CN105936867A - Diaphragma juglandis fructus vinegar and preparation method thereof - Google Patents
Diaphragma juglandis fructus vinegar and preparation method thereof Download PDFInfo
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- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12J—VINEGAR; PREPARATION OR PURIFICATION THEREOF
- C12J1/00—Vinegar; Preparation or purification thereof
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/23—Apiaceae or Umbelliferae (Carrot family), e.g. dill, chervil, coriander or cumin
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- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/25—Araliaceae (Ginseng family), e.g. ivy, aralia, schefflera or tetrapanax
- A61K36/258—Panax (ginseng)
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- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
- A61K36/481—Astragalus (milkvetch)
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- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/52—Juglandaceae (Walnut family)
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- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/81—Solanaceae (Potato family), e.g. tobacco, nightshade, tomato, belladonna, capsicum or jimsonweed
- A61K36/815—Lycium (desert-thorn)
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Abstract
The invention discloses a preparation method of a diaphragma juglandis fructus vinegar. The preparation method comprises the following steps: soaking, boiling, cooling through spraying water, performing saccharification and alcoholic fermentation, extracting traditional Chinese herbals by ultrasonic waves, carrying out vinegar fermented grain solid fermentation, spraying vinegar, decocting vinegar, and filling vinegar into bottles. The formula is scientific and reasonable, the nutritional and healthcare functions are comprehensive, moreover, the vinegar has the healthcare functions of tonifying kidney, promoting sperm generation, preventing aging, reliving fatigue, and enhancing the immunity, and meets the requirements of consumers, at the same time, the adopted traditional Chinese herbals have prominent medicinal effects and can be used as food; the raw material resources are wide, and the raw materials are safe, and do not have any side or toxic effect.
Description
Technical field
The invention belongs to food processing field, divert one's attention wood vinegar and preparation method thereof more particularly to a kind of Semen Juglandis.
Background technology
Existing vinegar is many based on flavoring agent, does not play its antioxidation, effect of health care etc.；Meanwhile,
Existing vinegar derived product mostly is allotment type fruit vinegar beverage, and sugar is too high unhealthy, and local flavor is single, market
The most wide.
Semen Juglandis Partition in Fructus Juglandis refers to wooden barrier film in the pit of Semen Juglandis.Generally ellipse, diameter 2.5-3cm.Core
Containing multiple chemical composition in Fructus Persicae barrier film, mainly contain flavone, saponin, polysaccharide, alkaloid, tannin etc..?
In Uygur's medical science, Partition in Fructus Juglandis be commonly used to the kidney invigorating, dispel cold, treat seminal emission, spermatorrhea, the enuresis, hematuria, leukorrhagia,
The multiple diseases such as dysentery, hyperhidrosis, oral ulcer, gingival hemorrhage.Semen Juglandis Partition in Fructus Juglandis does not has deep processing substantially at present
Utilizing, time most, it is the rubbish that same walnut shell is dropped together, and only small part crowd is at direct soaked drink
With, its effective ingredient can not get effectively leaching, and effect is the most obvious.The present invention selects the Chinese medicinal herbses such as Partition in Fructus Juglandis,
Add in vinegar solid ferment process, produce a kind of brand-new the kidney invigorating that has and rise essence, antioxidation, enhancing immunity
The vinegar of the effects such as power, without any side effects, long-term drink can be with nourishing and fit keeping function, regulation body constitution.
Summary of the invention
Goal of the invention: the present invention is directed to Semen Juglandis Partition in Fructus Juglandis deep processed product few, and function singleness, effect is the brightest
Aobvious problem, it is provided that a kind of Semen Juglandis is divert one's attention the production technology of wood vinegar, thus realizes making full use of raw material, food
With convenient, improve its nutritive value and economic worth.
