CN106280650A - Reflective insulation ancient painted pottery rock coating and preparation method thereof - Google Patents
Reflective insulation ancient painted pottery rock coating and preparation method thereof Download PDFInfo
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- CN106280650A CN106280650A CN201610651515.7A CN201610651515A CN106280650A CN 106280650 A CN106280650 A CN 106280650A CN 201610651515 A CN201610651515 A CN 201610651515A CN 106280650 A CN106280650 A CN 106280650A
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- 238000009413 insulation Methods 0.000 title claims abstract description 92
- 238000000576 coating method Methods 0.000 title claims abstract description 38
- 239000011248 coating agent Substances 0.000 title claims abstract description 37
- 239000011435 rock Substances 0.000 title claims abstract description 30
- 238000002360 preparation method Methods 0.000 title claims abstract description 17
- 239000004576 sand Substances 0.000 claims abstract description 33
- 239000000080 wetting agent Substances 0.000 claims abstract description 22
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 15
- 239000000839 emulsion Substances 0.000 claims abstract description 14
- 239000013530 defoamer Substances 0.000 claims abstract description 12
- 239000002562 thickening agent Substances 0.000 claims abstract description 11
- 239000001913 cellulose Substances 0.000 claims abstract description 10
- 229920002678 cellulose Polymers 0.000 claims abstract description 10
- 239000008367 deionised water Substances 0.000 claims abstract description 8
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 8
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 50
- 238000003756 stirring Methods 0.000 claims description 23
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 22
- 239000000843 powder Substances 0.000 claims description 16
- 239000006004 Quartz sand Substances 0.000 claims description 15
- 239000011347 resin Substances 0.000 claims description 15
- 229920005989 resin Polymers 0.000 claims description 15
- 235000010215 titanium dioxide Nutrition 0.000 claims description 15
- 239000012752 auxiliary agent Substances 0.000 claims description 14
- 239000000853 adhesive Substances 0.000 claims description 11
- 230000001070 adhesive effect Effects 0.000 claims description 11
- 239000002002 slurry Substances 0.000 claims description 11
- 239000004408 titanium dioxide Substances 0.000 claims description 7
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 5
- -1 polyoxy Polymers 0.000 claims description 5
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 claims description 4
- 238000001035 drying Methods 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 4
- 229910052799 carbon Inorganic materials 0.000 claims description 3
- 239000008187 granular material Substances 0.000 claims description 3
- 229910021389 graphene Inorganic materials 0.000 claims description 3
- 239000002245 particle Substances 0.000 claims description 3
- 229920001479 Hydroxyethyl methyl cellulose Polymers 0.000 claims description 2
- 241000047703 Nonion Species 0.000 claims description 2
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims description 2
- 239000002253 acid Substances 0.000 claims description 2
- 239000000443 aerosol Chemical class 0.000 claims description 2
- 125000000217 alkyl group Chemical group 0.000 claims description 2
- 239000004202 carbamide Substances 0.000 claims description 2
- 150000001875 compounds Chemical class 0.000 claims description 2
- 229920002635 polyurethane Polymers 0.000 claims description 2
- 239000004814 polyurethane Substances 0.000 claims description 2
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 claims description 2
- 239000004094 surface-active agent Substances 0.000 claims description 2
- 150000001336 alkenes Chemical class 0.000 claims 1
- 150000001734 carboxylic acid salts Chemical class 0.000 claims 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims 1
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 claims 1
- 230000000149 penetrating effect Effects 0.000 claims 1
- 239000002994 raw material Substances 0.000 abstract description 13
- 239000003973 paint Substances 0.000 abstract description 9
- 238000010276 construction Methods 0.000 abstract description 3
- 230000035515 penetration Effects 0.000 abstract description 3
- 239000000049 pigment Substances 0.000 abstract description 3
- 230000002159 abnormal effect Effects 0.000 abstract description 2
- 230000007613 environmental effect Effects 0.000 abstract description 2
- 238000011031 large-scale manufacturing process Methods 0.000 abstract description 2
- 230000035943 smell Effects 0.000 abstract description 2
- 239000007921 spray Substances 0.000 abstract description 2
- 230000000694 effects Effects 0.000 description 8
- 239000006185 dispersion Substances 0.000 description 6
- 238000005299 abrasion Methods 0.000 description 2
- 229910052681 coesite Inorganic materials 0.000 description 2
- 238000004040 coloring Methods 0.000 description 2
- 229910052906 cristobalite Inorganic materials 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000377 silicon dioxide Substances 0.000 description 2
