CN105968941A - Aqueous printing ink color sheet pigment and preparation method thereof - Google Patents
Aqueous printing ink color sheet pigment and preparation method thereof Download PDFInfo
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- CN105968941A CN105968941A CN201610551468.9A CN201610551468A CN105968941A CN 105968941 A CN105968941 A CN 105968941A CN 201610551468 A CN201610551468 A CN 201610551468A CN 105968941 A CN105968941 A CN 105968941A
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- ink color
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- 239000000049 pigment Substances 0.000 title claims abstract description 25
- 238000002360 preparation method Methods 0.000 title claims abstract description 9
- 238000003756 stirring Methods 0.000 claims abstract description 32
- 239000012860 organic pigment Substances 0.000 claims abstract description 16
- 239000012065 filter cake Substances 0.000 claims abstract description 11
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims description 45
- HZAXFHJVJLSVMW-UHFFFAOYSA-N 2-Aminoethan-1-ol Chemical compound NCCO HZAXFHJVJLSVMW-UHFFFAOYSA-N 0.000 claims description 28
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims description 28
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 28
- RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 claims description 27
- KHPCPRHQVVSZAH-HUOMCSJISA-N Rosin Natural products O(C/C=C/c1ccccc1)[C@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 KHPCPRHQVVSZAH-HUOMCSJISA-N 0.000 claims description 27
- KHPCPRHQVVSZAH-UHFFFAOYSA-N trans-cinnamyl beta-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OCC=CC1=CC=CC=C1 KHPCPRHQVVSZAH-UHFFFAOYSA-N 0.000 claims description 27
- 239000013530 defoamer Substances 0.000 claims description 14
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims description 13
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 13
- 239000004925 Acrylic resin Substances 0.000 claims description 13
- 229920000178 Acrylic resin Polymers 0.000 claims description 13
- 239000002270 dispersing agent Substances 0.000 claims description 12
- 239000000047 product Substances 0.000 claims description 11
- 238000004090 dissolution Methods 0.000 claims description 10
- 238000004898 kneading Methods 0.000 claims description 10
- 239000011259 mixed solution Substances 0.000 claims description 10
- 238000000034 method Methods 0.000 claims description 4
- 230000014759 maintenance of location Effects 0.000 claims description 2
- 238000002156 mixing Methods 0.000 abstract description 2
- 239000000203 mixture Substances 0.000 abstract 3
- 238000006243 chemical reaction Methods 0.000 abstract 2
- 239000001913 cellulose Substances 0.000 abstract 1
- 229920002678 cellulose Polymers 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- 230000018044 dehydration Effects 0.000 abstract 1
- 238000006297 dehydration reaction Methods 0.000 abstract 1
- 239000004014 plasticizer Substances 0.000 abstract 1
- 230000002265 prevention Effects 0.000 abstract 1
- 239000011347 resin Substances 0.000 abstract 1
- 229920005989 resin Polymers 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
- 239000003381 stabilizer Substances 0.000 abstract 1
- 230000000052 comparative effect Effects 0.000 description 6
- 238000004519 manufacturing process Methods 0.000 description 6
- 239000011248 coating agent Substances 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
- 239000006185 dispersion Substances 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000008187 granular material Substances 0.000 description 2
- 238000012805 post-processing Methods 0.000 description 2
- HMUNWXXNJPVALC-UHFFFAOYSA-N 1-[4-[2-(2,3-dihydro-1H-inden-2-ylamino)pyrimidin-5-yl]piperazin-1-yl]-2-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)ethanone Chemical compound C1C(CC2=CC=CC=C12)NC1=NC=C(C=N1)N1CCN(CC1)C(CN1CC2=C(CC1)NN=N2)=O HMUNWXXNJPVALC-UHFFFAOYSA-N 0.000 description 1
- YLZOPXRUQYQQID-UHFFFAOYSA-N 3-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)-1-[4-[2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidin-5-yl]piperazin-1-yl]propan-1-one Chemical compound N1N=NC=2CN(CCC=21)CCC(=O)N1CCN(CC1)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F YLZOPXRUQYQQID-UHFFFAOYSA-N 0.000 description 1
- AFCARXCZXQIEQB-UHFFFAOYSA-N N-[3-oxo-3-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)propyl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(CCNC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 AFCARXCZXQIEQB-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000004040 coloring Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000011164 primary particle Substances 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- 238000000275 quality assurance Methods 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
- C09D11/037—Printing inks characterised by features other than the chemical nature of the binder characterised by the pigment
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The invention discloses a preparation method of an aqueous printing ink color sheet pigment and relates to an organic pigment. The aqueous printing ink color sheet pigment is prepared by the following steps: mixing a filter cake with cellulose, a plasticizer, a stabilizer, resin and the like and putting the mixture into a reaction container; under stirring, raising the temperature and adding a hydrophilic chain solvent solution into the reaction container; stirring, keeping the heat, reacting and extruding until the mixture is uniform; and carrying out dehydration post-treatment on the mixture and drawing into a sheet shape, and crushing into the pigment color sheet. Ways of beading, granulating, sheeting and adding a flying prevention agent and the like can be obtained and the organic application pigment with non-flying property and easiness of being metered is obtained.
