CN105769618B - A kind of surface activator composition carrying high amounts of oil phase - Google Patents
A kind of surface activator composition carrying high amounts of oil phase Download PDFInfo
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- CN105769618B CN105769618B CN201410829324.6A CN201410829324A CN105769618B CN 105769618 B CN105769618 B CN 105769618B CN 201410829324 A CN201410829324 A CN 201410829324A CN 105769618 B CN105769618 B CN 105769618B
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Abstract
The invention discloses a kind of stable high oil phase content composition for personal nursing, the composition includes the lubricant component of 5 weight % or more and the surfactant that is made of cocounut oil acyl hydroxyethyl sulfonate and lauryl alcohol polyethers sulfosuccinate disodium.The application that the invention also discloses the compositions in personal care product.
Description
Technical field
The present invention relates to personal care fields, and in particular to one kind can carry the surfactant package of high amounts of oil phase
Object, the composition can be applied to individual's skin and hair cleaning product such as bath oil, mildy wash, leaves shampoo etc..
Background technique
In the product formulas such as shower cream, mildy wash it is general all can some greases etc. assign rouge agent to alleviate because of surfactant
Degreasing and caused by wash after have dry skin tight skin sense.
In domestic shower cream and mildy wash market in recent years, declare that the product for moistening effect is more and more.These products
In quite a few be the surfactant system of the non-soap base of expansion type.From the point of view of the conventional formulation experience of this field, this
The formula of a little products can be broadly divided into two kinds according to the ratio that grease wherein added etc. assigns rouge agent ingredient.First seed type
(i.e. most of formula belongs to the first seed type) is by about 5% tax rouge agent below of addition to reach improvement surfactant
Because of cleaning and degreasing and bring drying and tight feeling to skin.But this improvement can't reach and disappear
Expense person is for washing the requirement of rear skin moisturizing.On the other hand, the increase for assigning rouge agent content then often will cause the unstable of formula.
The product (few formula belongs to second of type) of second of type is then by surfactant package system appropriate
It adds higher proportion of grease etc. and assigns rouge agent to realize the effect of washing rear skin moisturizing, such as the Dove skin-active cream of Uniliver
White bath oil and the tender deep profit bath oil of nourishing series of the yulan grease of Procter & Gamble.Both products are all by " table living body system
High-content grease is added " formula technique realize moist skin sense of the bath oil after washing, wherein Dove skin-active cream body bath
Formula technique be by three Cocoamidopropyl betaine, laureth sodium sulfovinate and sodium cocoyl glycinate surfaces
The compounding of activating agent carries skin sense relatively more moist after more sunflower seed oil realization is washed, and the tender nourishing of yulan grease is
The formula technique of the deep profit bath oil of column is by trideceth sodium sulphate, laruyl alcohol sodium sulfovinate and lauroyl both sexes base second
The compounding of sour three surfactants of sodium, carry more vaseline and dormant oil realize wash after relatively moist skin sense.
Not yet discovery is using lauryl alcohol polyethers sulfosuccinate disodium and cocounut oil acyl hydroxyethyl sulfonate two so far
For kind surfactant compound to carry the composition of high amounts of oil phase, the composition is suitably applied personal care product's such as skin
In skin nursing and/or cleaning products (such as bath oil, mildy wash, leaves shampoo).
Summary of the invention
Lauryl alcohol polyethers sulfosuccinate disodium and cocounut oil acyl hydroxyl second are used the purpose of the present invention is to provide a kind of
Two kinds of surfactant compounds of sodium sulfonate are to carry the composition of high amounts of oil phase.It is made by the formula and preparation method of offer
This composition, stable skin and hair cleaning class component can be formed, also can be applied to various skin and hairs nursing and
Cleaning products such as bath oil, mildy wash, in leaves shampoo.
Therefore, the present invention provides a kind of stable high oil phase content composition for personal nursing, the compositions
Lubricant component comprising 5 weight % or more and by cocounut oil acyl hydroxyethyl sulfonate and lauryl alcohol polyethers sulfosuccinate disodium
The surfactant of composition.In one embodiment, cocounut oil acyl hydroxyethyl sulfonate and lauryl alcohol in composition of the invention
The total content of polyethers sulfosuccinate disodium is 15 weight %.In another embodiment, the present composition includes 10-
The cocounut oil acyl hydroxyethyl sulfonate of 13 weight % and the lauryl alcohol polyethers sulfosuccinate disodium of 2-5 weight %.
In an embodiment of the invention, composition includes the lubricant component of 10 weight % or more.Preferably at one
Embodiment in, the present composition include 20 weight % or more lubricant component.
