CN106319663A - Preparation method of pearl-healthcare enteromorpha prolifera regenerated fibers - Google Patents
Preparation method of pearl-healthcare enteromorpha prolifera regenerated fibers Download PDFInfo
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- CN106319663A CN106319663A CN201610690898.9A CN201610690898A CN106319663A CN 106319663 A CN106319663 A CN 106319663A CN 201610690898 A CN201610690898 A CN 201610690898A CN 106319663 A CN106319663 A CN 106319663A
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- entermorpha
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- regenerated fiber
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- 239000000835 fiber Substances 0.000 title claims abstract description 59
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- 241000196253 Ulva prolifera Species 0.000 title abstract 8
- 239000000243 solution Substances 0.000 claims abstract description 38
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 31
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 30
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 claims abstract description 24
- 239000011550 stock solution Substances 0.000 claims abstract description 23
- 239000000843 powder Substances 0.000 claims abstract description 21
- IAZDPXIOMUYVGZ-UHFFFAOYSA-N Dimethylsulphoxide Chemical compound CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 claims abstract description 18
- 238000009987 spinning Methods 0.000 claims abstract description 16
- 239000007822 coupling agent Substances 0.000 claims abstract description 7
- 239000002270 dispersing agent Substances 0.000 claims abstract description 7
- 238000002166 wet spinning Methods 0.000 claims abstract description 5
- 229920003043 Cellulose fiber Polymers 0.000 claims abstract description 3
- 230000000887 hydrating effect Effects 0.000 claims description 26
- 244000293323 Cosmos caudatus Species 0.000 claims description 20
- 235000005956 Cosmos caudatus Nutrition 0.000 claims description 20
- 239000005708 Sodium hypochlorite Substances 0.000 claims description 10
- SUKJFIGYRHOWBL-UHFFFAOYSA-N sodium hypochlorite Chemical compound [Na+].Cl[O-] SUKJFIGYRHOWBL-UHFFFAOYSA-N 0.000 claims description 10
- 230000036541 health Effects 0.000 claims description 9
- 239000007921 spray Substances 0.000 claims description 9
- 239000000203 mixture Substances 0.000 claims description 8
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 7
- 239000000194 fatty acid Substances 0.000 claims description 7
- 229930195729 fatty acid Natural products 0.000 claims description 7
- 150000004665 fatty acids Chemical class 0.000 claims description 7
- 238000010025 steaming Methods 0.000 claims description 5
- 239000007864 aqueous solution Substances 0.000 claims description 4
- 229920002678 cellulose Polymers 0.000 claims description 4
- 239000001913 cellulose Substances 0.000 claims description 4
- 230000007062 hydrolysis Effects 0.000 claims description 4
- 238000006460 hydrolysis reaction Methods 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 4
- 239000002245 particle Substances 0.000 claims description 4
- LFTLOKWAGJYHHR-UHFFFAOYSA-N N-methylmorpholine N-oxide Chemical group CN1(=O)CCOCC1 LFTLOKWAGJYHHR-UHFFFAOYSA-N 0.000 claims description 2
- 240000007594 Oryza sativa Species 0.000 claims 1
- 235000007164 Oryza sativa Nutrition 0.000 claims 1
- 235000009566 rice Nutrition 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 9
- 238000004061 bleaching Methods 0.000 abstract description 7
- 238000000034 method Methods 0.000 abstract description 7
- 230000008569 process Effects 0.000 abstract description 4
- 230000008929 regeneration Effects 0.000 abstract description 3
- 238000011069 regeneration method Methods 0.000 abstract description 3
- 239000004753 textile Substances 0.000 abstract description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 2
- 239000011049 pearl Substances 0.000 abstract 2
- 238000010411 cooking Methods 0.000 abstract 1
- 230000003301 hydrolyzing effect Effects 0.000 abstract 1
- 238000000465 moulding Methods 0.000 abstract 1
- 102000019197 Superoxide Dismutase Human genes 0.000 description 3
- 108010012715 Superoxide dismutase Proteins 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 238000001914 filtration Methods 0.000 description 3
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 3
- 229910052760 oxygen Inorganic materials 0.000 description 3
- 239000001301 oxygen Substances 0.000 description 3
- 239000004627 regenerated cellulose Substances 0.000 description 3
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- SJRJJKPEHAURKC-UHFFFAOYSA-N N-Methylmorpholine Chemical compound CN1CCOCC1 SJRJJKPEHAURKC-UHFFFAOYSA-N 0.000 description 2
- 239000002202 Polyethylene glycol Substances 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 150000002148 esters Chemical class 0.000 description 2
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 description 2
- 239000002105 nanoparticle Substances 0.000 description 2
- 229920001223 polyethylene glycol Polymers 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- 241000195493 Cryptophyta Species 0.000 description 1
