CN105753401A - Dry powder coating added with attapulgite mineral and preparation method thereof - Google Patents
Dry powder coating added with attapulgite mineral and preparation method thereof Download PDFInfo
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- CN105753401A CN105753401A CN201610056021.4A CN201610056021A CN105753401A CN 105753401 A CN105753401 A CN 105753401A CN 201610056021 A CN201610056021 A CN 201610056021A CN 105753401 A CN105753401 A CN 105753401A
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- attapulgite
- parts
- dry powder
- powder paint
- mineral
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- 229910052625 palygorskite Inorganic materials 0.000 title claims abstract description 107
- 229960000892 attapulgite Drugs 0.000 title claims abstract description 105
- 239000000843 powder Substances 0.000 title claims abstract description 79
- 229910052500 inorganic mineral Inorganic materials 0.000 title claims abstract description 41
- 239000011707 mineral Substances 0.000 title claims abstract description 39
- 238000002360 preparation method Methods 0.000 title claims abstract description 9
- 239000011248 coating agent Substances 0.000 title abstract description 25
- 238000000576 coating method Methods 0.000 title abstract description 25
- 239000011398 Portland cement Substances 0.000 claims abstract description 22
- 239000002994 raw material Substances 0.000 claims abstract description 21
- 230000008719 thickening Effects 0.000 claims abstract description 16
- 239000000945 filler Substances 0.000 claims abstract description 15
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 11
- 229910000329 aluminium sulfate Inorganic materials 0.000 claims abstract description 7
- 159000000013 aluminium salts Chemical class 0.000 claims abstract description 3
- 239000003973 paint Substances 0.000 claims description 52
- 230000000694 effects Effects 0.000 claims description 42
- 239000003638 chemical reducing agent Substances 0.000 claims description 22
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 17
- 239000007788 liquid Substances 0.000 claims description 13
- 238000003756 stirring Methods 0.000 claims description 12
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 claims description 11
- 238000002156 mixing Methods 0.000 claims description 11
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims description 10
- 239000004111 Potassium silicate Substances 0.000 claims description 9
- 238000007599 discharging Methods 0.000 claims description 9
- 229910052913 potassium silicate Inorganic materials 0.000 claims description 9
- 235000019353 potassium silicate Nutrition 0.000 claims description 9
- NNHHDJVEYQHLHG-UHFFFAOYSA-N potassium silicate Chemical compound [K+].[K+].[O-][Si]([O-])=O NNHHDJVEYQHLHG-UHFFFAOYSA-N 0.000 claims description 9
- 239000004115 Sodium Silicate Substances 0.000 claims description 8
- 238000010276 construction Methods 0.000 claims description 8
- PAZHGORSDKKUPI-UHFFFAOYSA-N lithium metasilicate Chemical compound [Li+].[Li+].[O-][Si]([O-])=O PAZHGORSDKKUPI-UHFFFAOYSA-N 0.000 claims description 8
- 229910052912 lithium silicate Inorganic materials 0.000 claims description 8
- 150000003839 salts Chemical class 0.000 claims description 8
- 235000019795 sodium metasilicate Nutrition 0.000 claims description 8
- 229910052911 sodium silicate Inorganic materials 0.000 claims description 8
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims description 8
- 238000005406 washing Methods 0.000 claims description 8
- MPPQGYCZBNURDG-UHFFFAOYSA-N 2-propionyl-6-dimethylaminonaphthalene Chemical compound C1=C(N(C)C)C=CC2=CC(C(=O)CC)=CC=C21 MPPQGYCZBNURDG-UHFFFAOYSA-N 0.000 claims description 7
- 239000012752 auxiliary agent Substances 0.000 claims description 7
- 238000010304 firing Methods 0.000 claims description 7
- 239000012535 impurity Substances 0.000 claims description 7
- 238000007873 sieving Methods 0.000 claims description 7
- 239000007921 spray Substances 0.000 claims description 7
- 229910052782 aluminium Inorganic materials 0.000 claims description 6
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 6
- 239000002689 soil Substances 0.000 claims description 6
- 229910000019 calcium carbonate Inorganic materials 0.000 claims description 5
- -1 hydroxyl Propyl Chemical group 0.000 claims description 5
- DIZPMCHEQGEION-UHFFFAOYSA-H aluminium sulfate (anhydrous) Chemical compound [Al+3].[Al+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O DIZPMCHEQGEION-UHFFFAOYSA-H 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 3
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 2
- 229910021536 Zeolite Inorganic materials 0.000 claims description 2
- 230000009471 action Effects 0.000 claims description 2
- 239000004568 cement Substances 0.000 claims description 2
- 239000003086 colorant Substances 0.000 claims description 2
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims description 2
- FPAFDBFIGPHWGO-UHFFFAOYSA-N dioxosilane;oxomagnesium;hydrate Chemical compound O.[Mg]=O.[Mg]=O.[Mg]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O FPAFDBFIGPHWGO-UHFFFAOYSA-N 0.000 claims description 2
- 238000007667 floating Methods 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 claims description 2
- 239000011863 silicon-based powder Substances 0.000 claims description 2
- 239000002023 wood Substances 0.000 claims description 2
- 239000010457 zeolite Substances 0.000 claims description 2
- 239000011833 salt mixture Substances 0.000 claims 2
- 239000005995 Aluminium silicate Substances 0.000 claims 1
- 239000004354 Hydroxyethyl cellulose Substances 0.000 claims 1
- 229920000663 Hydroxyethyl cellulose Polymers 0.000 claims 1
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 claims 1
- 239000000654 additive Substances 0.000 claims 1
- 230000000996 additive effect Effects 0.000 claims 1
