CN106053158A - Greenhouse gas sampling bottle - Google Patents
Greenhouse gas sampling bottle Download PDFInfo
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- CN106053158A CN106053158A CN201610554565.3A CN201610554565A CN106053158A CN 106053158 A CN106053158 A CN 106053158A CN 201610554565 A CN201610554565 A CN 201610554565A CN 106053158 A CN106053158 A CN 106053158A
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- 238000005070 sampling Methods 0.000 title claims abstract description 41
- 239000005431 greenhouse gas Substances 0.000 title claims abstract description 18
- 229920005549 butyl rubber Polymers 0.000 claims abstract description 31
- 239000007789 gas Substances 0.000 claims abstract description 26
- 239000004033 plastic Substances 0.000 claims abstract description 24
- 238000007789 sealing Methods 0.000 claims description 3
- 238000004458 analytical method Methods 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 230000009286 beneficial effect Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 229920001971 elastomer Polymers 0.000 description 2
- 238000002347 injection Methods 0.000 description 2
- 239000007924 injection Substances 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 230000007547 defect Effects 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000000284 extract Substances 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 238000004817 gas chromatography Methods 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
Classifications
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/02—Devices for withdrawing samples
- G01N1/22—Devices for withdrawing samples in the gaseous state
- G01N1/24—Suction devices
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
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- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Sampling And Sample Adjustment (AREA)
Abstract
本发明提出了一种温室气体采样瓶,其包括瓶身、滑动活塞、丁基胶塞、以及塑料瓶盖,其中所述瓶身呈中空的圆柱状,所述瓶身沿竖直方向延伸,所述滑动活塞安装在瓶身的顶端,瓶身顶端留一正方形压孔,所述丁基胶塞安装在瓶身的底端,所述塑料瓶盖位于瓶身的下方,通过螺旋丝口盖住瓶底,同时起到固定丁基胶塞的作用,防止瓶身漏气,且所述塑料瓶盖中间开设有直径为5mm的圆孔,所述圆孔用于采样时采样针可以直接穿过丁基胶塞,将气体注入瓶子中,同时测样时,进样针可以直接插入丁基胶塞,抽取瓶中的气体。
The present invention proposes a greenhouse gas sampling bottle, which includes a bottle body, a sliding piston, a butyl rubber stopper, and a plastic bottle cap, wherein the bottle body is a hollow cylinder, and the bottle body extends vertically. The sliding piston is installed on the top of the bottle body, a square pressure hole is left on the top of the bottle body, the butyl rubber plug is installed on the bottom end of the bottle body, the plastic bottle cap is located below the bottle body, and the screw thread cap Hold the bottom of the bottle, and at the same time play the role of fixing the butyl rubber stopper to prevent the bottle body from leaking, and a round hole with a diameter of 5mm is opened in the middle of the plastic bottle cap, and the sampling needle can be directly passed through the round hole when sampling. Through the butyl rubber stopper, the gas is injected into the bottle. At the same time, when measuring samples, the sampling needle can be directly inserted into the butyl rubber stopper to extract the gas in the bottle.
Description
技术领域technical field
本发明涉及一种采样瓶,尤其是涉及一种温室气体采样瓶。The invention relates to a sampling bottle, in particular to a greenhouse gas sampling bottle.
