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CN106093130B - Method and system for carrying out thermoelectric combined test on test article coated with electric composite grease - Google Patents

Method and system for carrying out thermoelectric combined test on test article coated with electric composite grease Download PDF

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CN106093130B
CN106093130B CN201610394103.XA CN201610394103A CN106093130B CN 106093130 B CN106093130 B CN 106093130B CN 201610394103 A CN201610394103 A CN 201610394103A CN 106093130 B CN106093130 B CN 106093130B
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resistance value
temperature rise
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CN106093130A (en
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张雪松
王景朝
周立宪
刘胜春
李军辉
刘臻
孙宝东
席永平
孙娜
牛海军
张军
邱书清
刘操兰
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State Grid Corp of China SGCC
China Electric Power Research Institute Co Ltd CEPRI
State Grid Henan Electric Power Co Ltd
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China Electric Power Research Institute Co Ltd CEPRI
State Grid Henan Electric Power Co Ltd
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    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
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    • G01N27/02Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating impedance
    • G01N27/04Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating impedance by investigating resistance
    • G01N27/041Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating impedance by investigating resistance of a solid body
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N25/00Investigating or analyzing materials by the use of thermal means
    • G01N25/20Investigating or analyzing materials by the use of thermal means by investigating the development of heat, i.e. calorimetry, e.g. by measuring specific heat, by measuring thermal conductivity

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Abstract

本发明涉及一种对涂有电力复合脂的试品进行热电联合试验的方法,所述方法包括:测量涂有电力复合脂的待测试品的电阻值;将涂有电力复合脂的待测试品放置在热电联合试验箱中;对输入电源的电压进行调节以获得经过调节的试验电压;将经过调节的试验电压连接到所述热电联合试验箱,从而为所述热电联合试验箱和所述热电联合试验箱中的待测试品供电;在当前工况下对涂有电力复合脂的待测试品进行热电联合试验;获得所述待测试品在当前工况的电阻值的实时数据和温升值的实时数据;确定待测试品的电阻值或温升值的实时数据是否是线性增加;以及如果电阻值或温升值的实时数据不是线性增加时,停止热电联合试验。

Figure 201610394103

The invention relates to a method for conducting a combined thermoelectric test on a sample coated with electric power compound grease, the method comprising: measuring the resistance value of the test object coated with electric power compound grease; place in the combined heat and power test box; adjust the voltage of the input power supply to obtain a regulated test voltage; connect the regulated test voltage to the combined heat and power test box, thereby providing the The power supply to the test object in the combined test chamber; the combined thermoelectric test is performed on the test object coated with the power compound grease under the current working condition; the real-time data of the resistance value of the test object under the current working condition and the temperature rise value are obtained. Real-time data; determine whether the real-time data of the resistance value or temperature rise value of the test object increases linearly; and if the real-time data of the resistance value or temperature rise value does not increase linearly, stop the combined heat and power test.

Figure 201610394103

Description

一种对涂有电力复合脂的试品进行热电联合试验的方法及 系统A method and method for conducting combined thermoelectric test on a sample coated with electrical compound grease system

技术领域technical field

本发明涉及计量领域,并且更具体地,涉及一种一种对涂有电力复合脂的试品进行热电联合试验的方法及系统。The present invention relates to the field of metrology, and more particularly, to a method and a system for performing combined thermoelectric test on a test sample coated with electrical compound grease.

背景技术Background technique

电力复合脂是一种电接触性能良好的中性导电敷料。电力复合脂适用于高低压电器母线搭接处接触面及各种电气接头处,可使接触电阻明显下降,从而获得良好的节电经济效益。电力复合脂广泛应用于换流站中的母线与母线、母线与设备接线端子连接处的接触面和开关触头的接触面上。相同和不同金属材质的导电体的连接均可使用电力复合脂,代替并优于紧固连接接触面的搪锡、镀银工艺,能较大地降低接触电阻,从而达到降低温升。Power compound grease is a neutral conductive dressing with good electrical contact performance. Power compound grease is suitable for the contact surface of the lap joint of high and low voltage electrical appliances and various electrical joints, which can significantly reduce the contact resistance and obtain good power-saving economic benefits. Power compound grease is widely used in the contact surface of the busbar and the busbar, the busbar and the equipment terminal connection and the contact surface of the switch contacts in the converter station. The electrical compound grease can be used for the connection of conductors of the same and different metal materials, which replaces and is superior to the tin-lining and silver-plating processes that fasten the contact surface of the connection, which can greatly reduce the contact resistance, thereby reducing the temperature rise.

电力复合脂提高母线连接处的导电性,增强了电网运行的安全性,节省了大量的电能损耗,还可避免接触面产生电化腐蚀。电力复合脂适用于各种不同环境,具有良好的耐高温、耐潮湿、抗氧化、抗霉菌及抗化学腐蚀性能,还具有高温不流淌、低温不龟裂、理化性能稳定、使用寿命长的特点,极大地提高了导电膏使用处的安全性能,为换流站的安全运行提供可靠的保证。Power compound grease improves the conductivity of the busbar connection, enhances the safety of power grid operation, saves a lot of power loss, and also avoids galvanic corrosion on the contact surface. Power compound grease is suitable for various environments. It has good high temperature resistance, moisture resistance, oxidation resistance, mildew resistance and chemical corrosion resistance. It also has the characteristics of no flow at high temperature, no cracking at low temperature, stable physical and chemical properties, and long service life. , which greatly improves the safety performance of the conductive paste, and provides a reliable guarantee for the safe operation of the converter station.

换流站电接触连接处的电力复合脂会随着时间逐渐老化最终失效,会导致电接触连接温度升高,从而造成事故。另外,换流站电接触连接位置处的电力复合脂往往处于通流和温度变化环境中,其老化是一个缓慢的过程,往往需要很长的时间。为了及时更换电接触连接处老化的电力复合脂以避免换流站此类事故的发生,建立换流站电接触连接处电力复合脂的老化模型,预测换流站中电力复合脂的老化寿命显得非常必要了。此外,在对电力复合脂的老化进行模拟时,通常要对涂有电力复合脂的试品进行热电联合试验,而现有技术中并没有进行热电联合试验的手段。The power compound grease at the electrical contact connection of the converter station will gradually age and eventually fail over time, which will cause the temperature of the electrical contact connection to rise, resulting in accidents. In addition, the power compound grease at the electrical contact connection position of the converter station is often in the environment of current flow and temperature change, and its aging is a slow process, which often takes a long time. In order to replace the aging power compound grease at the electrical contact connection in time to avoid such accidents in the converter station, an aging model of the power compound grease at the electrical contact connection of the converter station is established to predict the aging life of the power compound grease in the converter station. Very necessary. In addition, when simulating the aging of the power compound grease, a combined thermoelectric test is usually performed on the sample coated with the power compound grease, and there is no means for performing a combined thermoelectric test in the prior art.

发明内容SUMMARY OF THE INVENTION

为了及时更换电接触连接处老化的电力复合脂以避免换流站电接触连接处因温度升高造成事故,本申请建立了电力复合脂在热-电耦合作用下的加速老化模型,以预测换流站电力复合脂老化寿命。并且,为了确定加速老化模型中参数,本申请提供了电力复合脂热电联合试验方法,并提供了确定加速老化模型中参数的多元回归方法。In order to replace the aged power compound grease at the electrical contact connection in time to avoid accidents caused by the temperature rise at the electrical contact connection of the converter station, this application establishes an accelerated aging model of the power compound grease under the action of thermal-electric coupling to predict the conversion Stream station power compound grease aging life. In addition, in order to determine the parameters in the accelerated aging model, the present application provides a combined thermal and electrical test method for electric power compound grease, and provides a multiple regression method for determining the parameters in the accelerated aging model.