- 229940037003 alum Drugs 0.000 claims 1
- 235000012211 aluminium silicate Nutrition 0.000 claims 1
- 150000001669 calcium Chemical class 0.000 claims 1
- 239000001913 cellulose Substances 0.000 claims 1
- 229920002678 cellulose Polymers 0.000 claims 1
- 235000019447 hydroxyethyl cellulose Nutrition 0.000 claims 1
- 229920003063 hydroxymethyl cellulose Polymers 0.000 claims 1
- 229940031574 hydroxymethyl cellulose Drugs 0.000 claims 1
- FBAFATDZDUQKNH-UHFFFAOYSA-M iron chloride Chemical compound [Cl-].[Fe] FBAFATDZDUQKNH-UHFFFAOYSA-M 0.000 claims 1
- RUTXIHLAWFEWGM-UHFFFAOYSA-H iron(3+) sulfate Chemical class [Fe+3].[Fe+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O RUTXIHLAWFEWGM-UHFFFAOYSA-H 0.000 claims 1
- 229910000360 iron(III) sulfate Inorganic materials 0.000 claims 1
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims 1
- 229920000609 methyl cellulose Polymers 0.000 claims 1
- 239000001923 methylcellulose Substances 0.000 claims 1
- 239000003469 silicate cement Substances 0.000 claims 1
- 239000001509 sodium citrate Substances 0.000 claims 1
- NLJMYIDDQXHKNR-UHFFFAOYSA-K sodium citrate Chemical compound O.O.[Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O NLJMYIDDQXHKNR-UHFFFAOYSA-K 0.000 claims 1
- 235000002906 tartaric acid Nutrition 0.000 claims 1
- 239000011975 tartaric acid Substances 0.000 claims 1
- 239000000725 suspension Substances 0.000 abstract description 6
- 238000001556 precipitation Methods 0.000 abstract description 5
- 238000001179 sorption measurement Methods 0.000 abstract description 5
- 238000001035 drying Methods 0.000 abstract description 2
- 238000005189 flocculation Methods 0.000 abstract 1
- 230000016615 flocculation Effects 0.000 abstract 1
- 235000010755 mineral Nutrition 0.000 description 26
- 239000000306 component Substances 0.000 description 25
- 239000000047 product Substances 0.000 description 22
- 239000000463 material Substances 0.000 description 21
- 239000000243 solution Substances 0.000 description 11
- 238000000034 method Methods 0.000 description 10
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 9
- 239000011575 calcium Substances 0.000 description 7
- 241000276489 Merlangius merlangus Species 0.000 description 6
- 238000005188 flotation Methods 0.000 description 6
- 230000008569 process Effects 0.000 description 6
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 5
- 239000000853 adhesive Substances 0.000 description 5
- 230000001070 adhesive effect Effects 0.000 description 5
- 229910052791 calcium Inorganic materials 0.000 description 5
- 239000000428 dust Substances 0.000 description 5
- 229920001971 elastomer Polymers 0.000 description 5
- 239000000839 emulsion Substances 0.000 description 5
- 230000032683 aging Effects 0.000 description 4
- 230000036541 health Effects 0.000 description 4
- 229910001385 heavy metal Inorganic materials 0.000 description 4
- 150000002500 ions Chemical class 0.000 description 4
- 239000011505 plaster Substances 0.000 description 4
- 238000007665 sagging Methods 0.000 description 4
- 238000004513 sizing Methods 0.000 description 4
- 239000006004 Quartz sand Substances 0.000 description 3
- 239000002585 base Substances 0.000 description 3
- 239000000920 calcium hydroxide Substances 0.000 description 3
- 235000011116 calcium hydroxide Nutrition 0.000 description 3
- 238000006253 efflorescence Methods 0.000 description 3
- 239000010419 fine particle Substances 0.000 description 3
- 239000003292 glue Substances 0.000 description 3
- 239000004922 lacquer Substances 0.000 description 3
- 239000004816 latex Substances 0.000 description 3
- 229920000126 latex Polymers 0.000 description 3
- 239000011777 magnesium Substances 0.000 description 3
- 230000004224 protection Effects 0.000 description 3
- 206010037844 rash Diseases 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- 235000017166 Bambusa arundinacea Nutrition 0.000 description 2
- 244000271437 Bambusa arundinacea Species 0.000 description 2
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical class O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 2
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 238000009825 accumulation Methods 0.000 description 2
- 239000011149 active material Substances 0.000 description 2
- 239000003513 alkali Substances 0.000 description 2
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 2
- 239000000440 bentonite Substances 0.000 description 2
- 229910000278 bentonite Inorganic materials 0.000 description 2
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 description 2
- 230000033228 biological regulation Effects 0.000 description 2
- 239000003610 charcoal Substances 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 229910052681 coesite Inorganic materials 0.000 description 2
- 239000004567 concrete Substances 0.000 description 2
- 229910052593 corundum Inorganic materials 0.000 description 2
- 229910052906 cristobalite Inorganic materials 0.000 description 2
- 238000005034 decoration Methods 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- 238000007791 dehumidification Methods 0.000 description 2
- 239000000835 fiber Substances 0.000 description 2
- 235000019256 formaldehyde Nutrition 0.000 description 2
- 229910052749 magnesium Inorganic materials 0.000 description 2
- 238000012423 maintenance Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 239000004570 mortar (masonry) Substances 0.000 description 2
- 239000002244 precipitate Substances 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 230000008439 repair process Effects 0.000 description 2
- 239000000377 silicon dioxide Substances 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 229910052682 stishovite Inorganic materials 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 229910052905 tridymite Inorganic materials 0.000 description 2
