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CN105936689A - Asphalt reducing agent and preparation method thereof - Google Patents

Asphalt reducing agent and preparation method thereof Download PDF

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Publication number
CN105936689A
CN105936689A CN201610555133.4A CN201610555133A CN105936689A CN 105936689 A CN105936689 A CN 105936689A CN 201610555133 A CN201610555133 A CN 201610555133A CN 105936689 A CN105936689 A CN 105936689A
Authority
CN
China
Prior art keywords
reducing agent
mass parts
asphalt
colophonium
preparation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610555133.4A
Other languages
Chinese (zh)
Inventor
刘红飚
陈建刚
角述宾
任志远
高国岗
漆泰生
王庆高
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Yunnan Highway & Bridge Co Ltd
Original Assignee
Yunnan Highway & Bridge Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Yunnan Highway & Bridge Co Ltd filed Critical Yunnan Highway & Bridge Co Ltd
Priority to CN201610555133.4A priority Critical patent/CN105936689A/en
Publication of CN105936689A publication Critical patent/CN105936689A/en
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L13/00Compositions of rubbers containing carboxyl groups
    • C08L13/02Latex
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L63/00Compositions of epoxy resins; Compositions of derivatives of epoxy resins
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/03Polymer mixtures characterised by other features containing three or more polymers in a blend

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Road Paving Structures (AREA)
  • Compositions Of Macromolecular Compounds (AREA)

Abstract

The invention provides an asphalt reducing agent and a preparation method thereof, and relates to the technical field of asphalt, in particular to the asphalt reducing agent which is used for reducing aged asphalt and is good in reduction effect and the preparation method of the asphalt reducing agent. The asphalt reducing agent is characterized by being prepared by mixing, by mass, 20-30 parts of reducing agent base materials, 60-70 parts of 90# solvent oil and 10-15 parts of carboxy styrene-butadiene latex, wherein each part of the reducing agent base material comprises, by mass, 20-40 parts of kieselguhr, 40-50 parts of water-borne epoxy resin and 5-10 parts of waterborne polyurethane. According to the asphalt reducing agent and the preparation method thereof, aged asphalt paste on the surface layer of an asphalt pavement can be effectively updated and reduced; meanwhile, asphalt which is not subjected to aging is protected, the original feature is maintained, and the aging time is slowed down; compared with a traditional fog sealing layer, the asphalt reducing agent sealing layer mainly has the advantages that the asphalt aging action is activated, and the service time is prolonged.

