CN105995369A - Radix polygonati officinalis healthcare compound particle - Google Patents
Radix polygonati officinalis healthcare compound particle Download PDFInfo
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- CN105995369A CN105995369A CN201610355062.3A CN201610355062A CN105995369A CN 105995369 A CN105995369 A CN 105995369A CN 201610355062 A CN201610355062 A CN 201610355062A CN 105995369 A CN105995369 A CN 105995369A
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Preparation or treatment thereof
- A23L2/385—Concentrates of non-alcoholic beverages
- A23L2/39—Dry compositions
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Preparation or treatment thereof
- A23L2/52—Adding ingredients
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Preparation or treatment thereof
- A23L2/52—Adding ingredients
- A23L2/58—Colouring agents
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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Abstract
The invention provides a healthcare compound particle which is processed and produced by radix polygonati officinalis slices, mulberry fruits and fresh blueberry fruits. A preparation method for the healthcare compound particle comprises the following steps of: crushing radix polygonati officinalis and mixing the crushed radix polygonati officinalis with mulberry fruit residues; adding water and pectase to carry out enzymolysis; adding saccharose, a proper amount of yeast powder and lactobacillus powder to carry out anaerobic fermentation; filtering to obtain a radix polygonati officinalis feed liquid; and adding xylitol, mulberry pigment and sodium carboxymethyl cellulose to carry out spray-drying, thereby obtaining the radix polygonati officinalis healthcare compound particle. The radix polygonati officinalis is subjected to enzymolysis and fermentation, so that content of polysaccharides in the compound healthcare particle is effectively increased, smell of the radix polygonati officinalis is covered, and the anti-oxidization function of the compound healthcare particle is increased. The mulberry and the blueberry pigment are extracted and directly added into beverage, so that damages of lactic acid bacteria and saccharomycetes on mulberry pigment and blueberry pigment are effectively prevented in a fermentation process, and therefore, the anti-oxidization effect of the blueberry pigment is kept to the greatest extent. Meanwhile, the content of natural anthocyanin in finished product beverage is effectively improved, so that the natural healthcare effects of the blueberries and the mulberries are kept to the greatest extent.
Description
Technical field
The invention belongs to the technical field of food processing, relate to the production technology of a kind of Rhizoma Polygonati Odorati beverage, more specifically relate to
And one utilizes Rhizoma Polygonati Odorati sheet and Mulberry fruit and blueberry fresh fruit to be processed producing health care composite particles.
Background technology
Rhizoma Polygonati Odorati is medicine-food two-purpose medical material, tool yin nourishing, moisturize, heat clearing away, promote the production of body fluid, the effect such as cough-relieving, as tonic, cure mainly
The diseases such as consumption of YIN caused by febrile disease, deficiency-heat cough caused by dryness, heart disease, diabetes, tuberculosis, and high-grade nourishing food, delicacies and beverage can be made, have
Health-care effect, Rhizoma Polygonati Odorati root stock contains a large amount of Rhizoma Polygonati Odorati mucopolysaccharide, by D-Fructose, D-MANNOSE, D-Glucose and galacturonic acid
Being formed, mol ratio is 6:3:1:1.5；Rhizoma Polygonati Odorati levan A, B, C, D, AzeOH.The also spiral shell sterol Han Rhizoma Polygonati
Poa, Rhizoma Polygonati spiral shell sterol glycoside Pob, Poc, PO1, PO2, PO3, PO4, PO5, Rhizoma Polygonati furan sterol glycoside, Rhizoma Polygonati furan sterol glycoside Poc, Pod,
The steroids such as PO6, PO7, PO8 and PO9.