背景技术Background technique
当前温室气体研究中,多采用气相色谱分析,需要使用真空瓶采样。真空瓶采样一方面抽真空麻烦,真空度不好也会影响结果的准确性,另一方面,分析测定时从真空瓶抽取一次样品后,瓶内气体压力发生变化,第二次再抽取气体时,就跟第一次抽取的气体在浓度和压力方面有差异,如果第一次抽样体积偏大,由于压力问题,第二次就很难从中抽取气体来。为了克服利用真空瓶采样的缺点,我们发明一种不需要抽真空的采样瓶装置,本装置最大特点一是不用抽真空,二是进样抽样时能保持瓶内压力稳定,使得每次抽样取的气体样品基本一致。In the current greenhouse gas research, gas chromatography analysis is mostly used, and vacuum bottle sampling is required. On the one hand, it is troublesome to vacuumize the vacuum bottle sampling, and the poor vacuum degree will also affect the accuracy of the results. On the other hand, after the sample is drawn from the vacuum bottle once during analysis and measurement, the gas pressure in the bottle changes, and when the gas is drawn again , just as the concentration and pressure of the gas extracted for the first time are different, if the volume of the first sampling is too large, due to the pressure problem, it will be difficult to extract gas from it for the second time. In order to overcome the shortcomings of using vacuum bottles for sampling, we invented a sampling bottle device that does not require vacuuming. The gas samples are basically the same.
综上可知,现有技术存在如下缺点:1.抽真空麻烦,费时费力;2.真空度不够会影响结果准确定;3.进样时每抽取一次,瓶内压力和浓度会发生变化,影响下一次抽样,不利于多个指标的同时分析。鉴于上述缺陷,实有必要加以改进。In summary, the existing technology has the following disadvantages: 1. Vacuuming is troublesome, time-consuming and laborious; 2. Insufficient vacuum will affect the accuracy of the results; 3. Every time the sample is drawn, the pressure and concentration in the bottle will change, affecting The next sampling is not conducive to the simultaneous analysis of multiple indicators. In view of above-mentioned defective, be necessary to improve really.
发明内容Contents of the invention
本发明提出一种温室气体采样瓶,解决了现有技术抽真空麻烦,费时费力的缺陷。The invention proposes a greenhouse gas sampling bottle, which solves the defects of troublesome vacuuming and time-consuming and labor-intensive problems in the prior art.
本发明的技术方案是这样实现的:Technical scheme of the present invention is realized like this:
一种温室气体采样瓶,其包括瓶身、滑动活塞、丁基胶塞、以及塑料瓶盖,其中所述瓶身呈中空的圆柱状,所述瓶身沿竖直方向延伸,所述滑动活塞安装 在瓶身的顶端,瓶身顶端留有正方形压孔,所述丁基胶塞安装在瓶身的底端,所述塑料瓶盖位于瓶身的下方,通过螺旋丝口盖住瓶身底部,同时起到固定丁基胶塞的作用,防止瓶身漏气,且所述塑料瓶盖中间开设有直径为5mm的圆孔,所述圆孔用于采样时采样针可以直接穿过丁基胶塞,将气体注入瓶子中,同时测样时,进样针可以直接插入丁基胶塞,抽取瓶中的气体。A greenhouse gas sampling bottle, which includes a bottle body, a sliding piston, a butyl rubber stopper, and a plastic bottle cap, wherein the bottle body is a hollow cylinder, the bottle body extends vertically, and the sliding piston Installed on the top of the bottle body, there is a square pressure hole on the top of the bottle body, the butyl rubber stopper is installed at the bottom of the bottle body, the plastic bottle cap is located below the bottle body, and covers the bottom of the bottle body through the screw thread mouth , and at the same time play the role of fixing the butyl rubber stopper to prevent the bottle body from leaking, and a round hole with a diameter of 5mm is opened in the middle of the plastic bottle cap, and the sampling needle can pass through the butyl rubber directly through the round hole when sampling. The rubber stopper is used to inject gas into the bottle, and when measuring samples, the sampling needle can be directly inserted into the butyl rubber stopper to extract the gas in the bottle.
与现有技术相比,本发明具有如下有益效果:随着滑动活塞的运动,既可以赶走瓶内的气体,不需要抽真空,又可以通过丁基胶塞向瓶中注入气体,进行采样,同时进样时还能通过活塞的滑动改变体积而保持瓶内稳定的压力,有利于一次采样后多次进样和一个样同时测定多个指标。Compared with the prior art, the present invention has the following beneficial effects: With the movement of the sliding piston, the gas in the bottle can be driven away without vacuuming, and the gas can be injected into the bottle through the butyl rubber stopper for sampling At the same time, the volume can be changed through the sliding of the piston to maintain a stable pressure in the bottle during sample injection, which is conducive to multiple sample injections after one sample and simultaneous determination of multiple indicators in one sample.
