CN105748358B - A kind of agalloch eaglewood essence assigns running water and preparation method thereof - Google Patents
A kind of agalloch eaglewood essence assigns running water and preparation method thereof Download PDFInfo
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- CN105748358B CN105748358B CN201610151171.3A CN201610151171A CN105748358B CN 105748358 B CN105748358 B CN 105748358B CN 201610151171 A CN201610151171 A CN 201610151171A CN 105748358 B CN105748358 B CN 105748358B
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- agalloch eaglewood
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 130
- 241000271309 Aquilaria crassna Species 0.000 title claims abstract description 81
- 238000002360 preparation method Methods 0.000 title claims abstract description 34
- 238000003756 stirring Methods 0.000 claims abstract description 57
- QCDWFXQBSFUVSP-UHFFFAOYSA-N 2-phenoxyethanol Chemical compound OCCOC1=CC=CC=C1 QCDWFXQBSFUVSP-UHFFFAOYSA-N 0.000 claims abstract description 42
- 229960005323 phenoxyethanol Drugs 0.000 claims abstract description 42
- 239000010802 sludge Substances 0.000 claims abstract description 37
- 239000002994 raw material Substances 0.000 claims abstract description 28
- 238000010438 heat treatment Methods 0.000 claims abstract description 26
- 238000001914 filtration Methods 0.000 claims abstract description 17
- 230000002045 lasting effect Effects 0.000 claims abstract description 4
- 239000006228 supernatant Substances 0.000 claims description 15
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 12
- 239000007788 liquid Substances 0.000 claims description 9
- 238000000034 method Methods 0.000 claims description 8
- 238000000605 extraction Methods 0.000 claims description 5
- 239000000203 mixture Substances 0.000 claims description 4
- 239000000843 powder Substances 0.000 claims description 4
- 241001265525 Edgeworthia chrysantha Species 0.000 claims description 2
- 238000001035 drying Methods 0.000 claims description 2
- 238000000926 separation method Methods 0.000 claims description 2
- 238000010792 warming Methods 0.000 claims description 2
- 235000019441 ethanol Nutrition 0.000 claims 3
- 230000000694 effects Effects 0.000 abstract description 20
- 239000002537 cosmetic Substances 0.000 abstract description 5
- YPFDHNVEDLHUCE-UHFFFAOYSA-N propane-1,3-diol Chemical compound OCCCO YPFDHNVEDLHUCE-UHFFFAOYSA-N 0.000 abstract description 4
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 abstract 3
- 238000004945 emulsification Methods 0.000 description 26
- 230000001804 emulsifying effect Effects 0.000 description 13
- 238000011049 filling Methods 0.000 description 13
- 239000011259 mixed solution Substances 0.000 description 13
- 230000000052 comparative effect Effects 0.000 description 12
- 239000000341 volatile oil Substances 0.000 description 9
- 230000035515 penetration Effects 0.000 description 6
- 238000010612 desalination reaction Methods 0.000 description 5
- 230000036541 health Effects 0.000 description 5
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- 239000000047 product Substances 0.000 description 5
- 239000003814 drug Substances 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 239000002904 solvent Substances 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- 239000002253 acid Substances 0.000 description 3
- 230000008901 benefit Effects 0.000 description 3
- 239000003795 chemical substances by application Substances 0.000 description 3
- 238000000151 deposition Methods 0.000 description 3
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- 239000011148 porous material Substances 0.000 description 3
- 239000002453 shampoo Substances 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 description 2
- 208000003351 Melanosis Diseases 0.000 description 2
- 239000004909 Moisturizer Substances 0.000 description 2
- 239000004480 active ingredient Substances 0.000 description 2
- 230000032683 aging Effects 0.000 description 2
- 230000003260 anti-sepsis Effects 0.000 description 2
- 239000008280 blood Substances 0.000 description 2
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- 238000012986 modification Methods 0.000 description 2
- 230000001333 moisturizer Effects 0.000 description 2
- 238000004659 sterilization and disinfection Methods 0.000 description 2
- 230000002936 tranquilizing effect Effects 0.000 description 2
- 230000002087 whitening effect Effects 0.000 description 2
- IQGWPPQNIZBTBM-UHFFFAOYSA-N 2-aminoethanol;sulfuric acid Chemical compound NCCO.OS(O)(=O)=O IQGWPPQNIZBTBM-UHFFFAOYSA-N 0.000 description 1
- 206010000060 Abdominal distension Diseases 0.000 description 1
- 208000002874 Acne Vulgaris Diseases 0.000 description 1