Blue berry has another name called blue berry, belongs to Ericaceae Vaccinium plant, and fruit is blueness, in addition to containing abundant nutrition material, also
There is anthocyanin etc. can prevent cerebral neurastheria, cardiac function enhancing, improving eyesight and the unique activity material such as anticancer, the most international
Food and agricultural organization is classified as one of big health food of the mankind five.China northeast, East China, Central China, South China start to plant on a large scale at present
Planting suitable blue berry kind, Blueberry color mostly is milky or pink, urceolus or bell, sustainable one month of florescence with
On.Anthocyanidin in Blueberry can promote that the rhodopsin in retina cell regenerates, pre-myopia prevention, promotes vision.Blue berry
Fruit can play the effect of regulation blood glucose, makes patient vessel expand, thus reduces blood pressure, and cardioprotection, kidney prevent diabetes
Complication.Blueberry contains a large amount of biological active substances, is referred to as in fruit and vegerable " number one antioxidant ", and Blueberry can be protected
Protect cell, it is to avoid destroyed by peroxide, Blueberry have prevent functional disorder, improve impermanent memory, improve old people
Balance and the effect such as harmony.Free radical harmful in anthocyanidin energy purged body in Blueberry, prevent wrinkle of skin
Generate ahead of time, reduce dermatosis and ripple, the anthocyanidin of Blueberry even eliminates cicatrix, dispelling stain, skin whitening, and
And make skin the most smooth, high resilience.Blueberry can also delay cranial nerve aging, improve effect of memory, reinforcing
Blood vessel, improvement circulation, improvement are slept, are delayed hypomnesis, prevention heart disease, prophylaxis of cancer.
Fructus Mori, has another name called Fructus Mori, Mulberry sugarcane, Mulberry Fructus Jujubae, sorosis, crow mulberry etc., for the fruit ear of moraceae plants Mulberry.Color when Fructus Mori is tender
Green grass or young crops, sour in the mouth, time aging, color purple is black, succulence, and taste is sweet.Ripe Mulberry fruit is nutritious, every 100 grams of Fructus Mori moisture contents 81.8 grams,
1.8 grams of protein, 0.3 gram of fat.Cellulose 4.9 grams, carbohydrate 10 grams, ash 1.2 grams, carotene 30 microgram, thiamine
Element 0.02 milligram, 0.06 milligram of riboflavin, vitamin E 6.95 milligrams, 33 milligrams of potassium, 0.27 milligram of zinc, copper 0.08 milligram, selenium
4.8 microgram.Additionally, possibly together with tannic acid, malic acid, vitamin C and fatty acid etc..Its fat predominantly linoleic acid, oleic acid, palmitin
Acid, stearic acid and a small amount of octanoic acid, n-nonanoic acid, capric acid, myristic acid, linolenic acid etc..Chinese medicine thinks that Fructus Mori liver and kidney tonifying, YIN nourishing are supported
Blood, endogenous wind stopping, have cure mainly palpitation and insomnia, have a dizzy spell, tinnitus, constipation night sweat, scrofula, the disease such as articular instability.
Fructus Mori have and improve skin (including scalp) blood supply, nutrition skin, make skin delicate and the effect such as black hair, and energy
Slow down aging.Fructus Mori are that middle-aged and elderly people is healthy and strong U.S. face, the good fruit of defying age and good medicine.Often food Fructus Mori can alleviate eyes with improving eyesight
Tired dry and astringent symptom.Fructus Mori have immunologic enhancement.Fructus Mori have effect of gain to spleen, have enhancing to make hemolytic reaction
With, human body artery hardening, skeletal joint hardening can be prevented, enhance metabolism.It can promote the growth of erythrocyte, prevents
Leukopenia, and the diseases such as treatment diabetes, anemia, hypertension, hyperlipidemia, coronary heart disease, neurasthenia are had auxiliary merit
Effect.Fructus Mori has the effects such as promoting the production of body fluid to quench thirst, facilitating digestion, help defecation, and proper amount of edible can promote gastric secretion, stimulates enterokinesia
And release scorching.Motherland's medical science is thought, Fructus Mori are sweet in flavor and cold in property, has the effects such as the liver and the kidney tonifying, intestine moistening of promoting the production of body fluid, black hair improving eyesight.For
This, we are processed with Rhizoma Polygonati Odorati, blue berry as primary raw material by certain formula, processing technique, prevent color and luster brown stain and precipitation from asking
Topic, it is ensured that the antioxidation of product, then be modulated its mixture, is prepared good mouthfeel, nutritious on a large scale
Wine.
Summary of the invention
Present invention aim to provide that a kind of method is simple, low cost, there is anti-oxidation function, be easy to industry metaplasia
Producing, products obtained therefrom contains natural Fructus Mori and Blueberry pigment, in good taste, nutritious composite beverage preparation method.
Therefore, first purpose of the present invention is to provide the preparation method of a kind of fragrant solomonseal health-care composite particles, and step includes:
A, Rhizoma Polygonati Odorati is pulverized after mix with Fructus Mori marc, after the weight water such as addition, adding pectase is stirred uniformly,
Adjusting pH is 2～5, and enzymolysis 2～5h is put in fermentation tank, obtained enzymolysis solution.