Technical scheme: for realizing above-mentioned technical purpose, a kind of Semen Juglandis that proposes of the present invention is divert one's attention wood vinegar, a kind of
Semen Juglandis is divert one's attention the preparation method of wood vinegar, it is characterised in that comprise the steps:
(1) immersion and steaming and decocting: soak in Oryza glutinosa is poured into cylinder, then Oryza glutinosa pulled out, wash down, drip
Dry, then carry out steaming and decocting, to grog；
(2) trickle cooling: with cold water drip washing grog, then take washing water and carry out return pipe, the product temperature of making is uniform up and down,
Obtain the grog after drip washing；
(3) saccharifying and alcohol fermentation: be placed in container by the grog after drip washing, adds clinker weight 1.2-2.0%
Malt yeast and the active dry yeast of 0.4-0.6%, mix laggard row alcohol fermentation thoroughly, 7-10 days alcohol fermentation cycle,
Product temperature control, at 30-35 DEG C, obtains ripe swort, ripe swort alcoholic strength 10-12% (V/V), total acid
Within 0.5g/100ml；
(4) Chinese crude drug ultrasonic extraction: Chinese crude drug formula, in terms of major ingredient, according to mass percent be: 8-10%
Partition in Fructus Juglandis, the 6-8% Radix Astragali, 6-8% Radix Panacis Quinquefolii, 4-6% Fructus Lycii, 2-3% Radix Angelicae Sinensis, use ultrasonic extraction,
To Chinese medicine extraction liquid；
(5) raw vinegar solid fermentation: the Chinese medicine extraction liquid that step (4) obtains is added in ripe swort, so
After by mixing Chinese medicine extraction liquid ripe swort squeeze in fermentation vat, admix fermentation major ingredient Oryza glutinosa weight
The wheat bran of 120-150% and the rice husk of 60-80%, inoculate acetic acid bacteria, and inoculum concentration is the 10-15wt% of ripe swort,
Carry out solid-state layering fermentation 21-22 days, obtain raw vinegar material, unstrained spirits acid >=4.5g/100ml, raw vinegar material is proceeded to envelope
Unstrained spirits pond carries out sealing unstrained spirits, and preservation life is 5-10 days；
(6) vinegar is drenched: squeeze in vinegar spaying pool by the raw vinegar material that envelope unstrained spirits terminates, soak, add fermentation simultaneously
Major ingredient Oryza glutinosa weight 7.0-8.0% rice parching and the Sal of 1.0-1.5%, after soaking 6-8 hour, drench to put and given birth to
Vinegar liquid；
(7) vinegar and fill are decocted: decocted by raw vinegar, temperature 100-110 DEG C, decocting time 30-45min,
Adding the white sugar of 1wt%-2wt% (gross weight of the most raw vinegar) in decoction process, ripe vinegar liquid carries out hot filling,
Fill temperature is not less than 70 DEG C, and fill terminates i.e. to obtain Semen Juglandis and diverts one's attention wood vinegar finished product.
Preferably, in step (1), when soaking Oryza glutinosa, the water yield is higher than material surface 15-20cm, soaks
15-24 hour, temperature during steaming and decocting was 100-110 DEG C, and steaming and decocting 35-40min makes grog ripe and do not sticks with paste, interior
Without hard-core.
In step (2), the temperature of washing water is 40-50 DEG C, and after drip washing, mean temperature controls at 30 ± 2 DEG C.
Beneficial effect: compared with prior art, present invention have the advantage that
(1) inventive formulation is scientific and reasonable, and alimentary health-care function is comprehensive, have concurrently kidney-tonifying sperm-generating, defying age,
The health-care effecies such as resisting fatigue, enhancing human body immunity function, meet people pursue natural, keep healthy, compound disappearing
Take requirement；
(2) Chinese crude drug selected by the present invention is that pharmacological effect effect is obvious, and is integration of edible and medicinal herbs, raw material sources
Extensively it is easy to get, safe without toxic side effect；
(3) instant of the present invention, sour-sweet tasty and refreshing, is suitable for consumers in general, has wide market and sends out
Exhibition prospect.
Detailed description of the invention
Below by specific embodiment, the present invention is further described, it is noted that common for this area
For technical staff, under the premise without departing from the principles of the invention, it is also possible to make some modification and improvement, this
Also should be regarded as belonging to protection scope of the present invention a bit.
