[go: up one dir, main page]

CN105921760B - The process equipment and its processing technology of siller tin oxide - Google Patents

The process equipment and its processing technology of siller tin oxide Download PDF

Info

Publication number
CN105921760B
CN105921760B CN201610487184.8A CN201610487184A CN105921760B CN 105921760 B CN105921760 B CN 105921760B CN 201610487184 A CN201610487184 A CN 201610487184A CN 105921760 B CN105921760 B CN 105921760B
Authority
CN
China
Prior art keywords
powder
babinet
smelting apparatus
atomising device
tin oxide
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201610487184.8A
Other languages
Chinese (zh)
Other versions
CN105921760A (en
Inventor
孙珂杨
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
NINGBO KEYANG PRECIOUS METAL ALLOYS TECHNOLOGY Co Ltd
Original Assignee
NINGBO KEYANG PRECIOUS METAL ALLOYS TECHNOLOGY Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by NINGBO KEYANG PRECIOUS METAL ALLOYS TECHNOLOGY Co Ltd filed Critical NINGBO KEYANG PRECIOUS METAL ALLOYS TECHNOLOGY Co Ltd
Priority to CN201610487184.8A priority Critical patent/CN105921760B/en
Publication of CN105921760A publication Critical patent/CN105921760A/en
Application granted granted Critical
Publication of CN105921760B publication Critical patent/CN105921760B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00Making metallic powder or suspensions thereof
    • B22F9/02Making metallic powder or suspensions thereof using physical processes
    • B22F9/06Making metallic powder or suspensions thereof using physical processes starting from liquid material
    • B22F9/08Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying
    • B22F9/082Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying atomising using a fluid
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00Making metallic powder or suspensions thereof
    • B22F9/02Making metallic powder or suspensions thereof using physical processes
    • B22F9/06Making metallic powder or suspensions thereof using physical processes starting from liquid material
    • B22F9/08Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying
    • B22F9/082Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying atomising using a fluid
    • B22F2009/086Cooling after atomisation
    • B22F2009/0876Cooling after atomisation by gas

Landscapes

  • Apparatuses For Bulk Treatment Of Fruits And Vegetables And Apparatuses For Preparing Feeds (AREA)
  • Manufacture And Refinement Of Metals (AREA)

Abstract

The invention discloses the process equipment of siller tin oxide and its processing technologys, including smelting apparatus and PLC control system, smelting apparatus is connected with atomising device, valve is provided between smelting apparatus and atomising device, supercharging device and vacuum extractor are connected on atomising device, atomising device bottom is provided with powder ejiction opening, powder ejiction opening is connected with powder and collects screening plant, it includes babinet that powder, which collects screening plant, babinet is separated into coarse fodder chamber and fines chamber by partition board, babinet is provided with fumarole at powder ejiction opening, the feeding back device for connecting the smelting apparatus is provided on the coarse fodder chamber.The process equipment and its processing technology of this kind of siller tin oxide can reduce the metal powder of bulky grain, so that oxidization of metal powder is more abundant, product quality improves.