- 241001116389 Aloe Species 0.000 description 1
- 206010002383 Angina Pectoris Diseases 0.000 description 1
- 241001533085 Aquilaria sinensis Species 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- GPXJKVFRKZAYCC-LBPRGKRZSA-N Calacone Natural products O=C1[C@@H](C)CCC(C(C)C)=C1CCC(=C)C GPXJKVFRKZAYCC-LBPRGKRZSA-N 0.000 description 1
- 206010007247 Carbuncle Diseases 0.000 description 1
- 206010008570 Chloasma Diseases 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- OVRNDRQMDRJTHS-UHFFFAOYSA-N N-acelyl-D-glucosamine Natural products CC(=O)NC1C(O)OC(CO)C(O)C1O OVRNDRQMDRJTHS-UHFFFAOYSA-N 0.000 description 1
- OVRNDRQMDRJTHS-FMDGEEDCSA-N N-acetyl-beta-D-glucosamine Chemical compound CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O OVRNDRQMDRJTHS-FMDGEEDCSA-N 0.000 description 1
- MBLBDJOUHNCFQT-LXGUWJNJSA-N N-acetylglucosamine Natural products CC(=O)N[C@@H](C=O)[C@@H](O)[C@H](O)[C@H](O)CO MBLBDJOUHNCFQT-LXGUWJNJSA-N 0.000 description 1
- 244000061176 Nicotiana tabacum Species 0.000 description 1
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 1
- 241000589517 Pseudomonas aeruginosa Species 0.000 description 1
- 240000004808 Saccharomyces cerevisiae Species 0.000 description 1
- 241000191967 Staphylococcus aureus Species 0.000 description 1
- 244000269722 Thea sinensis Species 0.000 description 1
- 241000700647 Variola virus Species 0.000 description 1
- 229930003427 Vitamin E Natural products 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 206010000496 acne Diseases 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 229940006091 aloe polysaccharide Drugs 0.000 description 1
- 235000011399 aloe vera Nutrition 0.000 description 1
- 230000003712 anti-aging effect Effects 0.000 description 1
- 230000001153 anti-wrinkle effect Effects 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 150000001491 aromatic compounds Chemical class 0.000 description 1
- 229910052785 arsenic Inorganic materials 0.000 description 1
- RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic atom Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 description 1
- 208000006673 asthma Diseases 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- YAVVGPBYBUYPSR-UHFFFAOYSA-N benzene;oxygen Chemical compound [O].C1=CC=CC=C1 YAVVGPBYBUYPSR-UHFFFAOYSA-N 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 210000004958 brain cell Anatomy 0.000 description 1
- 210000000481 breast Anatomy 0.000 description 1
- GPXJKVFRKZAYCC-UHFFFAOYSA-N calacone Chemical compound CC(C)C1=C(CCC(C)=C)C(=O)C(C)CC1 GPXJKVFRKZAYCC-UHFFFAOYSA-N 0.000 description 1
- 235000021466 carotenoid Nutrition 0.000 description 1
- 150000001747 carotenoids Chemical class 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- OTAFHZMPRISVEM-UHFFFAOYSA-N chromone Chemical compound C1=CC=C2C(=O)C=COC2=C1 OTAFHZMPRISVEM-UHFFFAOYSA-N 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- LQZZUXJYWNFBMV-UHFFFAOYSA-N dodecan-1-ol Chemical compound CCCCCCCCCCCCO LQZZUXJYWNFBMV-UHFFFAOYSA-N 0.000 description 1
- 230000002500 effect on skin Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 150000002240 furans Chemical class 0.000 description 1
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 235000012907 honey Nutrition 0.000 description 1
- 239000003864 humus Substances 0.000 description 1
- 206010020718 hyperplasia Diseases 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 210000003734 kidney Anatomy 0.000 description 1
- 210000002429 large intestine Anatomy 0.000 description 1
- 238000005461 lubrication Methods 0.000 description 1
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 1
- 229910052753 mercury Inorganic materials 0.000 description 1
- 238000012009 microbiological test Methods 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 230000036651 mood Effects 0.000 description 1
- 210000003205 muscle Anatomy 0.000 description 1
- 229950006780 n-acetylglucosamine Drugs 0.000 description 1
- 210000005036 nerve Anatomy 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 230000000505 pernicious effect Effects 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 230000005808 skin problem Effects 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 210000002784 stomach Anatomy 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 238000004114 suspension culture Methods 0.000 description 1
- 239000000606 toothpaste Substances 0.000 description 1
- 229940034610 toothpaste Drugs 0.000 description 1
- 150000003648 triterpenes Chemical class 0.000 description 1
- 235000019165 vitamin E Nutrition 0.000 description 1
- 229940046009 vitamin E Drugs 0.000 description 1
- 239000011709 vitamin E Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/83—Thymelaeaceae (Mezereum family), e.g. leatherwood or false ohelo