- 229910001845 yogo sapphire Inorganic materials 0.000 description 2
- 235000008733 Citrus aurantifolia Nutrition 0.000 description 1
- 241000533950 Leucojum Species 0.000 description 1
- 239000004677 Nylon Substances 0.000 description 1
- 235000011941 Tilia x europaea Nutrition 0.000 description 1
- 230000006750 UV protection Effects 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 238000007605 air drying Methods 0.000 description 1
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 description 1
- 229910021502 aluminium hydroxide Inorganic materials 0.000 description 1
- 235000011128 aluminium sulphate Nutrition 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000010504 bond cleavage reaction Methods 0.000 description 1
- 230000001680 brushing effect Effects 0.000 description 1
- 229920003086 cellulose ether Polymers 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 230000015271 coagulation Effects 0.000 description 1
- 238000005345 coagulation Methods 0.000 description 1
- 210000001520 comb Anatomy 0.000 description 1
- 239000008358 core component Substances 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 238000000280 densification Methods 0.000 description 1
- 230000001877 deodorizing effect Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 238000006703 hydration reaction Methods 0.000 description 1
- 238000005213 imbibition Methods 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 239000010985 leather Substances 0.000 description 1
- 239000004571 lime Substances 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- 239000000391 magnesium silicate Substances 0.000 description 1
- 229910052919 magnesium silicate Inorganic materials 0.000 description 1
- 235000019792 magnesium silicate Nutrition 0.000 description 1
- ZADYMNAVLSWLEQ-UHFFFAOYSA-N magnesium;oxygen(2-);silicon(4+) Chemical compound [O-2].[O-2].[O-2].[Mg+2].[Si+4] ZADYMNAVLSWLEQ-UHFFFAOYSA-N 0.000 description 1
- 229920001778 nylon Polymers 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 238000005498 polishing Methods 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 239000010453 quartz Substances 0.000 description 1
- 238000005096 rolling process Methods 0.000 description 1
- 230000007017 scission Effects 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 238000013517 stratification Methods 0.000 description 1
- 239000004408 titanium dioxide Substances 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B40/00—Processes, in general, for influencing or modifying the properties of mortars, concrete or artificial stone compositions, e.g. their setting or hardening ability
- C04B40/0028—Aspects relating to the mixing step of the mortar preparation
- C04B40/0039—Premixtures of ingredients
- C04B40/0042—Powdery mixtures
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/00474—Uses not provided for elsewhere in C04B2111/00
- C04B2111/00482—Coating or impregnation materials
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Paints Or Removers (AREA)
- Curing Cements, Concrete, And Artificial Stone (AREA)
Abstract
The invention discloses dry powder coating added with attapulgite mineral and a preparation method thereof. On the basis that the total weight of the dry powder coating is 1000 parts, the dry powder coating is prepared from the following raw material components in parts by weight: 150 to 400 parts of portland cement, 50 to 500 parts of attapulgite, 5 to 50 parts of soluble aluminium salt, 2 to 7 parts of thickening water-retaining agent, 1 to 3 parts of retarder; 0 to 30 parts of color paste, and 450 to 550 parts of filler. The dry powder coating added with the attapulgite mineral adopts the attapulgite as a new-style internal filler, and the attapulgite has better adsorption capacity, and unique dispersibility, plasticity and viscous force, is heat-resistant and low in shrinkage rate after drying, and has no flocculation and no precipitation during suspension.
Description
Technical field
The present invention relates to a kind of coating, belong to house decorative material technical field, particularly relate to a kind of dry powder paint adding attapulgite mineral and preparation method thereof.
Background technology
General interior decoration is common round brush milk of lime, and this is a kind of ancient cheap and the traditional coating of health.
The general powder of lacquer putty for use on of Modern Decorative (coarse whiting and talcum powder) blends 107 or 108 building glues, plaster, rolls emulsion paint afterwards, convenient and quick.Wallpaper class ornament materials, after putty metope, adhesive on brush, spreads the stationery of the magnificent textured pattern such as decorative pattern picture.Dry goods ornament materials, with wallpaper is identical, the latter is with nylon, and fiber crops sheet etc. is main cloth.Being main material diatom ooze with various diatomite ash calcium rubber powders etc., leading environment protection health main body, surface effect is the maddest.
Milk of lime is a kind of conventional ornament materials, although environment protection health, but in early days white lime to cure, and the time is long, and later stage easy efflorescence, user's clothes etc. can be allowed to touch off powder, have a strong impact on practicality.Powder of lacquer putty for use on emulsion paint, 108 and 107 quality of the emulsion that powder of lacquer putty for use on is blent are poor containing harmful substances such as more free formaldehydes, and later stage latex viscosity is because of aging forfeiture, easily efflorescence, cause coming off with the hollowing of top layer emulsion paint, and because high molecular polymer, also can the therefore mouldy adverse effect such as aging running into the environment such as humidity.And the use cycle can discharge a large amount of VOC etc. to air.