Acetic acid bacteria used in the present invention provides for Hengshun Vinegar Industry Co., Ltd., Jingsu.
Embodiment 1
A kind of Semen Juglandis is divert one's attention the preparation method of wood vinegar, comprises the steps:
(1) immersion and steaming and decocting: soaking in pouring 500kg Oryza glutinosa into cylinder, the water yield is with higher than material surface
15-20cm is advisable；Different according to temperature, to soak winter 24 hours, its excess-three season soaks about 15 hours；
Being pulled out by rice after immersion, wash down, drain, then carry out steaming and decocting, temperature is 100 DEG C, and steaming and decocting 35min obtains
Grog, it is desirable to ripe and do not stick with paste, interior without hard-core；
(2) trickle cooling: with clean cold water drip washing grog, then the washing water taking about 40 DEG C carries out return pipe,
The product temperature of making is uniform up and down, and mean temperature controls at about 30 DEG C；
(3) saccharifying and alcohol fermentation: be placed in container by the grog after drip washing, adds clinker weight 1.2%
Malt yeast and the active dry yeast of 0.4%, mix laggard row alcohol fermentation thoroughly.7 days alcohol fermentation cycles, product temperature control
System is at 30 DEG C.The alcoholic strength 10% (V/V) of ripe swort, total acid 0.5g/100ml；
(4) Chinese crude drug ultrasonic extraction:
Chinese crude drug formula, in terms of major ingredient, 8% Partition in Fructus Juglandis, 6% Radix Astragali, 6% Radix Panacis Quinquefolii, 4% Fructus Lycii, 2% work as
Return.
By the Chinese medicine material mixing of above-mentioned preparation, add water and flooded powder 1-2cm, solid-liquid ratio 1: 10, then
Soak 1h, under the conditions of 60 DEG C, ultrasonic frequency 30khz, supersound extraction time 20min, be filtrated to get medicine
Juice, extracts medicine 3 times with clear water, united extraction liquid continuously；
(5) raw vinegar solid fermentation: above-mentioned Chinese medicine extraction liquid is added in swort, then swort is squeezed into fermentation
Chi Zhong, admixes wheat bran and the rice husk of 70% of fermentation major ingredient weight 120%, inoculates acetic acid bacteria, and inoculum concentration is wine
The 10% of wine with dregs amount, carries out solid-state layering fermentation 21-22 days, obtains raw vinegar material, unstrained spirits acid 4.5g/100ml.By vinegar
Unstrained spirits material proceeds to special envelope unstrained spirits pond to carry out sealing unstrained spirits, and preservation life is 7 days；
(6) vinegar is drenched: squeeze in vinegar spaying pool by the raw vinegar material that envelope unstrained spirits terminates, soak, add fermentation simultaneously
Major ingredient weight 7.0% rice parching and the Sal of 1.0%, after soaking 6 hours, pouring is put and is obtained raw vinegar liquid；
(7). decoct vinegar and fill: decocted by raw vinegar, temperature 100 DEG C, decocting time 30min, decoct
During add 1% white sugar.Ripe vinegar liquid carries out hot filling, fill temperature 75 DEG C, and fill terminates i.e. to obtain
Semen Juglandis is divert one's attention wood vinegar finished product.
Embodiment 2
A kind of Semen Juglandis is divert one's attention the preparation method of wood vinegar, comprises the steps:
(1) immersion and steaming and decocting: soaking in pouring 500kg Oryza glutinosa into cylinder, the water yield is with higher than material surface
15-20cm is advisable；Different according to temperature, to soak winter 24 hours, its excess-three season soaks about 15 hours；
Being pulled out by rice after immersion, wash down, drain, then carry out steaming and decocting, temperature is 105 DEG C, and steaming and decocting 35min obtains
Grog, it is desirable to ripe and do not stick with paste, interior without hard-core.