- A61K36/835—Aquilaria
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/965—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of inanimate origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/008—Preparations for oily skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Epidemiology (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Birds (AREA)
- Microbiology (AREA)
- Botany (AREA)
- Mycology (AREA)
- Biotechnology (AREA)
- Engineering & Computer Science (AREA)
- Dermatology (AREA)
- Emergency Medicine (AREA)
- Alternative & Traditional Medicine (AREA)
- Medical Informatics (AREA)
- Medicinal Chemistry (AREA)
- Pharmacology & Pharmacy (AREA)
- Chemical & Material Sciences (AREA)
- Cosmetics (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The present invention relates to Cosmetic Manufacture fields, provide a kind of agalloch eaglewood essence and assign running water and preparation method thereof, agalloch eaglewood essence is assigned running water by weight, is mainly made of following raw material：100 parts of water, 1,3 8~15 parts of propylene glycol, 0.6~0.8 part of Phenoxyethanol, 0.5~1.5 part of Lignum Aquilariae Resinatum extract, extra large 5.0~12.0 parts of sludge extract.Agalloch eaglewood essence assigns running water preparation method, and 1,3 propylene glycol are added in into water, lasting to stir, and is slowly heated heating, obtains mixed liquor I；After mixed liquor I is cooled down, Phenoxyethanol is slowly added to, uniform stirring is clear to mixed liquor, obtains mixed liquor I I；Lignum Aquilariae Resinatum extract, extra large sludge extract are sequentially added into mixed liquor I I, stirring after filtering, obtains agalloch eaglewood essence and assigns running water.This agalloch eaglewood essence, which assigns running water, can improve skin quality, lighten the stain；This preparation method can be further ensured that agalloch eaglewood essence assign running water improve skin quality, lighten the stain the effect of.
Description
Technical field
The present invention relates to Cosmetic Manufacture fields, and running water and preparation method thereof is assigned in particular to a kind of agalloch eaglewood essence.
Background technology
In cosmetic field, it is the good merchantable brand in skin care item to assign running water, Essence etc., and ingredient is exquisite, effect is powerful, skin care
Significant effect, can nourishes rough skin, reduce pore, desalinate obscure, skin whitening or even anti-aging, anti-wrinkle；It is broadly divided into
Two class of aqua and finish, and the raw material components that it is used are generally the nutriment after the concentration extracted from plant, animal.
Agalloch eaglewood, alias are honey perfume, lignum aquilariae resinatum, are dicotyledonous medicine Thymelaeceae magaphanerophytes, also refer to suspension culture of Aquilaria sinensis contains resin
Timber.There are many effect of agalloch eaglewood, not only have obvious curative effects to abdominal distension, stomach cold, kidney deficiency, asthma, moreover it can be used to treat angina pectoris
With bad odor carbuncle.In addition, also there is the extract of agalloch eaglewood sleeping to resist strongly fragrant, stable mood, the work(such as nervous, help qi-blood circulating of releiving
Effect.In the fields such as healthcare products and daily necessities, agalloch eaglewood is also widely used, such as：It agalloch eaglewood dish, Agilawood toothpaste, perfumed soap and washes
Hair agent, the anti-pharynx frost of agalloch eaglewood freshener, agalloch eaglewood, agalloch eaglewood safety are burnt incense, agilawood essential oil atomized liquid, fragrant product etc..
Application publication number is that the application for a patent for invention document of CN105105316A discloses a kind of agilawood essential oil atomized liquid, main
It is made of following raw material：In terms of mass fraction, 1~20 part of agilawood essential oil, 60~90 parts of natural botanical extraction liquid, wherein, institute
The component for stating agilawood essential oil includes：Aromatic compound and sesquiterpenoids, the group of the natural botanical extraction liquid
Divide and include N-acetyl-glucosamine, aloe gel and aloe polysaccharide.The preparation method of the agilawood essential oil atomized liquid includes：By institute
It states agilawood essential oil and is sequentially added with the natural botanical extraction liquid and is mixed evenly, obtained.The atomized liquid is mainly used for improving
Existing tobacco essence taste inclined sweet tea, generates the problems such as pernicious gas at poor taste.