本发明进一步的改进如下:Further improvement of the present invention is as follows:
进一步地,所述丁基胶塞的圆柱形凸起刚好能塞进瓶身,并密封不漏气。Further, the cylindrical protrusion of the butyl rubber stopper is just enough to be inserted into the body of the bottle, and the seal is airtight.
进一步地,所述瓶身由圆柱形塑料筒的构成。Further, the bottle body is made of a cylindrical plastic barrel.
进一步地,所述瓶身的底端外壁设有内螺纹。Further, the bottom outer wall of the bottle body is provided with internal threads.
进一步地,所述塑料瓶盖内的设有与瓶身低端外壁螺纹相配合的螺纹。Further, the inside of the plastic bottle cap is provided with threads that match the threads on the outer wall of the lower end of the bottle body.
进一步地,所述滑动活塞形似注射器的活塞,但长度只有2cm,既可以随瓶内气体压力的改变而滑动又可以起密封作用。Further, the sliding piston is similar to the piston of a syringe, but the length is only 2 cm, which can slide with the change of the gas pressure in the bottle and can also play a sealing role.
进一步地,所述滑动活塞的顶部直径大于滑动活塞的尾部直径。Further, the diameter of the top of the sliding piston is larger than the diameter of the tail of the sliding piston.
进一步地,所述滑动活塞的顶部与瓶身内径相配。Further, the top of the sliding piston matches the inner diameter of the bottle body.
附图说明Description of drawings
为了更清楚地说明本发明实施例或现有技术中的技术方案,下面将对实施例或现有技术描述中所需要使用的附图作简单地介绍,显而易见地,下面描述中的附图仅仅是本发明的一些实施例,对于本领域普通技术人员来讲,在不付出创造性劳动性的前提下,还可以根据这些附图获得其他的附图。In order to more clearly illustrate the technical solutions in the embodiments of the present invention or the prior art, the following will briefly introduce the drawings that need to be used in the description of the embodiments or the prior art. Obviously, the accompanying drawings in the following description are only These are some embodiments of the present invention. For those skilled in the art, other drawings can also be obtained according to these drawings without any creative effort.
图1为本发明的温室气体采样瓶的示意图。Fig. 1 is a schematic diagram of the greenhouse gas sampling bottle of the present invention.
其中:温室气体采样瓶100,瓶身11,滑动活塞12,丁基胶塞13,塑料瓶盖14,外螺纹15,瓶盖内螺纹16,瓶身顶部17,压孔18,圆孔20。Among them: greenhouse gas sampling bottle 100, bottle body 11, sliding piston 12, butyl rubber stopper 13, plastic bottle cap 14, external thread 15, bottle cap internal thread 16, bottle top 17, pressure hole 18, round hole 20.
具体实施方式detailed description
下面将结合本发明实施例中的附图,对本发明实施例中的技术方案进行清楚、完整地描述,显然,所描述的实施例仅仅是本发明一部分实施例,而不是全部的实施例。基于本发明中的实施例,本领域普通技术人员在没有作出创造性劳动前提下所获得的所有其他实施例,都属于本发明保护的范围。The following will clearly and completely describe the technical solutions in the embodiments of the present invention with reference to the accompanying drawings in the embodiments of the present invention. Obviously, the described embodiments are only some of the embodiments of the present invention, not all of them. Based on the embodiments of the present invention, all other embodiments obtained by persons of ordinary skill in the art without creative efforts fall within the protection scope of the present invention.