为了实现上述目标,本发明提供一种对涂有电力复合脂的试品进行热电联合试验的方法,所述方法包括:In order to achieve the above goals, the present invention provides a method for conducting a combined thermoelectric test on a test sample coated with an electrical compound grease, the method comprising:

测量涂有电力复合脂的待测试品的电阻值;Measure the resistance value of the DUT coated with the power compound grease;

将涂有电力复合脂的待测试品放置在热电联合试验箱中;Place the test object coated with the power compound grease in the combined heat and power test box;

对输入电源的电压进行调节以获得经过调节的试验电压;Adjust the voltage of the input power supply to obtain a regulated test voltage;

将经过调节的试验电压连接到所述热电联合试验箱,从而为所述热电联合试验箱和所述热电联合试验箱中的待测试品供电;connecting the regulated test voltage to the combined heat and power test box to supply power to the combined heat and power test box and the DUT in the combined heat and power test box;

在当前工况下对涂有电力复合脂的待测试品进行热电联合试验;Under the current working conditions, the combined thermoelectric test is carried out on the DUT coated with the power compound grease;

获得所述待测试品在当前工况的电阻值的实时数据和温升值的实时数据;Obtain the real-time data of the resistance value and the real-time data of the temperature rise value of the test object in the current working condition;

确定待测试品的电阻值或温升值的实时数据是否是线性增加;以及determine whether the real-time data of the resistance value or temperature rise of the DUT is a linear increase; and

如果电阻值或温升值的实时数据不是线性增加时,停止热电联合试验。If the real-time data of resistance value or temperature rise value does not increase linearly, stop the combined thermoelectric test.

优选地,其中如果电阻值或温升值的实时数据是线性增加时,则在下一工况下对涂有电力复合脂的待测试品进行热电联合试验,直到电阻值或温升值的实时数据中的一个不是线性增加时,停止热电联合试验。Preferably, if the real-time data of the resistance value or the temperature rise value is a linear increase, the combined thermoelectric test is performed on the test object coated with the power compound grease under the next working condition, until the resistance value or the real-time temperature rise value in the real-time data. When one does not increase linearly, stop the combined thermoelectric test.

优选地,其中热电联合试验箱的内部温度控制在20℃至22℃。Preferably, the internal temperature of the combined heat and power test box is controlled at 20°C to 22°C.

优选地,其中按照温升值130Tt/℃、150Tt/℃、170Tt/℃或190Tt/℃对待测试品供电。Preferably, the test article is powered according to the temperature rise value of 130Tt/°C, 150Tt/°C, 170Tt/°C or 190Tt/°C.

优选地,其中在每种工况下为待测试品供电3小时。Preferably, wherein the DUT is powered for 3 hours under each operating condition.

根据本发明的另一方面,提供一种对涂有电力复合脂的试品进行热电联合试验的系统,所述系统包括:According to another aspect of the present invention, there is provided a system for performing a combined thermoelectric test on a test sample coated with electrical compound grease, the system comprising:

电阻测量单元,测量涂有电力复合脂的待测试品的电阻值;The resistance measuring unit measures the resistance value of the DUT coated with the power compound grease;

热电联合试验箱,用于容纳涂有电力复合脂的待测试品;Combined thermoelectric test box, used to accommodate the test object coated with electric compound grease;

电压调节单元,对输入电源的电压进行调节以获得经过调节的试验电压;A voltage adjustment unit, which adjusts the voltage of the input power supply to obtain the adjusted test voltage;

电压输入单元,将经过调节的试验电压连接到所述热电联合试验箱,从而为所述热电联合试验箱和所述热电联合试验箱中的待测试品供电;a voltage input unit, connecting the regulated test voltage to the combined heat and power test box, so as to supply power to the combined heat and power test box and the DUT in the combined heat and power test box;

试验单元,在当前工况下对涂有电力复合脂的待测试品进行热电联合试验,获得所述待测试品在当前工况的电阻值的实时数据和温升值的实时数据,确定待测试品的电阻值或温升值的实时数据是否是线性增加;以及如果电阻值或温升值的实时数据不是线性增加时,停止热电联合试验。The test unit performs a combined thermoelectric test on the DUT coated with the power compound grease under the current working condition, obtains the real-time data of the resistance value and the real-time data of the temperature rise value of the DUT under the current working condition, and determines the DUT Whether the real-time data of the resistance value or the temperature rise value increases linearly; and if the real-time data of the resistance value or the temperature rise value does not increase linearly, stop the combined heat and power test.

优选地,其中如果试验单元确定电阻值或温升值的实时数据是线性增加时,则在下一工况下对涂有电力复合脂的待测试品进行热电联合试验,直到电阻值或温升值的实时数据中的一个不是线性增加时,停止热电联合试验。Preferably, if the test unit determines that the real-time data of the resistance value or the temperature rise value is a linear increase, the combined thermoelectric test is performed on the test object coated with the power compound grease under the next working condition, until the real-time data of the resistance value or the temperature rise value. When one of the data does not increase linearly, stop the combined heat and power test.

优选地,其中热电联合试验箱的内部温度控制在20℃至22℃。Preferably, the internal temperature of the combined heat and power test box is controlled at 20°C to 22°C.

优选地,其中按照温升值130Tt/℃、150Tt/℃、170Tt/℃或190Tt/℃对待测试品供电。Preferably, the test article is powered according to the temperature rise value of 130Tt/°C, 150Tt/°C, 170Tt/°C or 190Tt/°C.

优选地,其中在每种工况下为待测试品供电3小时。Preferably, wherein the DUT is powered for 3 hours under each operating condition.

附图说明Description of drawings

通过参考下面的附图,可以更为完整地理解本发明的示例性实施方式:Exemplary embodiments of the present invention may be more fully understood by reference to the following drawings:

图1为根据本发明实施方式的建立电力复合脂加速老化模型的流程图;1 is a flow chart of establishing an accelerated aging model of electric compound grease according to an embodiment of the present invention;

图2为根据本发明另一实施方式的建立电力复合脂加速老化模型的方法的流程图;FIG. 2 is a flowchart of a method for establishing an accelerated aging model of electric compound grease according to another embodiment of the present invention;

图3为根据本发明实施方式的试验电路的结构示意图;3 is a schematic structural diagram of a test circuit according to an embodiment of the present invention;

图4为根据本发明实施方式的加速老化试验的流程图;4 is a flowchart of an accelerated aging test according to an embodiment of the present invention;

图5为根据本发明另一实施方式的对涂有电力复合脂的试品进行热电联合试验的方法的流程图;以及。FIG. 5 is a flow chart of a method for performing a combined thermoelectric test on a test sample coated with a power compound grease according to another embodiment of the present invention; and.

图6为根据本发明另一实施方式的对涂有电力复合脂的试品进行热电联合试验的系统的结构示意图。FIG. 6 is a schematic structural diagram of a system for performing a combined thermoelectric test on a sample coated with an electrical compound grease according to another embodiment of the present invention.

具体实施方式Detailed ways

现在参考附图介绍本发明的示例性实施方式,然而,本发明可以用许多不同的形式来实施,并且不局限于此处描述的实施例,提供这些实施例是为了详尽地且完全地公开本发明,并且向所属技术领域的技术人员充分传达本发明的范围。对于表示在附图中的示例性实施方式中的术语并不是对本发明的限定。在附图中,相同的单元/元件使用相同的附图标记。Exemplary embodiments of the present invention will now be described with reference to the accompanying drawings, however, the present invention may be embodied in many different forms and is not limited to the embodiments described herein, which are provided for the purpose of this thorough and complete disclosure invention, and fully convey the scope of the invention to those skilled in the art. The terms used in the exemplary embodiments shown in the drawings are not intended to limit the invention. In the drawings, the same elements/elements are given the same reference numerals.