Application publication number be CN103054777A application for a patent for invention document disclose a kind of agalloch eaglewood Chinese medicine shampoo and
Its preparation method, the Chinese medicine shampoo contain Surfactant SDS or lauryl alcohol sulfuric acid ethanolamine salt, stabilizer, suitable
Lubrication prescription and agilawood essential oil, agilawood essential oil content are the 1.5~8% of total weight.The Chinese medicine shampoo can reach hair care effect,
And significant effect.
Although the Related product about Lignum Aquilariae Resinatum extract, agilawood essential oil is a lot of, played the role of also different；But
It is, in cosmetic field, Lignum Aquilariae Resinatum extract fully to be applied to Essence, is assigned in running water, improves skin quality, desalination color to reach
Spot, relieve soreness, tranquilizing the mind nourishing heart effect document be but rarely reported.
In view of this, it is special to propose the present invention.
Invention content
The first object of the present invention is that providing a kind of agalloch eaglewood essence assigns running water, and the agalloch eaglewood essence assigns running water can not only
It enough keeps the skin wet for skin, improves skin quality, lightens the stain, additionally it is possible to relieve soreness, tranquilizing the mind nourishing heart.
The second object of the present invention is to provide the preparation method that a kind of agalloch eaglewood essence assigns running water, this method is easy to operate,
Agalloch eaglewood essence tax running water active ingredient obtained is high, skin effect is good, and good absorption effect.
In order to realize the above-mentioned purpose of the present invention, spy uses following technical scheme：
A kind of agalloch eaglewood essence assigns running water, by weight, is mainly made of following raw material：100 parts of water, 1,3-PD 8
~15 parts, 0.6~0.8 part of Phenoxyethanol, 0.5~1.5 part of Lignum Aquilariae Resinatum extract, extra large 5.0~12.0 parts of sludge extract.
The designer of the present invention using east health as inspiration, by long-term exploration and trial and multiple experiment and
Effort, it is continuous to reform and innovate, it is special to determine Lignum Aquilariae Resinatum extract, extra large sludge extract as important source material, have devised the agalloch eaglewood
Essence assigns running water, takes full advantage of the intrinsic penetration power of Lignum Aquilariae Resinatum extract, and combine with 1,3-PD and Phenoxyethanol, improves
Its penetration, makes Lignum Aquilariae Resinatum extract directly reach skin corium, keeps the skin wet, and changes damaged cell.
Above-mentioned agalloch eaglewood essence is assigned in running water, and water is used as solvent, and for 1,3-PD as moisturizer, playing protects skin
Wet effect, Phenoxyethanol plays antisepsis, and Lignum Aquilariae Resinatum extract and extra large sludge extract play tune as skin conditioning agent
Manage the effect of skin skin quality.
The present invention also provides the preparation method that the agalloch eaglewood essence described in any of the above-described scheme assigns running water, including following step
Suddenly：
(1) 1,3-PD is added in into water, it is lasting to stir, and heating is slowly heated with the heating rate of 1-5 DEG C/min,
Obtain mixed liquor I；
(2) after mixed liquor I being cooled to 40-55 DEG C, Phenoxyethanol is slowly added to, uniform stirring is clear to mixed liquor, obtains
Obtain mixed liquor I I；
(3) Lignum Aquilariae Resinatum extract, extra large sludge extract are sequentially added into mixed liquor I I, stirring, after filtering, it is described heavy to obtain
Running water is assigned by essence China.
It in step (1), needs to add in 1,3-PD and is mixed into water, otherwise be easy to cause subsequent heat process
In, 1,3-PD is in direct contact with reaction vessel, and overheat chemically reacts；1,3-PD is added to the water, is made with water
For solvent, mitigation can be played.
The preparation process of above-mentioned agalloch eaglewood essence tax running water can improve the dissolubility of Lignum Aquilariae Resinatum extract, extra large sludge extract,
The agalloch eaglewood prepared essence is made to assign active ingredient in running water to be more easy to be absorbed by user.
Compared with prior art, beneficial effects of the present invention are：
(1) agalloch eaglewood essence of the present invention assigns running water with Lignum Aquilariae Resinatum extract, extra large sludge extract, 1,3- propylene glycol and Phenoxyethanol
It is prepared for raw material, not only fragrance is fresh, simple and elegant, but also can improve skin quality, can removing acne and freckle, diminution pore, desalination black
Element, skin whitening, through skin skin corium keep the skin wet for skin, solve small pox, chloasma, it is glossy have one's face covered with, pore is coarse, face
The skin problem such as color dimness.
(2) agalloch eaglewood essence of the present invention assigns the superpower penetration power and penetration that running water takes full advantage of agalloch eaglewood, can dredge blood
Pipe；Running water is assigned using agalloch eaglewood essence of the present invention and is sprayed on the positions such as lymph, oxter, can be dredged lymph, be prevented breast lobule hyperplasia.
