sending out of electronic product Heat is increasing, and therefore electronic product not only needs to be equipped with corresponding heat abstractor, it is also to be ensured that heat abstractor have excellent Heat-sinking capability, with time remove within electronic product electronic building brick work when produced heat energy, thereby ensure that electronics Product energy normal operation, and then the reliability enhanced product performance and the service life extending product.
In this regard, graphite flake (Graphite Sheet) is because having the low-density characteristic with respect to metal fin, and Have that high radiating/heat conduction, insulation be anticorrosive and the characteristic such as low thermal resistance, become at present to help electronic product to realize soon The preferred material of fast radiating/heat conduction.Graphite flake, except carrying out heat conduction along level, also vertically can carry out heat conduction, Particularly graphite flake be laminar structured, therefore more can be suitably used for the surface of any product, be beneficial to reach more preferably radiating/ The effect of heat conduction.
However, in the preparation process of traditional graphite flake, generally first acidification and company must be carried out to natural graphite flakes , to produce fluffy of graphite, then standing fluffy special time of graphite is to move back temperature taking-up for continuous high-temperature calcination.Afterwards, also Must be by fluffy for the graphite graphite flake being rolled into predetermined thickness, to complete the preparation of graphite flake.It should be noted that in single The preparation process of graphite flake, is only capable of obtaining a graphite flake, and such repeatable operation will take for substantial amounts of preparation time, and this will make stone The capacity efficiency of ink sheet cannot improve.
The preparation method of nano graphite flakes as a kind of in Patent No. 201310369027.3, is former with natural flake graphite Material, carries out to natural flake graphite aoxidizing intercalation processing using oxidant and intercalator, forms intercalation expansible graphite, using micro- Wave heating mode intercalation expansible graphite is carried out expanded, formed expanded graphite, thereafter, in organic solvent, using ultrasonic spoke Form nano graphite flakes according to stripping is carried out to expanded graphite;The inventive method is simple to operate, efficiency high, and safety is good, expands all Even;Its a diameter of 0.5~20 μm of prepared nano graphite flakes, thickness is 0.35~50nm, average thickness 35nm, peels off journey Degree is high, has roll-shaped, curling S-shaped, concavo-convex agglomerate shape different-shape, and heat conductivility is good, easily disperses in organic solvent.
A kind of and for example preparation method of graphite flake of Application No. 201410122837.3, including offer the first graphite flake, and And stick first and second release base material on first and second surface of the first graphite flake, then along the of the first graphite flake One side separates first and second release base material, and the first graphite flake is separated into second and third graphite flake in uniform thickness, The second graphite flake after compacting separates afterwards, and stick the 3rd release base material on the parting surface of the second graphite flake after compacting, So that along second side separation first and the 3rd release base material of the second graphite flake, and then it is equal that the second graphite flake is separated into thickness The the 4th and the 5th even graphite flake.When the preparation method of graphite flake proposed by the invention can reduce the preparation of conventional graphite piece Between, and also preparation flow can be simplified, reduces cost and minimizing are polluted.
Both the above preparation method all have impact on physical aspect and the chemical form of graphite flake crystal, the graphite prepared Deviation characteristically can be deposited.
Content of the invention
The technical problem to be solved in the invention is for above-mentioned the deficiencies in the prior art, and provides a kind of graphite material thin Thickness manchining feature device.
For solving above-mentioned technical problem, the technical solution used in the present invention is
A kind of graphite material minimal thickness manchining feature device, including preparation vessel, preparation vessel is circular groove structure, sets in described preparation vessel It is equipped with thinning apparatus, described thinning apparatus include main shaft, connect described main shaft and be provided with two lever arms, the activity described in two Arm is respectively hinged on main shaft, the lever arm described in two can relative motion, the end of described lever arm is provided with blade, described Graphite dust outlet and binding agent outlet are provided with blade, described main shaft is provided with hold-down devices;Arrange on described blade There is adsorbent equipment, described adsorbent equipment includes the many connecting rods through blade setting, and one end of connecting rod connects blade ground, another End connects lifting block;Described preparation vessel is provided with dust exhaust apparatus in the interior side wall of bottom, and the bottom of preparation vessel is provided with and adds Thermosphere.
As further preferred version, the blade on described two described lever arms can be connected with each other, described blade A long side be arc surface, the outlet of described graphite dust and binding agent outlet are located on arc surface, and blade rotates in preparation vessel Propulsion, its arc surface is the one side of propulsion.
As further preferred version, the section of described blade has gap apart from the side wall of preparation vessel.
As further preferred version, described lever arm is L-shaped structure, and its longer part connects main shaft, and it is relatively Short part connects blade.
As further preferred version, the width of described blade is the 1/5-1/10 of its length.
Beneficial effect
Compared with prior art, a kind of graphite material minimal thickness manchining feature device of the present invention, by the phase of two lever arms To rotation, drive blade that graphite solution is laid in preparation vessel, then pushed, obtain the graphite sheet of minimal thickness, absorption Device can be extracted after graphite sheet molding, does not damage graphite sheet, and zone of heating then can accelerate the one-tenth of graphite solution Type, specifically has advantages below:
1. rotating against of two blades can form rounded face, and graphite solution can be laid in preparation vessel, with pushing The graphite sheet that can be ultimately formed has thinner thickness, is easy to later stage cutting and specific occasion uses.
2. graphite dust outlet and binding agent outlet are arranged on blade, can be discharged while blade activity, Carry out increasing and decreasing injected volume according to the actual thickness of the graphite sheet being formed, be easy to control the thickness of the graphite sheet ultimately forming Degree.
3. adsorbent equipment utilizes connecting rod to pull blade bottom, forms negative pressure, thus convenient take out slim graphite sheet, keeps away Exempt from using other apparatuses, slim graphite sheet to be caused to damage.
4. dust exhaust apparatus can by unnecessary for the preparation vessel graphite dust being scattered cleaning it is ensured that molding graphite sheet light Damp degree and planarization.
Brief description
Fig. 1 is the structural representation of the present invention;
Fig. 2 is the structural representation of blade;
Wherein, 1- preparation vessel, 2- main shaft, 3- lever arm, 4- blade, 5- graphite dust exports, and 6- binding agent exports, and press-fits under 7- Put, 8- connecting rod, 9- lifting block, 10- dust exhaust apparatus.
Specific embodiment
Describe the preferred technical solution of the present invention below in conjunction with the accompanying drawings in detail.
As illustrated, a kind of graphite material minimal thickness manchining feature device of the present invention, including preparation vessel 1, preparation vessel 1 is Circular groove structure, is provided with thinning apparatus in described preparation vessel 1;
Described thinning apparatus include main shaft 2, and main shaft 2 is longitudinal rotary shaft, connect described main shaft 2 and are provided with two lever arms 3, Lever arm 3 described in two is respectively hinged on main shaft 2, and the lever arm 3 described in two can relative motion;
The end of described lever arm 3 is provided with blade 4, and described blade 4 is provided with graphite dust outlet 5 and binding agent outlet 6;
Adsorbent equipment is provided with described blade 4, described adsorbent equipment includes the many connecting rods 8 through blade 4 setting, connecting rod 8 One end connect blade 4 ground, the other end connect lifting block 9;
Described preparation vessel 1 is provided with dust exhaust apparatus 10 in the interior side wall of bottom, and the bottom of preparation vessel 1 is provided with zone of heating.
Hold-down devices 7 are provided with described main shaft 2, hold-down devices 7 can adjust the dynamics pushing and persistent period, push The pattern that device 7 is typically pushed using intermittence.
Blade 4 on described two described lever arms 3 can be connected with each other, and a long side of described blade 4 is arc surface, institute State graphite dust outlet 5 and binding agent outlet 6 is located on arc surface, blade 4 rotates propulsion in preparation vessel 1, and its arc surface is to push away The one side entered.
The section of described blade 4 has gap apart from the side wall of preparation vessel 1.
Described lever arm 3 is L-shaped structure, and its longer part connects main shaft 2, and its shorter part connects blade 4.
The width of described blade 4 is the 1/5-1/10 of its length.
The above, only the application preferably specific embodiment, but the protection domain of the application is not limited thereto, Any those familiar with the art in the technical scope that the application discloses, the change or replacement that can readily occur in, All should cover within the protection domain of the application.Therefore, the protection domain of the application should be with scope of the claims It is defined.