B, in enzymolysis solution, add 3～8% sucrose, appropriate yeast mycopowder and 2～4% lactobacillus powder, after stirring
Sealing carries out anaerobic fermentation, obtains fermentation liquid.
C, by after fermentation liquid filtered through gauze, then filter through microfilter, obtain Rhizoma Polygonati Odorati feed liquid.
D, by Rhizoma Polygonati Odorati feed liquid, xylitol, mulberry pigment, sodium carboxymethyl cellulose mix homogeneously by a certain percentage, obtain jade
Bamboo composite solution.
F, being spray-dried by Rhizoma Polygonati Odorati composite solution, inlet temperature is 165 DEG C～185 DEG C, leaving air temp be 65 DEG C～
85℃；The rotating speed 450 of sampling pump～700 revs/min, sample introduction pressure limit, 1～2MPa, obtains fragrant solomonseal health-care composite particles, room temperature
Lower storage.
Rhizoma Polygonati Odorati powder described in above-mentioned a step is 1kg:1～4kg with the weight ratio of Fructus Mori marc.
Pectase usage amount described in above-mentioned a step is 100～500g/100kg Fructus Mori marcs, at room temperature enzymolysis 2～
5h, wherein 1g pectinase activity requires at more than 3000IU, can buy from market purchasing and obtain.
% described in above-mentioned steps refers to solid kg and liquor capacity L ratio.
Add appropriate yeast described in above-mentioned b step and refer to weight kg is enzymolysis solution volume L the 2～5% of yeast powder；Send out
Ferment condition be fermentation temperature be 28～30 DEG C, fermentation time is 4～20 days.
Filtered through gauze described in above-mentioned step c refers to 2～3 layers of filtered through gauze, the pore size filter of microfilter be 0.6～
1.0μm。
Certain proportion described in above-mentioned Step d refers to Rhizoma Polygonati Odorati feed liquid 40～80 parts, mulberry pigment 10～20 parts, xylitol 5
～10 parts, sodium carboxymethyl cellulose 0.2～0.5 part.
Acquisition can directly be bought by above-mentioned yeast, it is also possible to obtain bacterium solution by conventional yeasts bacterium cultural method.
Above-mentioned lactic acid bacteria can directly buy acquisition, it is also possible to obtains bacterium solution by conventional lactic acid bacteria cultural method.
Second object of the present invention is to provide above-mentioned mulberry pigment and the preparation method of Fructus Mori marc, and its concrete steps are such as
Under:
(1) select Mulberry fruit and blueberry fresh fruit, after roguing is cleaned, crush with bruisher, obtain Fructus Mori pulp, add
A certain amount of ethanol water, with 0.1mol/L salt acid for adjusting pH value to 3.5～5.5, is stirred at room temperature extraction 20h～36h, mistake
Filter, repeats secondary, and merging filtrate, Fructus Mori marc is standby.
(2) filtrate carries out being evaporated to the 1/15～1/30 of original volume below 50 DEG C, upper LSA-20 macroporous resin
Absorption, with the 45 of 8BV～16BV～75% ethanol water carry out gradient elution, collect to obtain eluent.
(3) eluent is evaporated to do below 50 DEG C, obtains mulberry pigment.
Described in above-mentioned (1) step, the ratio of Mulberry fruit and blueberry fresh fruit is 2～5:3.
Adding the volume L of ethanol water described in above-mentioned steps (1) with the quality kg ratio of blueberry pulp is 3～6:1；Its
Middle ethanol water refers to 50～70% ethanol water.
The compound method of above-mentioned 50% ethanol water is: 50mL ethanol mixes after adding 50mL water.
Filter described in above-mentioned steps (1) and refer to 2～3 layers of filtered through gauze.
Described in above-mentioned steps (2), BV refers to column volume.
60% ethanol solution described in above-mentioned steps (2) refers to that 60mL ethanol mixes after adding 40mL water.
Technique effect:
1, by Rhizoma Polygonati Odorati is carried out enzymolysis and fermentation process, it is effectively increased polyoses content in compound health granule, covers again
Cover the abnormal smells from the patient of Rhizoma Polygonati Odorati itself, add the anti-oxidation function of compound health granule.
