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CN105951446A - 一种蚕丝柔顺剂 - Google Patents

一种蚕丝柔顺剂 Download PDF

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CN105951446A
CN105951446A CN201610521262.1A CN201610521262A CN105951446A CN 105951446 A CN105951446 A CN 105951446A CN 201610521262 A CN201610521262 A CN 201610521262A CN 105951446 A CN105951446 A CN 105951446A
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silkworm silk
parts
mixed liquor
softener
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蓝莉芬
蓝芬
唐站
蓝惠芬
黄正然
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Guangxi Nanning Mashan Donglong Sericulture LLC
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Guangxi Nanning Mashan Donglong Sericulture LLC
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Abstract

本发明公开了一种蚕丝柔顺剂，以重量份为单位，包括以下原料：表面活性剂80‑100份、消泡剂6‑10份、稳泡剂3‑5份、渗透剂2‑4份、乳化剂2‑3份、分散剂1‑2份、交联剂2‑4份、调节剂2‑3份、增稠剂2‑3份、防腐剂1‑2份、香味剂0.8‑1.2份、水700‑1000份。本发明的蚕丝柔顺剂杀菌性能优，对金黄色葡萄球菌、大肠杆菌、白色念珠菌的杀菌率均达到96％以上；本发明制备方法简单、方便可行，蚕丝柔顺剂制备成本低，有力于推广应用。

