CN105801084B - The preparation method of ceramic shale green body and the method that ceramic product is made with the green body - Google Patents
The preparation method of ceramic shale green body and the method that ceramic product is made with the green body Download PDFInfo
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- CN105801084B CN105801084B CN201610075743.4A CN201610075743A CN105801084B CN 105801084 B CN105801084 B CN 105801084B CN 201610075743 A CN201610075743 A CN 201610075743A CN 105801084 B CN105801084 B CN 105801084B
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- 239000000919 ceramic Substances 0.000 title claims abstract description 50
- 238000000034 method Methods 0.000 title claims abstract description 29
- 238000002360 preparation method Methods 0.000 title claims abstract description 10
- 239000000463 material Substances 0.000 claims abstract description 17
- 238000000465 moulding Methods 0.000 claims abstract description 10
- 238000010304 firing Methods 0.000 claims abstract description 9
- 235000015895 biscuits Nutrition 0.000 claims abstract description 8
- 238000004519 manufacturing process Methods 0.000 claims abstract description 6
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 16
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 14
- 239000002994 raw material Substances 0.000 claims description 13
- 239000010440 gypsum Substances 0.000 claims description 11
- 229910052602 gypsum Inorganic materials 0.000 claims description 11
- 239000005995 Aluminium silicate Substances 0.000 claims description 10
- 235000012211 aluminium silicate Nutrition 0.000 claims description 10
- 238000000227 grinding Methods 0.000 claims description 10
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims description 10
- 239000011505 plaster Substances 0.000 claims description 10
- 238000005096 rolling process Methods 0.000 claims description 9
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 8
- 229910052742 iron Inorganic materials 0.000 claims description 8
- 229910052573 porcelain Inorganic materials 0.000 claims description 8
- 239000010427 ball clay Substances 0.000 claims description 7
- 229920001343 polytetrafluoroethylene Polymers 0.000 claims description 6
- 239000004810 polytetrafluoroethylene Substances 0.000 claims description 6
- 239000010433 feldspar Substances 0.000 claims description 4
- 244000137852 Petrea volubilis Species 0.000 claims description 3
- 238000000498 ball milling Methods 0.000 claims description 3
- 239000000440 bentonite Substances 0.000 claims description 3
- 229910000278 bentonite Inorganic materials 0.000 claims description 3
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 claims description 3
- 239000012535 impurity Substances 0.000 claims description 3
- 238000002347 injection Methods 0.000 claims description 3
- 239000007924 injection Substances 0.000 claims description 3
- -1 polytetrafluoroethylene Polymers 0.000 claims description 3
- 238000003825 pressing Methods 0.000 claims description 3
- 239000004033 plastic Substances 0.000 claims description 2
- 238000010409 ironing Methods 0.000 claims 1
- 239000006148 magnetic separator Substances 0.000 claims 1
- 238000012546 transfer Methods 0.000 abstract description 7
- 238000007639 printing Methods 0.000 abstract description 6
- 230000000052 comparative effect Effects 0.000 description 6
- 238000005452 bending Methods 0.000 description 4
- 238000005034 decoration Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 2
- 238000005336 cracking Methods 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- 239000000741 silica gel Substances 0.000 description 2
- 229910002027 silica gel Inorganic materials 0.000 description 2
- 238000005299 abrasion Methods 0.000 description 1
- 230000003796 beauty Effects 0.000 description 1
- PASHVRUKOFIRIK-UHFFFAOYSA-L calcium sulfate dihydrate Chemical compound O.O.[Ca+2].[O-]S([O-])(=O)=O PASHVRUKOFIRIK-UHFFFAOYSA-L 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 210000003298 dental enamel Anatomy 0.000 description 1
- KZHJGOXRZJKJNY-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Si]=O.O=[Al]O[Al]=O.O=[Al]O[Al]=O.O=[Al]O[Al]=O KZHJGOXRZJKJNY-UHFFFAOYSA-N 0.000 description 1
- 238000007598 dipping method Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229910052863 mullite Inorganic materials 0.000 description 1
- 239000011022 opal Substances 0.000 description 1
- 238000010422 painting Methods 0.000 description 1
- 239000004014 plasticizer Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000012797 qualification Methods 0.000 description 1
- 239000010453 quartz Substances 0.000 description 1