- 235000012239 silicon dioxide Nutrition 0.000 description 2
- 229910052682 stishovite Inorganic materials 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 229910052905 tridymite Inorganic materials 0.000 description 2
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 1
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 1
- 229920003171 Poly (ethylene oxide) Polymers 0.000 description 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 150000001414 amino alcohols Chemical class 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000033228 biological regulation Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 150000007942 carboxylates Chemical class 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000005253 cladding Methods 0.000 description 1
- 238000005034 decoration Methods 0.000 description 1
- 238000002242 deionisation method Methods 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 239000012767 functional filler Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000003906 humectant Substances 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 229910044991 metal oxide Inorganic materials 0.000 description 1
- 150000004706 metal oxides Chemical class 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 238000005065 mining Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000010422 painting Methods 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 238000012216 screening Methods 0.000 description 1
- 238000010334 sieve classification Methods 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 238000003892 spreading Methods 0.000 description 1
- 239000004575 stone Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/004—Reflecting paints; Signal paints
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
- C09D133/04—Homopolymers or copolymers of esters
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Paints Or Removers (AREA)
- Application Of Or Painting With Fluid Materials (AREA)
Abstract
The invention discloses a kind of reflective insulation ancient painted pottery rock coating, component including following parts by weight: deionized water 83~100 parts, wetting agent 1~2 parts, cellulose 1~3 parts, PH regulator 1~1.5 parts, defoamer 1~1.5 parts, coalescents 10~15 parts, thickening agent 1~2 parts, emulsion 18~20 parts, reflective insulation sand 70~75 parts.The invention also discloses the preparation method of described reflective insulation ancient painted pottery rock coating.The reflective insulation ancient painted pottery rock coating of the present invention has the advantage that (1) uses complete aqueous, environmental protection raw material, and VOC < 0.5%, and abnormal smells from the patient is pure and fresh;(2) gained pigment coloration is stable, quality is good, and service life is long, flexible does not ftractures, weather-proof alkaline-resisting colour-fast, prevents water penetration;(3) easy construction flexibly, low cost, can spray, batch be coated with metope.The reflective heat-insulation paint preparation method of the present invention is simple, it is easy to large-scale production.
Description
Technical field
The invention belongs to technical field of coatings, particularly relate to the reflective insulation coloured silk of a kind of energy-saving and emission-reduction, the thickest slurry property
Tao Yan coating and preparation method thereof.
Background technology
Reflective heat-insulation paint is a kind of novel energy-saving construction coating for external wall, by have weather resisteant, colour retention,
The excellent water soluble acrylic acid elastic emulsion of adhesive force and stain resistance as main film forming substance, special titanium dioxide of simultaneously arranging in pairs or groups
With functional filler, including infrared pigment, hollow glass powder, metal-oxide, synthesis oil-in-water type hollow powder etc., and it is aided with other
Auxiliary agent is formulated.It makes use of and reflect near infrared principle to greatest extent, final realize to sunlight nearly 65% reflection,
Radiation and scattering, thus reach the effect of heat-insulation and heat-preservation, but this reflective heat-insulation paint coating is thin, and effect of heat insulation is inconspicuous,
Anti-wall crazing weak effect, decorative effect does not has that sand textured coating is luxurious texture.It addition, the reflective insulation sand wall paint on market
Purely rely on a small amount of functional raw material of interpolation to play the effect of reflective insulation, the most not only make gained coating lose roughing sand
Textured coating elegance texture, and have that reflection efficiency is low, paint film texture effect fuzzy, color is simple-minded, have no stereovision etc.
Defect.
Summary of the invention
Goal of the invention: the defect existed for existing reflective heat-insulation paint, the invention provides a kind of energy-saving and emission-reduction, efficiently
Reflective insulation ancient painted pottery rock coating of thick slurry property and preparation method thereof.