(3) during DOMS, running water spray muscle is assigned using agalloch eaglewood essence of the present invention, DOMS can be alleviated.
(4) agalloch eaglewood essence of the present invention assign running water can calm the nerves nourishing heart, help enhancing brain cell activity, promote memory and note
Meaning power, improves resourceful degree, refreshes the mind, and improves working efficiency.
Specific embodiment
Embodiment of the present invention is described in detail below in conjunction with embodiment, but those skilled in the art will
Understand, the following example is merely to illustrate the present invention, and is not construed as limiting the scope of the invention.It is not specified in embodiment specific
Condition person, the condition suggested according to normal condition or manufacturer carry out.Reagents or instruments used without specified manufacturer is
The conventional products that can be obtained by commercially available purchase.
The designer of the present invention using east health as inspiration, by long-term exploration and trial and multiple experiment and
Effort, it is continuous to reform and innovate, it is special to determine Lignum Aquilariae Resinatum extract, extra large sludge extract as important source material, have devised the agalloch eaglewood
Essence assigns running water.This agalloch eaglewood essence assigns running water, by weight, is mainly made of following raw material：100 parts of water, 1,3- the third two
8~15 parts of alcohol, 0.6~0.8 part of Phenoxyethanol, 0.5~1.5 part of Lignum Aquilariae Resinatum extract, extra large 5.0~12.0 parts of sludge extract.
This agalloch eaglewood essence assigns running water and takes full advantage of the intrinsic penetration power of Lignum Aquilariae Resinatum extract, and with 1,3-PD and benzene
Oxyethanol combines, and improves its penetration, Lignum Aquilariae Resinatum extract is made directly to reach skin corium, keep the skin wet, and changes damaged cell.
Above-mentioned agalloch eaglewood essence is assigned in running water, and water is used as solvent, and for 1,3-PD as moisturizer, playing protects skin
Wet effect, Phenoxyethanol plays antisepsis, and Lignum Aquilariae Resinatum extract and extra large sludge extract play tune as skin conditioning agent
Manage the effect of skin skin quality.
Experiment proves that rational amounts of components can preferably improve skin quality, desalination skin splash, preferably, by weight
Part meter is measured, is mainly made of following raw material：100 parts of water, 9.3~12.6 parts of 1,3-PD, 0.70~0.76 part of Phenoxyethanol,
0.6~1.3 part of Lignum Aquilariae Resinatum extract, extra large 5.8~11.3 parts of sludge extract.
It is further preferred that it by weight, is mainly made of following raw material：100 parts of water, 12.5 parts of 1,3-PD, benzene oxygen second
0.75 part of alcohol, 0.6 part of Lignum Aquilariae Resinatum extract, extra large 11.0 parts of sludge extract.
The present invention also provides the preparation method that the agalloch eaglewood essence described in any of the above-described scheme assigns running water, including following step
Suddenly：
(1) 1,3-PD is added in into water, it is lasting to stir, and heating is slowly heated, obtain mixed liquor I；
(2) after mixed liquor I is cooled down, Phenoxyethanol is slowly added to, uniform stirring is clear to mixed liquor, obtains mixed liquor
II；
(3) Lignum Aquilariae Resinatum extract, extra large sludge extract are sequentially added into mixed liquor I I, stirring, after filtering, it is described heavy to obtain
Running water is assigned by essence China.
It in step (1), needs to add in 1,3-PD and is mixed into water, otherwise be easy to cause subsequent heat process
In, 1,3-PD is in direct contact with reaction vessel, and overheat chemically reacts；1,3-PD is added to the water, is made with water
For solvent, mitigation can be played.
In step (1), stirring needs at the uniform velocity, and its mixing speed is unsuitable too fast, otherwise easily cause excessive thermal losses and
Water is lost and reduces the dissolution rate of raw material, preferably, the speed of the stirring is 20~30r/min.
In step (1), the speed of heat temperature raising should be controlled, it is unsuitable too fast, otherwise easily cause hot-spot；As excellent
Choosing, the heating speed for being slowly heated heating are 1~3 DEG C/min.
The stringent control of water temperature can not only ensure the abundant dissolving of 1,3-PD, additionally it is possible to play the sterilization of reagent
Disinfection.Preferably, in step (1), slow heating is warming up to 80~85 DEG C.
In step (2), the temperature of cooling is controlled, and in the case where keeping the temperature, add Phenoxyethanol；Temperature mistake
Height can cause partial material to volatilize or decompose.Preferably, the mixed liquor I is cooled to 40~45 DEG C.