如图1所示,一种温室气体采样瓶100,其包括瓶身11、滑动活塞12、丁基胶塞13、以及塑料瓶盖14。As shown in FIG. 1 , a greenhouse gas sampling bottle 100 includes a bottle body 11 , a sliding piston 12 , a butyl rubber stopper 13 , and a plastic bottle cap 14 .
所述瓶身11呈中空的圆柱状,所述瓶身11沿竖直方向延伸。所述滑动活塞12安装在瓶身11的顶端,瓶身11顶端留有一正方形压孔18。所述丁基胶塞13安装在瓶身11的底端,所述塑料瓶盖14位于瓶身11的下方,通过螺旋丝口盖住瓶底,同时起到固定丁基胶塞13的作用,防止瓶身漏气,且所述塑料瓶盖14中间开设有直径为5mm的圆孔20,该圆孔用于采样时注入气体和进样时抽出气体,瓶盖14的内螺旋丝16正好跟瓶身底部外螺纹15相配合,从而固定丁基胶塞13,防止瓶身11漏气。所述圆孔20用于采样时采样针可以直接穿过丁基胶塞13,将气体注入瓶子中,同时测样时,进样针可以直接插入丁基胶塞13,抽取瓶中的气体。The bottle body 11 is a hollow cylinder, and the bottle body 11 extends vertically. The sliding piston 12 is installed on the top of the bottle body 11, and a square pressure hole 18 is left on the top of the bottle body 11. Described butyl rubber stopper 13 is installed on the bottom of bottle body 11, and described plastic bottle cap 14 is positioned at the below of bottle body 11, covers the bottom of bottle by screw thread mouth, plays the effect of fixing butyl rubber stopper 13 simultaneously, Prevent the bottle body from leaking, and the middle of the plastic bottle cap 14 is provided with a circular hole 20 with a diameter of 5mm. This circular hole is used for injecting gas during sampling and extracting gas during sampling. The outer threads 15 at the bottom of the bottle body are matched to fix the butyl rubber stopper 13 to prevent the bottle body 11 from leaking. When the circular hole 20 is used for sampling, the sampling needle can directly pass through the butyl rubber stopper 13 to inject gas into the bottle, and when measuring samples, the sampling needle can be directly inserted into the butyl rubber stopper 13 to extract the gas in the bottle.
所述丁基胶塞13的圆柱形凸起刚好能塞进瓶身11,并密封不漏气,底端能盖住瓶身的口。所述瓶身11由圆柱形塑料筒的构成。所述瓶身11的底端外壁设有螺纹15。所述塑料瓶盖14的顶部设有与瓶身11低端外壁螺纹配合的螺纹16。所述滑动活塞12形似注射器的活塞,但长度只有2cm,既可以随瓶内气体 压力的改变而滑动又可以起密封作用。The cylindrical protrusion of the butyl rubber stopper 13 can just be plugged into the bottle body 11, and is sealed airtight, and the bottom end can cover the mouth of the bottle body. The bottle body 11 is made of a cylindrical plastic tube. The bottom outer wall of the bottle body 11 is provided with threads 15 . The top of the plastic bottle cap 14 is provided with a screw thread 16 threadedly engaged with the outer wall of the lower end of the bottle body 11 . Described sliding piston 12 is shaped like the piston of syringe, but length has only 2cm, both can slide with the change of gas pressure in the bottle and can play sealing effect again.
所述按压孔18正对着滑动活塞12的尾部中央位置。所述滑动活塞12的顶部直径大于滑动活塞12的尾部直径。所述滑动活塞12的顶部直径与瓶身11的内径密切相配。The pressing hole 18 is facing the central position of the tail of the sliding piston 12 . The diameter of the top of the sliding piston 12 is larger than the diameter of the tail of the sliding piston 12 . The top diameter of the sliding piston 12 closely matches the inner diameter of the bottle body 11 .