Technical scheme: the reflective insulation ancient painted pottery rock coating of the present invention, including the component of following parts by weight: deionized water 83
~100 parts, wetting agent 1~2 parts, cellulose 1~3 parts, PH regulator 1~1.5 parts, defoamer 1~1.5 parts, coalescents 10
~15 parts, thickening agent 1~2 parts, emulsion 18~20 parts, reflective insulation sand 70~75 parts.
Preferably, described wetting agent is alkyl polyoxyethylene carboxylate.
Described cellulose preferably less than viscosity methyl hydroxyethylcellulose.
The described preferred amino alcohol of PH regulator.
The preferred organic silicon defoamer of described defoamer.
The preferred alcohol ester of described coalescents 12.
The preferred pure-acrylic emulsion of described emulsion.
Described thickening agent preferably contracting urea polyurethane.
Further, described reflective insulation sand comprises the component of following parts by weight: quartz sand 83~90 parts, resin 8~
15 parts, non-ionic wetting agent 0.1~0.15 part, toner 1~1.5 parts, reflective insulation titanium white 1~2 parts, 1 part of reflective insulation powder, attached
Put forth effort auxiliary agent 0.2 part.
Wherein, described quartz sand preferred SiO2 content is the quartz sand of more than 96%.Thus can ensure that Si content, ability
Appropriateness abrasion, it is ensured that stablizing of color.If selecting the SiO2 content quartz sand less than 96%, then difference of wearing and tearing so that cladding face
Color is shallow, affects the texture of finished product.
Described resin preferred organosilicon hydroxy acryl acid resin.
Described non-ionic wetting agent preferred non-ion fluorin carbon surface active agent.
The preferred inorganic toner of described toner.
Described reflective insulation titanium dioxide then selects reflective insulation titanium white model by different lightness.
Described heat-insulating powder selects Graphene and aerosol to compound.It is further preferred that described Graphene and aerocolloidal heavy
Amount ratio is 1:30-50, more preferably 1:40.
The preferably single pyridine of described adhesive force auxiliary agent.
The preparation method of the reflective insulation ancient painted pottery rock coating of the present invention, comprises the steps:
(1) slurry is prepared:
First by deionized water and the wetting agent mixing of formula ratio, stir evenly;It is subsequently adding the cellulose thickener of formula ratio, stirs
Even;Continuously add the PH regulator of formula ratio, be ground to without granule after stirring evenly;Continue to put into the defoamer of formula ratio, film forming helps
Agent, stirs evenly;Continue to put into emulsion, stir evenly to obtain slurry;
(2) reflective insulation ancient painted pottery rock coating is prepared:
The reflective insulation sand of formula ratio is put in step (1) gained slurry, stirs evenly and get product.
Preferably, the preparation method of step (2) described reflective insulation sand is: first by resin and the nonionic profit of formula ratio
Humectant mixing stirs evenly, and adds the toner of formula ratio, is milled to fineness≤25 μm after stirring evenly;It is subsequently added the reflective insulation of formula ratio
Powder and reflective insulation titanium white, add adhesive force auxiliary agent and the quartz sand of formula ratio, stir evenly, drying reflective insulation after stirring evenly
Sand;Choose the reflective insulation sand that particle diameter is 10-180 mesh stand-by;The formula of wherein said reflective insulation sand comprises following weight
The component of number: quartz sand 83~90 parts, resin 8~15 parts, non-ionic wetting agent 0.1~0.15 part, toner 1~1.5 parts, instead
Penetrate heat insulation titanium white 1~2 parts, 1 part of reflective insulation powder, adhesive force auxiliary agent 0.2 part.
It is further preferred that described reflective insulation sand grains footpath is 60-80 mesh, preferably 70 mesh.
The preparation method of reflective insulation ancient painted pottery rock coating of the present invention is to be contaminated by quartz sand by moistening, coloring, low-temperature setting
Color becomes to have reflective insulation function natural colour sand shape, then is re-dubbed ancient painted pottery rock coating, integral production technique ratio with reflective insulation sand
Relatively innovating so that quality of colour is more stable, can form the style of single color or colorful different graphic, decorative pattern color reproducibility is good,
Weather-proof do not fade, the most true to nature.The present invention prepares gained reflective insulation ancient painted pottery rock coating and can be applicable to the special of various inner-outer wall
Decoration, has the luxurious effect of plane, hair side stone material.