After step (2), need to carry out the inspection ageing process of 72 hours, material body, can recovery room in ageing process
Temperature.
Preferably, in step (2), the speed of stirring is 20~30r/min.
Preferably, in step (3), mixing time is 5~15 minutes.
Lignum Aquilariae Resinatum extract and extra large sludge extract can directly buy acquisition, can also process preparation.It is provided below one
The preparation method of kind Lignum Aquilariae Resinatum extract and a kind of preparation method of extra large sludge extract.
Wherein, the preparation method of Lignum Aquilariae Resinatum extract is：(1) agalloch eaglewood of Edgeworthia chrysantha is taken, after being cut into small pieces, is crushed to 15 mesh
Agalloch eaglewood powder；(2) water is added in into agalloch eaglewood powder, is heated to 100 DEG C, and keep temperature 12h, then carried out refrigerated separation, obtain
Obtain Lignum Aquilariae Resinatum extract (or being linaloe oil).Above-mentioned Lignum Aquilariae Resinatum extract includes chromone, triterpene, calacone and furans acid.
The extracting method of extra large sludge extract is：Green mud and black mud are taken, after 30 DEG C of drying, is cooled to room temperature, by mass ratio
It is 1:1 green mud and the mixture of black mud are placed in ethanol solution (mass fraction 75%, volume are 8 times of volume of mixture)
Extraction centrifuges 30min for 24 hours, with the speed of 2500r/min, takes supernatant, obtains extra large sludge extract and (or is extracted for extra large mud
Liquid).Green mud is collected in anaerobic environment, and the deposition for not undergoing excessive scale is decomposed, rich in carotenoid, vitamin E, mainly
The antioxidant effect as obtained by depositing blue-green alge, can be applied to dryness and sensitive.The black mud is in deeper lake,
Large-scale deposition is lived through to decompose, than green mud degree of oxidation bigger, rich in humus acid and aliphatic acid, can be applied to oiliness and
Problem skin.
Embodiment 1
Take following raw material：Water 100g, 1,3-PD 12.5g, Phenoxyethanol 0.75g, Lignum Aquilariae Resinatum extract 0.6g, sea are become silted up
Mud extract 11.0g.
Follow the steps below preparation：
(1) water is first added in into the emulsification pot cleaned up, then 1,3-PD is added in into emulsification pot, with 25r/min
Speed continue mixed solution in stirring and emulsifying pot, and 85 DEG C are to slowly warm up to the speed of 1 DEG C/min, stop heating, obtain
Obtain mixed liquor I；
(2) mixed liquor I is cooled to 45 DEG C, is slowly added to Phenoxyethanol, persistently stirred with the speed of 25r/min, uniformly
Stirring is clear to mixed liquor, obtains mixed liquor I I；
(3) Lignum Aquilariae Resinatum extract, extra large sludge extract are sequentially added into mixed liquor I I again, after stirring 10min, filtering takes
Supernatant obtains the agalloch eaglewood essence and assigns running water；
(4) it detects the agalloch eaglewood essence and assigns running water, it is filling after qualified.
Embodiment 2
Take following raw material：Water 100g, 1,3-PD 8g, Phenoxyethanol 0.6g, Lignum Aquilariae Resinatum extract 0.5g, extra large mud carry
Take object 5.0g.
Follow the steps below preparation：
(1) water is first added in into the emulsification pot cleaned up, then 1,3-PD is added in into emulsification pot, with 25r/min
Speed continue mixed solution in stirring and emulsifying pot, and 85 DEG C are to slowly warm up to the speed of 1 DEG C/min, stop heating, obtain
Obtain mixed liquor I；
(2) mixed liquor I is cooled to 45 DEG C, is slowly added to Phenoxyethanol, persistently stirred with the speed of 25r/min, uniformly
Stirring is clear to mixed liquor, obtains mixed liquor I I；
(3) Lignum Aquilariae Resinatum extract, extra large sludge extract are sequentially added into mixed liquor I I again, after stirring 10min, filtering takes
Supernatant obtains the agalloch eaglewood essence and assigns running water；
(4) it detects the agalloch eaglewood essence and assigns running water, it is filling after qualified.
Embodiment 3
Take following raw material：Water 100g, 1,3-PD 15g, Phenoxyethanol 0.8g, Lignum Aquilariae Resinatum extract 1.5g, extra large mud
Extract 12.0g.