In one embodiment, cocounut oil acyl hydroxyethyl sulfonate and lauryl alcohol polyethers sulfosuccinic in the present composition
The weight ratio of acid esters disodium is 2:1 to 6:1.In one preferred embodiment, cocounut oil acyl hydroxyl second sulphur in the present composition
The weight ratio of sour sodium and lauryl alcohol polyethers sulfosuccinate disodium is 3:1.
In one embodiment, the present composition also includes glycerol.In one preferred embodiment, of the invention
Composition includes the glycerol of 20 weight %.
On the other hand, the invention further relates to a kind of lubricant component comprising 5 weight % or more and by cocounut oil acyl hydroxyl second sulphur
The composition for the surfactant that sour sodium and lauryl alcohol polyethers sulfosuccinate disodium are constituted is in personal care product
Using.In one embodiment, personal care product is cleaning products.For example, personal care product can be foaming
Type washing-off type skin cleaning product.In a specific embodiment, personal care product is bath oil, mildy wash, hair washing
The products such as cream.
Specific embodiment
Unless otherwise defined, all technical and scientific terms used herein have fields ordinary skill people of the present invention
The identical meanings that member is commonly understood by.Although can be used for implementing or testing with similar or equivalent any method and material described herein
The present invention, but described herein is preferred method and material.For the purpose of the present invention, following term is defined below.
Terms used herein " about " refers to that difference can compared with the quantity of reference product, level, numerical value, dimension, size or dosage
Quantity, level, numerical value, dimension, size or the dosage of up to 30%, 20% or 10%.Percentage composition used herein, unless
It is otherwise noted, is by weight.
In full piece specification and claims, Unless Otherwise Requested, following word "comprising" and its variant " containing "
It is understood to mean that with " comprising " including the entirety or step or one group of entirety or step, but is not excluded for any other whole
Body or step or other one group of entirety or step.
The present invention is had been surprisingly found that based on following: by lauryl alcohol polyethers sulfosuccinate disodium and cocounut oil acyl hydroxyl second sulphur
After two kinds of surfactants of sour sodium compound according to a certain percentage, up to 24.75% lubricant component can not only be carried, and
Can be formed stable personal care product (such as expansion type skin and hair cleaning products).
Therefore, the present invention is for the first time by lauryl alcohol polyethers sulfosuccinate disodium and two kinds of tables of cocounut oil acyl hydroxyethyl sulfonate
Face activating agent compounding, for carrying the oily phase of high-content, to form the composition of stable high amounts of oil phase.In addition, this hair
Bright composition is also applied in personal care product, forms the stable personal care product of carrying high amounts of oil phase.
Below with reference to specific embodiment, the present invention is further explained.It should be appreciated, however, that these embodiments are only used for
It is bright the present invention and be not meant to limit the scope of the invention.The test method of actual conditions is not specified in the following example, usually
According to normal conditions, or according to the normal condition proposed by manufacturer.Unless otherwise indicated, all percentage and number be by weight
Meter.
Raw material used in the present composition is as shown in table 1.
Table 1
Embodiment 1: the preparation of preparation high amounts of oil phase
The preparation of high amounts of oil phase of the present invention is prepared according to formula shown in following table.
In the formula of embodiment 1, lubricant component gross activity object (purification olive oil, docosanol and cocounut oil acyl hydroxyl second sulphur
The summation of free fatty acid in sour sodium) weight percentage be 24.75 weight %.
The specific preparation process of preparation described in embodiment 1 is as follows:
Each raw material of 1.A phase sequentially adds main beaker, while stirring 70~80 DEG C of heat value, until sufficiently melting and mixing
It is even.
2.70~80 DEG C, B phase is added to enter A phase.
3. being cooled to 60~65 DEG C, C phase is added, stirs evenly.
4. being stirred evenly main beaker is added after D phase and deionized water 1:1 premix.
5. being stirred evenly main beaker is added after E phase and deionized water 1:1 premix.
6. whether sampling and testing Material pH (Material is uniformly mixed with deionized water 1:10) is 5.0~6.0, if pH is lower than
5.0 are added sodium hydroxide adjusting, if pH is higher than 6.0, add citric acid adjusting.
7. system is cooled to 50 DEG C, G phase is added, stirs evenly.
8. supplementing the moisture of evaporation, stir evenly.Cooperation finishes, and the preparation of the high oil phase content of the present invention is prepared.
Embodiment 2: the preparation of preparation high amounts of oil phase
The preparation of high amounts of oil phase of the present invention is prepared according to formula shown in following table.