Beneficial effect: be compared to reflective heat-insulation paint of the prior art, the reflective insulation ancient painted pottery rock coating of the present invention
Having the advantage that (1) uses complete aqueous, environmental protection raw material, and VOC < 0.5%, abnormal smells from the patient is pure and fresh;(2) gained coating
Coloring stabilized, quality is good, service life is long, flexible does not ftractures, weather-proof alkaline-resisting colour-fast, prevents water penetration;(3) easy construction spirit
Alive, low cost, can spray, criticize painting metope.The reflective heat-insulation paint preparation method of the present invention is simple, it is easy to large-scale production.
Detailed description of the invention
Raw material sources:
Defoamer is from Henkel KGaA company;
Resin is from Wa Ke company of the U.S.;
Toner is from Sol company of the U.S.;
Reflective insulation titanium dioxide is from Heng Shi Man of Britain;
Reflective insulation powder is from Minnesota Mining and Manufacturing Company;
Remaining raw material, auxiliary agent are purchased from You Chang chemical company of China.
Embodiment 1
In the present embodiment, reflective insulation ancient painted pottery rock coating comprises the raw material of following weight portion:
Deionized water 90 parts, wetting agent 1.5 parts, cellulose 2 parts, PH regulator 1 part, defoamer 1 part, coalescents 12
Part, thickening agent 1 part, emulsion 19 parts, 72 parts of reflective insulation sand.
Wherein, reflective insulation sand used comprises following raw material: resin 10 parts, non-ionic wetting agent 0.1 part, toner
1.2 parts, reflective insulation titanium white 1.5 parts, heat-insulating powder 1 part, adhesive force auxiliary agent 0.2 part, quartz sand 85 parts.
In the present embodiment, the preparation method of reflective insulation ancient painted pottery rock coating comprises the following steps:
(1) reflective insulation sand is prepared:
The raw material of required corresponding number is taken according to the formula of reflective insulation sand in the present embodiment;First by resin and non-from
Sub-wetting agent joins in container, stirs evenly 5-10min under the rotating speed of 50-100 rev/min;Then agitation limit in limit adds toner, and
Regulation speed of agitator is 1000-1200 rev/min, after stirring evenly 5-10min, enters sand mill dispersion and is milled to fineness≤25um;With
Rear addition reflective insulation powder and reflective insulation titanium white, high speed dispersion 20min under the rotating speed of 1000-1200 rev/min;Finally add
Adhesive force auxiliary agent and quartz sand, dry 30min under the conditions of 150 DEG C and i.e. obtain reflective insulation sand after stirring;Use reciprocating sieve classification
Screening particle diameter is that the reflective insulation sand of 10-180 mesh is stand-by.
(2) slurry is prepared: take the raw material of required corresponding number according to the present embodiment invention Formulations Formula;First by deionization
Water and wetting agent add in container, disperse 2-3min, until being completely dissolved under the rotating speed of 600-800 rev/min;It is subsequently adding fibre
Dimension element thickening agent, under 1000-1200 rev/min of rotating speed, stirs evenly 5-10min;Continuously add PH regulator, 1000-1200 turn/
High speed dispersion 10-20min under the rotating speed divided, is ground to without granule;Input defoamer, coalescents, 500-600 rev/min, low speed
Dispersion 5-10min;Putting into emulsion, 500-600 rev/min, low speed dispersion 5-10min i.e. obtains slurry.
(3) by formula ratio, step (1) is prepared gained reflective insulation sand and put in step (2) gained slurry, at 500-600
Rev/min rotating speed under, low speed dispersion 10-15min get product.
Embodiment 2
In the present embodiment, reflective insulation ancient painted pottery rock coating comprises the raw material of following weight portion:
Deionized water 83 parts, wetting agent 1 part, cellulose 1 part, PH regulator 1 part, defoamer 1 part, coalescents 10 parts,
Thickening agent 1 part, emulsion 18 parts, 70 parts of reflective insulation sand.