Description

Colophonium reducing agent and preparation method thereof
Technical field
The present invention relates to field of bitumen technology, especially one is used for reducing aged asphalt, and the good Colophonium of reduction effect is also Former dose and preparation method thereof.
Background technology
Along with the fast development of China's communication, it is extremely to be necessary that built highway carries out preventive maintenance 's.The technology of Preventive maintenance for highway is the most, but one of Colophonium reducing agent technology the most most practical, maximally effective, can be extensively The preventive maintenance being used in each standard highway on.This technology is when road surface occurs that aging, loose, crack, pit, water damage During the local early diseases such as evil idea, Colophonium reducing agent is sprayed on bituminous paving, to recover the performance of asphalt pavement material, improves Pavement Condition, delaying aging, in the effective service life extending bituminous paving, reduces the fare of life-span of highway.
Summary of the invention
To be solved by this invention is exactly to occur after existing bituminous paving life-time service catabiosis to reduce bituminous paving to make By performance and the problem in life-span, it is provided that one is used for reducing aged asphalt, Colophonium reducing agent that reduction effect is good and preparation side thereof Method.
Colophonium reducing agent of the present invention and preparation method thereof, it is characterised in that this reducing agent includes going back of 20~30 mass parts Former dose of base material, 60~70 mass parts No. 90 solvent naphthas and the carboxylic styrene butadiene latex of 10~15 mass parts be mixed to prepare, wherein Every part of reducing agent base material comprises 20~40 mass parts kieselguhr, 40~50 mass parts aqueous epoxy resins and 5~10 mass Part aqueous polyurethane.
Described Colophonium reducing agent is prepared by following steps:
(1), prepare reducing agent base material: take 40~50 mass parts aqueous epoxy resins, add 20~40 mass parts kieselguhr and 5~ 10 mass parts aqueous polyurethanes, obtain reducing agent base solution after mix is uniform;
(2), the reducing agent base solution that will obtain in step 1, take in the funnel that 20~30 mass parts pour high speed shear instrument into, beat Drive the switch of high speed shear instrument, the most uniformly pour No. 90 solvent naphthas of 60~70 mass parts simultaneously into, shear time be 30s~ 60s, then opens the flowing water Valve of funnel, collects and obtains semi-finished product;
(3), by step 2 being collected after the semi-finished product obtained are heated to 120 DEG C, the carboxylic styrene butadiene latex of 10~15 mass parts is added Persistently mix, obtain Colophonium reducing agent.
Colophonium reducing agent of the present invention and preparation method thereof, technique is simple, easy to use, directly by the Colophonium for preparing also Former dose is sprayed on asphalt roads, it is possible to effective renewal and reduction bituminous paving top layer have occurred and that aging asphalt cement Body, protects the part Colophonium being not yet aging simultaneously so that it is " maintaining original performance, slow down ageing time ", the drip of the present invention Blue or green reducing agent sealing is compared with tradition mist sealing, and main advantage is to activate aged asphalt effect, extends the use time.
Detailed description of the invention
Embodiment 1: a kind of Colophonium reducing agent and preparation method thereof, this reducing agent include 20 mass parts reducing agent base material, No. 90 solvent naphthas of 60 mass parts and the carboxylic styrene butadiene latex of 10 mass parts are mixed to prepare, and wherein wrap in every part of reducing agent base material Containing 20 mass parts kieselguhr, 40 mass parts aqueous epoxy resins and 5 mass parts aqueous polyurethanes.Colophonium reducing agent is by following Step prepares:
(1), prepare reducing agent base material: take 40 mass parts aqueous epoxy resins, add 20 mass parts kieselguhr and 5 mass parts aqueouss Polyurethane, obtains reducing agent base solution after mix is uniform;
(2), the reducing agent base solution that will obtain in step 1, take in the funnel that 20 mass parts pour high speed shear instrument into, open height The switch of speed boxshear apparatus, the most uniformly pours No. 90 solvent naphthas of 60 mass parts into simultaneously, and shear time is 30s, then opens The flowing water Valve of funnel, collects and obtains semi-finished product;
(3), will collect after the semi-finished product obtained are heated to 120 DEG C in step 2, the carboxylic styrene butadiene latex adding 10 mass parts continues Mixing, obtains Colophonium reducing agent.
Case one: the individual village Class I highway test to reduction effect
A, matrix pitch reduction situation
B, road surface three norms reduction situation
Embodiment 2: a kind of Colophonium reducing agent and preparation method thereof, this reducing agent include 30 mass parts reducing agent base material, No. 90 solvent naphthas of 70 mass parts and the carboxylic styrene butadiene latex of 15 mass parts are mixed to prepare, and wherein wrap in every part of reducing agent base material Containing 40 mass parts kieselguhr, 50 mass parts aqueous epoxy resins and 10 mass parts aqueous polyurethanes.Colophonium reducing agent by with Lower step prepares:
(1), prepare reducing agent base material: take 50 mass parts aqueous epoxy resins, add 40 mass parts kieselguhr and 10 mass parts water Property polyurethane, mix uniformly after obtain reducing agent base solution;
(2), the reducing agent base solution that will obtain in step 1, take in the funnel that 30 mass parts pour high speed shear instrument into, open height The switch of speed boxshear apparatus, the most uniformly pours No. 90 solvent naphthas of 70 mass parts into simultaneously, and shear time is 60s, then opens The flowing water Valve of funnel, collects and obtains semi-finished product;
(3), will collect after the semi-finished product obtained are heated to 120 DEG C in step 2, the carboxylic styrene butadiene latex adding 15 mass parts continues Mixing, obtains Colophonium reducing agent.
Embodiment 3: a kind of Colophonium reducing agent and preparation method thereof, reducing agent include the reducing agent base material of 25 mass parts, 65 No. 90 solvent naphthas of mass parts and the carboxylic styrene butadiene latex of 13 mass parts are mixed to prepare, and wherein comprise in every part of reducing agent base material 30 mass parts kieselguhr, 45 mass parts aqueous epoxy resins and 7 mass parts aqueous polyurethanes.Colophonium reducing agent is by following step Rapid prepared:
(1), prepare reducing agent base material: take 45 mass parts aqueous epoxy resins, add 30 mass parts kieselguhr and 7 mass parts aqueouss Polyurethane, obtains reducing agent base solution after mix is uniform;
(2), the reducing agent base solution that will obtain in step 1, take in the funnel that 25 mass parts pour high speed shear instrument into, open height The switch of speed boxshear apparatus, the most uniformly pours No. 90 solvent naphthas of 65 mass parts into simultaneously, and shear time is 45s, then opens The flowing water Valve of funnel, collects and obtains semi-finished product;
(3), will collect after the semi-finished product obtained are heated to 120 DEG C in step 2, the carboxylic styrene butadiene latex adding 13 mass parts continues Mixing, obtains Colophonium reducing agent.

Claims (2)

1. Colophonium reducing agent and preparation method thereof, it is characterised in that this reducing agent includes the reducing agent base of 20~30 mass parts Material, 60~70 mass parts No. 90 solvent naphthas and the carboxylic styrene butadiene latex of 10~15 mass parts be mixed to prepare, wherein every part also Former dose of base material comprises 20~40 mass parts kieselguhr, 40~50 mass parts aqueous epoxy resins and 5~10 mass parts aqueouss Polyurethane.
2. Colophonium reducing agent as claimed in claim 1 and preparation method thereof, it is characterised in that described Colophonium reducing agent passes through Following steps prepare:
(1), prepare reducing agent base material: take 40~50 mass parts aqueous epoxy resins, add 20~40 mass parts kieselguhr and 5~ 10 mass parts aqueous polyurethanes, obtain reducing agent base solution after mix is uniform;
(2), the reducing agent base solution that will obtain in step 1, take in the funnel that 20~30 mass parts pour high speed shear instrument into, beat Drive the switch of high speed shear instrument, the most uniformly pour No. 90 solvent naphthas of 60~70 mass parts simultaneously into, shear time be 30s~ 60s, then opens the flowing water Valve of funnel, collects and obtains semi-finished product;
(3), by step 2 being collected after the semi-finished product obtained are heated to 120 DEG C, the carboxylic styrene butadiene latex of 10~15 mass parts is added Persistently mix, obtain Colophonium reducing agent.
CN201610555133.4A 2016-07-15 2016-07-15 Asphalt reducing agent and preparation method thereof Pending CN105936689A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610555133.4A CN105936689A (en) 2016-07-15 2016-07-15 Asphalt reducing agent and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610555133.4A CN105936689A (en) 2016-07-15 2016-07-15 Asphalt reducing agent and preparation method thereof

Publications (1)

Publication Number Publication Date
CN105936689A true CN105936689A (en) 2016-09-14

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610555133.4A Pending CN105936689A (en) 2016-07-15 2016-07-15 Asphalt reducing agent and preparation method thereof

Country Status (1)

Country Link
CN (1) CN105936689A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108126475A (en) * 2017-12-28 2018-06-08 安徽昊源化工集团有限公司 A kind of method for improving decarburization hydrogen purity

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1628152A (en) * 2002-05-14 2005-06-15 巴斯福公司 Improved asphalt emulsions for treatment of road surfaces
CN104177743A (en) * 2014-09-15 2014-12-03 重庆罗兹沃柯交通科技有限公司 Novel asphalt pavement fog seal maintenance material and preparation method thereof
CN104312175A (en) * 2014-10-16 2015-01-28 盐城工学院 Asphalt modifier, modified emulsified asphalt, modified asphalt mixture and respective preparation methods thereof
CN104497603A (en) * 2015-01-06 2015-04-08 山西省交通科学研究院 Water-borne epoxy composite-containing emulsified asphalt cold-recycling agent and preparation method thereof
CN105061846A (en) * 2015-09-14 2015-11-18 广西大学 Asphalt pavement reducing agent and preparation method for same

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1628152A (en) * 2002-05-14 2005-06-15 巴斯福公司 Improved asphalt emulsions for treatment of road surfaces
CN104177743A (en) * 2014-09-15 2014-12-03 重庆罗兹沃柯交通科技有限公司 Novel asphalt pavement fog seal maintenance material and preparation method thereof
CN104312175A (en) * 2014-10-16 2015-01-28 盐城工学院 Asphalt modifier, modified emulsified asphalt, modified asphalt mixture and respective preparation methods thereof
CN104497603A (en) * 2015-01-06 2015-04-08 山西省交通科学研究院 Water-borne epoxy composite-containing emulsified asphalt cold-recycling agent and preparation method thereof
CN105061846A (en) * 2015-09-14 2015-11-18 广西大学 Asphalt pavement reducing agent and preparation method for same

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
沥青生产与应用技术手册编委会编: "《沥青生产与应用技术手册》", 31 May 2010 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108126475A (en) * 2017-12-28 2018-06-08 安徽昊源化工集团有限公司 A kind of method for improving decarburization hydrogen purity

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Application publication date: 20160914