Description

一种蚕丝柔顺剂
【技术领域】
本发明属于柔顺剂制备技术领域，具体涉及一种蚕丝柔顺剂。
【背景技术】
传统方式加工蚕丝被的工艺简单，品种极为单一，以传统工艺加工的蚕丝被经使用后，丝纤维易缠结、粘连，随之弹性和保暖性将会随之降低，需要经常翻拆、扯松，才能保持蚕丝被原有的优良服饰性能。
为赋予蚕丝优良的膨松、柔软、高弹等性能，需对蚕丝进行精加工，使蚕丝纤维空隙膨大，制成的蚕丝棉具有膨松、高弹性、纤维间不结板的特点。通过对蚕丝进行膨化处理，可增加蚕丝纤维膨松性、高弹性、柔软性，可有效防止丝纤维间不粘丝、缠结，提高蚕丝被的实用性。
蚕丝柔顺剂的作用就好像是为蚕丝纤维的表面均匀地上一层保护膜，蚕丝纤维表面由于吸附了柔顺剂，蚕丝纤维间的摩擦系数降低了、可移动性增强了，蚕丝纤维固有的平滑、延伸、压缩性能也得到了恢复，所以蚕丝变得更加柔软、蓬松、有弹性。在目前蚕丝进行精加工过程中需要用到蚕丝柔顺剂，但是效果并不是很好，还不能满足工厂实际生产的需求。
【发明内容】
本发明提供一种蚕丝柔顺剂，以解决蚕丝纤维易缠结、粘连，随之弹性和保暖性将会随之降低等问题。本发明的蚕丝柔顺剂杀菌性能优，对金黄色葡萄球菌、大肠杆菌、白色念珠菌的杀菌率均达到96％以上；本发明制备方法简单、方便可行，蚕丝柔顺剂制备成本低，有力于推广应用。
为了解决以上技术问题，本发明采用以下技术方案：
一种蚕丝柔顺剂，以重量份为单位，包括以下原料：表面活性剂80-100份、消泡剂6-10份、稳泡剂3-5份、渗透剂2-4份、乳化剂2-3份、分散剂1-2份、交联剂2-4份、调节剂2-3份、增稠剂2-3份、防腐剂1-2份、香味剂0.8-1.2份、水700-1000份；
所述表面活性剂为聚丙烯酰胺；
所述稳泡剂为聚乙烯醇；
所述乳化剂为单硬脂酸甘油酯；
所述交联剂磷酸二乙酯；
所述蚕丝柔顺剂的制备方法，包括以下步骤：
S1：将表面活性剂加入水中，升温至44-46℃搅拌溶解，制得混合液Ⅰ；
S2：向步骤S1制得的混合液Ⅰ加入渗透剂、乳化剂、分散剂、交联剂、增稠剂，加热至58-62℃，在超声波作用下，在转速为200-300r/min搅拌处理25-30min，制得混合液Ⅱ；
S3：停止加热和超声波作用，向步骤S2制得的混合液Ⅱ加入消泡剂和稳泡剂，在转速为100-300r/min下搅拌5-10min，制得混合液Ⅲ；
S4：向步骤S3制得的混合液Ⅲ中加入防腐剂和香味剂，在转速为100-200r/min下搅拌3-5min，制得混合液Ⅳ；
S5：向步骤S4制得的混合液Ⅳ中加入调节剂，使pH值为5-5.4，制得蚕丝柔顺剂。
进一步地，所述消泡剂为硅烷改性丙酸酯。
进一步地，所述渗透剂烷基苯磺酸钾。
进一步地，所述分散剂月桂醇硫酸钾。
进一步地，所述调节剂为醋酸。
进一步地，所述增稠剂为卡拉胶。
进一步地，所述防腐剂为喹氧灵。
进一步地，所述香味剂为薰衣草精油。
本发明具有以下有益效果：
(1)本发明蚕丝柔顺剂杀菌性能优，对金黄色葡萄球菌、大肠杆菌、白色念珠菌的杀菌率均达到96％以上；
(2)本发明蚕丝柔顺剂的再润湿性能平均值为15s，与目前其它相关产品的再润湿性能(以毛细效应时间计)平均值为30-40s相比，本发明是目前现有产品效果的2-2.67倍，可见本发明蚕丝柔顺剂的再润湿性能更好；
(3)本发明制备方法简单、方便可行，蚕丝柔顺剂制备成本低，有力于推广应用。
【具体实施方式】
为便于更好地理解本发明，通过以下实施例加以说明，这些实施例属于本发明的保护范围，但不限制本发明的保护范围。
在实施例中，所述蚕丝柔顺剂，以重量份为单位，包括以下原料：表面活性剂80-100份、消泡剂6-10份、稳泡剂3-5份、渗透剂2-4份、乳化剂2-3份、分散剂1-2份、交联剂2-4份、调节剂2-3份、增稠剂2-3份、防腐剂1-2份、香味剂0.8-1.2份、水700-1000份。
所述表面活性剂为聚丙烯酰胺。
所述消泡剂为硅烷改性丙酸酯。
所述稳泡剂为聚乙烯醇。
所述渗透剂烷基苯磺酸钾。
所述乳化剂为单硬脂酸甘油酯。
所述分散剂月桂醇硫酸钾。
所述交联剂磷酸二乙酯。
所述调节剂为醋酸。
所述增稠剂为卡拉胶。
所述防腐剂为喹氧灵。
所述香味剂为薰衣草精油。
所述蚕丝柔顺剂的制备方法，包括以下步骤：
S1：将表面活性剂加入水中，升温至44-46℃搅拌溶解，制得混合液Ⅰ；
S2：向步骤S1制得的混合液Ⅰ加入渗透剂、乳化剂、分散剂、交联剂、增稠剂，加热至58-62℃，在超声波作用下，在转速为200-300r/min搅拌处理25-30min，制得混合液Ⅱ；
S3：停止加热和超声波作用，向步骤S2制得的混合液Ⅱ加入消泡剂和稳泡剂，在转速为100-300r/min下搅拌5-10min，制得混合液Ⅲ；
S4：向步骤S3制得的混合液Ⅲ中加入防腐剂和香味剂，在转速为100-200r/min下搅拌3-5min，制得混合液Ⅳ；
S5：向步骤S4制得的混合液Ⅳ中加入调节剂，使pH值为5-5.4，制得蚕丝柔顺剂。