除非另有说明,此处使用的术语(包括科技术语)对所属技术领域的技术人员具有通常的理解含义。另外,可以理解的是,以通常使用的词典限定的术语,应当被理解为与其相关领域的语境具有一致的含义,而不应该被理解为理想化的或过于正式的意义。Unless otherwise defined, terms (including scientific and technical terms) used herein have the commonly understood meanings to those skilled in the art. In addition, it is to be understood that terms defined in commonly used dictionaries should be construed as having meanings consistent with the context in the related art, and should not be construed as idealized or overly formal meanings.

图1为根据本发明实施方式的建立电力复合脂加速老化模型的方法100的流程图。电接触连接电力复合脂的老化主要受到电流、温度、盐雾、振动、紫外光等因素的影响。根据对线路和换流站内电接触连接的实际现场分析,本发明专利认为影响电接触连接部位电力复合脂老化性能最主要的两个因素为:电流和温度。另外,由于在电接触连接运行电流和耐受温度变化时,电力复合脂失效时间过长,造成试验周期太长或者试验数据太少。为了缩短电力复合脂老化试验周期和得到大量老化数据,本申请涂电力复合脂样品的电热联合加速寿命试验,并对得到的寿命数据进行威布尔分布检验,并进行参数估计,从而得到威布尔分布特征寿命和形状参数。如图1所示,方法100从步骤101处开始。FIG. 1 is a flowchart of a method 100 for establishing an accelerated aging model of an electrical compound grease according to an embodiment of the present invention. The aging of electrical contact connection electrical compound grease is mainly affected by factors such as current, temperature, salt spray, vibration, and ultraviolet light. According to the actual on-site analysis of the electrical contact connection in the line and the converter station, the patent of the present invention believes that the two most important factors affecting the aging performance of the electrical compound grease at the electrical contact connection part are: current and temperature. In addition, when the electrical contact is connected to the operating current and withstands temperature changes, the failure time of the power compound grease is too long, resulting in too long a test period or too little test data. In order to shorten the aging test period of the electric compound grease and obtain a large amount of aging data, the electro-thermal combined accelerated life test of the electric compound grease coated samples in the present application is carried out, and the Weibull distribution test is carried out on the obtained life data, and the parameters are estimated, so as to obtain the Weibull distribution Characteristic lifetime and shape parameters. As shown in FIG. 1 , method 100 begins at step 101 .

优选地,在步骤101,利用试验电路在多种工况下进行对涂有电力复合脂的待测试品进行热电联合试验,获得所述待测试品在多种工况中每种工况下的电阻值和温升值的数据,以确定每种工况下的电阻值或温升值的线性区间和拐点值。优选地,利用试验电路在多种工况下进行对涂有电力复合脂的待测试品进行热电联合试验,获得所述待测试品在多种工况中每种工况下的电阻值和温升值的数据,当电阻值或温升值中的一个出现拐点时,停止热电联合试验。或者,当电阻值和温升值均未出现拐点时,增加通过待测试品的电流,直到电阻值或温升值中的一个出现拐点时,停止热电联合试验(将在下面进行详细介绍)。优选地,待测试品可以是涂有电力复合脂的电极。Preferably, in step 101, a combined thermoelectric test is performed on the product to be tested coated with the power compound grease under various working conditions by using a test circuit, and the test circuit is obtained under each working condition of the multiple working conditions. The data of resistance value and temperature rise value to determine the linear interval and inflection point value of resistance value or temperature rise value under each operating condition. Preferably, a combined thermoelectric test is performed on the object to be tested coated with the power compound grease under various operating conditions using a test circuit, and the resistance value and temperature of the object to be tested under each operating condition under various operating conditions are obtained. The value-added data, when either the resistance value or the temperature-rise value has an inflection point, the combined thermoelectric test is stopped. Alternatively, when there is no inflection point in both the resistance value and the temperature rise value, increase the current through the DUT until an inflection point occurs in either the resistance value or the temperature rise value, and stop the combined thermoelectric test (described in detail below). Preferably, the object to be tested may be an electrode coated with electrical compound grease.

优选地,在步骤102处,确定多种工况中每种工况下的电阻值或温升值的拐点值之间的差值是否在预定范围之内。通常,随着通电时间的持续,待测试品的电阻值和温升值会明显升高。但是,不同的待测试品在不同的环境下电阻值和温升值升高的线性区间是不同。此外,当出现拐点时,通常将拐点值作为线性区间结束点。Preferably, at step 102, it is determined whether the difference between the resistance value or the inflection point value of the temperature rise value under each of the plurality of operating conditions is within a predetermined range. Generally, the resistance value and temperature rise value of the DUT will increase significantly as the power-on time continues. However, the linear ranges of resistance value and temperature rise value increase are different for different DUTs in different environments. Also, when an inflection point occurs, the inflection point value is usually used as the end point of the linear interval.

优选地,在步骤103处,如果多种工况中每种工况下电阻值或温升值的拐点值之间的差值在预定范围之内并且电力复合脂的老化原理相同,则基于威布尔分布建立初始模型。优选地,所述基于威布尔分布的电力复合脂加速老化模型为:Preferably, at step 103, if the difference between the resistance value or the inflection point value of the temperature rise value under each of the multiple operating conditions is within a predetermined range and the aging principle of the power compound grease is the same, then based on Weibull The distribution builds the initial model. Preferably, the Weibull distribution-based accelerated aging model of electric compound grease is:

lnη=a1+a2I(1+ε)R+b1/T+b2I(1+ε)/T,lnη=a 1 +a 2 I(1+ε)R+b 1 /T+b 2 I(1+ε)/T,

其中,η为威布尔分布特征寿命,T为绝对温度,I为通过待测试品的电流,R是未涂电力复合脂的电连接处电阻值,εR—涂电力复合脂后的电连接处电阻值的改变值,a1、a2、b1和b2是常数。Among them, η is the Weibull distribution characteristic life, T is the absolute temperature, I is the current passing through the test object, R is the resistance value of the electrical connection without coating the electric compound grease, εR is the electrical connection resistance after the electric compound grease is applied The change in value, a1, a2, b1 and b2 are constants.

优选地,在步骤104处,根据多种工况中每种工况下电阻值和温升值的数据对初始模型中的初始参数进行多元线性回归分析,以确定基于威布尔分布的电力复合脂加速老化模型。Preferably, at step 104, multiple linear regression analysis is performed on the initial parameters in the initial model according to the data of the resistance value and the temperature rise value under each of the various operating conditions, so as to determine the acceleration of the electric compound grease based on the Weibull distribution Aging model.

图2为根据本发明另一实施方式的建立电力复合脂加速老化模型的的方法200的流程图。如图2所示,方法200从步骤201开始。优选地,在步骤201处,利用试验电路在多种工况下进行对涂有电力复合脂的待测试品进行热电联合试验。优选地,热电联合试验获得所述待测试品在多种工况中每种工况下的电阻值和温升值的数据,以确定每种工况下的电阻值或温升值的线性区间和拐点值。FIG. 2 is a flowchart of a method 200 for establishing an accelerated aging model of an electrical compound grease according to another embodiment of the present invention. As shown in FIG. 2 , method 200 begins with step 201 . Preferably, at step 201, a combined thermoelectric test is performed on the DUT coated with the power compound grease under various operating conditions using a test circuit. Preferably, the combined thermoelectric test obtains the data of the resistance value and the temperature rise value of the test object under each working condition in various working conditions, so as to determine the linear interval and inflection point of the resistance value or the temperature rise value under each working condition value.