It is operated according to following steps：
(1) water is first added in into the emulsification pot cleaned up, then 1,3-PD is added in into emulsification pot, with 25r/min
Speed continue mixed solution in stirring and emulsifying pot, and 85 DEG C are to slowly warm up to the speed of 1 DEG C/min, stop heating, obtain
Obtain mixed liquor I；
(2) mixed liquor I is cooled to 50 DEG C, is slowly added to Phenoxyethanol, persistently stirred with the speed of 25r/min, uniformly
Stirring is clear to mixed liquor, obtains mixed liquor I I；
(3) Lignum Aquilariae Resinatum extract, extra large sludge extract are sequentially added into mixed liquor I I again, after stirring 10min, filtering takes
Supernatant obtains the agalloch eaglewood essence and assigns running water；
(4) it detects the agalloch eaglewood essence and assigns running water, it is filling after qualified.
Embodiment 4
Take following raw material：Water 100g, 1,3-PD 9.3g, 0.7g parts, Lignum Aquilariae Resinatum extract 0.6g of Phenoxyethanol, sea are become silted up
Mud extract 5.8g.
It is operated according to following steps：
(1) water is first added in into the emulsification pot cleaned up, then 1,3-PD is added in into emulsification pot, with 25r/min
Speed continue mixed solution in stirring and emulsifying pot, and 85 DEG C are to slowly warm up to the speed of 1 DEG C/min, stop heating, obtain
Obtain mixed liquor I；
(2) mixed liquor I is cooled to 45 DEG C, is slowly added to Phenoxyethanol, persistently stirred with the speed of 25r/min, uniformly
Stirring is clear to mixed liquor, obtains mixed liquor I I；
(3) Lignum Aquilariae Resinatum extract, extra large sludge extract are sequentially added into mixed liquor I I again, after stirring 10min, filtering takes
Supernatant obtains the agalloch eaglewood essence and assigns running water；
(4) it detects the agalloch eaglewood essence and assigns running water, it is filling after qualified.
Embodiment 5
Take following raw material：Water 100g, 1,3-PD 12.6g, Phenoxyethanol 0.76g, Lignum Aquilariae Resinatum extract 1.3g, sea are become silted up
Mud extract 11.3g.
It is operated according to following steps：
(1) water is first added in into the emulsification pot cleaned up, then 1,3-PD is added in into emulsification pot, with 25r/min
Speed continue mixed solution in stirring and emulsifying pot, and 85 DEG C are to slowly warm up to the speed of 1 DEG C/min, stop heating, obtain
Obtain mixed liquor I；
(2) mixed liquor I is cooled to 45 DEG C, is slowly added to Phenoxyethanol, persistently stirred with the speed of 25r/min, uniformly
Stirring is clear to mixed liquor, obtains mixed liquor I I；
(3) Lignum Aquilariae Resinatum extract, extra large sludge extract are sequentially added into mixed liquor I I again, after stirring 10min, filtering takes
Supernatant obtains the agalloch eaglewood essence and assigns running water；
(4) it detects the agalloch eaglewood essence and assigns running water, it is filling after qualified.
Embodiment 6
Take following raw material：Water 100g, 1,3-PD 12.5g, Phenoxyethanol 0.75g, Lignum Aquilariae Resinatum extract 0.6g, sea are become silted up
Mud extract 11.0g.
Follow the steps below preparation：
(1) water is first added in into the emulsification pot cleaned up, then 1,3-PD is added in into emulsification pot, with 30r/min
Speed continue mixed solution in stirring and emulsifying pot, and 85 DEG C are to slowly warm up to the speed of 3 DEG C/min, stop heating, obtain
Obtain mixed liquor I；
(2) mixed liquor I is cooled to 45 DEG C, is slowly added to Phenoxyethanol, persistently stirred with the speed of 25r/min, uniformly
Stirring is clear to mixed liquor, obtains mixed liquor I I；
(3) Lignum Aquilariae Resinatum extract, extra large sludge extract are sequentially added into mixed liquor I I again, after stirring 10min, filtering takes
Supernatant obtains the agalloch eaglewood essence and assigns running water；
(4) it detects the agalloch eaglewood essence and assigns running water, it is filling after qualified.
Embodiment 7
Take following raw material：Water 100g, 1,3-PD 12.5g, Phenoxyethanol 0.75g, Lignum Aquilariae Resinatum extract 0.6g, sea are become silted up
Mud extract 11.0g.