Wallpaper class ornament materials, its bottom is still the easily efflorescence of putty ground, and adhesive is typically based on formaldehydes, and bubble easily occurs in work progress, plays drum etc., and the later stage is mouldy, adhesion side easily tilting etc., and construction smell in early days is heavier.The poor dry goods of wearability resistance to soiling is decorated, and with wallpaper is similar to shortcoming, and surface easy dust stratification dirt, easy grain raising etc., adhesive and coloring agent can cause secondary pollution to air.The decoration of diatom ooze class, because of based on ash calcium and rubber powder, lack aggregate, the reasons such as coagulated material is more weak, cause surface more weak, insufficient strength, and because surface effect is the most coarse, easily accumulating dust, resistance to water is poor, and be relatively easy to produce secondary dust pollution, because of containing the more difficult control of the quality such as rubber powder.
Because in attapulgite SiO2, Al2O3A big well-behaved unreacted Ca (OH) in sizing material can be reacted2Deng alkaline matter, and because attapulgite is natural a kind of inorganic mineral, what the later stage was formed is also a kind of inorganic gel, so ultraviolet resistance is aging, etc. show in weatherability superior will not image height molecule such, passage macromolecular chain constantly becomes oxidation scission over time, causes quality in later stage dramatic decrease problem.
General organic gas, it can be attracted in the fine pore size of attapulgite, because attapulgite deodorizing, the utilization in decolouring is relatively broad, and its effect is several times of common bamboo charcoal, and distinctive active bond more can fetter heavy metal ion, does not allow its secondary precipitation.
Attapulgite has the most excellent chain layer structure, common attapulgite slurry just can form the coating of one layer of smooth exquisiteness as paint at body surface, there is oiliness gloss, therefore this material has the exquisiteness not available for other dry powder paints, does not the most produce the contaminative of generic latex or paint.Also having in prior art uses attapulgite to make the patent document of coating as filler, but the effect of attapulgite is not given full play to, so technique effect is barely satisfactory, requires further improvement formula.
Summary of the invention
It is an object of the invention to provide a kind of dry powder paint adding attapulgite mineral, be used as novel inner stuffing with attapulgite, attapulgite has good adsorption capacity, unique dispersiveness, plasticity and viscous force, high temperature resistant, dried shrinkage factor is little, and suspending does not flocculates does not precipitates.
Another object of the present invention is to provide the preparation method of the dry powder paint of a kind of above-mentioned interpolation attapulgite mineral.
The object of the invention to solve the technical problems realizes by the following technical solutions.A kind of dry powder paint adding attapulgite mineral proposed according to the present invention, in terms of the dry powder paint gross weight of 1000 parts, comprises the raw material components of following weight portion:
Portland cement 150～400 parts；Attapulgite 50～500 parts；Aluminum soluble salt 5-50 part；Thickening water-loss reducer 2～7 parts；Retarder 1～3 parts；Mill base 0-30 part；Filler 450-550 part.
The dry powder paint of the present invention, it is also possible to comprise the raw material components of following weight portion:
Portland cement 300～380 parts；Attapulgite 80～200 parts；Aluminum soluble salt 10-40 part；Thickening water-loss reducer 2～4 parts；Retarder 1～2 parts；Mill base 1～15 parts；Filler 487-540 part.
The dry powder paint of the present invention, it is also possible to comprise the raw material components of following weight portion:
The preparation method of the dry powder paint of above-mentioned interpolation attapulgite mineral, comprises following processing step:
1) by tradition attapulgite raw ore through airing, mill and just can use after sieving, it is also possible to through washing, flotation, removal of impurities, after dryness in the sun or strengthen activity after firing, be ground to more than 350 mesh；
2) dicalcium powder selecting fineness to be more than 150 mesh, and possess the portland cement of more than 100 mesh fineness, it is respectively put in a mixing bowl fully dispersed；
3) by step 1) attapulgite mix with other auxiliary agents together with, in above-mentioned steps 2) powder lot dispersing add after 15 minutes, dispersed with stirring discharging after 20 minutes；
4) by step 3) all finished products of discharging through 160 mesh vibratory sieves filter after, both dry powder paint finished product.
The present invention adds the dry powder paint of attapulgite mineral, and its preparation method also comprises step 5) cause the production of liquid and construction:
By sodium metasilicate or potassium silicate lithium metasilicate, being made into corresponding density according to desirable effect is 1.1～1.5g/mm3The aqueous solution, be added into prodan (5%～15% according to silicate addition are added)) after curing agent, roll, brush, the mode such as spray adds step 4 to) dry powder paint surface, both finished product.
By technique scheme, the present invention has the advantage that and has the beneficial effect that:
1) being used as novel inner stuffing with attapulgite in this product, attapulgite is a kind of chain transition structure with fiber pattern layer, and main component is Shuifu County's magnesium silicate, and chemical formula is Mg5(H2O)4[Si4O10]2(OH)2.4H2O.It is commonly called as magnesium palygorskite, palygorskite, mountain leather etc..Attapulgite has good adsorption capacity, unique dispersiveness, plasticity and viscous force, and high temperature resistant, dried shrinkage factor is little, and suspending does not flocculates does not precipitates.