- 230000007115 recruitment Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000005245 sintering Methods 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
- C04B33/132—Waste materials; Refuse; Residues
- C04B33/1324—Recycled material, e.g. tile dust, stone waste, spent refractory material
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3418—Silicon oxide, silicic acids or oxide forming salts thereof, e.g. silica sol, fused silica, silica fume, cristobalite, quartz or flint
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3427—Silicates other than clay, e.g. water glass
- C04B2235/3463—Alumino-silicates other than clay, e.g. mullite
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P40/00—Technologies relating to the processing of minerals
- Y02P40/60—Production of ceramic materials or ceramic elements, e.g. substitution of clay or shale by alternative raw materials, e.g. ashes
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Environmental & Geological Engineering (AREA)
- Dispersion Chemistry (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Devices For Post-Treatments, Processing, Supply, Discharge, And Other Processes (AREA)
- Decoration By Transfer Pictures (AREA)
Abstract
The invention discloses a kind of preparation method of ceramic shale green body and the methods that ceramic product is made with the green body.The preparation method of high-intensitive ceramic shale green body of the invention, including following production stage：(1) it is dry to prepare (2) molding (3) repaired biscuit (4) for blank.The method that ceramic product is made of the invention, shale green body obtained, it is color to carry out print using stamp material, then apply ceramic clear frit, by conventional firing, is eventually fabricated underglaze colour domestic ceramic product in aforementioned manners.High-strength ceramic shale green body produced by the present invention, it is color suitable for directly carrying out print on shale green body using the color machine of transfer print.Shale billet surface is smooth, and intensity is high, and during ceramic product is made, when carrying out printing coloured silk using stamp material, shale green body is not damaged, prints coloured picture case complete display.
Description
Technical field
The present invention relates to ceramic field, the preparation method of specifically a kind of high-strength ceramic shale green body and with the green body system
At the method for ceramic product.
Background technique
The decorative appearance mode of domestic ceramics has：White tire is decorated with transparent or opal glaze；Color glaze is decorated with coloured glaze；It is color
It draws, with color material colored drawing or decal paper, painted decoration can also be divided into overglaze color, underglaze colour, in-glaze decoration.
Colored drawing flower face is in enamel layer hereinafter, referred to as underglaze colour, and glaze layer protects colored drawing flower face, has health, beauty etc. excellent
Point.Hand painting or decal paper are all the more processes of recruitment, and production efficiency is lower, and cost is also higher.It has been created in ceramic industry
New transfer prints color technology and technique, prints color machine using transfer and colorant is directly printed to surface of ceramic products.Due to domestic ceramics
Device shape diversification, printing color print head is made of soft silica gel, the printing suitable for arc product.
Since transfer prints color process, silica gel print head pressure needs certain pressure, ceramic when being attached to surface of ceramic products
It needs to make product that there is certain intensity by biscuiting (800-900 DEG C) after molding, is suitable for print coloured silk, printed color product and carried out again
Glazing and firing.Conventional ceramic ware for daily use shale blank strength after molding is lower (bending strength is in 1.5MPa or so),
It is easy to damaged in the color process of print, if shale blank strength is improved (bending strength reaches 2.5MPa), print coloured silk can be born
Pressure.Coloured silk is printed directly on shale green body, without biscuiting, with save the cost and can be raised labour productivity, product decoration effect
More preferably.Domestic ceramics industry will improve household ceramic blank intensity, make it the transfer print coloured silk directly on shale green body, become
The project of technological innovation and research of technique.
Summary of the invention
To solve the above problems, the present invention provides a kind of preparation method of high-strength ceramic shale green body and with the green body
The method that ceramic product is made.