优选地,在步骤202处,确定电阻值或温升值中的一个是否出现拐点。优选地,当电阻值或温升值中的一个出现拐点时,停止热电联合试验。或者,当电阻值和温升值均未出现拐点时,增加通过待测试品的电流,直到电阻值或温升值中的一个出现拐点时,停止热电联合试验(将在下面进行详细介绍)。优选地,待测试品可以是涂有电力复合脂的电极。Preferably, at step 202, it is determined whether an inflection point occurs in one of the resistance value or the temperature rise value. Preferably, the combined thermoelectric test is stopped when an inflection point occurs in either the resistance value or the temperature rise value. Alternatively, when there is no inflection point in both the resistance value and the temperature rise value, increase the current through the DUT until an inflection point occurs in either the resistance value or the temperature rise value, and stop the combined thermoelectric test (described in detail below). Preferably, the object to be tested may be an electrode coated with electrical compound grease.

优选地,在步骤203处,热电联合试验结束并且对试验数据进行分析。Preferably, at step 203, the combined heat and power test ends and the test data is analyzed.

优选地,在步骤204处,确定电力复合脂老化的统计规律。并且在步骤205处,对统计规律进行假设检验。优选地,如果统计规律通过假设检验,则建立模型(下面会详细介绍);如果统计规律未通过假设检验,则返回步骤204。(下面会详细介绍)如果如果优选地,方法200使用威布尔分布来分析电力复合脂的老化分布特性。其中,威布尔分布的老化数据统计分析基于如下两个前提:Preferably, at step 204, a statistical law of electrical complex lipid aging is determined. And at step 205, a hypothesis test is performed on the statistical law. Preferably, if the statistical law passes the hypothesis test, a model is established (which will be described in detail below); if the statistical law fails the hypothesis test, return to step 204 . (detailed below) If and preferably, the method 200 uses a Weibull distribution to analyze the aging distribution characteristics of the electrical compound grease. Among them, the statistical analysis of aging data of Weibull distribution is based on the following two premises:

A1.在各个不同试验水平下,电力复合脂的老化均服从威布尔分布,即老化分布类型不会随着加速试验水平改变而发生改变;以及A1. Under each test level, the aging of the power compound grease obeys the Weibull distribution, that is, the aging distribution type does not change with the change of the accelerated test level; and

A2.在各个不同试验水平下,电力复合脂的老化失效机理必须保持一致。A2. Under different test levels, the aging failure mechanism of power compound grease must be consistent.

若满足假定A1和A2,就能确定电力复合脂的老化服从威布尔分布。根据不同工况下电力复合脂老化试验数据,利用MATLAB的统计功能wblplot函数进行数据分析,可以绘出各个试验点下的威布尔概率图。把相同试验温度的电力复合脂样品寿命数据分为一组,并在威布尔概率图上绘出。由于每个试验温度下都有n个不同的试验电流等级,所以每个威布尔概率图上都有n条威布尔概率线。如果在一个电流和温度等级下,电力复合脂n个样品的寿命概率数据点都近似位于威布尔概率图中同一条直线的周围,就可以假定电力复合脂样品的老化数据满足威布尔分布的假定A1和A2,则样品寿命服从威布尔分布。If the assumptions A1 and A2 are satisfied, it can be determined that the aging of the power compound grease follows a Weibull distribution. According to the aging test data of the power compound grease under different working conditions, using the wblplot function of the MATLAB statistical function to analyze the data, the Weibull probability diagram under each test point can be drawn. The life data of the electric compound grease samples at the same test temperature are grouped into one group and plotted on the Weibull probability map. Since there are n different test current levels at each test temperature, there are n Weibull probability lines on each Weibull probability map. If the lifetime probability data points of n samples of the electrical compound grease are all approximately around the same straight line in the Weibull probability plot at a current and temperature level, it can be assumed that the aging data of the electrical compound grease sample satisfies the assumption of the Weibull distribution A1 and A2, the sample lifetime obeys Weibull distribution.

优选地,在步骤206处,基于威布尔分布建立初始模型。优选地,将电、热两个因子同时附加到电力复合脂时的失效时间比单独作用时的失效时间要短得多。这种附加并不是热老化和电老化的简单代数叠加,因此电热联合加速寿命模型须考虑两个因子之间的相互作用。在步骤206处,本申请确定电力复合脂电热联合加速老化模型,该模型推导如下:Preferably, at step 206, an initial model is established based on the Weibull distribution. Preferably, the failure time when both the electrical and thermal factors are added to the electrical compound grease at the same time is much shorter than the failure time when they are applied individually. This addition is not a simple algebraic superposition of thermal and electrical aging, so the combined electro-thermal accelerated life model must consider the interaction between the two factors. At step 206, the present application determines a combined accelerated aging model of electric power compound grease, which is derived as follows:

lnη=a+b/T (1)lnη=a+b/T (1)

a=a1+a2I(1+ε)R (2)a=a 1 +a 2 I(1+ε)R (2)

b=b1+b2I(1+ε)R (3)b=b 1 +b 2 I(1+ε)R (3)

令U=I(1+ε)RLet U=I(1+ε)R

lnη=(a1+a2U)+(b1+b2U)/T (4)lnη=(a 1 +a 2 U)+(b 1 +b 2 U)/T (4)

由公式4进一步推得It is further deduced from Equation 4

lnη=a1+a2I(1+ε)R+b1/T+b2I(1+ε)/T (5)lnη=a 1 +a 2 I(1+ε)R+b 1 /T+b 2 I(1+ε)/T (5)

其中,η为威布尔分布特征寿命,T为绝对温度,I为通过待测试品的电流,R是未涂电力复合脂的电连接处电阻值,εR—涂电力复合脂后的电连接处电阻值的改变值,a1、a2、b1和b2是常数。Among them, η is the Weibull distribution characteristic life, T is the absolute temperature, I is the current passing through the test object, R is the resistance value of the electrical connection without coating the electric compound grease, εR is the electrical connection resistance after the electric compound grease is applied The change in value, a1, a2, b1 and b2 are constants.

从公式(5)中可以看出,若把lnη当作因变量,并把I、T、εR当作三个自变量,就可以将该模型转换成标准多元线性回归模型公式。利用热电联合试验数据,并结合给出的模型可以利用MATLAB编程实现模型参数的多元线性回归估计,从而得出电力复合脂寿命预测模型具体表达式。It can be seen from formula (5) that if lnη is regarded as the dependent variable, and I, T, εR are regarded as three independent variables, the model can be converted into a standard multiple linear regression model formula. Using the combined thermal and electric test data, combined with the given model, the multiple linear regression estimation of the model parameters can be realized by MATLAB programming, and the specific expression of the life prediction model of the power compound grease can be obtained.

优选地,在步骤207处,根据多种工况中每种工况下电阻值和温升值的数据对初始模型中的初始参数进行多元线性回归分析。Preferably, at step 207, multiple linear regression analysis is performed on the initial parameters in the initial model according to the data of the resistance value and the temperature rise value under each of the multiple operating conditions.

优选地,在步骤208处,如果初始模型中的初始参数符合要求,则将所述初始模型确定为基于威布尔分布的电力复合脂加速老化模型。Preferably, at step 208, if the initial parameters in the initial model meet the requirements, the initial model is determined to be a Weibull distribution-based accelerated aging model for electrical compound grease.

图3为根据本发明实施方式的试验电路的结构示意图。如图3所示,试验电路300包括:220V交流电源301,自耦合调压器302,降压变压器303,保护电阻304,耦合电容器305,热电联合试验箱306,待测试品307,接地线308以及接地端309。FIG. 3 is a schematic structural diagram of a test circuit according to an embodiment of the present invention. As shown in FIG. 3 , the test circuit 300 includes: a 220V AC power supply 301 , a self-coupling voltage regulator 302 , a step-down transformer 303 , a protection resistor 304 , a coupling capacitor 305 , a combined thermoelectric test box 306 , a product to be tested 307 , and a ground wire 308 and ground terminal 309 .