2, Fructus Mori and Blueberry pigment extraction are added directly in beverage again, effectively prevent during the fermentation, lactic acid
Bacterium and yeast, to mulberry pigment and the destruction of Blueberry pigment, at utmost retain Blueberry pigment antioxidation.Meanwhile, effectively
Improve the natural anthocyanidin content of finished beverage, farthest remain blue berry and natural health that Fructus Mori itself is had
Effect.
3, utilize the marc after extracting pigment through lactic acid bacteria and yeast fermentation, utilize the feature producing lactic acid, can be effective
Ground extends mulberry pigment and Blueberry pigment holding time, is also beneficial to improve the mouthfeel of this health care granule.
4, this health beverage both make use of Blueberry pigment to improve vision and oxidation resistance, makes full use of again blood sugar lowering in Fructus Mori
Class material, is allowed to more can be suitable for diabetes patients.
Detailed description of the invention
Below, the present invention will be further detailed by embodiment, but it is not limited to the arbitrary of these embodiments
Individual or similar example.
Embodiment one
Select the 150kg Mulberry fruit without rotting and 100kg blueberry fresh fruit raw material is cleaned, smashed to pieces, making beating, obtain Fructus Mori
Pulp.Taking 250kg Fructus Mori pulp, add 60% ethanol water 300L, with 0.1mol/L salt acid for adjusting pH value to 4, room temperature is stirred
Mixing extraction 24h, 2 layers of filtered through gauze, repeat secondary, merging filtrate, filtering residue is standby, and the filtrate of gained is concentrating under reduced pressure below 50 DEG C
To the 1/30 of original volume, upper LSA-20 macroporous resin adsorption, with the 45 of 12BV～75% ethanol water carry out gradient elution,
Collecting to obtain eluent, eluent is evaporated to do below 50 DEG C, obtains mulberry pigment.
Embodiment two
Gained Fructus Mori marc 150kg in Example one, adds Rhizoma Polygonati Odorati powder 100kg and water 250kg, adds pectase
250g, stirs, and adjusting pH is 3.5, after room temperature enzymolysis 4h, puts in fermentation tank, obtains about 400L enzymolysis solution.In enzymolysis solution
Add 20kg white sugar, 10kg yeast powder and 10kg lactic acid bacteria, seal after stirring, carry out anaerobic fermentation, control fermentation temperature
Degree is 28～30 DEG C, and fermentation time is 6 days, obtains fermentation liquid.With 3 layers of gauze by filtering fermentation liquor, then with aperture be 0.6～
The microfilter of 1.0 μm filters, and is Rhizoma Polygonati Odorati feed liquid.By 1.2kg Rhizoma Polygonati Odorati feed liquid, 100g xylitol, 400g Fructus Mori color
Element (gained in embodiment one), 6g sodium carboxymethyl cellulose, mix homogeneously, obtain Rhizoma Polygonati Odorati composite solution, directly carry out spray dried
Dry, inlet temperature is 165 DEG C～185 DEG C, and leaving air temp is 65 DEG C～85 DEG C；The rotating speed 450 of sampling pump～700 revs/min, sample introduction
Pressure limit, 1～2MPa, obtains fragrant solomonseal health-care composite particles, preserves under room temperature, uses anthrone-sulphate method to measure fragrant solomonseal rhizome polyoses
Content.
Embodiment three
Gained Fructus Mori marc 250kg in Example one, adds Rhizoma Polygonati Odorati powder 100kg and water 350kg, adds pectase
500g, stirs, and adjusting pH is 3.5, after room temperature enzymolysis 4h, puts in fermentation tank, obtains about 600L enzymolysis solution.In enzymolysis solution
Add 25kg white sugar, 15kg yeast powder and 12kg lactic acid bacteria, seal after stirring, carry out anaerobic fermentation, control fermentation temperature
Degree is 28～30 DEG C, and fermentation time is 8 days, obtains fermentation liquid.With 3 layers of gauze by filtering fermentation liquor, then with aperture be 0.6～
The microfilter of 1.0 μm filters, and is Rhizoma Polygonati Odorati feed liquid.By 1.5g Rhizoma Polygonati Odorati feed liquid, 120g xylitol, 350g mulberry pigment
(gained in embodiment one), 6g sodium carboxymethyl cellulose, mix homogeneously, obtain Rhizoma Polygonati Odorati composite solution, be directly spray-dried,
Inlet temperature is 165 DEG C～185 DEG C, and leaving air temp is 65 DEG C～85 DEG C；The rotating speed 450 of sampling pump～700 revs/min, sample introduction pressure
Power scope, 1～2MPa, obtains fragrant solomonseal health-care composite particles, preserves under room temperature.