The preparation method of high-intensitive ceramic shale green body of the invention, which is characterized in that including following production stage：
(1) prepared by blank
Take kaolin 42-46 parts by weight, feldspar 18-22 parts by weight, quartzy 14-16 parts by weight, ball clay 6-8 parts by weight give up
Porcelain 6-8 parts by weight, bentonite 2-4 parts by weight, kieselguhr 4-6 parts by weight are as raw material；
--- above-mentioned useless porcelain is the scrap that daily ceramic product generates after firing, and scrap hammering is fragmentated with hammer
It is made；Above-mentioned kaolin is the kaolin for originating from Fujian Longyan, is made after eluriating and removing partial impurities；
After above-mentioned raw materials are mixed plus clear water carries out wet ball grinding, crosses 220 meshes through ball milling raw material, and the raw material that is sieved, which is crossed, to be removed
Iron machine removes iron, through passing through filter press filters pressing into clod except iron material, clod is carried out pugging by pug mill, preparation mass contains
The blank of water rate 22-33% is spare；
(the basic role that material is applied in above-mentioned blank formulation；
Kaolin, feldspar, quartz are the basic materials in three system of household porcelain production raw material formula, constitute domestic ceramics
The main body of product.During material utilization amount matches, the shape of the plasticity of product molding, the reaction of sintering process material and mullite is taken into account
The effects of whiteness with higher at, product.
Useless porcelain is the material through being burnt into, and can suitably reduce the temperature of product firing, shortens firing time, saving is produced into
Sheet and a kind of waste utilization.
Ball clay can make molding shale green body intensity with higher when dry, but be easy to that shale body drying is caused to be received
Contracting increases, and causes blank cracking.Therefore, additional amount should appropriateness.
Bentonite is the plasticizer of ceramic batch, can improve the plasticity of blank, be used cooperatively with ball clay, can be correspondingly steady
Determine the intensity of shale green body.
Kieselguhr can improve the viscosity of blank, with ball clay, swelling soil interaction, can make the qualification rate of product molding process
It improves, blank strength is maintained.)
(2) it forms
Above-mentioned spare blank is taken, roll forming is carried out using roller head machine；Forming process uses rolling depression method at a slow speed,
The rolling time of every green body is that (conventional every green body rolling time was 9-10 seconds in 15-16 seconds；Use rolling depression method energy at a slow speed
Make to form the raising of shale green density, intensity correspondinglys increase)；
--- above-mentioned roller head machine is equipped with roll die, including male model and master mold；Male model is made of polytetrafluoroethylene (PTFE)；It is female
Mould is made of the three A superfine land plasters that three power plastering Co., Ltd of Jingmen Macheng town produces；After master mold is made, in use
Blank is stated, is deployed into the mud that concentration is 50 Baume degrees with clear water, mud injection plaster mold is intracavitary, and mud stops in die cavity
30-40 minutes, reduce the alkalinity on gypsum mold surface；After the mud residence time arrives, mud eliminating in plaster mold is rushed with clear water
Gypsum mold is washed, cleaned gypsum mold spontaneously dries spare；It (is to roll product with the effect that mud embathes gypsum mold
Product is easy demoulding, the pug of product not sticking mould in molding)
(3) repaired biscuit
Reconditioning is carried out to through molding billet surface；First keep billet surface smooth billet surface fine grinding with sand paper, then uses
Silk stocking wrap up blocky ivalon, add clear water to carry out fine grinding to billet surface, keep billet surface smooth, be conducive to subsequent print
It is color；
(4) dry
Green body through repaired biscuit naturally dries to quality moisture content 6-8%, obtains high-intensitive ceramic shale green body.
The method that ceramic product is made of the invention, which is characterized in that shale green body obtained in aforementioned manners, using print
It is color that flower material carries out print, then applies ceramic clear frit, by conventional firing, is eventually fabricated underglaze colour domestic ceramic product.