优选地,220V交流电源301为输入电源,其连接到自耦合调压器的两端。优选地,自耦合调压器302,用于调节试验电压。优选地,降压变压器303的一次侧的一端连接到自耦合调压器302可调节端,用于来降低电压。降压变压器303的一次侧的另一端接地。优选地,保护电阻304,起限流保护作用,其连接到降压变压器303的二次侧的一端。耦合电容器305与保护电阻304的一端以及降压变压器303的二次侧的另一端,用于将试验电压返回给控制台以进行显示。优选地,热电联合试验箱306的一端与耦合电容器的一端连接,并且热电联合试验箱306的另一端接地。热电联合试验箱306用于容纳待测试品,并且其内部尺寸为1000×1000×1000(mm)、可调温度范围-60~100℃并且温度波动度±0.2℃。优选地,待测试品307包括试验电极及样品。其中样品可以是电力复合脂。优选地,接地线308,用于接地端与接地极的连接。热电联合试验箱的接地端309,用于试验接地。Preferably, the 220V AC power supply 301 is an input power supply, which is connected to both ends of the self-coupling voltage regulator. Preferably, a self-coupled voltage regulator 302 is used to adjust the test voltage. Preferably, one end of the primary side of the step-down transformer 303 is connected to the adjustable end of the self-coupling voltage regulator 302 for reducing the voltage. The other end of the primary side of the step-down transformer 303 is grounded. Preferably, the protection resistor 304, which plays the role of current limiting protection, is connected to one end of the secondary side of the step-down transformer 303. One end of the coupling capacitor 305 and the protection resistor 304 and the other end of the secondary side of the step-down transformer 303 are used to return the test voltage to the console for display. Preferably, one end of the combined heat and power test box 306 is connected to one end of the coupling capacitor, and the other end of the combined heat and power test box 306 is grounded. The combined thermoelectric test box 306 is used for accommodating the object to be tested, and its internal size is 1000×1000×1000 (mm), the adjustable temperature range is -60~100°C, and the temperature fluctuation degree is ±0.2°C. Preferably, the DUT 307 includes a test electrode and a sample. Wherein the sample can be a power complex grease. Preferably, the ground wire 308 is used for the connection between the ground terminal and the ground electrode. The ground terminal 309 of the combined heat and power test box is used for grounding the test.

优选地,试验过程中,可通过调节热电联合试验箱的内部温度来控制电力复合脂样品老化温度。试验时应保证热-电联合试验箱内部温度的均匀性,以达到在试验内进行试验箱内样品电热联合加速老化试验的目的。Preferably, during the test, the aging temperature of the power compound grease sample can be controlled by adjusting the internal temperature of the combined heat and power test chamber. During the test, the uniformity of the internal temperature of the combined heat-electric test box should be ensured, so as to achieve the purpose of conducting the combined electric-heat combined accelerated aging test of the sample in the test box during the test.

优选地,试验可以分为如下几个工况进行,并且试验流程如图4所示。图4为根据本发明实施方式的加速老化试验的流程图。优选地,试验步骤如下:Preferably, the test can be divided into the following several working conditions, and the test flow is shown in Figure 4. 4 is a flow chart of an accelerated aging test according to an embodiment of the present invention. Preferably, the test steps are as follows:

步骤401,在试验前,测试待测试品的电阻值并且随后将待测试品放置在热电联合试验箱中。Step 401 , before the test, test the resistance value of the object to be tested and then place the object to be tested in a combined thermoelectric test box.

步骤402,按照温升值130Tt/℃对待测试品接通电流、热电联合试验箱的内部温度控制在20℃~22℃之间变化、通电流时间h=3小时。Step 402 , according to the temperature rise value of 130Tt/°C, the current is connected to the test object, the internal temperature of the combined heat and power test chamber is controlled to vary between 20°C and 22°C, and the current-on time h=3 hours.

步骤403,测量待测试品的接触电阻值R1和温升值K1。Step 403 , measure the contact resistance value R1 and the temperature rise value K1 of the DUT.

步骤404,重复步骤402-403共19次(共60小时),并记录每次试验的电阻值和温升值。Step 404, repeat steps 402-403 for a total of 19 times (a total of 60 hours), and record the resistance value and temperature rise value of each test.

步骤405,判断待测试品的电阻值或温升值是否是线性增加,即确定有无出现拐点值。In step 405, it is determined whether the resistance value or the temperature rise value of the DUT increases linearly, that is, it is determined whether there is an inflection point value.

步骤406,如果待测试品的电阻值或温升值出现拐点,则停止试验,否则,在步骤407,按照温升值150Tt/℃对待测试品接通电流、热电联合试验箱的内部温度控制在20℃~22℃之间变化、通电流时间h=3小时。Step 406, if the resistance value or temperature rise value of the product to be tested has an inflection point, then stop the test, otherwise, in step 407, according to the temperature rise value of 150Tt/℃, the current is connected to the product to be tested, and the internal temperature of the combined thermoelectric test box is controlled at 20 °C Changes between ~22°C, current passing time h=3 hours.

步骤408,重复步骤407共20次(共60小时),并记录每次试验的电阻值和温升值。Step 408, repeat step 407 for a total of 20 times (60 hours in total), and record the resistance value and temperature rise value of each test.

步骤409,判断待测试品的电阻值或温升值是否是线性增加,即确定有无出现拐点值。Step 409 , determine whether the resistance value or the temperature rise value of the DUT increases linearly, that is, determine whether there is an inflection point value.

步骤410,如果待测试品的电阻值或温升值出现拐点,则停止试验,否则,在步骤411,按照温升值170Tt/℃对待测试品接通电流、热电联合试验箱的内部温度控制在20℃~22℃之间变化、通电流时间h=3小时。In step 410, if the resistance value or temperature rise value of the product to be tested has an inflection point, the test is stopped; otherwise, in step 411, the current is connected to the product to be tested according to the temperature rise value of 170Tt/°C, and the internal temperature of the combined thermoelectric test box is controlled at 20°C. Changes between ~22°C, current passing time h=3 hours.

步骤412,重复步骤411共20次(共60小时),并记录每次试验的电阻值和温升值。Step 412, repeat step 411 for a total of 20 times (60 hours in total), and record the resistance value and temperature rise value of each test.

步骤413,判断待测试品的电阻值或温升值是否是线性增加,即确定有无出现拐点值。Step 413 , determine whether the resistance value or the temperature rise value of the DUT increases linearly, that is, determine whether there is an inflection point value.

步骤414,如果待测试品的电阻值或温升值出现拐点,则停止试验,否则,在步骤415,按照温升值190Tt/℃对待测试品接通电流、热电联合试验箱的内部温度控制在20℃~22℃之间变化、通电流时间h=3小时。Step 414, if the resistance value or temperature rise value of the product to be tested has an inflection point, then stop the test, otherwise, in step 415, according to the temperature rise value of 190Tt/℃, the current is connected to the product to be tested, and the internal temperature of the combined thermoelectric test box is controlled at 20 °C Changes between ~22°C, current passing time h=3 hours.

步骤416,重复步骤415共20次(共60小时),并记录每次试验的电阻值和温升值。Step 416, repeat step 415 for a total of 20 times (60 hours in total), and record the resistance value and temperature rise value of each test.

步骤417处结束。Step 417 ends.

图5为根据本发明另一实施方式的对涂有电力复合脂的试品进行热电联合试验的方法500的流程图。方法500利用试验电路在多种工况下进行对涂有电力复合脂的待测试品进行热电联合试验。优选地,热电联合试验获得所述待测试品在多种工况中每种工况下的电阻值和温升值的数据,以确定每种工况下的电阻值或温升值的线性区间和拐点值。FIG. 5 is a flowchart of a method 500 for performing a combined thermoelectric test on a test sample coated with a power compound grease according to another embodiment of the present invention. The method 500 utilizes a test circuit to perform a combined thermoelectric test on a DUT coated with a power compound grease under various operating conditions. Preferably, the combined thermoelectric test obtains the data of the resistance value and the temperature rise value of the test object under each working condition in various working conditions, so as to determine the linear interval and inflection point of the resistance value or the temperature rise value under each working condition value.