Description

The process equipment and its processing technology of siller tin oxide
Technical field
The invention belongs to metal fabrication techniques fields, the specifically process equipment and its processing technology of siller tin oxide.
Background technology
With the development of science and technology, demand of the industry manufacture field to electromechanical compo is increasing, while also its performance is referred to Mark requires higher and higher.Sliver oxidized tin contactor materials are the novel non-toxic electrical contact materials that have developed rapidly in recent years, have heat steady It sets, the advantages that resistance to arc erosion and resistance fusion welding are strong, is the ideal material at present in contactor, relay field.
Existing siller tin oxide processing technology step is:By silver ingot, tin is placed in melting and ingot casting in smelting furnace, then will be golden Belong to ingot and be processed into clast, aoxidizes to obtain the mixing material based on siller tin oxide through high temperature and pressure, it is broken through over mechanical processing, Clast is press-formed in punching block, is then squeezed into item, band at high temperature, siller tin oxide item, band are obtained using drawing Material.
The existing method that clast is made in ingot is usually used ball mill ball milling or uses spray-on process, ball mill It may repeatedly be acted on by grinding compression in mechanical milling process, be caused to be present on the particle surface intrinsic or newborn At crack extesion, and then it is broken or generate plastic deformation to be directed at its.Certain level-one that is generated when the particle is constantly crushed Newly particle is just difficult to further levigate, this is because the crackle on new grain surface is thinner, and a certain minimum fracture occurs The cause that the crackle probability of stress also reduces.When shattering process continues, required finished breaking stress may increase Greatly to the degree for making particle generate plastic deformation.At this point, with the generation of plastic deformation, particle just will not be most by levigate.Cause This, can be there are one granularity limiting value when grinding material, that is to say, that when the grinding of material enters the range of ultra-fine grinding, The pulverization of ball mill is just more and more difficult.All there is an actual grinding limit in most of grinding systems, this One limit depends on grinding product particle and generates the tendency built up again mainly, and builds up and set up between broken The physical equilibrium come.Long extension Ball-milling Time is skimble-skamble, only results in the increase of energy consumption, because of meticulous particle The elastic energy made needed for crack extesion can not be effectively stored, therefore powder particle made from ball-milling method is relatively large, rear It is difficult in continuous oxidation process fully oxidized.Spray-on process has more advantage in contrast, and spray-on process is to lead to molten metal liquid It crosses high pressure to spray from nozzle, the method for forming powder after the drop cooling of ejection, the powder that spray-on process sprays is relative to ball milling The powder smaller that machine ball milling comes out can aoxidize more fully during subsequent oxidation, and the particle that spray-on process nozzle sprays also has Size, when due to spray it is uneven caused by there are the drops of some bulky grains, second is that the drop due to ejection is not coagulating also Big liquid is formed after contact before knot, the powder of bulky grain is had after the droplet formation powder sprayed so as to cause spray-on process End causes subsequent oxidation process to be difficult to fully oxidized.
Invention content
In view of the shortcomings of the prior art, providing the process equipment and its processing technology of siller tin oxide, this kind silver aoxidizes the present invention The process equipment and its processing technology of tin can reduce the metal powder of bulky grain, so that oxidization of metal powder is more filled Point, product quality improves.
In order to solve the above-mentioned technical problem, the present invention is addressed by following technical proposals:The processing of siller tin oxide is set It is standby, including smelting apparatus and PLC control system, the smelting apparatus be connected with atomising device, the smelting apparatus and institute It states and is provided with valve between atomising device, supercharging device and vacuum extractor, the atomization are connected on the atomising device Bottom of device is provided with powder ejiction opening, and the powder ejiction opening is connected with powder and collects screening plant, the powder collection screen Screening device includes babinet, and the partition board for keeping the connection of babinet upper end is vertically arranged in the middle part of the babinet, and the partition board divides babinet It is divided into coarse fodder chamber and fines chamber, the babinet is provided with fumarole, the fumarole connection at the powder ejiction opening It includes being provided with out on motor and impeller, with the babinet of the fumarole opposite side to have air-jet device, the air-jet device Stomata, the venthole are equipped with check valve, and the air inlet of the air-jet device is connected with refrigerating plant, fines bottom of chamber portion It is provided with discharge port, the feeding back device for connecting the smelting apparatus is provided on the coarse fodder chamber.The equipment passes through vacuum means Setting the air evacuated in atomising device prevents the molten metal in atomising device from being aoxidized, and passes through refrigerating plant and air-jet device Cooperation sprays cold air so that the molten metal rapid curing that atomising device sprays, to prevent molten metal from being contacted after ejection It bonds and forms bulky grain powder, while blowing so that the powder of bulky grain drops into coarse fodder intracavitary, short grained powder drops into The powder of fines intracavitary, bulky grain backs into smelting apparatus refuse from feeding back device, so that being come out from discharge port Powder be all fine powder, be conducive to the later stage oxidation.
In above-mentioned technical proposal, it is preferred that the feeding back device includes being connected to coarse fodder chamber both sides to have feed back pipeline, described Feed back pipeline is formed into a loop and connects the smelting apparatus, and the chain of head and the tail connection, the chain are provided in the feed back pipeline Be provided on item with the matched delivery board of feed back pipe diameter, be provided on the feed back pipeline matched with the chain Sprocket wheel is connected with the sprocket wheel on the output shaft on the motor, and when the electric motor starting, the sprocket wheel and the impeller are same When rotate.Make the operation that the air-flow at fumarole is not interfered with during feed back using this structure, by impeller and chain Wheel is by motor control while unlatching is so that chain will be run when blowing device works, and prevents the coarse fodder in coarse fodder chamber Accumulation is excessively fallen into fines case, while the structure generates certain vibration to prevent powder from accumulating at runtime.