2) in the core component that the dry powder paint of the present invention uses, the water retention property of attapulgite and contained SiO2, Al2O3Can fully promote the Ca (OH) in cement2Deng alkaline matter generation hydration reaction, increase adhesive force and the hardness strength of gel rubber material；The component producing the effect such as adhesiveness, dicoration after all using nonmetallic mineral, construction because of the core ingredient (the cellulose ethers component except for increasing early stage water retention property) in this material is entirely inorganic mineral, so having the highest weatherability, it is significantly larger than high score subclass material service life, reaches the life-span identical with body of wall.
3) attapulgite is presently the most widely applied and is used as decolorising agent (utilizing its absorption property), its effect is several times of common bamboo charcoal, distinctive active bond more can fetter heavy metal ion, do not allow its secondary precipitation, so this material can be effectively prevented material and the situation of the accumulation of salt in the surface soil occurs.
4) without putty layer, directly can directly construct at plaster mortar wall surface, save artificial, and because blending rubber powder layer without putty so that body of wall service life is substantially with the metope same life-span, and reduces putty layer to indoor secondary pollution.
5) add inorganic toner, allow its unique color effect, increase decorative effect, and weatherability wall look decline few.
6) can by drawing, press, also other artistic craft of reeling off raw silk from cocoons make various effect, see the maddest, can be fine and smooth.
7) if being applicable in exterior wall or interior wall matte effect, then complete at plaster, economy-combat grinds off except the caused vestige of artificial chopper, after removing surface loose dirt with dust catcher, with causing liquid rolling, spraying or brush one times, naturally dried through 24 hours, period can not contact water or greasy dirt, after process, whole metope is that dumb light is smooth, seamless connects, thin scabrid dumb light mineral facing properties.
Detailed description of the invention
The dry powder paint adding attapulgite mineral of the present invention, in terms of the dry powder paint gross weight of 1000 parts, comprises the raw material components of following weight portion:
Portland cement 150～400 parts；Attapulgite 50～500 parts；Aluminum soluble salt 5-50 part；Thickening water-loss reducer 2～7 parts；Retarder 1～3 parts；Mill base 0-30 part；Filler 450-550 part.
Introduce effect and the performance of each raw material components individually below:
1, attapulgite: play water-retaining property, the anti-layering of thickening, increase plasticity and be easy to construction attachment, the calcium and magnesium alkaline matter in sizing material, absorption are agreed with reaction etc. by the later stage, increase later strength density, weaken the phenomenons such as the accumulation of salt in the surface soil.Increase weather resistance, and have the strongest suction-operated for the heavy metal ion in material, prevent heavy metal ion secondary precipitation health risk.And the film formation surface of uniqueness, unique silk skating sense and gloss (the generally active attapulgite after washing de-iron).
2, portland cement: inorganic gel materials, plays gel adhewsive action.
3, thickening water-loss reducer: keep moisture, allow the abundant aquation of silicate, play synergy with attapulgite.
4, retarder: control the open hour, improves the effects such as interval time of constructing.
5, filler: improve internal performance such as (light calcium carbonate powder, silicon powder, zeolite powder) etc., can provide enough active material for the later stage.
6, water reducer: moisture in minimizing system and reach working viscosity, increase later stage packing and intensity cohesive force.
7, activity aluminium salt: aluminum soluble salt or sulfuric acid root type soluble-salt, it is provided that microdilatancy, density, strengthens impervious water resistant ability and surface durability against pollution can be according to exquisiteness precipitation regulation filler mesh number.
8, liquid is caused: be mainly composed of soluble silicate (potassium silicate, sodium metasilicate lithium metasilicate) when coated surface, react with unreacted active materials such as the Strong oxdiative calcium on film, moisture in solution more can deep layer penetrate into, and the fully the most whole coating of aquation can the more solid and more rapid improve of intensity again to allow internal mineral；More can improve weathering resistance, the snowflake calcium crystallizable mineral of generation is that coating hardness rises scratch resistance capability as time go on and also improves.
Below by way of concrete preferred embodiment, the present invention is described in further detail, but the present invention is not limited in below example.The unit of following weight portion can be g or kg.
Embodiment
1
A kind of dry powder paint adding attapulgite mineral, comprises each raw material components of following weight portion:
Coarse whiting 512 parts, attapulgite 100 parts, white portland cement (or grey do cool tone) 350 parts, retarder 1 part, titanium dioxide 35 parts, thickening water-loss reducer 2 parts.
The process of preparing of the dry powder paint of above-mentioned interpolation attapulgite mineral comprises the following steps:
1) by tradition attapulgite raw ore through airing, mill and just can use after sieving, can also be through washing, flotation, removal of impurities, after dryness in the sun or strengthen activity after firing, after being ground to more than 350 mesh, now attapulgite purity, suspension adsorptivity all improves a lot, and has excellent distinctive film forming.Moist.Can be through with high whiteness attapulgite as raw material or atlapulgite as needed whiteness to require, this can adjust according to needed for product；
2) dicalcium powder selecting fineness to be more than 150 mesh, and possess the portland cement of more than 100 mesh fineness, it is respectively put in a mixing bowl fully dispersed；
3) attapulgite is mixed with other auxiliary agents together with add after in kind minute at above-mentioned powder lot dispersing, dispersed with stirring discharging after 20 minutes；
4) all finished products are after 160 mesh vibratory sieves filter, and both obtained finished product；
5) cause liquid to produce and construct, by sodium metasilicate or potassium silicate lithium metasilicate, being made into the solution (1.1～1.5g/mm of corresponding density according to desirable effect3, be added into prodan (5%～15% according to silicate addition are added)) after curing agent, roll, brush, the mode such as spray adds attapulgite's surface to, such attapulgite modified presents matte effect.