High-strength ceramic shale green body produced by the present invention is suitable for printing color machine using transfer directly enterprising in shale green body
Row print is color.Shale billet surface is smooth, intensity height (bending strength reaches 2.5MPa after tested), in the process that ceramic product is made
In, when carrying out printing coloured silk using stamp material, shale green body is not damaged, prints coloured picture case complete display.
Specific embodiment
Embodiment：
(1) prepared by blank
Take 45 parts by weight of kaolin, 20 parts by weight of feldspar, quartzy 15 parts by weight, 7 parts by weight of ball clay, 7 parts by weight of porcelain of giving up are swollen
Moisten native 3 parts by weight, 5 parts by weight of kieselguhr are as raw material；
--- above-mentioned useless porcelain is the scrap that daily ceramic product generates after firing, and scrap hammering is fragmentated with hammer
It is made；Above-mentioned kaolin is the kaolin for originating from Fujian Longyan, is made after eluriating and removing partial impurities；
After above-mentioned raw materials are mixed plus clear water carries out wet ball grinding, crosses 220 meshes through ball milling raw material, and the raw material that is sieved, which is crossed, to be removed
Iron machine removes iron, through passing through filter press filters pressing into clod except iron material, clod is carried out pugging by pug mill, preparation mass contains
The blank of water rate 23% is spare；
(2) it forms
Above-mentioned spare blank is taken, roll forming is carried out using roller head machine；Forming process uses rolling depression method at a slow speed,
The rolling time of every green body is 15 seconds；
--- above-mentioned roller head machine is equipped with roll die, including male model and master mold；Male model is made of polytetrafluoroethylene (PTFE)；It is female
Mould is made of the three A superfine land plasters that three power plastering Co., Ltd of Jingmen Macheng town produces；After master mold is made, in use
Blank is stated, is deployed into the mud that concentration is 50 Baume degrees with clear water, mud injection plaster mold is intracavitary, and mud stops in die cavity
35 minutes, reduce the alkalinity on gypsum mold surface；After the mud residence time arrives, mud eliminating in plaster mold is rinsed with clear water
Gypsum mold, cleaned gypsum mold spontaneously dry spare；
(3) repaired biscuit
Reconditioning is carried out to through molding billet surface；First keep billet surface smooth billet surface fine grinding with sand paper, then uses
Silk stocking wrap up blocky ivalon, add clear water to carry out fine grinding to billet surface, keep billet surface smooth, be conducive to subsequent print
It is color；
(4) dry
Green body through repaired biscuit naturally dries to quality moisture content 7%, obtains the high-strength ceramic shale base of the present embodiment
Body.
Shale green body made from Example, stamp material made of the method using Patent No. 201310104767.4 are logical
It crosses the color machine of transfer print and carries out print coloured silk, then apply ceramic clear frit, be burnt by 1300 DEG C, be eventually fabricated the underglaze colour of the present embodiment
Domestic ceramic product.
High-strength ceramic shale billet surface made from the present embodiment is smooth, and intensity is high, and (bending strength reaches after tested
2.5MPa), during ceramic product is made, when carrying out printing coloured silk using stamp material, shale green body is not damaged, and print coloured picture case is clear
It is clear complete.
Comparative example 1：Unlike embodiment, ball clay is added without in blank.Manufactured shale blank strength is poor, is being made
During the print of ceramic product is color, shale green body is unable to undergo pressure and damaged.
Comparative example 2：Unlike embodiment, kieselguhr is added without in blank.The viscosity and plasticity of blank decline, and cause
Shale blank cracking is scrapped in forming process.
Comparative example 3：Unlike embodiment, in the matched mold of roller head machine, the materials of plaster master are using general
Logical land plaster, does not use high strength gypsum powder, plaster master surface of internal cavity difference of hardness.In roll-forming process master mold surface of internal cavity
Abrasion is generated, causes pug sticking to mould that green body is caused to be scrapped.
Comparative example 4：Unlike embodiment, plaster master does not use mud dipping to handle.Plaster master surface alkalinty
Too big, in roll-forming process, green body generates modification due to not easy mold release.