优选地,方法500确定电阻值或温升值中的一个是否出现拐点。优选地,当电阻值或温升值中的一个出现拐点时,停止热电联合试验。或者,当电阻值和温升值均未出现拐点时,增加通过待测试品的电流,直到电阻值或温升值中的一个出现拐点时,停止热电联合试验。优选地,待测试品可以是涂有电力复合脂的电极。Preferably, method 500 determines whether an inflection point occurs in one of the resistance value or the temperature rise value. Preferably, the combined thermoelectric test is stopped when an inflection point occurs in either the resistance value or the temperature rise value. Or, when there is no inflection point in both the resistance value and the temperature rise value, increase the current passing through the test object until the resistance value or the temperature rise value has an inflection point, and stop the combined thermoelectric test. Preferably, the object to be tested may be an electrode coated with electrical compound grease.

优选地,在步骤501,测量涂有电力复合脂的待测试品的电阻值。通常,需要测量涂有电力复合脂的待测试品在未进行热电联合试验之前的电阻值,以作为电阻值升高的测量基础。Preferably, in step 501, the resistance value of the DUT coated with the power compound grease is measured. Usually, it is necessary to measure the resistance value of the DUT coated with the power compound grease before the combined thermoelectric test is carried out, as the measurement basis for the increase of the resistance value.

优选地,在步骤502,将涂有电力复合脂的待测试品放置在热电联合试验箱中。热电联合试验箱用于容纳待测试品,并且其内部尺寸为1000×1000×1000(mm)、可调温度范围-60~100℃并且温度波动度±0.2℃。优选地,将热电联合试验箱的内部温度控制在20℃至22℃。Preferably, in step 502, the DUT coated with the electrical compound grease is placed in a combined thermoelectric test chamber. The combined thermoelectric test box is used to accommodate the test object, and its internal size is 1000×1000×1000 (mm), the adjustable temperature range is -60~100°C, and the temperature fluctuation is ±0.2°C. Preferably, the internal temperature of the combined heat and power test box is controlled at 20°C to 22°C.

优选地,在步骤503,对输入电源的电压进行调节以获得经过调节的试验电压。例如,将220V交流电源作为输入电源,其连接到自耦合调压器的两端。方法500使用自耦合调压器来调节试验电压。此外,降压变压器的一次侧的一端连接到自耦合调压器可调节端,用于来降低电压。降压变压器的一次侧的另一端接地。优选地,热电联合试验箱的一端与耦合电容器的一端连接,并且热电联合试验箱的另一端接地。Preferably, in step 503, the voltage of the input power supply is adjusted to obtain an adjusted test voltage. For example, take a 220V AC power supply as the input power supply, which is connected to both ends of the self-coupled voltage regulator. The method 500 uses a self-coupling voltage regulator to regulate the test voltage. In addition, one end of the primary side of the step-down transformer is connected to the adjustable end of the self-coupling voltage regulator for reducing the voltage. The other end of the primary side of the step-down transformer is grounded. Preferably, one end of the combined heat and power test box is connected to one end of the coupling capacitor, and the other end of the combined heat and power test box is grounded.

优选地,在步骤504,将经过调节的试验电压连接到所述热电联合试验箱,从而为所述热电联合试验箱和所述热电联合试验箱中的待测试品供电。Preferably, in step 504, the regulated test voltage is connected to the combined heat and power test box to supply power to the combined heat and power test box and the DUT in the combined heat and power test box.

优选地,在步骤505,在当前工况下对涂有电力复合脂的待测试品进行热电联合试验。例如,按照温升值130Tt/℃对待测试品接通电流、热电联合试验箱的内部温度控制在20℃~22℃之间变化、通电流时间h=3小时。测量待测试品的接触电阻值R1和温升值K,并且重复上述步骤共19次(共60小时),并记录每次试验的电阻值和温升值。Preferably, in step 505, a combined thermoelectric test is performed on the DUT coated with the power compound grease under the current operating conditions. For example, according to the temperature rise value of 130Tt/°C, the current is connected to the test object, the internal temperature of the combined heat and power test box is controlled to change between 20°C and 22°C, and the current-on time h=3 hours. Measure the contact resistance value R1 and temperature rise value K of the product to be tested, and repeat the above steps for a total of 19 times (60 hours in total), and record the resistance value and temperature rise value of each test.

优选地,在步骤506,获得所述待测试品在当前工况的电阻值的实时数据和温升值的实时数据。Preferably, in step 506, the real-time data of the resistance value and the real-time data of the temperature rise value of the DUT under the current working condition are obtained.

优选地,在步骤507,确定待测试品的电阻值或温升值的实时数据是否是线性增加。Preferably, in step 507, it is determined whether the real-time data of the resistance value or the temperature rise value of the DUT is a linear increase.

优选地,在步骤508,如果电阻值或温升值的实时数据不是线性增加时,停止热电联合试验。Preferably, in step 508, if the real-time data of the resistance value or the temperature rise value does not increase linearly, the combined heat and power test is stopped.

优选地,在步骤509,如果电阻值或温升值的实时数据是线性增加时,则在下一工况下对涂有电力复合脂的待测试品进行热电联合试验,直到电阻值或温升值的实时数据中的一个不是线性增加时,停止热电联合试验。优选地,下一工况例如是:按照温升值150Tt/℃对待测试品接通电流、热电联合试验箱的内部温度控制在20℃~22℃之间变化、通电流时间h=3小时;按照温升值170Tt/℃对待测试品接通电流、热电联合试验箱的内部温度控制在20℃~22℃之间变化、通电流时间h=3小时;以及按照温升值190Tt/℃对待测试品接通电流、热电联合试验箱的内部温度控制在20℃~22℃之间变化、通电流时间h=3小时。Preferably, in step 509, if the real-time data of the resistance value or the temperature rise value increases linearly, the combined thermoelectric test is performed on the test object coated with the power compound grease under the next working condition, until the real-time data of the resistance value or the temperature rise value increases. When one of the data does not increase linearly, stop the combined heat and power test. Preferably, the next working condition is, for example: according to the temperature rise value of 150Tt/℃, the current is connected to the test object, the internal temperature of the combined heat and power test box is controlled to change between 20 °C and 22 °C, and the current passing time is h=3 hours; according to The temperature rise value is 170Tt/℃, the current is connected to the test object, the internal temperature of the combined thermoelectric test box is controlled to change between 20℃~22℃, the current passing time is h=3 hours; and the test object is connected according to the temperature rise value 190Tt/℃ The internal temperature of the combined current and heat and power test box is controlled to vary between 20°C and 22°C, and the current-on time h=3 hours.

图6为根据本发明另一实施方式的对涂有电力复合脂的试品进行热电联合试验的系统600的结构示意图。系统600利用试验电路在多种工况下进行对涂有电力复合脂的待测试品进行热电联合试验。优选地,热电联合试验获得所述待测试品在多种工况中每种工况下的电阻值和温升值的数据,以确定每种工况下的电阻值或温升值的线性区间和拐点值。FIG. 6 is a schematic structural diagram of a system 600 for performing a combined thermoelectric test on a test sample coated with electrical compound grease according to another embodiment of the present invention. The system 600 uses a test circuit to perform a combined thermoelectric test on the DUT coated with the power compound grease under various operating conditions. Preferably, the combined thermoelectric test obtains the data of the resistance value and the temperature rise value of the test object under each working condition in various working conditions, so as to determine the linear interval and inflection point of the resistance value or the temperature rise value under each working condition value.