Embodiment
2
A kind of dry powder paint adding attapulgite mineral, comprises each raw material components of following weight portion:
Essentially identical with above-described embodiment 1, difference is each original shared mass fraction, embodiment adds modified feedstock bentonite, increases the smooth degree of construction.Each component quality is respectively as follows:
Portland cement 250 parts, coarse whiting 416 parts, attapulgite 300 parts, thickening water-loss reducer 3 parts, bentonite 30 parts, retarder 1 part.
The process of preparing of the dry powder paint of above-mentioned interpolation attapulgite mineral comprises the following steps:
1) by tradition attapulgite raw ore through airing, mill and just can use after sieving, can also be through washing, flotation, removal of impurities, after dryness in the sun or strengthen activity after firing, after being ground to more than 350 mesh, now attapulgite purity, suspension adsorptivity all improves a lot, and has excellent distinctive film forming.Moist.Can be through with high whiteness attapulgite as raw material or atlapulgite as needed whiteness to require, this can adjust according to needed for product；
2) dicalcium powder selecting fineness to be more than 150 mesh, and possess the portland cement of more than 100 mesh fineness, it is respectively put in a mixing bowl fully dispersed；
3) attapulgite is mixed with other auxiliary agents together with add after in kind minute at above-mentioned powder lot dispersing, dispersed with stirring discharging after 20 minutes；
4) all finished products are after 160 mesh vibratory sieves filter, and both obtained finished product；
5) cause liquid to produce and construct, by sodium metasilicate or potassium silicate lithium metasilicate, being made into the solution (1.1～1.5g/mm of corresponding density according to desirable effect3, be added into prodan (5%～15% according to silicate addition are added)) after curing agent, roll, brush, the mode such as spray adds attapulgite's surface to, such attapulgite modified presents matte effect.
Embodiment
3
A kind of dry powder paint adding attapulgite mineral, comprises each raw material components of following weight portion:
Essentially identical with above-described embodiment 1, difference be mass fraction between each component not etc. not add concavo-convex content functional etc. to increase coating sophistication and adsorption and dehumidification, each component is respectively as follows:
Portland cement 400 parts, attapulgite 400 parts, thickening water-loss reducer 3 parts, coarse whiting filler 120 parts, fine particle calcium carbonate 30 parts.Retarder 1 part, attapulgite 46 parts.
The process of preparing of the dry powder paint of above-mentioned interpolation attapulgite mineral comprises the following steps:
1) by tradition attapulgite raw ore through airing, mill and just can use after sieving, can also be through washing, flotation, removal of impurities, after dryness in the sun or strengthen activity after firing, after being ground to more than 350 mesh, now attapulgite purity, suspension adsorptivity all improves a lot, and has excellent distinctive film forming.Moist.Can be through with high whiteness attapulgite as raw material or atlapulgite as needed whiteness to require, this can adjust according to needed for product；
2) dicalcium powder selecting fineness to be more than 150 mesh, and possess the portland cement of more than 100 mesh fineness, it is respectively put in a mixing bowl fully dispersed；
3) attapulgite is mixed with other auxiliary agents together with add after in kind minute at above-mentioned powder lot dispersing, dispersed with stirring discharging after 20 minutes；
4) all finished products are after 160 mesh vibratory sieves filter, and both obtained finished product；
5) cause liquid to produce and construct, by sodium metasilicate or potassium silicate lithium metasilicate, being made into the solution (1.1～1.5g/mm of corresponding density according to desirable effect3, be added into prodan (5%～15% according to silicate addition are added)) after curing agent, roll, brush, the mode such as spray adds attapulgite's surface to, such attapulgite modified presents matte effect.
Embodiment
4
A kind of dry powder paint adding attapulgite mineral, comprises each raw material components of following weight portion:
Essentially identical with above-described embodiment 1, what difference was mass fraction between each component not etc. does not adds activared carbon sulfur aluminium salt content to increase coating consistency and secondary repair function etc., and each component is respectively as follows:
Portland cement 380 parts, thickening water-loss reducer 3 parts, coarse whiting filler 520 parts, fine particle calcium carbonate 30 parts, activared carbon sulfur aluminium salt 20 parts, attapulgite 47 parts.This formula is because adding enough activared carbon sulfur aluminium salt, therefore coating makes later stage coating waterproof in densification and the secondary repair ability of micro-cracks at aluminium hydroxide and the aluminium sulfate etc. that the middle and later periods can produce glue, can be widely used in the high humidity atmosphere such as moist underground garage and use.
Embodiment
5
A kind of dry powder paint adding attapulgite mineral, comprises each raw material components of following weight portion:
Essentially identical with above-described embodiment 1, difference be mass fraction between each component not etc. not add water reducer smooth and easy to increase coating initial stage moisture content and construction, each component is respectively as follows:
Portland cement 380 parts, attapulgite 80 parts, thickening water-loss reducer 6 part 80～120 mesh quartz sand fillers 550 parts, water reducer 3 points.This fills a prescription because adding enough water reducers and with quartz sand, therefore coating can reduce coating glue state moisture in the stirring phase, and aggregate quartz sand in hardness by later stage coating, can be widely used in outdoor or coarse artistic effect and use.