(2). trickle cools down: with clean cold water drip washing grog, then the washing water taking about 45 DEG C carries out return pipe,
The product temperature of making is uniform up and down, and mean temperature controls at about 30 DEG C；
(3). saccharifying and alcohol fermentation: the grog after drip washing is placed in container, add clinker weight 1.6%
Malt yeast and the active dry yeast of 0.5%, mix laggard row alcohol fermentation thoroughly.8 days alcohol fermentation cycles, product temperature
Control at 32 DEG C.The alcoholic strength 10% (V/V) of ripe swort, total acid 0.3g/100ml；
(4) Chinese crude drug ultrasonic extraction
Chinese crude drug formula, in terms of major ingredient, 9% Partition in Fructus Juglandis, 8% Radix Astragali, 6% Radix Panacis Quinquefolii, 5% Fructus Lycii, 2% work as
Return.
By the Chinese medicine material mixing of above-mentioned preparation, add water and flooded powder 1-2cm, solid-liquid ratio 1: 10, then
Soak 1.5h, under the conditions of 60 DEG C, ultrasonic frequency 30khz, supersound extraction time 30min, be filtrated to get
Medicine juice, extracts medicine 3 times with clear water, united extraction liquid continuously.
(5) raw vinegar solid fermentation: above-mentioned Chinese medicine extraction liquid is added in swort, then swort is squeezed into fermentation
Chi Zhong, admixes wheat bran and the rice husk of 75% of fermentation major ingredient weight 135%, inoculates acetic acid bacteria, and inoculum concentration is wine
The 12% of wine with dregs amount, carries out solid-state layering fermentation 21-22 days, obtains raw vinegar material, unstrained spirits acid 5.0g/100ml.By vinegar
Unstrained spirits material proceeds to special envelope unstrained spirits pond to carry out sealing unstrained spirits, and preservation life is 8 days.
(6) vinegar is drenched: squeeze in vinegar spaying pool by the raw vinegar material that envelope unstrained spirits terminates, soak, add fermentation simultaneously
Major ingredient weight 7.5% rice parching and the Sal of 1.2%, after soaking 6 hours, pouring is put and is obtained raw vinegar liquid；
(7) vinegar and fill are decocted: decocted by raw vinegar, temperature 110 DEG C, decocting time 40min, decocted
Journey is added the white sugar of 1.5%.Ripe vinegar liquid carries out hot filling, fill temperature 80 DEG C, and fill terminates i.e. to obtain
Semen Juglandis is divert one's attention wood vinegar finished product.
Embodiment 3
A kind of Semen Juglandis is divert one's attention the preparation method of wood vinegar, comprises the steps:
(1) immersion and steaming and decocting: soaking in pouring 500kg Oryza glutinosa into cylinder, the water yield is with higher than material surface
15-20cm is advisable；Different according to temperature, to soak winter 24 hours, its excess-three season soaks about 15 hours；
Being pulled out by rice after immersion, wash down, drain, then carry out steaming and decocting, temperature is 110 DEG C, and steaming and decocting 40min obtains
Grog, it is desirable to ripe and do not stick with paste, interior without hard-core.
(2) trickle cooling: with clean cold water drip washing grog, then the washing water taking about 50 DEG C carries out return pipe,
The product temperature of making is uniform up and down, and mean temperature controls at about 32 DEG C；
(3) saccharifying and alcohol fermentation: be placed in container by the grog after drip washing, adds clinker weight 2.0%
Malt yeast and the active dry yeast of 0.6%, mix laggard row alcohol fermentation thoroughly.10 days alcohol fermentation cycles, product temperature control
System is at 35 DEG C.The alcoholic strength 12% (V/V) of ripe swort, total acid 0.2g/100ml；
(4) Chinese crude drug ultrasonic extraction
Chinese crude drug formula, in terms of major ingredient, 10% Partition in Fructus Juglandis, 8% Radix Astragali, 8% Radix Panacis Quinquefolii, 6% Fructus Lycii, 3%
Radix Angelicae Sinensis.
By the Chinese medicine material mixing of above-mentioned preparation, add water and flooded powder 1-2cm, solid-liquid ratio 1: 10, then
Soak 2h, under the conditions of 60 DEG C, ultrasonic frequency 30khz, supersound extraction time 40min, be filtrated to get medicine
Juice, extracts medicine 3 times with clear water, united extraction liquid continuously.