In above-mentioned technical proposal, it is preferred that the refrigerating plant 9 is connected with nitrogen cylinder 711, and nitrogen is filled in refrigerating plant 9 Gas prevents air from entering babinet, prevents metal by oxidation and so that returning to smelting apparatus so that the ejection nitrogen of fumarole 74 Interior metal is difficult to be melted.
The processing technology of the process equipment of siller tin oxide, includes the following steps:1, silver ingot, tin slab the melting is put into fill Set interior melting;2, start the vacuum extractor and evacuate the air in the atomising device, open the valve by the gold of melting Category is put into atomising device and closes the valve;3, starting the motor makes the impeller and the sprocket wheel rotate, Start the refrigerating plant, starts the supercharging device and nitrogen supercharging is filled with to atomising device.
In above-mentioned technical proposal, it is preferred that further include being filled with nitrogen to replace in the babinet between step 2 and step 3 The step of air.
Compared with prior art, the present invention having the advantages that:The equipment evacuates atomization dress by vacuum extractor Air in setting prevents the molten metal in atomising device from being aoxidized, and is sprayed by refrigerating plant and air-jet device cooperation cold Gas so that the molten metal rapid curing that atomising device sprays is formed greatly to prevent molten metal from contacting to bond after ejection Particle powder, while blowing so that the powder of bulky grain drops into coarse fodder intracavitary, short grained powder drops into fines intracavitary, greatly The powder of particle backs into smelting apparatus refuse from feed back pipeline, so that the powder come out from discharge port is all thin Small powder is conducive to later stage oxidation, and impeller and sprocket wheel are controlled by motor and opened simultaneously so that working in blowing device When chain will run, prevent coarse fodder in coarse fodder chamber from accumulating and excessively fall into fines case.
Description of the drawings
Fig. 1 is the structural schematic diagram of the embodiment of the present invention.
Fig. 2 is the left view of Fig. 1.
Fig. 3 is the attachment structure schematic diagram of chain and delivery board.
Specific implementation mode
Present invention is further described in detail with reference to the accompanying drawings and detailed description:Referring to Fig. 1 to Fig. 3, silver-colored oxygen Change the process equipment of tin, including smelting apparatus 1 and PLC control system, the smelting apparatus 1 is connected with atomising device 2, described Valve 3 is provided between smelting apparatus 1 and the atomising device 2, be connected on the atomising device 2 supercharging device 4 and Vacuum extractor 5,2 bottom of the atomising device are provided with powder ejiction opening 21, and the powder ejiction opening 21 is connected with powder receipts Collect screening plant 6, it includes babinet 7 that the powder, which collects screening plant 6, and 7 middle part of the babinet, which is vertically arranged with, to keep on babinet 7 Hold the partition board 71 of connection, the partition board 71 that babinet 7 is separated into coarse fodder chamber 72 and fines chamber 73, the babinet 7 is close to described Fumarole 74 is provided at powder ejiction opening 21, the fumarole 74 is connected with air-jet device 8, and the air-jet device 8 includes electricity Venthole 75 is provided on machine and impeller, with the babinet 7 of 74 opposite side of the fumarole, the venthole 75 is equipped with single To valve 76, the air inlet of the air-jet device 8 is connected with refrigerating plant 9, and 73 bottom of fines chamber is provided with discharge port 77, institute State the feeding back device 10 for being provided on coarse fodder chamber 72 and connecting the smelting apparatus 1.The equipment is evacuated by vacuum extractor and is atomized Air in device prevents the molten metal in atomising device from being aoxidized, and is sprayed by refrigerating plant and air-jet device cooperation cold Gas so that the molten metal rapid curing that atomising device sprays is formed greatly to prevent molten metal from contacting to bond after ejection Particle powder, while blowing so that the powder of bulky grain drops into coarse fodder intracavitary, short grained powder drops into fines intracavitary, greatly The powder of particle backs into smelting apparatus refuse from feeding back device, so that the powder come out from discharge port is all thin Small powder is conducive to later stage oxidation.
The feeding back device 10 includes being connected to 72 both sides of coarse fodder chamber to have feed back pipeline 78, the feed back pipeline 78 to be formed back Road simultaneously connects the smelting apparatus 1, and the chain 79 of head and the tail connection is provided in the feed back pipeline 78, is arranged on the chain 79 There is the delivery board 710 with 78 match of pipe diameter of feed back pipeline, is provided on the feed back pipeline 78 and is matched with the chain 79 Sprocket wheel, be connected with the sprocket wheel on the output shaft on the motor, the sprocket wheel and the impeller when the electric motor starting It rotates simultaneously.Make the operation that the air-flow at fumarole is not interfered with during feed back using this structure, by impeller with By motor control, unlatching prevents thick in coarse fodder chamber so that chain will be run when blowing device works sprocket wheel simultaneously Material heap product is excessively fallen into fines case, while the structure generates certain vibration to prevent powder from accumulating at runtime.
The refrigerating plant 9 is connected with nitrogen cylinder 711, is filled with nitrogen in refrigerating plant 9 so that fumarole 74 sprays Nitrogen prevents air from entering babinet, prevents metal by oxidation and so that the metal returned in smelting apparatus is difficult to be melted.
The processing technology of the process equipment of siller tin oxide, includes the following steps:1, silver ingot, tin slab the melting is put into fill Set melting in 1;2, start the vacuum extractor 5 and evacuate air in the atomising device 2, opening the valve 3 will melt Metal be put into atomising device 2 and close the valve 3;3, start the motor and make the impeller and the sprocket wheel Rotation, starts the refrigerating plant 9, starts the supercharging device 4 and be filled with nitrogen supercharging to atomising device 2.
Further include the steps that being filled with nitrogen to replace air in the babinet 7 between step 2 and step 3.