Embodiment
6
A kind of dry powder paint adding attapulgite mineral, comprises each raw material components of following weight portion:
Essentially identical with above-described embodiment 1, difference is that the later stage has used and inspires liquid, and coating so can be allowed to play guarantor's look Hardening resistant effect after indoor are as artistic color effect, and each component is respectively as follows:
Portland cement 380 parts, attapulgite 50 parts, thickening water-loss reducer 3 parts, water reducer 4 parts, 40～150 mesh quartz sands 550 parts, 1.25g/mm3Density potassium silicate solution this formula a is because using color art effect, but there will be the dim eclipsed problem of dry powder paint color and luster, therefore coating after dry latter three days under air humidity is less than 80% premise, brushing is at coating surface, uniformly brush, the most moistening not sagging, allow its natural air drying, so effect more color is the most gorgeous truly, density etc..
The process of preparing of the dry powder paint of above-mentioned interpolation attapulgite mineral comprises the following steps:
1) by tradition attapulgite raw ore through airing, mill and just can use after sieving, can also be through washing, flotation, removal of impurities, after dryness in the sun or strengthen activity after firing, after being ground to more than 350 mesh, now attapulgite purity, suspension adsorptivity all improves a lot, and has excellent distinctive film forming.Moist.Can be through with high whiteness attapulgite as raw material or atlapulgite as needed whiteness to require, this can adjust according to needed for product；
2) dicalcium powder selecting fineness to be more than 150 mesh, and possess the portland cement of more than 100 mesh fineness, it is respectively put in a mixing bowl fully dispersed；
3) attapulgite is mixed with other auxiliary agents together with add after in kind minute at above-mentioned powder lot dispersing, dispersed with stirring discharging after 20 minutes；
4) all finished products are after 160 mesh vibratory sieves filter, and both obtained finished product；
5) cause liquid to produce and construct, by sodium metasilicate or potassium silicate lithium metasilicate, being made into the solution (1.1～1.5g/mm of corresponding density according to desirable effect3, be added into prodan (5%～15% according to silicate addition are added)) after curing agent, roll, brush, the mode such as spray adds attapulgite's surface to, such attapulgite modified presents matte effect.
Embodiment
7
A kind of dry powder paint adding attapulgite mineral, comprises each raw material components of following weight portion:
Essentially identical with above-described embodiment 1, difference be mass fraction between each component not etc. not add attapulgite content functional etc. to increase coating sophistication and adsorption and dehumidification, each component is respectively as follows:
Portland cement 400 parts, attapulgite 400 parts, thickening water-loss reducer 3 parts, coarse whiting filler 120 parts, fine particle calcium carbonate 30 parts.Retarder 1 part, attapulgite 46 parts.
The process of preparing of the dry powder paint of above-mentioned interpolation attapulgite mineral comprises the following steps:
1) by tradition attapulgite raw ore through airing, mill and just can use after sieving, can also be through washing, flotation, removal of impurities, after dryness in the sun or strengthen activity after firing, after being ground to more than 350 mesh, now attapulgite purity, suspension adsorptivity all improves a lot, and has excellent distinctive film forming.Moist.Can be through with high whiteness attapulgite as raw material or atlapulgite as needed whiteness to require, this can adjust according to needed for product；
2) dicalcium powder selecting fineness to be more than 150 mesh, and possess the portland cement of more than 100 mesh fineness, it is respectively put in a mixing bowl fully dispersed；
3) attapulgite is mixed with other auxiliary agents together with add after in kind minute at above-mentioned powder lot dispersing, dispersed with stirring discharging after 20 minutes；
4) all finished products are after 160 mesh vibratory sieves filter, and both obtained finished product；
5) cause liquid to produce and construct, by sodium metasilicate or potassium silicate lithium metasilicate, being made into the solution (1.1～1.5g/mm of corresponding density according to desirable effect3, be added into prodan (5%～15% according to silicate addition are added)) after curing agent, roll, brush, the mode such as spray adds attapulgite's surface to, such attapulgite modified presents matte effect.
Effect application test example
The present invention adds the dry powder paint of attapulgite mineral, and its construction and methods for using them can be expressed as follows:
1, select or artificial should be solid by the surface of all metopes, be dried, cleaning is not rocked, without greasy dirt, wax stain and other loose materials；
2, the surface painted should carry out polishing and remove surface paint film, in case later stage pull-away causes object adhesive force to reduce；
3, newly pouring mixed earth after having poured, need maintenance six weeks, the mortar surface newly plastered at least maintenance preventing because bottom cracking shrinks for seven days；
4, the poly-soil of old coagulation and the face of plastering should clean up, and cut loosening, and water dries after rinsing constructs again；
5, ground loosens, and water imbibition is strong or the cleaning of surface floating dust difficulty, can construct after first processing by interfacial agents；
6, first discharge water and add powder afterwards, use electric mixer to stir into paste, it is to avoid first powder causes bottom powder lot dispersing uneven；
7, the ratio of mud is 25～50:100；
8, stirring needs fully, to be as the criterion without powder ball, uses after slightly stirring after stirring after standing 5 minutes；
9, sizing material should be finished according to controlling under weather condition in 4 hours.Should rejecting that top layer skinning is big need not.It is sure not to use being dried after sizing material adds water again.