Comparative examples one
Select the 150kg Mulberry fruit without rotting and 100kg blueberry fresh fruit raw material is cleaned, smashed to pieces, making beating, obtain Fructus Mori
Pulp, adds Rhizoma Polygonati Odorati powder 100kg and water 250kg, adds pectase 250g, stir, and adjusting pH is 3.5, room temperature enzymolysis 4h
After, put in fermentation tank, obtain about 400L enzymolysis solution；20kg white sugar, 10kg yeast powder and 10kg breast is added in enzymolysis solution
Acid bacterium, seals after stirring, and carries out anaerobic fermentation, and controlling fermentation temperature is 28～30 DEG C, and fermentation time is 6 days, is sent out
Ferment liquid.With 3 layers of gauze by filtering fermentation liquor, then filter with the microfilter that aperture is 0.6～1.0 μm, be jade
Bamboo feed liquid.By 1.2kg Rhizoma Polygonati Odorati feed liquid, 100g xylitol, 6g sodium carboxymethyl cellulose, mix homogeneously, obtain Rhizoma Polygonati Odorati composite solution,
Directly being spray-dried, inlet temperature is 165 DEG C～185 DEG C, and leaving air temp is 65 DEG C～85 DEG C；The rotating speed 450 of sampling pump
～700 revs/min, sample introduction pressure limit, 1～2MPa, obtains fragrant solomonseal health-care composite particles, preserves under room temperature.
Comparative examples two
Select the 150kg Mulberry fruit without rotting and 100kg blueberry fresh fruit raw material is cleaned, smashed to pieces, making beating, obtain blue berry
Pulp.Taking Rhizoma Polygonati Odorati powder 100kg, add water 250kg, add pectase 250g, stir, adjusting pH is 3.5, room temperature enzymolysis
After 4h, put in fermentation tank, obtain enzymolysis solution.20kg white sugar, 20kg yeast powder and 10kg lactic acid bacteria is added in enzymolysis solution,
Sealing after stirring, carry out anaerobic fermentation, controlling fermentation temperature is 28～30 DEG C, and fermentation time is 6 days, obtains fermentation liquid,
Add blueberry pulp, with 3 layers of gauze by filtering fermentation liquor, then carried out with the microfilter that aperture is 0.6～1.0 μm
Filter, is Rhizoma Polygonati Odorati feed liquid.By 1.2kg Rhizoma Polygonati Odorati feed liquid, 100g xylitol, 6g sodium carboxymethyl cellulose, mix homogeneously, obtain Rhizoma Polygonati Odorati
Composite solution, is directly spray-dried, and inlet temperature is 165 DEG C～185 DEG C, and leaving air temp is 65 DEG C～85 DEG C；Sampling pump
Rotating speed 450～700 revs/min, sample introduction pressure limit, 1～2MPa, obtains fragrant solomonseal health-care composite particles, under room temperature preserve.
Attached: the antioxidation contrast of various products
Precision weighs DPPH8.0mg, and with anhydrous alcohol solution and be settled in 200mL brown volumetric flask, obtaining concentration is
The DPPH solution of 0.004%, keeps in Dark Place, standby.After various sample 5g room temperatures are placed a period of time, DPPH reagent is used to enter
The mensuration of row antioxidation is shown in Table 1.
Table 1 various fragrant solomonseal health-care composite particles product is to DPPH antioxidation
Attached: DPPH method measures antioxidative concrete grammar: take respectively different trial each sample solution (0.24,0.48,
0.72,0.96,1.20mg/mL) 1.0mL, puts in 10mL centrifuge tube, adds the DPPH solution of 3.0mL, and room temperature lucifuge is reacted
30min, simultaneously with dehydrated alcohol as blank, measures light absorption value at 517nm wavelength.Calculate DPPH by following equation freely to remove
Rate.
The free clearance rate of DPPH (%)=A0-(AS-Ac)/A0× 100%
In formula, A0The absorbance of 1.0mL distilled water+3.0mLDPPH solution
AS1.0mL the absorbance of sample solution+3.0mLDPPH solution
AcThe absorbance of 1.0mL sample solution+3.0mL dehydrated alcohol
To test in triplicate, try to achieve the most on duty for the day of clearance rate.