- 150000001204 N-oxides Chemical group 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 238000013475 authorization Methods 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- LYCAIKOWRPUZTN-UHFFFAOYSA-N ethylene glycol Natural products OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 1
- -1 glycol ester Chemical class 0.000 description 1
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 1
- 238000002372 labelling Methods 0.000 description 1
- 239000004310 lactic acid Substances 0.000 description 1
- 235000014655 lactic acid Nutrition 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 239000002574 poison Substances 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 229920000151 polyglycol Polymers 0.000 description 1
- 239000010695 polyglycol Substances 0.000 description 1
- 230000002062 proliferating effect Effects 0.000 description 1
- 150000003254 radicals Chemical class 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000028327 secretion Effects 0.000 description 1
- 230000009759 skin aging Effects 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 238000009898 sodium hypochlorite bleaching Methods 0.000 description 1
- 238000007711 solidification Methods 0.000 description 1
- 230000008023 solidification Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 239000003643 water by type Substances 0.000 description 1
- 230000002087 whitening effect Effects 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F2/00—Monocomponent artificial filaments or the like of cellulose or cellulose derivatives; Manufacture thereof
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
Landscapes
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Textile Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Artificial Filaments (AREA)
Abstract
The invention discloses a preparation method of pearl-healthcare enteromorpha prolifera regenerated fibers, and relates to the technical field of textiles. The preparation method of pearl-healthcare enteromorpha prolifera regenerated fibers comprises the following steps: crushing and hydrolyzing enteromorpha prolifera; adding sodium hydroxide; cooking, adding ethanol, removing water, and bleaching to obtain enteromorpha prolifera regeneration fiber stock solution; then, adding dimethyl sulfoxide, N, N-dimethylformamide, pearl powder, a coupling agent and a dispersant to obtain enteromorpha prolifera regeneration cellulose fiber spinning solution; and finally, molding according to a wet-spinning process. The preparation method provided by the invention enables enteromorpha prolifera regenerated fibers to have healthcare effect of pearls, and solves the problem that the enteromorpha prolifera regenerated fibers does not have the healthcare effect.
Description
Technical field
The present invention relates to textile technology field, the preparation method of a kind of pearl health-care type Entermorpha regenerated fiber.
Background technology
From the beginning of 2008, large-scale Entermorpha disaster all can be broken out in annual June～surrounding waters, Qingdao in August, though Entermorpha
The most nontoxic, but prolific Entermorpha also can shielded from sunlight, affect the growth of seabed algae, dead Entermorpha also can consume sea
Oxygen in water, and its secretion chemical substance also other marine organisms can be adversely affected.So annual Entermorpha calamity
A large amount of manpower and materials will be spent to salvage Entermorpha when of evil outburst, the research on utilization for Entermorpha the most gradually increases.Invention is specially
Profit 201310496954.1(Authorization Notice No. CN103590124B) preparation method of Entermorpha regenerated celulose fibre, disclose one
The method planting the regenerated celulose fibre utilizing Entermorpha slurry to be raw material production, this method comprises the following steps: pulverized by Entermorpha
It is placed on hydrating solution in hydrating solution；Adding sodium hydroxide in hydrating solution, then steaming and decocting obtains mixed liquor A；To mixed liquor
A adds ethanol, then removes moisture removal, obtain Entermorpha pulp；In Entermorpha pulp, add sodium hypochlorite bleaching obtain Entermorpha regeneration
Fiber stock solution；In Entermorpha regenerated fiber stock solution, add dimethyl sulfoxide and N, N-dimethylformamide obtains Entermorpha regenerated fiber
Cellulose fiber spinning solution；Entermorpha regenerated celulose fibre spinning solution is sent into extruding spinning liquid thread in spray webbing equipment, then
Concentrate and solidification, and elongate under the effect of take-up force and thin down to as Entermorpha regenerated celulose fibre.
The fiber that this scheme obtains only has the characteristic of general fiber, and now with the raising day by day of living standard,
People more and more pay close attention to living environment, working environment and the health of self, the most more carry out the health-care effect of functional underwear
More focus on, if so the technology of preparing of Entermorpha regenerated fiber is made certain improvements so that it is increase health-care effect, be bound to non-
Often it is received by the market.
Summary of the invention
The present invention provides the preparation method of a kind of pearl health-care type Entermorpha regenerated fiber, and it can solve Entermorpha regenerated fiber
The problem without health-care effect.
In order to solve the problems referred to above, the technical solution adopted in the present invention is: this pearl health-care type Entermorpha regenerated fiber
Preparation method, comprise the steps:
Step 1: Entermorpha is pulverized and is placed in hydrating solution hydrolysis 60-420 minute；The volume of described hydrating solution is Entermorpha body
Long-pending 2-3 times, described hydrating solution is the aqueous solution of 4-methyhnorpholine-N-oxide and ethanol, 4-methyl in hydrating solution
The weight/mass percentage composition of methylmorpholine-N-oxide is 20%-30%, and the weight/mass percentage composition of ethanol is 2.5%-4.0%；
Step 2: add sodium hydroxide in hydrating solution, adds according to the amount adding 5-15g sodium hydroxide in 1L hydrating solution
Sodium hydroxide, obtains mixed liquor after the fatty acid that then steaming and decocting is removed in Entermorpha for 20-30 minute under 80-90 DEG C of temperature conditions
A；
Step 3: add ethanol in mixed liquor A, then remove moisture removal, obtain the Entermorpha pulp that content of cellulose is higher；
Step 4: add sodium hypochlorite in Entermorpha pulp and Entermorpha pulp is bleached to obtain Entermorpha regenerated fiber stock solution, according to 1L
The amount adding 0.25-0.4g sodium hypochlorite in Entermorpha pulp adds sodium hypochlorite, and in bleaching process, temperature conditions is 35-40 DEG C,
Bleaching time is 50-100 minute；
Step 5: add dimethyl sulfoxide and DMF, Entermorpha regenerated cellulose in Entermorpha regenerated fiber stock solution
In fiber spinning dope, the volume mass percentage concentration of dimethyl sulfoxide is 1-5ml/kg, the volume of N, N-dimethylformamide
Mass percentage concentration is 0.5-1.5ml/kg；Being additionally added Margarita powder, coupling agent and dispersant, the particle diameter of described Margarita powder is 50
Nanometer～200 nanometers, addition is that 100 weight portion Entermorpha regenerated fiber stock solutions add Margarita powder 2 weight portion～6 weight portions, institute
The addition stating coupling agent is that 100 weight portion Entermorpha regenerated fiber stock solutions add coupling agent 0.8 weight portion～2 weight portions, described
The addition of dispersant is that 100 weight portion Entermorpha regenerated fiber stock solutions add dispersant 5 weight portion～15 weight portions, mistake after mixing
Filter, obtains Margarita powder health Entermorpha regenerated celulose fibre spinning solution；
Step 6: Margarita powder health Entermorpha regenerated celulose fibre spinning solution is sent in spray webbing equipment, spray by wet spinning
Silk technological forming.
Owing to have employed technique scheme, the present invention compared with prior art has the advantages that
The pearl health-care type Entermorpha regenerated fiber of the present invention can all be uniformly distributed nanoparticle at fibrous inside and outer surface, for a long time
Pearl nano particle in contact skin, fiber and skin intimate contact, the lactic acid in perspiration can divide treasure by dissolution fiber middles
Pearl nutritional labeling, is absorbed by skin, promotes the activity of human skin superoxide dismutase (SOD), suppresses melanic
Synthesis keeps whitening skin Sydney；Additionally, due to SOD has the effect understanding free radical, skin aging can be prevented wrinkling, also may be used
Remove skin surface hot pox poison, there is speckle dispelling, except pox, maintenance skin, effect of anti-ultraviolet.