It addition, such as need artistic effect, then after first plaster background color, utilization instrument cylinder wood grain round brush combs etc., after making effect, wait and inspire liquid on low-humidity environment after drying, entering environment the wettest, opening by silicate mass ratio interpolation 13%～16% silicate solutions density is 1.1～1.5g/mm3, uniform paint surfaces moistens, it is impossible to have sagging, and sagging with towel sagging liquid, dries at once afterwards naturally, without any VOC, environmentally friendly, indoor use when this type of scheme.
Table 1 below introduces the performance introduction contrasting each series of products respectively.
Table 1 contrasts the performance data of each series of products
Resistance to water presses first method test tertiary effluent test in GB/T1733-1993.Alkali resistance is tested by GB/T9265 regulation.Artificial ageing resistance is tested by GB/T9780.
Be can be seen that by the result of above-mentioned table 1, be can be seen that by the result of above-mentioned table 1, for traditional milk of lime, will largely improve with in resistance to water alkali resistance in appearance, and for New-type latex paint, it and all improves a lot in high alkalinity in weatherability, and promote mainly the diatom ooze of environmental protection often in these two weaknesses the biggest, therefore may certify that the high handling property of the concrete emulsion paint of mineral coating of concave convex rod soil type, have the performance coating products of a kind of excellence of the no pollution with environment-friendly materials.
The above, it it is only presently preferred embodiments of the present invention, not the present invention is made any pro forma restriction, therefore it is every without departing from technical solution of the present invention content, any simple modification, equivalent variations and the modification made above example according to the technical spirit of the present invention, all still falls within the range of technical solution of the present invention.
Claims (10)
1. the dry powder paint adding attapulgite mineral, it is characterised in that: with the dry powder paint gross weight of 1000 parts
Meter, comprises the raw material components of following weight portion:
Portland cement 150～400 parts；Attapulgite 50～500 parts；Aluminum soluble salt 5-50 part；Thickening water-loss reducer 2～7
Part；Retarder 1～3 parts；Mill base 0-30 part；Filler 450-550 part.
The dry powder paint of interpolation attapulgite mineral the most according to claim 1, it is characterised in that: comprise following
The raw material components of weight portion:
Portland cement 300～380 parts；Attapulgite 80～200 parts；Aluminum soluble salt 10-40 part；Thickening water-loss reducer
2～4 parts；Retarder 1～2 parts；Mill base 1～15 parts；Filler 487-540 part.
The dry powder paint of interpolation attapulgite mineral the most according to claim 1, it is characterised in that: comprise following
The raw material components of weight portion:
The dry powder paint of interpolation attapulgite mineral the most according to claim 1, it is characterised in that: also comprise 1-10
The water reducer of weight portion, for example, comprise how based water reducer, wood calcium class water reducer.
The dry powder paint of interpolation attapulgite mineral the most according to claim 1, it is characterised in that: described solvable
Property aluminium salt comprise alum, aluminum sulfate ferric sulfate and aluminum sulfate salt-mixture, aluminum sulfate and iron chloride salt-mixture.
The dry powder paint of interpolation attapulgite mineral the most according to claim 1, it is characterised in that: described slow setting
Agent is tartaric acid or the additive of the had deferred action such as sodium citrate or both mixing；
Described thickening water-loss reducer comprises ... the mixing of any one or more in waiting；Methylcellulose hydroxymethyl cellulose hydroxyl
Propyl cellulose, hydroxyethyl cellulose；
Described filler comprises dicalcium powder, light calcium carbonate powder, silicon powder, zeolite powder, talcum powder, in kaolin etc. any one or
Multiple mixing.
The dry powder paint of interpolation attapulgite mineral the most according to claim 1, it is characterised in that: described concavo-convex
Rod soil is the original soil of non-modified and passes through modified attapulgite and atlapulgite.
The dry powder paint of interpolation attapulgite mineral the most according to claim 1, is characterised by: described silicate
Cement is white or other colors, the cement grade portland cement more than 32.5.
9. the preparation method of the dry powder paint adding attapulgite mineral, it is characterised in that: comprise the steps of
1) by tradition attapulgite raw ore through airing, mill and just can use after sieving, it is also possible to through washing, floating
Choosing, removal of impurities, after dryness in the sun or strengthen activity after firing, it is ground to more than 350 mesh；
2) dicalcium powder selecting fineness to be more than 150 mesh, and possess the portland cement of more than 100 mesh fineness, respectively
Put in a mixing bowl fully dispersed；
3) by step 1) attapulgite mix with other auxiliary agents together with, in above-mentioned steps 2) powder lot dispersing 15 points
Add after clock, dispersed with stirring discharging after 20 minutes；
4) by step 3) all finished products of discharging through 160 mesh vibratory sieves filter after, both dry powder paint finished product.
The preparation method of the dry powder paint of interpolation attapulgite mineral the most according to claim 9, it is characterised in that:
Also comprise step 5) cause the production of liquid and construction:
By sodium metasilicate or potassium silicate lithium metasilicate, being made into corresponding density according to desirable effect is 1.1～1.5g/mm3Water-soluble
Liquid, is added into prodan (5%～15% according to silicate addition are added)) after curing agent, roll, brush,
The modes such as spray add step 4 to) dry powder paint surface, both finished product.
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| CN111303682A (en) * | 2020-04-20 | 2020-06-19 | 攀钢集团工程技术有限公司 | Special flexible putty powder for metal fluorocarbon paint |
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