Claims (4)

1. the process equipment of siller tin oxide, including smelting apparatus(1)And PLC control system, the smelting apparatus(1)It is connected with Atomising device(2), it is characterised in that:The smelting apparatus(1)And the atomising device(2)Between be provided with valve(3), institute State atomising device(2)On be connected with supercharging device(4)And vacuum extractor(5), the atomising device(2)Bottom is provided with powder Expect ejiction opening(21), the powder ejiction opening(21)It is connected with powder and collects screening plant(6), the powder collection screening plant (6)Including babinet(7), the babinet(7)Middle part is vertically arranged with holding babinet(7)The partition board of upper end connection(71), it is described every Plate(71)By babinet(7)It is separated into coarse fodder chamber(72)And fines chamber(73), the babinet(7)Close to the powder ejiction opening (21)Place is provided with fumarole(74), the fumarole(74)It is connected with air-jet device(8), the air-jet device(8)Including electricity Machine and impeller, with the fumarole(74)The babinet of opposite side(7)On be provided with venthole(75), the venthole(75) It is equipped with check valve(76), the air-jet device(8)Air inlet be connected with refrigerating plant(9), the fines chamber(73)Bottom It is provided with discharge port(77), the coarse fodder chamber(72)On be provided with the connection smelting apparatus(1)Feeding back device(10), described Feeding back device(10)Including being connected to coarse fodder chamber(72)The feed back pipeline of both sides(78), the feed back pipeline(78)Forming circuit is simultaneously Connect the smelting apparatus(1), the feed back pipeline(78)Inside it is provided with the chain of head and the tail connection(79), the chain(79)On It is provided with and the feed back pipeline(78)The delivery board of match of pipe diameter(710), the feed back pipeline(78)On be provided with it is described Chain(79)Matched sprocket wheel is connected with the sprocket wheel on the output shaft on the motor, the chain when the electric motor starting Wheel rotates simultaneously with the impeller.
2. the process equipment of siller tin oxide as described in claim 1, it is characterised in that:The refrigerating plant(9)It is connected with nitrogen Gas cylinder(711).
3. the processing technology of the process equipment of application siller tin oxide as described in claim 1, it is characterised in that including following step Suddenly:1, silver ingot, tin slab are put into the smelting apparatus(1)Interior melting;2, start the vacuum extractor(5)Evacuate the atomization Device(2)Interior air opens the valve(3)Molten metal is put into atomising device(2)It is interior and close the valve (3);3, starting the motor makes the impeller and the sprocket wheel rotate, and starts the refrigerating plant(9), start the increasing Pressure device(4)To atomising device(2)It is filled with nitrogen supercharging.
4. the processing technology of the process equipment of siller tin oxide as claimed in claim 3, it is characterised in that:Step 2 and step 3 it Between further include being filled with nitrogen to replace the babinet(7)The step of interior air.
CN201610487184.8A 2016-06-29 2016-06-29 The process equipment and its processing technology of siller tin oxide Active CN105921760B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610487184.8A CN105921760B (en) 2016-06-29 2016-06-29 The process equipment and its processing technology of siller tin oxide

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610487184.8A CN105921760B (en) 2016-06-29 2016-06-29 The process equipment and its processing technology of siller tin oxide

Publications (2)

Publication Number Publication Date
CN105921760A CN105921760A (en) 2016-09-07
CN105921760B true CN105921760B (en) 2018-08-14

Family

ID=56828785

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610487184.8A Active CN105921760B (en) 2016-06-29 2016-06-29 The process equipment and its processing technology of siller tin oxide

Country Status (1)

Country Link
CN (1) CN105921760B (en)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109108274B (en) * 2018-10-24 2024-02-20 云南锡业新材料有限公司 Method for rapidly and efficiently treating tin-base alloy spherical welding powder return material
CN114260456A (en) * 2021-12-18 2022-04-01 江苏申隆锌业有限公司 Adopt innoxious apparatus for producing of atomizing preparation zinc powder