Description
Technical field
The invention belongs to pigment ink field, particularly to a kind of water color ink color chips pigment and preparation method thereof.
Background technology
Relatively pigment dispersion before form, the original color obtained by production process is referred to as wet cake, also needs further commercial treatment, including pulverize and be dried etc. process.In dry run, thin granules of pigments can produce cohesion so that it is particle diameter is compared with the big manyfold of primary granule, thus cannot be directly used to coloring.As also needing to three steps before pigment uses from the point of view of user: moistening → refinement → stabilisation mixing dispersion.Traditional commercialization is run counter in application.Through technical finesse province and user major part production process and optimize the important quality index such as produced ink and the color strength of coating, fineness, glossiness with pigment building-up process primary partical, grinding man-hour when producing coating is greatly shortened.Primary partical approach makes pigment manufacturing process avoid dry/pulverizing process.
Summary of the invention
Solve the technical problem that: for the demand, invention especially provides a kind of water color ink color chips pigment and preparation method thereof.
Technical scheme: in order to solve the problems referred to above, the invention discloses a kind of water color ink color chips pigment, is made up of the component comprising following weight portion:
Water-borne acrylic resin
3-8 part,
Acrylic acid rosin 6-15 part,
Maleic rosin
7-14 part,
Ethyl acetate 10-15 part,
Isopropanol 4-7 part,
Aqueous organic pigment color cake
25-32 part,
Water 40-50 part,
Ethanolamine 2-5 part,
Defoamer 0.1-1 part.
Further, described a kind of water color ink color chips pigment, it is made up of the component comprising following weight portion:
Water-borne acrylic resin
5 parts,
Acrylic acid rosin 10 parts,
Maleic rosin
10 parts,
Ethyl acetate 13 parts,
Isopropanol
5 parts,
Aqueous organic pigment color cake
30 parts,
45 parts of water,
Ethanolamine 4 parts,
Defoamer 0.5 part
Preferably, described a kind of water color ink color chips pigment, also include non-ionic hyperbranched macromolecular dispersant 0-0.5 weight portion.
A kind of preparation method of water color ink color chips pigment, the method comprises the following steps:
(1) respectively the most aqueous acrylic resin 3-8 part, acrylic acid rosin 6-15 part, maleic rosin 7-14 part, ethyl acetate 10-15 part, isopropanol 4-7 part, ethanolamine 2-5 part mixed dissolution are uniform；
(2) the most aqueous organic pigment color cake 25-32 part adds the mixed solution after step (1) is uniformly dissolved in kneading machine while stirring, after stirring under the conditions of temperature is 50-70 DEG C, is incubated 15-30min；
(3) add non-ionic hyperbranched macromolecular dispersant 0-0.5 weight portion, add water 40-50 part, defoamer 0.1-1 part, continue stirring 30min；
(4) after the product entrance pressure filter of step (3) being filtered squeezing, filter cake is dried goods in blocks through pelleter.