(5) raw vinegar solid fermentation: above-mentioned Chinese medicine extraction liquid is added in swort, then swort is squeezed into fermentation
Chi Zhong, admixes wheat bran and the rice husk of 80% of fermentation major ingredient weight 150%, inoculates acetic acid bacteria, and inoculum concentration is wine
The 15% of wine with dregs amount, carries out solid-state layering fermentation 21 days, obtains raw vinegar material, unstrained spirits acid 5.5g/100ml.By raw vinegar
Material proceeds to special envelope unstrained spirits pond to carry out sealing unstrained spirits, and preservation life is 10 days.
(6) vinegar is drenched: squeeze in vinegar spaying pool by the raw vinegar material that envelope unstrained spirits terminates, soak, add fermentation simultaneously
Major ingredient weight 8.0% rice parching and the Sal of 1.5%, after soaking 8 hours, pouring is put and is obtained raw vinegar liquid；
(7) vinegar and fill are decocted: decocted by raw vinegar, temperature 110 DEG C, decocting time 45min, decocted
Journey is added the white sugar of 2%.Ripe vinegar liquid carries out hot filling, and fill temperature 85 DEG C, fill terminates i.e. to obtain core
Fructus Persicae is divert one's attention wood vinegar finished product.
For above example, total flavones and the total saponin content of wood vinegar of diverting one's attention Semen Juglandis are determined respectively,
And using commercially available common vinegar as comparison, result is as shown in table 1.
Assay method:
(1) general flavone content: after flavone compound in sample is carried out extraction purification, use spectrophotography
Under 510nm wavelength, measure its absorbance, compare with rutin standard substance, carry out determining of total flavones in determinand
It is fixed to measure.
(2) total saponin content: after saponins compound in sample is carried out extraction purification, use spectrophotography
Under 560nm wavelength, measure its absorbance, compare with ginsenoside Re's standard substance, carry out total soap in determinand
The quantitative determination of glycosides.
Table 1
| Testing index | Embodiment 1 | Embodiment 2 | Embodiment 3 | Commercially available common vinegar |
| The content of total flavones | 1.877mg/ml | 1.925mg/ml | 2.118mg/ml | 0.865mg/ml |
| The content of total saponins | 1.083mg/ml | 1.236mg/ml | 1.365mg/ml | 0.787mg/ml |
In sum, inventive formulation is scientific and reasonable, and alimentary health-care function is comprehensive, has kidney-tonifying sperm-generating, anti-ageing concurrently
Always, the health-care effect such as resisting fatigue, enhancing human body immunity function, meet people pursue natural, keep healthy, compound
Consumption requirement.
Claims (3)
1. a Semen Juglandis is divert one's attention the preparation method of wood vinegar, it is characterised in that comprise the steps:
(1) immersion and steaming and decocting: soak in Oryza glutinosa is poured into cylinder, then Oryza glutinosa pulled out, wash down, drip
Dry, then carry out steaming and decocting, to grog；
(2) trickle cooling: with cold water drip washing grog, then take washing water and carry out return pipe, the product temperature of making is uniform up and down,
Obtain the grog after drip washing；
(3) saccharifying and alcohol fermentation: be placed in container by the grog after drip washing, adds clinker weight 1.2-2.0%
Malt yeast and the active dry yeast of 0.4-0.6%, mix laggard row alcohol fermentation thoroughly, 7-10 days alcohol fermentation cycle,
Product temperature control, at 30-35 DEG C, obtains ripe swort, ripe swort alcoholic strength 10-12% (V/V), total acid
Within 0.5g/100ml；
(4) Chinese crude drug ultrasonic extraction: Chinese crude drug formula, in terms of major ingredient, according to mass percent be: 8-10%
Partition in Fructus Juglandis, the 6-8% Radix Astragali, 6-8% Radix Panacis Quinquefolii, 4-6% Fructus Lycii, 2-3% Radix Angelicae Sinensis, use ultrasonic extraction,
To Chinese medicine extraction liquid；
(5) raw vinegar solid fermentation: the Chinese medicine extraction liquid that step (4) obtains is added in ripe swort, so
After by mixing Chinese medicine extraction liquid ripe swort squeeze in fermentation vat, admix fermentation major ingredient Oryza glutinosa weight
The wheat bran of 120-150% and the rice husk of 60-80%, inoculate acetic acid bacteria, and inoculum concentration is the 10-15wt% of ripe swort,
Carry out solid-state layering fermentation 21-22 days, obtain raw vinegar material, unstrained spirits acid >=4.5g/100ml, raw vinegar material is proceeded to envelope
Unstrained spirits pond carries out sealing unstrained spirits, and preservation life is 5-10 days；
(6) vinegar is drenched: squeeze in vinegar spaying pool by the raw vinegar material that envelope unstrained spirits terminates, soak, add fermentation simultaneously
Major ingredient Oryza glutinosa weight 7.0-8.0% rice parching and the Sal of 1.0-1.5%, after soaking 6-8 hour, drench to put and given birth to
Vinegar liquid；
(7) vinegar and fill are decocted: decocted by raw vinegar, temperature 100-110 DEG C, decocting time 30-45min,
Adding the white sugar of 1wt%-2wt% in decoction process, ripe vinegar liquid carries out hot filling, and fill temperature is not less than
70 DEG C, fill terminates i.e. to obtain Semen Juglandis and diverts one's attention wood vinegar finished product.
Semen Juglandis the most according to claim 1 is divert one's attention the preparation method of wood vinegar, it is characterised in that step (1)
In, when soaking Oryza glutinosa, the water yield is higher than material surface 15-20cm, soaks 15-24 hour, temperature during steaming and decocting
Degree is 100-110 DEG C, and steaming and decocting 35-40min makes grog ripe and do not sticks with paste, interior without hard-core.
Semen Juglandis the most according to claim 1 is divert one's attention the preparation method of wood vinegar, it is characterised in that step (2)
In, the temperature of washing water is 40-50 DEG C, and after drip washing, mean temperature controls at 30 ± 2 DEG C.
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| CN107012065A (en) * | 2017-06-02 | 2017-08-04 | 江苏恒顺醋业股份有限公司 | A kind of brewing method rich in anthocyanidin vinegar |
| CN107674815A (en) * | 2017-11-17 | 2018-02-09 | 江苏恒顺醋业股份有限公司 | The preparation method of vinegar is twisted with the fingers a kind ofly |
| CN107988036A (en) * | 2018-01-24 | 2018-05-04 | 石嘴山市田园食品有限公司 | The method that solid fermentation method produces medlar vinegar |
| CN108330053A (en) * | 2018-04-03 | 2018-07-27 | 镇江市恒升酿造有限公司 | A kind of flavor aromatic vinegar brewage process |
| CN108841563A (en) * | 2018-08-10 | 2018-11-20 | 宁夏万兴和食品加工有限公司 | A kind of manufacture craft of solid state process five cereals vinegar |
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| CN107012065A (en) * | 2017-06-02 | 2017-08-04 | 江苏恒顺醋业股份有限公司 | A kind of brewing method rich in anthocyanidin vinegar |
| CN107674815A (en) * | 2017-11-17 | 2018-02-09 | 江苏恒顺醋业股份有限公司 | The preparation method of vinegar is twisted with the fingers a kind ofly |
| CN107988036A (en) * | 2018-01-24 | 2018-05-04 | 石嘴山市田园食品有限公司 | The method that solid fermentation method produces medlar vinegar |
| CN107988036B (en) * | 2018-01-24 | 2021-02-23 | 石嘴山市田园食品有限公司 | Method for producing medlar vinegar by solid fermentation method |
| CN108330053A (en) * | 2018-04-03 | 2018-07-27 | 镇江市恒升酿造有限公司 | A kind of flavor aromatic vinegar brewage process |
| CN108841563A (en) * | 2018-08-10 | 2018-11-20 | 宁夏万兴和食品加工有限公司 | A kind of manufacture craft of solid state process five cereals vinegar |
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Application publication date: 20160914 |