如图1所示,系统600包括:电阻测量单元601、热电联合试验箱602、电压调节单元603、电压输入单元604以及试验单元605。其中电阻测量单元601用于测量涂有电力复合脂的待测试品的电阻值。通常,需要测量涂有电力复合脂的待测试品在未进行热电联合试验之前的电阻值,以作为电阻值升高的测量基础。As shown in FIG. 1 , the system 600 includes: a resistance measurement unit 601 , a combined heat and power test box 602 , a voltage adjustment unit 603 , a voltage input unit 604 and a test unit 605 . The resistance measurement unit 601 is used to measure the resistance value of the DUT coated with the power compound grease. Usually, it is necessary to measure the resistance value of the DUT coated with the power compound grease before the combined thermoelectric test is carried out, as the measurement basis for the increase of the resistance value.

优选地,热电联合试验箱602用于容纳涂有电力复合脂的待测试品。热电联合试验箱602用于容纳待测试品,并且其内部尺寸为1000×1000×1000(mm)、可调温度范围-60~100℃并且温度波动度±0.2℃。优选地,将热电联合试验箱602的内部温度控制在20℃至22℃。Preferably, the combined thermoelectric test box 602 is used to accommodate the test object coated with the electrical compound grease. The combined thermoelectric test box 602 is used for accommodating the object to be tested, and its internal size is 1000×1000×1000 (mm), the adjustable temperature range is -60~100°C, and the temperature fluctuation degree is ±0.2°C. Preferably, the internal temperature of the combined heat and power test box 602 is controlled at 20°C to 22°C.

优选地,电压调节单元603用于对输入电源的电压进行调节以获得经过调节的试验电压。例如,将220V交流电源作为输入电源,其连接到自耦合调压器的两端。系统600使用自耦合调压器来调节试验电压。此外,降压变压器的一次侧的一端连接到自耦合调压器可调节端,用于来降低电压。降压变压器的一次侧的另一端接地。优选地,热电联合试验箱的一端与耦合电容器的一端连接,并且热电联合试验箱的另一端接地。Preferably, the voltage adjustment unit 603 is used to adjust the voltage of the input power supply to obtain the adjusted test voltage. For example, take a 220V AC power supply as the input power supply, which is connected to both ends of the self-coupled voltage regulator. System 600 uses a self-coupling voltage regulator to regulate the test voltage. In addition, one end of the primary side of the step-down transformer is connected to the adjustable end of the self-coupling voltage regulator for reducing the voltage. The other end of the primary side of the step-down transformer is grounded. Preferably, one end of the combined heat and power test box is connected to one end of the coupling capacitor, and the other end of the combined heat and power test box is grounded.

优选地,电压输入单元604,将经过调节的试验电压连接到所述热电联合试验箱,从而为所述热电联合试验箱和所述热电联合试验箱中的待测试品供电。Preferably, the voltage input unit 604 connects the regulated test voltage to the combined heat and power test box, so as to supply power to the combined heat and power test box and the DUT in the combined heat and power test box.

优选地,试验单元605在当前工况下对涂有电力复合脂的待测试品进行热电联合试验,获得所述待测试品在当前工况的电阻值的实时数据和温升值的实时数据,确定待测试品的电阻值或温升值的实时数据是否是线性增加;以及如果电阻值或温升值的实时数据不是线性增加时,停止热电联合试验。其中,当前工况例如是按照温升值130Tt/℃对待测试品接通电流、热电联合试验箱的内部温度控制在20℃~22℃之间变化、通电流时间h=3小时。其中下一工况例如是按照温升值150Tt/℃对待测试品接通电流、热电联合试验箱的内部温度控制在20℃~22℃之间变化、通电流时间h=3小时;按照温升值170Tt/℃对待测试品接通电流、热电联合试验箱的内部温度控制在20℃~22℃之间变化、通电流时间h=3小时;以及按照温升值190Tt/℃对待测试品接通电流、热电联合试验箱的内部温度控制在20℃~22℃之间变化、通电流时间h=3小时。Preferably, the test unit 605 performs a combined thermoelectric test on the DUT coated with the power compound grease under the current working condition, obtains real-time data of the resistance value and real-time data of the temperature rise value of the DUT under the current working condition, and determines Whether the real-time data of the resistance value or temperature rise value of the test object increases linearly; and if the real-time data of the resistance value or temperature rise value does not increase linearly, stop the combined thermoelectric test. Among them, the current working conditions are, for example, the current is connected to the test object according to the temperature rise value of 130Tt/℃, the internal temperature of the combined heat and power test box is controlled to change between 20°C and 22°C, and the current-on time h=3 hours. Among them, the next working condition is, for example, according to the temperature rise value of 150Tt/℃, the current is connected to the test object, the internal temperature of the combined thermoelectric test box is controlled to change between 20℃~22℃, and the current passing time is h=3 hours; according to the temperature rise value of 170Tt /℃ The current is connected to the test object, the internal temperature of the combined thermoelectric test box is controlled to change between 20℃~22℃, the current passing time is h=3 hours; The internal temperature of the combined test box was controlled to vary between 20°C and 22°C, and the current-carrying time h=3 hours.

优选地,根据本发明的优选实施方式,下一工况的选取可以是按照温升值升高来逐步选取,直到电阻值或温升值的实时数据不是线性增加,即出现拐点,为止。已经通过参考少量实施方式描述了本发明。然而,本领域技术人员所公知的,正如附带的专利权利要求所限定的,除了本发明以上公开的其他的实施例等同地落在本发明的范围内。Preferably, according to the preferred embodiment of the present invention, the selection of the next working condition may be gradually selected according to the increase of the temperature rise value, until the real-time data of the resistance value or the temperature rise value does not increase linearly, that is, an inflection point occurs. The present invention has been described with reference to a few embodiments. However, as is known to those skilled in the art, other embodiments than the above disclosed invention are equally within the scope of the invention, as defined by the appended patent claims.

通常地,在权利要求中使用的所有术语都根据他们在技术领域的通常含义被解释,除非在其中被另外明确地定义。所有的参考“一个/所述/该[装置、组件等]”都被开放地解释为所述装置、组件等中的至少一个实例,除非另外明确地说明。这里公开的任何方法的步骤都没必要以公开的准确的顺序运行,除非明确地说明。Generally, all terms used in the claims are to be interpreted according to their ordinary meaning in the technical field, unless explicitly defined otherwise herein. All references to "a/the/the [means, component, etc.]" are open to interpretation as at least one instance of said means, component, etc., unless expressly stated otherwise. The steps of any method disclosed herein do not have to be performed in the exact order disclosed, unless explicitly stated.

Claims (6)