Preferably, the preparation method of described a kind of water color ink color chips pigment, in described step (2), temperature is 60 DEG C, and temperature retention time is 20min.
Beneficial effect: the present invention is by having the feature that production technology simplifies after adding non-ionic hyperbranched macromolecular dispersant, acrylic acid rosin, maleic rosin, ethyl acetate, special organic pigment wet cake；Save the post processing energy and production equipment and artificial simultaneously, improve post processing production environment and discharge；The primary particle diameter of finished product and moistening produce for base ink and provide the quality assurance.
Detailed description of the invention
Embodiment 1
(1) respectively the most aqueous acrylic resin 8 parts, acrylic acid rosin 6 parts, maleic rosin 14 parts, ethyl acetate 15 parts, isopropanol 4 parts, 5 parts of mixed dissolutions of ethanolamine are uniform；(2) the most aqueous organic pigment color cake 32 parts adds the mixed solution after step (1) is uniformly dissolved in kneading machine while stirring, after stirring under the conditions of temperature is 70 DEG C, is incubated 30min；(3) add non-ionic hyperbranched macromolecular dispersant 0.5 weight portion, add 50 parts of water, defoamer 1 part, continue stirring 30min；(4) after the product entrance pressure filter of step (3) being filtered squeezing, filter cake is dried goods in blocks through pelleter.
Embodiment 2
(1) respectively the most aqueous acrylic resin 3 parts, acrylic acid rosin 15 parts, maleic rosin 7 parts, ethyl acetate 10 parts, isopropanol 7 parts, 2 parts of mixed dissolutions of ethanolamine are uniform；(2) the most aqueous organic pigment color cake 25 parts adds the mixed solution after step (1) is uniformly dissolved in kneading machine while stirring, after stirring under the conditions of temperature is 50 DEG C, is incubated 15min；(3) add non-ionic hyperbranched macromolecular dispersant 0.1 weight portion, add 40 parts of water, defoamer 0.1 part, continue stirring 30min；(4) after the product entrance pressure filter of step (3) being filtered squeezing, filter cake is dried goods in blocks through pelleter.
Embodiment 3
(1) respectively the most aqueous acrylic resin 4 parts, acrylic acid rosin 12 parts, maleic rosin 12 parts, ethyl acetate 11 parts, isopropanol 5 parts, 3 parts of mixed dissolutions of ethanolamine are uniform；(2) the most aqueous organic pigment color cake 26 parts adds the mixed solution after step (1) is uniformly dissolved in kneading machine while stirring, after stirring under the conditions of temperature is 70 DEG C, is incubated 30min；(3) add non-ionic hyperbranched macromolecular dispersant 0.2 weight portion, add 42 parts of water, defoamer 0.5 part, continue stirring 30min；(4) after the product entrance pressure filter of step (3) being filtered squeezing, filter cake is dried goods in blocks through pelleter.
Embodiment 4
(1) respectively the most aqueous acrylic resin 6 parts, acrylic acid rosin 8 parts, maleic rosin 8 parts, ethyl acetate 14 parts, isopropanol 6 parts, 4 parts of mixed dissolutions of ethanolamine are uniform；(2) the most aqueous organic pigment color cake 30 parts adds the mixed solution after step (1) is uniformly dissolved in kneading machine while stirring, after stirring under the conditions of temperature is 50 DEG C, is incubated 15min；(3) add non-ionic hyperbranched macromolecular dispersant 0.4 weight portion, add 48 parts of water, defoamer 0.1 part, continue stirring 30min；(4) after the product entrance pressure filter of step (3) being filtered squeezing, filter cake is dried goods in blocks through pelleter.