Detailed description of the invention
Below in conjunction with specific embodiment, the invention will be further described:
Embodiment one:
The preparation method of a kind of pearl health-care type Entermorpha regenerated fiber, comprises the steps:
Step 1: Entermorpha is pulverized and is placed in hydrating solution hydrolysis 60 minutes；The volume of described hydrating solution is Entermorpha volume
2 times, described hydrating solution is the aqueous solution of 4-methyhnorpholine-N-oxide and ethanol, 4-methyl morpholine-N-in hydrating solution
The weight/mass percentage composition of oxide is 20%, and the weight/mass percentage composition of ethanol is 2.5%；
Step 2: add sodium hydroxide in hydrating solution, adds hydrogen-oxygen according to the amount adding 5g sodium hydroxide in 1L hydrating solution
Change sodium, after the fatty acid that then steaming and decocting is removed in Entermorpha for 30 minutes under 80 DEG C of temperature conditionss, obtain mixed liquor A；
Step 3: add ethanol in mixed liquor A, then remove moisture removal, obtain the Entermorpha pulp that content of cellulose is higher；
Step 4: add sodium hypochlorite in Entermorpha pulp and Entermorpha pulp is bleached to obtain Entermorpha regenerated fiber stock solution, according to 1L
The amount adding 0.4g sodium hypochlorite in Entermorpha pulp adds sodium hypochlorite, and in bleaching process, temperature conditions is 40 DEG C, bleaching time
It it is 100 minutes；
Step 5: add dimethyl sulfoxide and DMF, Entermorpha regenerated cellulose in Entermorpha regenerated fiber stock solution
In fiber spinning dope, the volume mass percentage concentration of dimethyl sulfoxide is 1-5ml/kg, the volume of N, N-dimethylformamide
Mass percentage concentration is 0.5-1.5ml/kg；It is additionally added Margarita powder, HK-540 and fatty acid polyethylene glycol ester, described Margarita powder
Particle diameter be 50 nanometers～200 nanometers, addition be 100 weight portion Entermorpha regenerated fiber stock solutions add Margarita powder 2 weight portions, institute
The addition stating HK-540 is that 100 weight portion Entermorpha regenerated fiber stock solutions add HK-540 0.8 weight portion, described fatty acid polyglycol
The addition of glycol ester is that 100 weight portion Entermorpha regenerated fiber stock solutions add fatty acid polyethylene glycol ester 5 weight portion, after mixing
Filtering, wherein filtering accuracy is≤50 μm, obtains Margarita powder health Entermorpha regenerated celulose fibre spinning solution；
Step 6: Margarita powder health Entermorpha regenerated celulose fibre spinning solution is sent in spray webbing equipment, spray by wet spinning
Silk technological forming.
Embodiment two:
The preparation method of a kind of pearl health-care type Entermorpha regenerated fiber, comprises the steps:
Step 1: Entermorpha is pulverized and is placed in hydrating solution hydrolysis 420 minutes；The volume of described hydrating solution is Entermorpha volume
3 times, described hydrating solution is the aqueous solution of 4-methyhnorpholine-N-oxide and ethanol, 4-methyl morpholine in hydrating solution-
The weight/mass percentage composition of N-oxide is 30%, and the weight/mass percentage composition of ethanol is 4.0%；
Step 2: add sodium hydroxide in hydrating solution, adds hydrogen-oxygen according to the amount adding 5g sodium hydroxide in 1L hydrating solution
Change sodium, after the fatty acid that then steaming and decocting is removed in Entermorpha for 20 minutes under 80 DEG C of temperature conditionss, obtain mixed liquor A；
Step 3: add ethanol in mixed liquor A, then remove moisture removal, obtain the Entermorpha pulp that content of cellulose is higher；
Step 4: add sodium hypochlorite in Entermorpha pulp and Entermorpha pulp is bleached to obtain Entermorpha regenerated fiber stock solution, according to 1L
The amount adding 0.25g sodium hypochlorite in Entermorpha pulp adds sodium hypochlorite, and in bleaching process, temperature conditions is 35 DEG C, bleaching time
It it is 50 minutes；
Step 5: add dimethyl sulfoxide and DMF, Entermorpha regenerated cellulose in Entermorpha regenerated fiber stock solution
In fiber spinning dope, the volume mass percentage concentration of dimethyl sulfoxide is 1-5ml/kg, the volume of N, N-dimethylformamide
Mass percentage concentration is 0.5-1.5ml/kg；Being additionally added Margarita powder, A-171 and methyl anyl alcohol, the particle diameter of described Margarita powder is 50
Nanometer～200 nanometers, addition is that 100 weight portion Entermorpha regenerated fiber stock solutions add Margarita powder 6 weight portion, described A-171's
Addition is that 100 weight portion Entermorpha regenerated fiber stock solutions add A-171 2 weight portion, and the addition of described methyl anyl alcohol is 100
Weight portion Entermorpha regenerated fiber stock solution adds methyl anyl alcohol 15 weight portion, filters after mixing, and wherein filtering accuracy is≤50 μm,
To Margarita powder health Entermorpha regenerated celulose fibre spinning solution；
Step 6: Margarita powder health Entermorpha regenerated celulose fibre spinning solution is sent in spray webbing equipment, spray by wet spinning
Silk technological forming.