Polyoses content contrast table in table 2 various fragrant solomonseal health-care composite particles product
| Product | Polyoses content/100g |
| Embodiment two | 25.25g |
| Embodiment three | 23.67g |
| Comparative examples one | 13.26g |
| Comparative examples two | 14.84g |
Claims (8)
1. a preparation method for fragrant solomonseal health-care composite particles, step includes:
A, Rhizoma Polygonati Odorati is pulverized after mix with Fructus Mori marc, after the weight water such as addition, adding pectase is stirred uniformly, tune pH
It is 2～5, enzymolysis 2～5h, put in fermentation tank, obtain enzymolysis solution.
B, in enzymolysis solution, add 3～8% sucrose, appropriate yeast mycopowder and 2～4% lactobacillus powder, seal after stirring
Carry out anaerobic fermentation, obtain fermentation liquid.
C, by after fermentation liquid filtered through gauze, then filter through microfilter, obtain Rhizoma Polygonati Odorati feed liquid.
D, by Rhizoma Polygonati Odorati feed liquid, xylitol, mulberry pigment, sodium carboxymethyl cellulose mix homogeneously by a certain percentage, obtain Rhizoma Polygonati Odorati multiple
Close solution.
F, being spray-dried by Rhizoma Polygonati Odorati composite solution, inlet temperature is 165 DEG C～185 DEG C, and leaving air temp is 65 DEG C～85 DEG C；
The rotating speed 450 of sampling pump～700 revs/min, sample introduction pressure limit, 1～2MPa, obtains fragrant solomonseal health-care composite particles, stores under room temperature
Hide.
2. the process of claim 1 wherein that Rhizoma Polygonati Odorati powder described in a step is 1kg:1～4kg with the weight ratio of Fructus Mori marc；Really
Glue enzyme usage amount is 100～500g/100kg Fructus Mori marcs.
3. the process of claim 1 wherein that adding appropriate yeast described in b step refers to that weight kg of yeast powder is enzymolysis liquid
The 2～5% of long-pending L；Fermentation condition be fermentation temperature be 28～30 DEG C, fermentation time is 4～20 days.
4. the process of claim 1 wherein that filtered through gauze described in step c refers to 2～3 layers of filtered through gauze, microfilter
Pore size filter is 0.6～1.0 μm.
5. the process of claim 1 wherein that certain proportion described in Step d refers to Rhizoma Polygonati Odorati feed liquid 40～80 parts, mulberry pigment 10
～20 parts, xylitol 5～10 parts, sodium carboxymethyl cellulose 0.2～0.5 part.
6. the method for Claims 1 to 5, wherein said mulberry pigment and the preparation method of Fructus Mori marc, it specifically comprises the following steps that
(1) select Mulberry fruit and blueberry fresh fruit, after roguing is cleaned, crush with bruisher, obtain Fructus Mori pulp, add certain
The ethanol water of amount, with 0.1mol/L salt acid for adjusting pH value to 3.5～5.5, is stirred at room temperature extraction 20h～36h, filters, weight
Multiple secondary, merging filtrate, Fructus Mori marc is standby.
(2) filtrate carries out being evaporated to the 1/15～1/30 of original volume below 50 DEG C, upper LSA-20 macroporous resin adsorption,
With the 45 of 8BV～16BV～75% ethanol water carry out gradient elution, collect to obtain eluent.
(3) eluent is evaporated to do below 50 DEG C, obtains mulberry pigment.
7. the method for claim 6, wherein described in (1) step, the ratio of Mulberry fruit and blueberry fresh fruit is 2～5:3.
8. the method for claim 6, wherein adds the volume L of ethanol water and the quality of blueberry pulp described in (1) step
Kg ratio is 3～6:1；Wherein ethanol water refers to 50～70% ethanol water.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106901363A (en) * | 2017-03-02 | 2017-06-30 | 云南省林业科学院 | A kind of preparation method of olive pomace ferment |
| CN106923128A (en) * | 2017-04-25 | 2017-07-07 | 怀化学院 | A kind of radix polygonati officinalis lactic fermentation health drink and preparation method thereof |
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| CN106923128A (en) * | 2017-04-25 | 2017-07-07 | 怀化学院 | A kind of radix polygonati officinalis lactic fermentation health drink and preparation method thereof |
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