Claims (5)

1. a kind of graphite material minimal thickness manchining feature device it is characterised in that:Including preparation vessel(1), preparation vessel(1)For circular groove Structure, described preparation vessel(1)Inside it is provided with thinning apparatus, described thinning apparatus include main shaft(2), connect described main shaft(2)If It is equipped with two lever arms(3), lever arm described in two(3)It is respectively hinged at main shaft(2)On, lever arm described in two(3) Can relative motion, described lever arm(3)End be provided with blade(4), described blade(4)On be provided with graphite dust outlet (5)With binding agent outlet(6), described main shaft(2)On be provided with hold-down devices(7);Described blade(4)On be provided with absorption dress Put, described adsorbent equipment is included through blade(4)Many connecting rods of setting(8), connecting rod(8)One end connect blade(4)Ground, The other end connects lifting block(9);Described preparation vessel(1)It is provided with dust exhaust apparatus in the interior side wall of bottom(10), preparation vessel (1)Bottom be provided with zone of heating.
2. a kind of graphite material minimal thickness manchining feature device according to claim 1 it is characterised in that:Described two institutes State lever arm(3)On blade(4)Can be connected with each other, described blade(4)A long side be arc surface, described graphite dust goes out Mouthful(5)With binding agent outlet(6)On arc surface, blade(4)In preparation vessel(1)Rotation propulsion, its arc surface is propulsion Simultaneously.
3. a kind of graphite material minimal thickness manchining feature device according to claim 1 it is characterised in that:Described blade (4)Section apart from preparation vessel(1)Side wall there is gap.
4. a kind of graphite material minimal thickness manchining feature device according to claim 1 it is characterised in that:Described lever arm (3)For L-shaped structure, its longer part connection main shaft(2), its shorter part connection blade(4).
5. a kind of graphite material minimal thickness manchining feature device according to claim 1 it is characterised in that:Described blade (4)Width be its length 1/5-1/10.
CN201610772759.0A 2016-08-31 2016-08-31 A kind of graphite material thin thickness manchining feature device Active CN106396519B (en)

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20040131533A1 (en) * 2001-05-03 2004-07-08 Spacie Christopher John Extrusion of graphite bodies
CN102897747A (en) * 2012-10-24 2013-01-30 无锡东恒新能源材料有限公司 Carbon nanotube purification system
CN206033254U (en) * 2016-08-31 2017-03-22 无锡东恒新能源科技有限公司 Slim graphite material makes extraction element

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20040131533A1 (en) * 2001-05-03 2004-07-08 Spacie Christopher John Extrusion of graphite bodies
CN102897747A (en) * 2012-10-24 2013-01-30 无锡东恒新能源材料有限公司 Carbon nanotube purification system
CN206033254U (en) * 2016-08-31 2017-03-22 无锡东恒新能源科技有限公司 Slim graphite material makes extraction element

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