1. A method for modeling electrical composite grease accelerated aging, the method comprising:
the method comprises the following steps of carrying out a combined heat and power test on a to-be-tested sample coated with electric composite grease under various working conditions by using a test circuit, obtaining data of a resistance value and a temperature rise value of the to-be-tested sample under each working condition in the various working conditions, and determining a linear interval and an inflection point value of the resistance value or the temperature rise value under each working condition, wherein the data comprises the following steps:
the test circuit is used for carrying out the combined heat and power test on the to-be-tested sample coated with the electric composite grease under various working conditions,
acquiring real-time data of the resistance value and the temperature rise value of the to-be-tested sample under the current working condition, and determining whether the resistance value or the real-time data of the temperature rise value of the to-be-tested sample is linearly increased or not; and stopping the combined heat and power test if the real-time data of the resistance value or the temperature rise value is not linearly increased;
if the test unit determines that the real-time data of the resistance value or the temperature rise value is linearly increased, performing a combined heat and power test on the to-be-tested sample coated with the electric composite grease under the next working condition, and stopping the combined heat and power test until one of the real-time data of the resistance value or the temperature rise value is not linearly increased;
determining whether a difference between the resistance value or the inflection point value of the temperature increase value for each of the plurality of operating conditions is within a predetermined range,
if the difference value between the inflection point values of the resistance value or the temperature rise value under each working condition in the multiple working conditions is within a preset range and the aging principle of the power compound grease is the same, establishing an initial model based on Weibull distribution; the electric composite grease accelerated aging model based on Weibull distribution is as follows:
lnη=a1+a2I(1+)R+b1/T+b2I(1+)/T,
wherein eta is the characteristic life of Weibull distribution, T is the absolute temperature, I is the current passing through the sample to be tested, R is the resistance value of the electric connection part without being coated with the electric composite grease, R is the change value of the resistance value of the electric connection part after being coated with the electric composite grease, and a1, a2, b1 and b2 are constants;
performing multiple linear regression analysis on initial parameters in the initial model according to data of the resistance value and the temperature rise value under each working condition in multiple working conditions to determine a power composite grease accelerated aging model based on Weibull distribution;
wherein the test circuit comprises: the device comprises a 220V alternating current power supply, a self-coupling voltage regulator, a step-down transformer, a protective resistor, a coupling capacitor, a combined heat and power test box, a to-be-tested sample, a grounding wire and a grounding end;
the 220V alternating current power supply is an input power supply and is connected to two ends of the self-coupling voltage regulator;
the self-coupling voltage regulator is used for regulating the test voltage;
one end of the primary side of the step-down transformer is connected to the adjustable end of the self-coupling regulator and used for reducing voltage, and the other end of the primary side of the step-down transformer is grounded;
the protective resistor plays a role of current-limiting protection and is connected to one end of the secondary side of the step-down transformer;
the coupling capacitor is connected with one end of the protective resistor and the other end of the secondary side of the step-down transformer and used for returning the test voltage to the console for displaying;
one end of the combined heat and power test box is connected with one end of the coupling capacitor, the other end of the combined heat and power test box is grounded, the combined heat and power test box is used for accommodating a to-be-tested sample, the inner size of the combined heat and power test box is 1000 multiplied by 1000mm, the adjustable temperature range is-60-100 ℃, and the temperature fluctuation degree is +/-0.2 ℃;
the test sample to be tested comprises a test electrode and a sample, wherein the sample is the electric composite grease;
the grounding wire is used for connecting the grounding end with the grounding electrode;
and the grounding end is used for grounding in a test mode.
2. The method as claimed in claim 1, wherein the performing, by using the test circuit, the combined heat and power test on the sample coated with the electrical compound grease under multiple working conditions to obtain data of the resistance value and the temperature rise value of the sample under each of the multiple working conditions, so as to determine the linear interval and the inflection point value of the resistance value or the temperature rise value under each working condition, includes:
the method comprises the steps of carrying out a combined heat and power test on a to-be-tested sample coated with electric composite grease under various working conditions by using a test circuit, obtaining data of a resistance value and a temperature rise value of the to-be-tested sample under each working condition in the various working conditions, and stopping the combined heat and power test when an inflection point appears in one of the resistance value or the temperature rise value.
3. The method as claimed in claim 1, wherein the performing, by using the test circuit, the combined heat and power test on the sample coated with the electrical compound grease under multiple working conditions to obtain data of the resistance value and the temperature rise value of the sample under each of the multiple working conditions, so as to determine the linear interval and the inflection point value of the resistance value or the temperature rise value under each working condition, includes:
the method comprises the steps of carrying out thermoelectric combined test on a to-be-tested sample coated with electric composite grease under various working conditions by using a test circuit, obtaining data of a resistance value and a temperature rise value of the to-be-tested sample under each working condition in the various working conditions, increasing current passing through the to-be-tested sample when no inflection point appears in the resistance value and the temperature rise value, and stopping the thermoelectric combined test until the inflection point appears in one of the resistance value or the temperature rise value.
4. A system for establishing an electrical composite grease accelerated aging model, the system comprising:
the device comprises an obtaining device, a test circuit and a control device, wherein the obtaining device is used for carrying out a combined heat and power test on a to-be-tested sample coated with electric composite grease under various working conditions by utilizing the test circuit to obtain data of a resistance value and a temperature rise value of the to-be-tested sample under each working condition in various working conditions so as to determine a linear interval and an inflection point value of the resistance value or the temperature rise value under each working condition;
the test device is used for carrying out a combined heat and power test on a to-be-tested sample coated with the electric composite grease under various working conditions by using a test circuit, obtaining real-time data of the resistance value and the temperature rise value of the to-be-tested sample under the current working condition, and determining whether the real-time data of the resistance value or the temperature rise value of the to-be-tested sample is linearly increased or not; and stopping the combined heat and power test if the real-time data of the resistance value or the temperature rise value is not linearly increased; if the test unit determines that the real-time data of the resistance value or the temperature rise value is linearly increased, performing a combined heat and power test on the to-be-tested sample coated with the electric composite grease under the next working condition, and stopping the combined heat and power test until one of the real-time data of the resistance value or the temperature rise value is not linearly increased;
a determination device that determines whether a difference between the resistance value or the inflection point value of the temperature increase value in each of the plurality of operating conditions is within a predetermined range,
the device for establishing the electric power composite grease comprises a device for establishing an initial model based on Weibull distribution if the difference value between the inflection point values of the resistance value or the temperature rise value under each working condition in a plurality of working conditions is within a preset range and the aging principle of the electric power composite grease is the same; the electric composite grease accelerated aging model based on Weibull distribution is as follows:
lnη=a1+a2I(1+)R+b1/T+b2I(1+)/T,
wherein eta is the characteristic life of Weibull distribution, T is the absolute temperature, I is the current passing through the sample to be tested, R is the resistance value of the electric connection part without being coated with the electric composite grease, R is the change value of the resistance value of the electric connection part after being coated with the electric composite grease, and a1, a2, b1 and b2 are constants; performing multiple linear regression analysis on initial parameters in the initial model according to data of the resistance value and the temperature rise value under each working condition in multiple working conditions to determine a Weibull distribution-based electric power compound grease accelerated aging model
Wherein the test circuit comprises: the device comprises a 220V alternating current power supply, a self-coupling voltage regulator, a step-down transformer, a protective resistor, a coupling capacitor, a combined heat and power test box, a to-be-tested sample, a grounding wire and a grounding end;
the 220V alternating current power supply is an input power supply and is connected to two ends of the self-coupling voltage regulator;
the self-coupling voltage regulator is used for regulating the test voltage;
one end of the primary side of the step-down transformer is connected to the adjustable end of the self-coupling regulator and used for reducing voltage, and the other end of the primary side of the step-down transformer is grounded;
the protective resistor plays a role of current-limiting protection and is connected to one end of the secondary side of the step-down transformer;
the coupling capacitor is connected with one end of the protective resistor and the other end of the secondary side of the step-down transformer and used for returning the test voltage to the console for displaying;
one end of the combined heat and power test box is connected with one end of the coupling capacitor, the other end of the combined heat and power test box is grounded, the combined heat and power test box is used for accommodating a to-be-tested sample, the inner size of the combined heat and power test box is 1000 multiplied by 1000mm, the adjustable temperature range is-60-100 ℃, and the temperature fluctuation degree is +/-0.2 ℃;
the test sample to be tested comprises a test electrode and a sample, wherein the sample is the electric composite grease;
the grounding wire is used for connecting the grounding end with the grounding electrode;
and the grounding end is used for grounding in a test mode.
5. The system as claimed in claim 4, wherein the obtaining device performs the combined heat and power test on the test object coated with the electrical compound grease under a plurality of working conditions by using the test circuit, obtains data of the resistance value and the temperature rise value of the test object under each working condition, and stops the combined heat and power test when an inflection point appears in one of the resistance value or the temperature rise value.
6. The system as claimed in claim 4, wherein the obtaining device performs the combined heat and power test on the sample coated with the electric compound grease under a plurality of operating conditions by using the test circuit, obtains data of the resistance value and the temperature rise value of the sample under each operating condition, and increases the current passing through the sample when the resistance value and the temperature rise value do not have an inflection point, and stops the combined heat and power test until the inflection point appears in one of the resistance value and the temperature rise value.
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