It is prepared according to 1 the method for embodiment, obtains the preparation of high amounts of oil phase of the invention.
In the preparation of embodiment 2, lubricant component gross activity object (purification olive oil, docosanol and cocounut oil acyl hydroxyl second sulphur
The summation of free fatty acid in sour sodium) weight percentage be 10.33 weight %.
Embodiment 3: the preparation of preparation high amounts of oil phase
The preparation of high amounts of oil phase of the present invention is prepared according to formula shown in following table.
It is prepared according to 1 the method for embodiment, obtains the preparation of high amounts of oil phase of the invention.
In the preparation of embodiment 3, lubricant component gross activity object (purification olive oil, docosanol and cocounut oil acyl hydroxyl second sulphur
The summation of free fatty acid in sour sodium) weight percentage be 13.75 weight %.
Embodiment 4: the preparation of preparation high amounts of oil phase
The preparation of high amounts of oil phase of the present invention is prepared according to formula shown in following table.
It is prepared according to 1 the method for embodiment, obtains the preparation of high amounts of oil phase of the invention.
In the preparation of embodiment 4, lubricant component gross activity object (purification olive oil, docosanol and cocounut oil acyl hydroxyl second sulphur
The summation of free fatty acid in sour sodium) weight percentage be 14.0 weight %.
Embodiment 5: the preparation of preparation high amounts of oil phase
The preparation of high amounts of oil phase of the present invention is prepared according to formula shown in following table.
It is prepared according to 1 the method for embodiment, obtains the preparation of high amounts of oil phase of the invention.
In the preparation of embodiment 5, lubricant component gross activity object (purification olive oil, docosanol and cocounut oil acyl hydroxyl second sulphur
The summation of free fatty acid in sour sodium) weight percentage be 14.3 weight %.
Embodiment 6: the preparation of preparation high amounts of oil phase
The preparation of high amounts of oil phase of the present invention is prepared according to formula shown in following table.
It is prepared according to 1 the method for embodiment, obtains the preparation of high amounts of oil phase of the invention.
In the preparation of embodiment 6, lubricant component gross activity object (purification olive oil, docosanol and cocounut oil acyl hydroxyl second sulphur
The summation of free fatty acid in sour sodium) weight percentage be 14.3 weight %.
Embodiment 7: the preparation of preparation high amounts of oil phase
The preparation of high amounts of oil phase of the present invention is prepared according to formula shown in following table.
It is prepared according to 1 the method for embodiment, obtains the preparation of high amounts of oil phase of the invention.
In the preparation of embodiment 7, lubricant component gross activity object (purification olive oil, docosanol and cocounut oil acyl hydroxyl second sulphur
The summation of free fatty acid in sour sodium) weight percentage be 19.75 weight %.
Embodiment 8: the study on the stability of the preparation of high amounts of oil phase of the present invention
One, material and equipment
Two, step
1, it after the completion of configuring Material, is sub-packed in 5 transparent plastic drug packages of 50mlPET, screws bottle cap, and paste respectively
Upper label marks formula number, indwelling temperature, indwelling time on label, for use.
2, by the difference indwelling of above-mentioned 5 bottles of samples in -15 DEG C of refrigerator freezing layers, 5 DEG C of insulating boxs, 40 DEG C of insulating boxs, 48 DEG C of perseverances
Incubator and room temperature environment.
3,1 month, 2 months and 3 months stability of each sample is investigated respectively.
4, the judgment criteria of " stability passes through investigation ": following 2 conditions need while meeting, and have any one that cannot expire
Foot is as unstable, fails to pass through study on the stability.
1. sample is in -15 DEG C of refrigerator freezing layers, 5 DEG C of insulating boxs, 40 DEG C of insulating boxs, 48 DEG C of insulating boxs and room temperature environment
When indwelling, there is not water outlet, layering, discoloration, obvious coarse phenomenon；
2. the sample of the indwelling in -15 DEG C of refrigerator freezing floor, 5 DEG C of insulating boxs, 40 DEG C of insulating boxs, 48 DEG C of insulating boxs replys room
Wen Hou can be returned to knot paste state, and without there is water outlet, layering, discoloration and obvious coarse phenomenon.
As a result as shown in the table:
In the formula of embodiment 1, cocounut oil acyl hydroxyethyl sulfonate and lauryl alcohol polyethers sulfosuccinate disodium are kept
Gross activity object 15%, active matter additive amount ratio be 3:1, addition purification olive oil 20% mentioned to guarantee formulation stability
High glycerine additive amount is to 20%.The embodiment research cocounut oil acyl hydroxyethyl sulfonate and lauryl alcohol polyethers sulfosuccinate disodium
Bearing capacity of the formula system of compounding to 20% purification olive oil.The results show that stability has passed through investigation, no layering is existing
As.Meanwhile the system can stablize the grease of carrying up to 24.75%.