温室气体采样瓶100的制造方法如下:The manufacturing method of the greenhouse gas sampling bottle 100 is as follows:
第一步:瓶身的制作,瓶身可由一定直径的圆柱形塑料筒,一端即底部外口有螺旋丝口,以便配塑料盖子,瓶身内部光滑均匀,一般滑动活塞可以像注射器的活塞一样可滑动。瓶身另一端即顶部粘结有中央留有正方形压孔的塑料盖。The first step: the production of the bottle body, the bottle body can be made of a cylindrical plastic barrel with a certain diameter, and one end, that is, the bottom outer mouth, has a screw thread mouth, so that it can be equipped with a plastic cap. The inside of the bottle body is smooth and even, and the general sliding piston can be like the piston of a syringe Can slide. The other end of the bottle body, that is, the top, is bonded with a plastic cover with a square pressure hole in the center.
第二步:活动活塞的制作,活动活塞的外径跟瓶身内径相配,既能滑动,又能密封不漏气,就像注射器的活塞一样。The second step: the production of the movable piston. The outer diameter of the movable piston matches the inner diameter of the bottle body, which can not only slide, but also seal airtight, just like the piston of a syringe.
第三步:丁基胶塞,丁基胶塞圆柱形凸起刚好能塞进瓶身,并密封不漏气,底部能盖住瓶身的口。The third step: butyl rubber stopper, the cylindrical protrusion of the butyl rubber stopper is just enough to be inserted into the bottle body, and it is sealed and airtight, and the bottom of the butyl rubber stopper can cover the mouth of the bottle body.
第四部:塑料外盖,外盖内螺纹跟瓶身底部外螺纹相配,以便能盖住底部并起固定胶塞,防止漏气的作用。塑料盖中间开直径5mm的圆孔,供采样注入气体和测样时抽取气体之用。The fourth part: Plastic outer cover, the inner thread of the outer cover matches the outer thread of the bottom of the bottle body, so as to cover the bottom and fix the rubber stopper to prevent air leakage. A circular hole with a diameter of 5mm is opened in the middle of the plastic cover for sampling the injected gas and extracting the gas during sampling.
与现有技术相比,本发明具有如下有益效果:随着滑动活塞的移动,既可以赶走瓶身里空气,不用抽真空,又可以通过丁基胶塞注入气体样品,同时测样时通过丁基胶塞抽取气体时,因压力改变,活塞也会滑动,而保持瓶身内稳定的气体样品体积和压力,不影响下次抽取气体,满足多次和多个指标的测定。Compared with the prior art, the present invention has the following beneficial effects: with the movement of the sliding piston, the air in the bottle can be driven away without vacuuming, and the gas sample can be injected through the butyl rubber plug, and at the same time, the sample can be measured through When the butyl rubber stopper extracts gas, the piston will also slide due to the pressure change, so as to maintain a stable gas sample volume and pressure in the bottle, which will not affect the next extraction of gas, and can meet the determination of multiple and multiple indicators.
以上所述仅为本发明的较佳实施例而已,并不用以限制本发明,凡在本发明的精神和原则的内,所作的任何修改、等同替换、改进等,均应包含在本发明的保护范围的内。The above descriptions are only preferred embodiments of the present invention, and are not intended to limit the present invention. Any modifications, equivalent replacements, improvements, etc. made within the spirit and principles of the present invention shall be included in the scope of the present invention. within the scope of protection.
Claims (8)
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CN113358426A (en) * | 2021-06-11 | 2021-09-07 | 重庆师范大学 | Acquisition device and method for measuring emission contribution of endogenous greenhouse gases in shallow water body |
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CN105223044A (en) * | 2015-09-18 | 2016-01-06 | 国网河南伊川县供电公司 | A kind of safe collector of gas relay |
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CN113358426A (en) * | 2021-06-11 | 2021-09-07 | 重庆师范大学 | Acquisition device and method for measuring emission contribution of endogenous greenhouse gases in shallow water body |
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Application publication date: 20161026 |