下面通过更具体的实施例对本发明进行说明。
实施例1
一种蚕丝柔顺剂，以重量份为单位，包括以下原料：表面活性剂90份、消泡剂8份、稳泡剂4份、渗透剂3份、乳化剂2份、分散剂2份、交联剂3份、调节剂3份、增稠剂2份、防腐剂2份、香味剂1份、水850份。
所述表面活性剂为聚丙烯酰胺。
所述消泡剂为硅烷改性丙酸酯。
所述稳泡剂为聚乙烯醇。
所述渗透剂烷基苯磺酸钾。
所述乳化剂为单硬脂酸甘油酯。
所述分散剂月桂醇硫酸钾。
所述交联剂磷酸二乙酯。
所述调节剂为醋酸。
所述增稠剂为卡拉胶。
所述防腐剂为喹氧灵。
所述香味剂为薰衣草精油。
所述蚕丝柔顺剂的制备方法，包括以下步骤：
S1：将表面活性剂加入水中，升温至45℃搅拌溶解，制得混合液Ⅰ；
S2：向步骤S1制得的混合液Ⅰ加入渗透剂、乳化剂、分散剂、交联剂、增稠剂，加热至60℃，在超声波作用下，在转速为300r/min搅拌处理25min，制得混合液Ⅱ；
S3：停止加热和超声波作用，向步骤S2制得的混合液Ⅱ加入消泡剂和稳泡剂，在转速为200r/min下搅拌8min，制得混合液Ⅲ；
S4：向步骤S3制得的混合液Ⅲ中加入防腐剂和香味剂，在转速为200r/min下搅拌3min，制得混合液Ⅳ；
S5：向步骤S4制得的混合液Ⅳ中加入调节剂，使pH值为5.2，制得蚕丝柔顺剂。
实施例2
一种蚕丝柔顺剂，以重量份为单位，包括以下原料：表面活性剂80份、消泡剂6份、稳泡剂3份、渗透剂2份、乳化剂2份、分散剂1份、交联剂2份、调节剂2份、增稠剂2份、防腐剂1份、香味剂0.8份、水700份。
所述表面活性剂为聚丙烯酰胺。
所述消泡剂为硅烷改性丙酸酯。
所述稳泡剂为聚乙烯醇。
所述渗透剂烷基苯磺酸钾。
所述乳化剂为单硬脂酸甘油酯。
所述分散剂月桂醇硫酸钾。
所述交联剂磷酸二乙酯。
所述调节剂为醋酸。
所述增稠剂为卡拉胶。
所述防腐剂为喹氧灵。
所述香味剂为薰衣草精油。
所述蚕丝柔顺剂的制备方法，包括以下步骤：
S1：将表面活性剂加入水中，升温至44℃搅拌溶解，制得混合液Ⅰ；
S2：向步骤S1制得的混合液Ⅰ加入渗透剂、乳化剂、分散剂、交联剂、增稠剂，加热至58℃，在超声波作用下，在转速为200r/min搅拌处理30min，制得混合液Ⅱ；
S3：停止加热和超声波作用，向步骤S2制得的混合液Ⅱ加入消泡剂和稳泡剂，在转速为100r/min下搅拌10min，制得混合液Ⅲ；
S4：向步骤S3制得的混合液Ⅲ中加入防腐剂和香味剂，在转速为1000r/min下搅拌5min，制得混合液Ⅳ；
S5：向步骤S4制得的混合液Ⅳ中加入调节剂，使pH值为5，制得蚕丝柔顺剂。
实施例3
一种蚕丝柔顺剂，以重量份为单位，包括以下原料：表面活性剂100份、消泡剂10份、稳泡剂5份、渗透剂4份、乳化剂3份、分散剂2份、交联剂4份、调节剂3份、增稠剂3份、防腐剂2份、香味剂1.2份、水1000份。
所述表面活性剂为聚丙烯酰胺。
所述消泡剂为硅烷改性丙酸酯。
所述稳泡剂为聚乙烯醇。
所述渗透剂烷基苯磺酸钾。
所述乳化剂为单硬脂酸甘油酯。
所述分散剂月桂醇硫酸钾。
所述交联剂磷酸二乙酯。
所述调节剂为醋酸。
所述增稠剂为卡拉胶。
所述防腐剂为喹氧灵。
所述香味剂为薰衣草精油。
所述蚕丝柔顺剂的制备方法，包括以下步骤：
S1：将表面活性剂加入水中，升温至46℃搅拌溶解，制得混合液Ⅰ；
S2：向步骤S1制得的混合液Ⅰ加入渗透剂、乳化剂、分散剂、交联剂、增稠剂，加热至62℃，在超声波作用下，在转速为300r/min搅拌处理25min，制得混合液Ⅱ；
S3：停止加热和超声波作用，向步骤S2制得的混合液Ⅱ加入消泡剂和稳泡剂，在转速为300r/min下搅拌5min，制得混合液Ⅲ；
S4：向步骤S3制得的混合液Ⅲ中加入防腐剂和香味剂，在转速为200r/min下搅拌3min，制得混合液Ⅳ；
S5：向步骤S4制得的混合液Ⅳ中加入调节剂，使pH值为5.4，制得蚕丝柔顺剂。
性能测试：
(1)采用本发明实施例1-3的蚕丝柔顺剂与市售普通柔顺剂对蚕丝进行清漂洗，其柔顺度和色强度检测结果如下表1所示。
表1 柔顺度和色强度检测
(2)杀菌性能进行检测：对本发明实施例1-3的蚕丝柔顺剂的杀菌性能进行检测，其杀菌力结果为：金黄色葡萄球菌97％-98％，大肠杆菌96％-97％，白色念珠菌96％-97％。
(3)按照《衣物柔顺剂再润湿性能的测定》标准中规定的试验程序，对本发明实施例1-3中的蚕丝柔顺剂的再润湿性能进行试验，结果如下表2所示。
表2 蚕丝柔顺剂的再润湿性能测试
从表2可以看出本发明蚕丝柔顺剂的再润湿性能平均值为15s，而目前其它相关产品的再润湿性能(以毛细效应时间计)平均为30-40s，即本发明是目前现有产品效果的2-2.67倍，可见本发明蚕丝柔顺剂的再润湿性能好。
以上内容不能认定本发明的具体实施只局限于这些说明，对于本发明所属技术领域的普通技术人员来说，在不脱离本发明构思的前提下，还可以做出若干简单推演或替换，都应当视为属于本发明由所提交的权利要求书确定的专利保护范围。

Claims (8)

1.一种蚕丝柔顺剂，其特征在于，以重量份为单位，包括以下原料：表面活性剂80-100份、消泡剂6-10份、稳泡剂3-5份、渗透剂2-4份、乳化剂2-3份、分散剂1-2份、交联剂2-4份、调节剂2-3份、增稠剂2-3份、防腐剂1-2份、香味剂0.8-1.2份、水700-1000份；
所述表面活性剂为聚丙烯酰胺；
所述稳泡剂为聚乙烯醇；
所述乳化剂为单硬脂酸甘油酯；
所述交联剂磷酸二乙酯；
所述蚕丝柔顺剂的制备方法，包括以下步骤：
S1：将表面活性剂加入水中，升温至44-46℃搅拌溶解，制得混合液Ⅰ；
S2：向步骤S1制得的混合液Ⅰ加入渗透剂、乳化剂、分散剂、交联剂、增稠剂，加热至58-62℃，在超声波作用下，在转速为200-300r/min搅拌处理25-30min，制得混合液Ⅱ；
S3：停止加热和超声波作用，向步骤S2制得的混合液Ⅱ加入消泡剂和稳泡剂，在转速为100-300r/min下搅拌5-10min，制得混合液Ⅲ；
S4：向步骤S3制得的混合液Ⅲ中加入防腐剂和香味剂，在转速为100-200r/min下搅拌3-5min，制得混合液Ⅳ；
S5：向步骤S4制得的混合液Ⅳ中加入调节剂，使pH值为5-5.4，制得蚕丝柔顺剂。
2.根据权利要求1所述的蚕丝柔顺剂，其特征在于，所述消泡剂为硅烷改性丙酸酯。
3.根据权利要求1所述的蚕丝柔顺剂，其特征在于，所述渗透剂烷基苯磺酸钾。
4.根据权利要求1所述的蚕丝柔顺剂，其特征在于，所述分散剂月桂醇硫酸钾。
5.根据权利要求1所述的蚕丝柔顺剂，其特征在于，所述调节剂为醋酸。
6.根据权利要求1所述的蚕丝柔顺剂，其特征在于，所述增稠剂为卡拉胶。
7.根据权利要求1所述的蚕丝柔顺剂，其特征在于，所述防腐剂为喹氧灵。
8.根据权利要求1所述的蚕丝柔顺剂，其特征在于，所述香味剂为薰衣草精油。
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