Wherein, reflective insulation sand used comprises following raw material:
Quartz sand 83 parts, resin 8 parts, non-ionic wetting agent 0.1 part, toner 1 part, reflective insulation titanium dioxide 1 part, reflect every
1 part of hot powder, adhesive force auxiliary agent 0.2 part.
In the present embodiment, the preparation method of reflective insulation ancient painted pottery rock coating is with embodiment 1, except the weight portion of component is different.
Embodiment 3
In the present embodiment, reflective insulation ancient painted pottery rock coating comprises the raw material of following weight portion:
Deionized water 100 parts, wetting agent 2 parts, cellulose 3 parts, PH regulator 1.5 parts, defoamer 1.5 parts, coalescents
15 parts, thickening agent 2 parts, emulsion 20 parts, 75 parts of reflective insulation sand.
Wherein, reflective insulation sand used comprises following raw material:
Quartz sand 90 parts, resin 15 parts, non-ionic wetting agent 0.15 part, toner 1.5 parts, reflective insulation titanium dioxide 2 parts, instead
Penetrate heat-insulating powder 1 part, adhesive force auxiliary agent 0.2 part.
In the present embodiment, the preparation method of reflective insulation ancient painted pottery rock coating is with embodiment 1, except the weight portion of component is different.
Performance test
The coating of Example 1 preparation carries out technology for detection, and result is as follows:
1. appearance of film: hard to tell whether it is true or false with lithotome effect.
2. drying time: surface drying < 2h.
3. spreading area: 1.8~2kg/ square metre.
4. artificial ageing resistance: 1000h is unchanged.
5. resistance to water: 120h is unchanged.
6. alkali resistance: 120h is unchanged.
7. abrasion resistance: 10000 times, without damaged.
8. reflective insulation index, is detected by JG/T235-2014 " architectural reflective heat-insulation paint ", result such as following table.
From test result, the reflective insulation ancient painted pottery rock pigment coloration of the present invention is stable, quality is good, and service life is long,
Flexible do not ftracture, weather-proof alkaline-resisting colour-fast, and prevent water penetration.
Claims (9)
1. a reflective insulation ancient painted pottery rock coating, it is characterised in that include the component of following parts by weight: deionized water 83~100
Part, wetting agent 1~2 parts, cellulose 1~3 parts, PH regulator 1~1.5 parts, defoamer 1~1.5 parts, coalescents 10~15
Part, thickening agent 1~2 parts, emulsion 18~20 parts, reflective insulation sand 70~75 parts.
Reflective insulation ancient painted pottery rock coating the most according to claim 1, it is characterised in that: described wetting agent is alkyl polyoxy second
Olefinic carboxylic acid salt;Described cellulose is low viscosity methyl hydroxyethylcellulose;Described emulsion is pure-acrylic emulsion;Described thickening agent is contracting
Urea polyurethane;Described coalescents is alcohol ester 12.
Reflective insulation ancient painted pottery rock coating the most according to claim 1, it is characterised in that: described reflective insulation sand comprises as follows
The component of parts by weight: quartz sand 83~90 parts, resin 8~15 parts, non-ionic wetting agent 0.1~0.15 part, toner 1~1.5
Part, reflective insulation titanium dioxide 1~2 parts, 1 part of reflective insulation powder, adhesive force auxiliary agent 0.2 part.
Reflective insulation ancient painted pottery rock coating the most according to claim 3, it is characterised in that: SiO in described quartz sand2Content is
More than 96%.
Reflective insulation ancient painted pottery rock coating the most according to claim 3, it is characterised in that: described resin is organosilicon hydroxyl third
Olefin(e) acid resin;Described non-ionic wetting agent is non-ion fluorin carbon surface active agent;Described toner is for selecting inorganic toner;Described attachment
Power auxiliary agent is menu pyridine.
Reflective insulation ancient painted pottery rock coating the most according to claim 3, it is characterised in that: described reflective insulation titanium dioxide needs to press
Require to select model according to different lightness.
Reflective insulation ancient painted pottery rock coating the most according to claim 3, it is characterised in that: described reflective insulation powder be Graphene and
Aerosol compounds with the weight ratio of 1:30-50 and forms.