Comparative example 5：Unlike embodiment, the rolling time of every green body is 10 seconds in roll forming.Manufactured mud
Matter green density is poor, intensity decline.
Comparative example 6：Silk stocking are not used to wrap up blocky unit of plastic fine grinding product table unlike embodiment, in green body repaired biscuit
Face.Billet surface is not smooth enough, and during ceramic product is made, the color pattern definition of transferred print is poor.
Claims (2)
1. the preparation method of ceramic shale green body, which is characterized in that including following production stage：
(1) prepared by blank
Kaolin 42-46 parts by weight are taken, feldspar 18-22 parts by weight, quartzy 14-16 parts by weight, ball clay 6-8 parts by weight, give up porcelain 6-8
Parts by weight, bentonite 2-4 parts by weight, kieselguhr 4-6 parts by weight are as raw material；
The useless porcelain is the scrap that daily ceramic product generates after firing, with hammer by scrap hammering fragmentate it is obtained；Institute
Stating kaolin is the kaolin for originating from Fujian Longyan, is made after eluriating and removing partial impurities；
After above-mentioned raw materials are mixed plus clear water carries out wet ball grinding, crosses 220 meshes through ball milling raw material, and the raw material that is sieved crosses magnetic separator de-ironing
Except clod is passed through pug mill and carries out pugging, prepare mass moisture content by iron through passing through filter press filters pressing into clod except iron material
The blank of 22-33% is spare；
(2) it forms
Above-mentioned spare blank is taken, roll forming is carried out using roller head machine；Forming process is using rolling depression method at a slow speed, and every
The rolling time of green body is 15-16 seconds；
The roller head machine is equipped with roll die, including male model and master mold；Male model is made of polytetrafluoroethylene (PTFE)；Master mold is Jingmen
Three A superfine land plasters of three power plastering Co., Ltd of city Macheng town production are made；After master mold is made, using above-mentioned blank,
It is deployed into the mud that concentration is 50 Baume degrees with clear water, mud injection plaster mold is intracavitary, and mud stops 30-40 points in die cavity
Clock reduces the alkalinity on gypsum mold surface；After the mud residence time arrives, by mud eliminating in plaster mold, gypsum is rinsed with clear water
Mold, cleaned gypsum mold spontaneously dry spare；
(3) repaired biscuit
Reconditioning is carried out to through molding billet surface；First keep billet surface smooth billet surface fine grinding with sand paper, then uses silk stocking
Blocky plastic sponge is wrapped up, adds clear water to carry out fine grinding to billet surface, keeps billet surface smooth, it is color to be conducive to subsequent print；
(4) dry
Green body through repaired biscuit naturally dries to quality moisture content 6-8%, obtains high-intensitive ceramic shale green body.
2. the method that ceramic product is made, which is characterized in that the shale green body made from claim 1 the method, using print
It is color that flower material carries out print, then applies ceramic clear frit, by conventional firing, is eventually fabricated underglaze colour domestic ceramic product.
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|---|---|---|---|---|
| CN101337806A (en) * | 2008-08-08 | 2009-01-07 | 饶国良 | Spodumene-matrix heat resisting ceramic materials |
| CN102584179A (en) * | 2011-01-10 | 2012-07-18 | 福建省德化县宁昌陶瓷有限公司 | Ceramic product prepared from waste ceramic and preparation method thereof |
| CN102249653A (en) * | 2011-06-03 | 2011-11-23 | 饶国良 | Petalite heat-resisting ceramic material with strong forming stability |
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Denomination of invention: Preparation method of ceramic argillaceous body and method for making ceramic products from the body Effective date of registration: 20211028 Granted publication date: 20181116 Pledgee: China Co. truction Bank Corp Chaozhou branch Pledgor: GUANGDONG HAOMING CERAMIC SCIENCE AND TECHNOLOGY Co.,Ltd. Registration number: Y2021980011504 |