Embodiment 5
(1) respectively the most aqueous acrylic resin 5 parts, acrylic acid rosin 10 parts, maleic rosin 10 parts, ethyl acetate 13 parts, isopropanol 5 parts, 4 parts of mixed dissolutions of ethanolamine are uniform；(2) the most aqueous organic pigment color cake 30 parts adds the mixed solution after step (1) is uniformly dissolved in kneading machine while stirring, after stirring under the conditions of temperature is 60 DEG C, is incubated 20min；(3) add non-ionic hyperbranched macromolecular dispersant 0.4 weight portion, add 45 parts of water, defoamer 0.5 part, continue stirring 30min；(4) after the product entrance pressure filter of step (3) being filtered squeezing, filter cake is dried goods in blocks through pelleter.
Comparative example 1
(1) respectively the most aqueous acrylic resin 8 parts, ethyl acetate 15 parts, isopropanol 4 parts, 5 parts of mixed dissolutions of ethanolamine are uniform；(2) the most aqueous organic pigment color cake 32 parts adds the mixed solution after step (1) is uniformly dissolved in kneading machine while stirring, after stirring under the conditions of temperature is 70 DEG C, is incubated 30min；(3) add non-ionic hyperbranched macromolecular dispersant 0.5 weight portion, add 50 parts of water, defoamer 1 part, continue stirring 30min；(4) after the product entrance pressure filter of step (3) being filtered squeezing, filter cake is dried goods in blocks through pelleter.
Comparative example 2
(1) maleic rosin 14 parts, ethyl acetate 15 parts, isopropanol 4 parts, 5 parts of mixed dissolutions of ethanolamine are taken the most by weight uniform；(2) the most aqueous organic pigment color cake 32 parts adds the mixed solution after step (1) is uniformly dissolved in kneading machine while stirring, after stirring under the conditions of temperature is 70 DEG C, is incubated 30min；(3) add non-ionic hyperbranched macromolecular dispersant 0.5 weight portion, add 50 parts of water, defoamer 1 part, continue stirring 30min；(4) after the product entrance pressure filter of step (3) being filtered squeezing, filter cake is dried goods in blocks through pelleter.
Comparative example 3
(1) respectively the most aqueous acrylic resin 8 parts, acrylic acid rosin 6 parts, maleic rosin 14 parts, ethyl acetate 15 parts, isopropanol 4 parts, 5 parts of mixed dissolutions of ethanolamine are uniform；(2) the most aqueous organic pigment color cake 32 parts adds the mixed solution after step (1) is uniformly dissolved in kneading machine while stirring, after stirring under the conditions of temperature is 70 DEG C, is incubated 30min；(3) add 50 parts of water, defoamer 1 part, continue stirring 30min；(4) after the product entrance pressure filter of step (3) being filtered squeezing, filter cake is dried goods in blocks through pelleter.
The water color ink color chips pigment test result prepared is as shown in the table:
| Test event (specification) | Transparency (4 ~ 6) | Concentration (3 ~ 7) | Fineness (Max6.0) |
| Embodiment 1 | 5 | 6 | 2 |
| Embodiment 2 | 5 | 7 | 2 |
| Embodiment 3 | 5 | 7 | 2 |
| Embodiment 4 | 5 | 6 | 2 |
| Embodiment 5 | 6 | 7 | 1 |
| Comparative example 1 | 2 | 4 | 6 |
| Comparative example 2 | 2 | 3 | 5 |
| Comparative example 3 | 1 | 2 | 6 |
The invention is not restricted to embodiment here, those skilled in the art should be within scope according to the announcement of the present invention, the improvement made without departing from scope and amendment.
Claims (5)
1. a water color ink color chips pigment, it is characterised in that be made up of the component comprising following weight portion:
Water-borne acrylic resin
3-8 part,
Acrylic acid rosin
6-15 part,
Maleic rosin
7-14 part,
Ethyl acetate
10-15 part,
Isopropanol
4-7 part,
Aqueous organic pigment color cake
25-32 part,
Water
40-50 part,
Ethanolamine
2-5 part,
Defoamer
0.1-1 part.
A kind of water color ink color chips pigment the most according to claim 1, it is characterised in that be made up of the component comprising following weight portion:
Water-borne acrylic resin
5 parts,
Acrylic acid rosin
10 parts,
Maleic rosin
10 parts,
Ethyl acetate
13 parts,
Isopropanol
5 parts,
Aqueous organic pigment color cake
30 parts,
Water
45 parts,
Ethanolamine
4 parts,
Defoamer
0.5 part.
A kind of water color ink color chips pigment the most according to claim 1, it is characterised in that described component also includes non-ionic hyperbranched macromolecular dispersant 0-0.5 weight portion.
4. the preparation method of a water color ink color chips pigment, it is characterised in that the method comprises the following steps:
(1) respectively the most aqueous acrylic resin 3-8 part, acrylic acid rosin 6-15 part, maleic rosin 7-14 part, ethyl acetate 10-15 part, isopropanol 4-7 part, ethanolamine 2-5 part mixed dissolution are uniform；
(2) the most aqueous organic pigment color cake 25-32 part adds the mixed solution after step (1) is uniformly dissolved in kneading machine while stirring, after stirring under the conditions of temperature is 50-70 DEG C, is incubated 15-30min；
(3) add non-ionic hyperbranched macromolecular dispersant 0-0.5 weight portion, add water 40-50 part, defoamer 0.1-1 part, continue stirring 30min；
(4) after the product entrance pressure filter of step (3) being filtered squeezing, filter cake is dried goods in blocks through pelleter.
The preparation method of a kind of water color ink color chips pigment the most according to claim 4, it is characterised in that in described step (2), temperature is 60 DEG C, and temperature retention time is 20min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610551468.9A CN105968941A (en) | 2016-07-14 | 2016-07-14 | Aqueous printing ink color sheet pigment and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610551468.9A CN105968941A (en) | 2016-07-14 | 2016-07-14 | Aqueous printing ink color sheet pigment and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105968941A true CN105968941A (en) | 2016-09-28 |
Family
ID=56952397
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610551468.9A Pending CN105968941A (en) | 2016-07-14 | 2016-07-14 | Aqueous printing ink color sheet pigment and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105968941A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109181404A (en) * | 2018-06-04 | 2019-01-11 | 珠海市誉达伟业科技有限公司 | Pigment preparations color chips and preparation method thereof |
| CN109385138A (en) * | 2018-11-06 | 2019-02-26 | 厦门易统水墨有限公司 | A kind of aqueous solid soluble ink and processing technology again |
| CN114940841A (en) * | 2022-07-13 | 2022-08-26 | 山东盛驰新材料有限公司 | Pigment for water-based ink and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2001081377A (en) * | 1999-09-17 | 2001-03-27 | Canon Inc | Ink, ink set, ink cartridge, recording unit, colored image- recording unit and ink-jet recording |
| CN101117450A (en) * | 2007-07-23 | 2008-02-06 | 江南大学 | A kind of preparation method of nonionic hyperbranched polymer dispersant for organic pigment |
-
2016
- 2016-07-14 CN CN201610551468.9A patent/CN105968941A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2001081377A (en) * | 1999-09-17 | 2001-03-27 | Canon Inc | Ink, ink set, ink cartridge, recording unit, colored image- recording unit and ink-jet recording |
| CN101117450A (en) * | 2007-07-23 | 2008-02-06 | 江南大学 | A kind of preparation method of nonionic hyperbranched polymer dispersant for organic pigment |
Non-Patent Citations (2)
| Title |
|---|
| 李德贵: ""碱溶性苯乙烯-丙烯酸树脂的合成及应用"", 《中国优秀硕士学位论文全文数据库 工程科技I辑》 * |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109181404A (en) * | 2018-06-04 | 2019-01-11 | 珠海市誉达伟业科技有限公司 | Pigment preparations color chips and preparation method thereof |
| CN109385138A (en) * | 2018-11-06 | 2019-02-26 | 厦门易统水墨有限公司 | A kind of aqueous solid soluble ink and processing technology again |
| CN114940841A (en) * | 2022-07-13 | 2022-08-26 | 山东盛驰新材料有限公司 | Pigment for water-based ink and preparation method thereof |
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Application publication date: 20160928 |