8. the preparation method of arbitrary described reflective insulation ancient painted pottery rock coating in claim 1-7, it is characterised in that include walking as follows
Rapid:
(1) slurry is prepared:
First by deionized water and the wetting agent mixing of formula ratio, stir evenly;It is subsequently adding the cellulose thickener of formula ratio, stirs evenly;
Continuously add the PH regulator of formula ratio, be ground to without granule after stirring evenly;Continue to put into the defoamer of formula ratio, coalescents,
Stir evenly;Continue to put into emulsion, stir evenly to obtain slurry;
(2) reflective insulation ancient painted pottery rock coating is prepared:
The reflective insulation sand of formula ratio is put in step (1) gained slurry, stirs evenly and get product.
The preparation method of reflective insulation ancient painted pottery rock coating the most according to claim 8, it is characterised in that: step (2) is described instead
The preparation method penetrating heat insulating sand is: first resin and the non-ionic wetting agent mixing of formula ratio is stirred evenly, adds the color of formula ratio
Powder, is milled to fineness≤25 μm after stirring evenly;It is subsequently added reflective insulation powder and the reflective insulation titanium white of formula ratio, adds after stirring evenly
The adhesive force auxiliary agent of formula ratio and quartz sand, stir evenly, drying reflective insulation sand;Choose reflection that particle diameter is 10-180 mesh every
Hot sand is stand-by;The formula of wherein said reflective insulation sand comprises the component of following parts by weight: quartz sand 83~90 parts, resin
8~15 parts, non-ionic wetting agent 0.1~0.15 part, toner 1~1.5 parts, reflective insulation titanium white 1~2 parts, reflective insulation powder 1
Part, adhesive force auxiliary agent 0.2 part.
Priority Applications (1)
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CN108047802A (en) * | 2017-12-12 | 2018-05-18 | 天津市荣新涂料股份有限公司 | A kind of aqueous reflective heat-insulation paint and preparation method thereof |
CN108795202A (en) * | 2018-07-10 | 2018-11-13 | 太仓市美航涂料有限公司 | A kind of sound-insulating and heat-insulating elasticity stone paint |
CN110255969A (en) * | 2019-06-19 | 2019-09-20 | 郑州科威科建筑材料有限公司 | A kind of reflective insulation sand and preparation method thereof |
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CN103709847A (en) * | 2013-12-26 | 2014-04-09 | 深圳市嘉达高科产业发展有限公司 | Colored reflective heat-insulating paint based on modified titanium white and preparation method thereof |
CN104150797A (en) * | 2014-07-25 | 2014-11-19 | 浙江曼得丽涂料有限公司 | Artificial colour sand and preparation method thereof |
CN104312341A (en) * | 2014-09-24 | 2015-01-28 | 上海宇培特种建材有限公司 | Reflective heat-insulation type really stone paint and preparation method thereof |
CN105131764A (en) * | 2015-08-20 | 2015-12-09 | 浙江好途程节能科技有限公司 | Reflective heat-insulation texture coating and preparation method thereof |
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JP2007217586A (en) * | 2006-02-17 | 2007-08-30 | Yamamoto Yogyo Kako Co Ltd | Heat-insulating coating and heat-insulating material |
CN103709847A (en) * | 2013-12-26 | 2014-04-09 | 深圳市嘉达高科产业发展有限公司 | Colored reflective heat-insulating paint based on modified titanium white and preparation method thereof |
CN104150797A (en) * | 2014-07-25 | 2014-11-19 | 浙江曼得丽涂料有限公司 | Artificial colour sand and preparation method thereof |
CN104312341A (en) * | 2014-09-24 | 2015-01-28 | 上海宇培特种建材有限公司 | Reflective heat-insulation type really stone paint and preparation method thereof |
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CN108047802A (en) * | 2017-12-12 | 2018-05-18 | 天津市荣新涂料股份有限公司 | A kind of aqueous reflective heat-insulation paint and preparation method thereof |
CN108795202A (en) * | 2018-07-10 | 2018-11-13 | 太仓市美航涂料有限公司 | A kind of sound-insulating and heat-insulating elasticity stone paint |
CN110255969A (en) * | 2019-06-19 | 2019-09-20 | 郑州科威科建筑材料有限公司 | A kind of reflective insulation sand and preparation method thereof |
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