Claims (1)
1. a preparation method for pearl health-care type Entermorpha regenerated fiber, comprises the steps:
Step 1: Entermorpha is pulverized and is placed in hydrating solution hydrolysis 60-420 minute；The volume of described hydrating solution is Entermorpha body
Long-pending 2-3 times, described hydrating solution is the aqueous solution of 4-methyhnorpholine-N-oxide and ethanol, 4-methyl in hydrating solution
The weight/mass percentage composition of methylmorpholine-N-oxide is 20%-30%, and the weight/mass percentage composition of ethanol is 2.5%-4.0%；
Step 2: add sodium hydroxide in hydrating solution, obtains mixed liquor A after the fatty acid during then Entermorpha is removed in steaming and decocting；
Step 3: add ethanol in mixed liquor A, then remove moisture removal, obtain the Entermorpha pulp that content of cellulose is higher；
Step 4: add sodium hypochlorite in Entermorpha pulp and Entermorpha pulp is bleached to obtain Entermorpha regenerated fiber stock solution；
Step 5: add dimethyl sulfoxide in Entermorpha regenerated fiber stock solution and N,N-dimethylformamide obtains Entermorpha regenerated fiber
Cellulose fiber spinning solution；
It is characterized in that:
In described step 5, being additionally added Margarita powder, coupling agent and dispersant, the particle diameter of described Margarita powder is that 50 nanometers～200 are received
Rice, addition is that 100 weight portion Entermorpha regenerated fiber stock solutions add Margarita powder 2 weight portion～6 weight portions, adding of described coupling agent
Entering amount is that 100 weight portion Entermorpha regenerated fiber stock solutions add coupling agent 0.8 weight portion～2 weight portions, the addition of described dispersant
Amount is that 100 weight portion Entermorpha regenerated fiber stock solutions add dispersant 5 weight portion～15 weight portions, filters, obtain Margarita after mixing
Powder health Entermorpha regenerated celulose fibre spinning solution；
Step 6: Margarita powder health Entermorpha regenerated celulose fibre spinning solution is sent in spray webbing equipment, spray by wet spinning
Silk technological forming.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610690898.9A CN106319663A (en) | 2016-08-20 | 2016-08-20 | Preparation method of pearl-healthcare enteromorpha prolifera regenerated fibers |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610690898.9A CN106319663A (en) | 2016-08-20 | 2016-08-20 | Preparation method of pearl-healthcare enteromorpha prolifera regenerated fibers |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106319663A true CN106319663A (en) | 2017-01-11 |
Family
ID=57743680
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610690898.9A Pending CN106319663A (en) | 2016-08-20 | 2016-08-20 | Preparation method of pearl-healthcare enteromorpha prolifera regenerated fibers |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107868988A (en) * | 2017-11-15 | 2018-04-03 | 金剑梅 | A kind of preparation method of the silk fiber of high health properties |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1772980A (en) * | 2004-11-10 | 2006-05-17 | 上海新型纺纱技术开发中心 | Pearl viscose rayon and producing method thereof |
| CN103060938A (en) * | 2012-11-26 | 2013-04-24 | 浙江理工大学 | Method for manufacturing functional viscose fibers |
| CN103590124B (en) * | 2012-12-27 | 2015-07-15 | 青岛海芬海洋生物科技有限公司 | Preparation method of enteromorpha regenerated cellulose fibers |
-
2016
- 2016-08-20 CN CN201610690898.9A patent/CN106319663A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1772980A (en) * | 2004-11-10 | 2006-05-17 | 上海新型纺纱技术开发中心 | Pearl viscose rayon and producing method thereof |
| CN103060938A (en) * | 2012-11-26 | 2013-04-24 | 浙江理工大学 | Method for manufacturing functional viscose fibers |
| CN103590124B (en) * | 2012-12-27 | 2015-07-15 | 青岛海芬海洋生物科技有限公司 | Preparation method of enteromorpha regenerated cellulose fibers |
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| Title |
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| 郑伟等: "《新型护肤纤维及其纺织品的发展动向》", 《第七届功能性纺织品及纳米技术研讨会论文集》 * |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107868988A (en) * | 2017-11-15 | 2018-04-03 | 金剑梅 | A kind of preparation method of the silk fiber of high health properties |
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