In the test of embodiment 2-5, when cocounut oil acyl hydroxyethyl sulfonate and lauryl alcohol polyethers sulfosuccinate disodium
Gross activity object maintain under 15% equal conditions, the active matter additive amount ratio both adjusted separately is 2:1,3:1,4:1
And 6:1.The result shows that cocounut oil acyl hydroxyethyl sulfonate and this two surfactants of lauryl alcohol polyethers sulfosuccinate disodium
It can make formula that can carry the grease of high level under different adding proportions.Without dividing in study on the stability
Layer phenomenon, can form the stable stable formula that can carry high level grease.
The formula of embodiment 6 is roughly the same with embodiment 5, and difference is that glycerol in formula is reduced to 0 by inventor, grinds
Study carefully the effect that glycerol carries this stability of formula of higher fat content.The results show that the formula is at 40 DEG C and 48
DEG C place during, although not being layered, compared with the result of experimental example 5, Material viscosity is significantly thinning, it can be seen that, it is sweet
The addition of oil helps to improve the high-temperature stability of Material.
In the formula of embodiment 7, Cocoamidopropyl betaine is substituted into lauryl alcohol polyethers sulfosuccinate two
Sodium is combined with cocounut oil acyl hydroxyethyl sulfonate.The active matter adding proportion of cocounut oil acyl hydroxyethyl sulfonate and Cocoamidopropyl betaine
3:1, gross activity object content 15% are constant.The embodiment research cocounut oil acyl hydroxyethyl sulfonate and Cocoamidopropyl betaine are answered
With whether equally can stablize carrying higher proportion grease；Cocounut oil acyl hydroxyethyl sulfonate and lauryl alcohol polyether sulphur are examined simultaneously
The combination of base succinate disodium carries the importance of the grease of higher proportion for stablizing.As the result is shown: cocounut oil acyl hydroxyl second sulphur
The surfactant package of sour sodium and Cocoamidopropyl betaine can not form the carrying higher proportion by study on the stability
The formula of grease.From the test it can also be seen that cocounut oil acyl hydroxyethyl sulfonate and lauryl alcohol polyethers sulfosuccinate disodium
Combination for formed can be extremely important by the formula of the carrying higher proportion grease of study on the stability.
Claims (6)
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| CN107049816A (en) * | 2017-04-25 | 2017-08-18 | 佛山市富馨科技实业有限公司 | One kind hair washing, face cleaning and take a shower three-in-one purification breast and preparation method |
| CN111286411B (en) * | 2018-12-10 | 2022-08-26 | 上海家化联合股份有限公司 | Cleaning composition for hard surface cleaning |
| CN119280108B (en) * | 2024-12-10 | 2025-04-04 | 广州源大生物科技有限公司 | Bath oil lotion with soothing effect and preparation method thereof |
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| CN102525874A (en) * | 2012-03-09 | 2012-07-04 | 浙江农林大学 | Lily-contained Chinese herbal medicine facial cleanser and preparation method thereof |
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| KR100469770B1 (en) * | 2002-05-20 | 2005-02-02 | 김해숙 | a soap weak acid of manufacturing method and thereof product |
| US20040259744A1 (en) * | 2003-12-19 | 2004-12-23 | Meidong Yang | Skin and hair cleansers containing sulfur |
| DE102004032734A1 (en) * | 2004-03-18 | 2005-10-06 | Henkel Kgaa | Prebiotic substances for deodorants |
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| CN102525874A (en) * | 2012-03-09 | 2012-07-04 | 浙江农林大学 | Lily-contained Chinese herbal medicine facial cleanser and preparation method thereof |
Non-Patent Citations (1)
| Title |
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| "L"occitane (欧舒丹) Olive Daily Shampoo";Photek;《获取网址：http://www.cosdna.com/chs/cosmetic_58d794674.html》;20121112;正文表格部分 |
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Effective date of registration: 20250327 Address after: 3rd Floor, Building 1, No. 527 Baoding Road, Hongkou District, Shanghai 200082 Patentee after: Shanghai Guangsheng Synthetic Biotechnology Co.,Ltd. Country or region after: China Address before: No.527 Baoding Road, Hongkou District, Shanghai 200082 Patentee before: Shanghai Jahwa United Co.,Ltd. Country or region before: China |