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3655837A (en) * 1969-06-18 1972-04-11 Republic Steel Corp Process for producing metal powder
CN2626613Y (en) * 2003-06-08 2004-07-21 戴丽达 Ducting type permanent magnet automatic iron remover
CN101362206A (en) * 2008-10-09 2009-02-11 陈新国 Preparation method of continuous high quality soldering powder
CN101707155A (en) * 2009-09-24 2010-05-12 温州宏丰电工合金有限公司 Method for preparing tin oxide reinforced silver-based electrical contact materials
CN201817055U (en) * 2010-09-25 2011-05-04 杭州华达喷射真空设备有限公司 Chain plate type sprocket driving and tensioning pipeline conveying appliance
CN105023773A (en) * 2014-04-25 2015-11-04 三菱电机株式会社 Ag-oxide electric contact material, producing method and producing device thereof, breaker, and electromagnetic contactor
CN105359241A (en) * 2013-06-24 2016-02-24 三菱电机株式会社 Electrical contact material and method for manufacturing same

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3655837A (en) * 1969-06-18 1972-04-11 Republic Steel Corp Process for producing metal powder
CN2626613Y (en) * 2003-06-08 2004-07-21 戴丽达 Ducting type permanent magnet automatic iron remover
CN101362206A (en) * 2008-10-09 2009-02-11 陈新国 Preparation method of continuous high quality soldering powder
CN101707155A (en) * 2009-09-24 2010-05-12 温州宏丰电工合金有限公司 Method for preparing tin oxide reinforced silver-based electrical contact materials
CN201817055U (en) * 2010-09-25 2011-05-04 杭州华达喷射真空设备有限公司 Chain plate type sprocket driving and tensioning pipeline conveying appliance
CN105359241A (en) * 2013-06-24 2016-02-24 三菱电机株式会社 Electrical contact material and method for manufacturing same
CN105023773A (en) * 2014-04-25 2015-11-04 三菱电机株式会社 Ag-oxide electric contact material, producing method and producing device thereof, breaker, and electromagnetic contactor

Also Published As

Publication number Publication date
CN105921760A (en) 2016-09-07

Similar Documents

Publication Publication Date Title
CN104475743B (en) A kind of preparation method of superfine spherical titanium and titanium alloy powder
CN108161019B (en) Powder making method of induction heating and radio frequency plasma combined atomization powder making system
CN101912973B (en) Method and device for preparing uniform solidified particles by orifice injection
CN105945295B (en) A kind of process equipment and its processing technology of siller tin oxide
CN101474675B (en) Method for recycle of copper alloy from waste circuit board and cyclic reconstruction of powder metallurgical product as well as device system thereof
CN110079691B (en) Molybdenum-copper alloy with low molybdenum content and preparation method thereof
CN1243624C (en) Method for manufacturing metallic partiless and its device manufactured metallic partiles
CN104308168B (en) The preparation method of a kind of fine grain hypoxemia spherical titanium and titanium alloy powder
CN105921760B (en) The process equipment and its processing technology of siller tin oxide
US20200130065A1 (en) Method for producing water-atomized prealloyed powder with high cold press formability
CN1775428A (en) Method and apparatus for preparing rapid-solidified hydrogen-storage alloy powder material
CN109226775A (en) A kind of preparation method of the dedicated titanium powder of porous titanium film or titanium alloy powder
CN1270864A (en) Ultrasonic atomization of low-oxygen titanium with high-purity gas andtitanium alloy powder preparing process and product thereof
CN106148750B (en) The process equipment and its processing technology of silver copper oxide
CN1286604C (en) Method for preparing copper powder by water atomization method
CN204818071U (en) Preparation metal spherical powder's for vibration material disk device
CN208696304U (en) A kind of device of low-voltage direct plasma gun preparation 3D printing titanium valve
CN114226738A (en) A kind of powder preparation method and powder stirring mill for 3D printing
CN111558725A (en) A method for producing atomized iron powder by spraying after reduction of scrap steel
CN106424743A (en) Production method for high-strength and high-modulus additive manufacturing materials
CN115351284A (en) Be applied to multistage processing unit of sendust powder of metal magnetic powder core
CN117205862A (en) High-temperature plasma powder making equipment based on high-pressure argon circulation
CN116140607A (en) Preparation device and method of 3D printing titanium alloy powder with fluidity
CN110681868B (en) Efficient and environment-friendly production method of high-performance forged manganese
CN1212212C (en) One-step gas atomization iron powder

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant