CN105949914A - Waterborne glass baking paint and preparation method thereof - Google Patents
Waterborne glass baking paint and preparation method thereof Download PDFInfo
- Publication number
- CN105949914A CN105949914A CN201610438606.2A CN201610438606A CN105949914A CN 105949914 A CN105949914 A CN 105949914A CN 201610438606 A CN201610438606 A CN 201610438606A CN 105949914 A CN105949914 A CN 105949914A
- Authority
- CN
- China
- Prior art keywords
- water
- glass baking
- baking paint
- agent
- based glass
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
- C09D133/04—Homopolymers or copolymers of esters
- C09D133/06—Homopolymers or copolymers of esters of esters containing only carbon, hydrogen and oxygen, the oxygen atom being present only as part of the carboxyl radical
- C09D133/08—Homopolymers or copolymers of acrylic acid esters
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Paints Or Removers (AREA)
Abstract
The invention discloses waterborne glass baking paint. The waterborne glass baking paint is characterized by being prepared from, by weight, 400-600 parts of modified acrylic resin, 200-350 parts of rutile titanium dioxide, 100-120 parts of amino resin, 100-150 parts of 2% hydroxyethyl cellulose, 20-30 parts of a coupling agent, 10-15 parts of a coalescing agent, 5-6 parts of a waterborne dispersing agent, 3-5 parts of a waterborne defoaming agent, 2-3 parts of a waterborne paint defoaming agent, 2-5 parts of a substrate wetting agent and 3-5 parts of a smoothing and flowing agent. The waterborne glass baking paint is environmentally friendly and good in adhesive force, alcohol resistance and water resistance. The invention further provides a preparation method of the waterborne glass baking paint.
Description
[technical field]
The present invention relates to a kind of Water-based glass baking paint and preparation method thereof.
[background technology]
In wood furniture decoration application, Water-based glass baking paint is exactly water miscible glass baking varnish,
Traditional oiliness glass baking varnish adds Tianna solution equal solvent and is used as diluent, and aqueous glass
Baking vanish adds water purification and is used as diluent, and after general unsaturated polyester varnish film forming, paint film is harder
Crisp, poor in flexibility, modified with polyurethanes, improve the pliability of paint film, logical
Cross glass dust and Tissuemat E starches the wearability that improve paint film.Existing Water-based glass baking paint
Glossiness, weatherability are poor, and hardness is little, and adhesive force is more weak, even some Water-based glass baking paint
Also use organic or virulent solvent.
Along with the water paint application on glass that improves of people's environmental consciousness is subject to greatly
Pay attention to, use polyurethane aqueous dispersion body, water-soluble polypropylene acid resin, urethane type and modification
Adhesive force, resistance to alcohol is there is in mono-component aqueous glass lacquer prepared by acrylic resin in glass substrate
Property, resistance to water, abrasion performance difference and the shortcoming such as hardness is low, cause service life short, and propylene
Acid resin and amino curing agent proportioning, coupling agent consumption be to paint film resistance to water, alcohol resistance,
Wearability and the principal element of hardness impact.
[summary of the invention]
The invention aims to provide a kind of environmental protection, and adhesive force, alcohol resistance, resistance to water
The Water-based glass baking paint that energy is good.
It is another object of the present invention to the preparation method in order to provide this Water-based glass baking paint.
The present invention uses below scheme:
A kind of Water-based glass baking paint, it is characterised in that: it is made up of the component of following weight ratio:
A kind of Water-based glass baking paint as above, it is characterised in that: described acrylic resin modified
Be acrylic acid methyl ester., ethyl acrylate, propyl acrylate, butyl acrylate, amyl acrylate,
Any 2 kinds or the mixture of 3 kinds in 2-EHA, Isooctyl acrylate monomer.
A kind of Water-based glass baking paint as above, it is characterised in that: described amino resins choosing
With in the melamine resin of height methyl-etherified or aqueous terminal isocyanate group firming agent
A kind of.
A kind of Water-based glass baking paint as above, it is characterised in that: described coalescents selects second
Alcohol, isopropanol, propylene glycol, sec-butyl alcohol, n-butyl alcohol, carbitol, propylene glycol monomethyl ether, the third two
The one of alcohol butyl ether.
A kind of Water-based glass baking paint as above, it is characterised in that: described coupling agent is silica
Alkane coupling agent.
A kind of stone-like coating as above, is preferably made up of the component of following weight ratio:
The preparation method of Water-based glass baking paint as above, it is characterised in that: by detail below
Prepared by step:
A, put into 2% hydroxyethyl cellulose, aqueous dispersion successively, start shooting 400-600 rev/min
Clock stirs 5 minutes；
B, under 400-600 rev/min of speed state, add aqueous defoamer, base material moistening
Agent stirs 5 minutes；
C, add rutile titanium white lead, by 1000-1200 rev/min of speed high speed dispersion 15
Minute；
D, horizontal sand mill sand milling, fineness is used to reach less than 15 microns again；
E, sequentially add water paint deaeration agent, smooth and flowable, coupling agent, furtherance film
Agent disperses 5 minutes with 600-800 rev/min；
F, it is eventually adding acrylic resin modified and 500-700 rev/min of amino resins stirring
10 minutes, detection packaging.
In sum, beneficial effects of the present invention:
A kind of Water-based glass baking paint of the present invention, the acrylic resin modified and amino tree by regulation
The proportioning of fat, the consumption etc. of coupling agent change the performance of Water-based glass baking paint, prepare
The low-VOC aqueous glass baking varnish of environment-friendly type, has a high hardness number, good resistance to water, resistance to
Alcohol and wearability, higher adhesive force, improve service life, there is the good feature of environmental protection
Can, construction is simple, and storage is stable.
[detailed description of the invention]
Below in conjunction with specific embodiment, the invention will be further described:
Embodiment 1:
A kind of Water-based glass baking paint, it is characterised in that: it is made up of the component of following weight ratio:
Above-mentioned Water-based glass baking paint, is prepared by step in detail below:
A, put into 2% hydroxyethyl cellulose, aqueous dispersion successively, start shooting 400-600/ minute
Turn stirring 5 minutes.；
B, under 400-600 rev/min of speed state, add aqueous defoamer, base material moistening
Agent stirs 5 minutes；
C, add rutile titanium white lead, by 1000-1200 rev/min of speed high speed dispersion 15
Minute；
D, horizontal sand mill sand milling, fineness is used to reach less than 15 microns again；
E, sequentially add water paint deaeration agent, smooth and flowable, coupling agent, furtherance film
Agent disperses 5 minutes with 600-800 rev/min；
F, it is eventually adding acrylic resin modified and 500-700 rev/min of amino resins stirring
10 minutes, detection packaging.
Embodiment 2:
A kind of Water-based glass baking paint, it is characterised in that: it is made up of the component of following weight ratio:
Above-mentioned Water-based glass baking paint, is prepared by step in detail below:
A, put into 2% hydroxyethyl cellulose, aqueous dispersion successively, start shooting 400-600/ minute
Turn stirring 5 minutes.；
B, under 400-600 rev/min of speed state, add aqueous defoamer, base material moistening
Agent stirs 5 minutes；
C, add rutile titanium white lead, by 1000-1200 rev/min of speed high speed dispersion 15
Minute；
D, horizontal sand mill sand milling, fineness is used to reach less than 15 microns again；
E, sequentially add water paint deaeration agent, smooth and flowable, coupling agent, furtherance film
Agent disperses 5 minutes with 600-800 rev/min；
F, it is eventually adding acrylic resin modified and 500-700 rev/min of amino resins stirring
10 minutes, detection packaging.
Embodiment 3:
A kind of Water-based glass baking paint, it is characterised in that: it is made up of the component of following weight ratio:
Above-mentioned Water-based glass baking paint, is prepared by step in detail below:
A, put into 2% hydroxyethyl cellulose, aqueous dispersion successively, start shooting 400-600/ minute
Turn stirring 5 minutes.；
B, under 400-600 rev/min of speed state, add aqueous defoamer, base material moistening
Agent stirs 5 minutes；
C, add rutile titanium white lead, by 1000-1200 rev/min of speed high speed dispersion 15
Minute；
D, horizontal sand mill sand milling, fineness is used to reach less than 15 microns again；
E, sequentially add water paint deaeration agent, smooth and flowable, coupling agent, furtherance film
Agent disperses 5 minutes with 600-800 rev/min；
F, it is eventually adding acrylic resin modified and 500-700 rev/min of amino resins stirring
10 minutes, detection packaging.
Embodiment 4:
A kind of Water-based glass baking paint, it is characterised in that: it is made up of the component of following weight ratio:
Above-mentioned Water-based glass baking paint, is prepared by step in detail below:
A, put into 2% hydroxyethyl cellulose, aqueous dispersion successively, start shooting 400-600/ minute
Turn stirring 5 minutes.；
B, under 400-600 rev/min of speed state, add aqueous defoamer, base material moistening
Agent stirs 5 minutes；
C, add rutile titanium white lead, by 1000-1200 rev/min of speed high speed dispersion 15
Minute；
D, horizontal sand mill sand milling, fineness is used to reach less than 15 microns again；
E, sequentially add water paint deaeration agent, smooth and flowable, coupling agent, furtherance film
Agent disperses 5 minutes with 600-800 rev/min；
F, it is eventually adding acrylic resin modified and 500-700 rev/min of amino resins stirring
10 minutes, detection packaging.
Embodiment 5:
A kind of Water-based glass baking paint, it is characterised in that: it is made up of the component of following weight ratio:
Above-mentioned Water-based glass baking paint, is prepared by step in detail below:
A, put into 2% hydroxyethyl cellulose, aqueous dispersion successively, start shooting 400-600/ minute
Turn stirring 5 minutes.；
B, under 400-600 rev/min of speed state, add aqueous defoamer, base material moistening
Agent stirs 5 minutes；
C, add rutile titanium white lead, by 1000-1200 rev/min of speed high speed dispersion 15
Minute；
D, horizontal sand mill sand milling, fineness is used to reach less than 15 microns again；
E, sequentially add water paint deaeration agent, smooth and flowable, coupling agent, furtherance film
Agent disperses 5 minutes with 600-800 rev/min；
F, it is eventually adding acrylic resin modified and 500-700 rev/min of amino resins stirring
10 minutes, detection packaging.
The performance test such as following table of embodiment 1～5 gained Water-based glass baking paint:
| Project | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | |
| Hardness/HB | 4 | 5 | 6 | 5 | 4 | GB/T 6739-2006 |
| Adhesive force | 0 grade | 0 grade | 0 grade | 0 grade | 0 grade | GB/T9286-1998 |
| Wearability | 1 grade | 1 grade | 1 grade | 1 grade | 1 grade | GB/T4893.8-1985 |
| Resistance to water/H | 170 | 210 | 182 | 183 | 190 | GB/T1733—1993 |
| Alkali resistance/H | 170 | 210 | 182 | 183 | 190 | GB9274 |
| Alcohol resistance/H | 170 | 210 | 182 | 183 | 190 | GB/T1763—1979 |
As can be known from the above table, the Water-based glass baking paint prepared, in hardness, wearability, attachment
The performances such as power, resistance to water and alcohol resistance all reach or are better than standard.
Claims (7)
1. a Water-based glass baking paint, it is characterised in that: it is made up of the component of following weight ratio:
2. according to a kind of Water-based glass baking paint described in right 1, it is characterised in that: described modification
Acrylic resin be acrylic acid methyl ester., ethyl acrylate, propyl acrylate, butyl acrylate,
In amyl acrylate, 2-EHA, Isooctyl acrylate monomer any 2 kinds or 3
The mixture planted.
3. according to a kind of Water-based glass baking paint described in right 1, it is characterised in that: described ammonia
Base resin selects the melamine resin of height methyl-etherified or aqueous terminal isocyanate group solid
One in agent.
4. according to a kind of Water-based glass baking paint described in right 1, it is characterised in that: described film forming
Selection of auxiliary ethanol, isopropanol, propylene glycol, sec-butyl alcohol, n-butyl alcohol, carbitol, propylene glycol
Methyl ether, the one of propandiol butyl ether.
5. according to a kind of Water-based glass baking paint described in right 1, it is characterised in that: described coupling
Agent is silicone coupling agents.
6. according to a kind of Water-based glass baking paint described in right 1, it is characterised in that: by following heavy
The component of amount ratio is made:
7. a preparation method for the Water-based glass baking paint described in any one of claim 1-6, its
It is characterised by: prepared by step in detail below:
A, put into 2% hydroxyethyl cellulose, aqueous dispersion successively, start shooting 400-600 rev/min
Clock stirs 5 minutes；
B, under 400-600 rev/min of speed state, add aqueous defoamer, base material moistening
Agent stirs 5 minutes；
C, add rutile titanium white lead, by 1000-1200 rev/min of speed high speed dispersion 15
Minute；
D, horizontal sand mill sand milling, fineness is used to reach less than 15 microns again；
E, sequentially add water paint deaeration agent, smooth and flowable, coupling agent, furtherance film
Agent disperses 5 minutes with 600-800 rev/min；
F, it is eventually adding acrylic resin modified and 500-700 rev/min of amino resins stirring
10 minutes, detection packaging.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610438606.2A CN105949914A (en) | 2016-06-16 | 2016-06-16 | Waterborne glass baking paint and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610438606.2A CN105949914A (en) | 2016-06-16 | 2016-06-16 | Waterborne glass baking paint and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105949914A true CN105949914A (en) | 2016-09-21 |
Family
ID=56906792
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610438606.2A Pending CN105949914A (en) | 2016-06-16 | 2016-06-16 | Waterborne glass baking paint and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105949914A (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106833213A (en) * | 2017-03-08 | 2017-06-13 | 深圳市赛亚气雾剂有限公司 | A kind of environment-friendly waterborne aerosol paint and preparation method thereof |
| CN107815192A (en) * | 2017-11-17 | 2018-03-20 | 湖南太子化工涂料有限公司 | A kind of Water-based glass baking paint |
| CN108342134A (en) * | 2018-01-09 | 2018-07-31 | 河北晨阳工贸集团有限公司 | Aqueous ceramic paint and preparation method thereof and ceramics and preparation method thereof |
| CN108976952A (en) * | 2018-08-06 | 2018-12-11 | 中山市明日涂料材料有限公司 | A kind of novel environment-friendly water-based glass baking varnish and preparation method thereof |
| CN109401559A (en) * | 2018-09-26 | 2019-03-01 | 无锡市太湖防腐材料有限公司 | A kind of stainless steel vacuum cup aqueous amino-stoving varnish and preparation method thereof |
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| CN101845255A (en) * | 2010-03-09 | 2010-09-29 | 汉森漆业(福建)有限公司 | Water-based baking paint for glass substrate and preparation and use methods thereof |
| CN101885935A (en) * | 2010-07-14 | 2010-11-17 | 福州德贤化工有限公司 | Water-based bulb paint |
| CN102585630A (en) * | 2011-12-19 | 2012-07-18 | 青岛爱尔家佳新材料有限公司 | Water-based glass baking paint and preparation method thereof |
| CN102888163A (en) * | 2012-10-25 | 2013-01-23 | 南京长江涂料有限公司 | Water-based paint for Christmas glass ornaments, and preparation method and application thereof |
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| CN104164145A (en) * | 2014-07-15 | 2014-11-26 | 合肥科润节能建材有限公司 | Water-based baked industrial paint |
| CN104946049A (en) * | 2015-07-08 | 2015-09-30 | 安庆联泰电子科技有限公司 | Environment-friendly water-based glass baking lacquer |
-
2016
- 2016-06-16 CN CN201610438606.2A patent/CN105949914A/en active Pending
Patent Citations (8)
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| CN101845255A (en) * | 2010-03-09 | 2010-09-29 | 汉森漆业(福建)有限公司 | Water-based baking paint for glass substrate and preparation and use methods thereof |
| CN101885935A (en) * | 2010-07-14 | 2010-11-17 | 福州德贤化工有限公司 | Water-based bulb paint |
| CN102585630A (en) * | 2011-12-19 | 2012-07-18 | 青岛爱尔家佳新材料有限公司 | Water-based glass baking paint and preparation method thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106833213A (en) * | 2017-03-08 | 2017-06-13 | 深圳市赛亚气雾剂有限公司 | A kind of environment-friendly waterborne aerosol paint and preparation method thereof |
| CN107815192A (en) * | 2017-11-17 | 2018-03-20 | 湖南太子化工涂料有限公司 | A kind of Water-based glass baking paint |
| CN108342134A (en) * | 2018-01-09 | 2018-07-31 | 河北晨阳工贸集团有限公司 | Aqueous ceramic paint and preparation method thereof and ceramics and preparation method thereof |
| CN108976952A (en) * | 2018-08-06 | 2018-12-11 | 中山市明日涂料材料有限公司 | A kind of novel environment-friendly water-based glass baking varnish and preparation method thereof |
| CN109401559A (en) * | 2018-09-26 | 2019-03-01 | 无锡市太湖防腐材料有限公司 | A kind of stainless steel vacuum cup aqueous amino-stoving varnish and preparation method thereof |
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Application publication date: 20160921 |