Follow the steps below preparation：
(1) water is first added in into the emulsification pot cleaned up, then 1,3-PD is added in into emulsification pot, with 30r/min
Speed continue mixed solution in stirring and emulsifying pot, and 85 DEG C are to slowly warm up to the speed of 3 DEG C/min, stop heating, obtain
Obtain mixed liquor I；
(2) mixed liquor I is cooled to 40 DEG C, is slowly added to Phenoxyethanol, persistently stirred with the speed of 25r/min, uniformly
Stirring is clear to mixed liquor, obtains mixed liquor I I；
(3) Lignum Aquilariae Resinatum extract, extra large sludge extract are sequentially added into mixed liquor I I again, after stirring 10min, filtering takes
Supernatant obtains the agalloch eaglewood essence and assigns running water；
(4) it detects the agalloch eaglewood essence and assigns running water, it is filling after qualified.
Comparative example 1
Take following raw material：Water 100g, 1,3-PD 12.5g, Phenoxyethanol 0.75g, Lignum Aquilariae Resinatum extract 0.6g.
Follow the steps below preparation：
(1) water is first added in into the emulsification pot cleaned up, then 1,3-PD is added in into emulsification pot, with 25r/min
Speed continue mixed solution in stirring and emulsifying pot, and 85 DEG C are to slowly warm up to the speed of 1 DEG C/min, stop heating, obtain
Obtain mixed liquor I；
(2) mixed liquor I is cooled to 45 DEG C, is slowly added to Phenoxyethanol, persistently stirred with the speed of 25r/min, uniformly
Stirring is clear to mixed liquor, obtains mixed liquor I I；
(3) Lignum Aquilariae Resinatum extract is added in into mixed liquor I I again, after stirring 10min, filtering takes supernatant, obtains the tax
Running water；
(4) the tax running water is detected, it is filling after qualified.
Comparative example 2
Take following raw material：Water 100g, 1,3-PD 12.5g, Phenoxyethanol 0.75g, extra large sludge extract 11.0g.
Follow the steps below preparation：
(1) water is first added in into the emulsification pot cleaned up, then 1,3-PD is added in into emulsification pot, with 25r/min
Speed continue mixed solution in stirring and emulsifying pot, and 85 DEG C are to slowly warm up to the speed of 1 DEG C/min, stop heating, obtain
Obtain mixed liquor I；
(2) mixed liquor I is cooled to 45 DEG C, is slowly added to Phenoxyethanol, persistently stirred with the speed of 25r/min, uniformly
Stirring is clear to mixed liquor, obtains mixed liquor I I；
(3) extra large sludge extract is added in into mixed liquor I I again, after stirring 10min, filtering takes supernatant, described in acquisition
Assign running water；
(4) the tax running water is detected, it is filling after qualified.
Comparative example 3
Take following raw material：Water 100g, 1,3-PD 12.5g, Phenoxyethanol 0.75g, Lignum Aquilariae Resinatum extract 1.0g, sea are become silted up
Mud extract 3.0g.
Follow the steps below preparation：
(1) water is first added in into the emulsification pot cleaned up, then 1,3-PD is added in into emulsification pot, with 25r/min
Speed continue mixed solution in stirring and emulsifying pot, and 85 DEG C are to slowly warm up to the speed of 1 DEG C/min, stop heating, obtain
Obtain mixed liquor I；
(2) mixed liquor I is cooled to 45 DEG C, is slowly added to Phenoxyethanol, persistently stirred with the speed of 25r/min, uniformly
Stirring is clear to mixed liquor, obtains mixed liquor I I；
(3) after Lignum Aquilariae Resinatum extract, extra large sludge extract are sequentially added into mixed liquor I I again, after stirring 10min, filtering,
Supernatant is taken, the agalloch eaglewood essence is obtained and assigns running water；
(4) it detects the agalloch eaglewood essence and assigns running water, it is filling after qualified.
Comparative example 4
Take following raw material：Water 100g, 1,3-PD 12.5g, Phenoxyethanol 0.75g, Lignum Aquilariae Resinatum extract 0.3g, sea are become silted up
Mud extract 15.0g.
It is operated according to following steps：
(1) water is first added in into the emulsification pot cleaned up, then 1,3-PD is added in into emulsification pot, with 25r/min
Speed continue mixed solution in stirring and emulsifying pot, and 85 DEG C are to slowly warm up to the speed of 1 DEG C/min, stop heating, obtain
Obtain mixed liquor I；
(2) mixed liquor I is cooled to 45 DEG C, is slowly added to Phenoxyethanol, persistently stirred with the speed of 25r/min, uniformly
Stirring is clear to mixed liquor, obtains mixed liquor I I；
(3) after Lignum Aquilariae Resinatum extract, extra large sludge extract are sequentially added into mixed liquor I I again, after stirring 10min, filtering,
Supernatant is taken, the agalloch eaglewood essence is obtained and assigns running water；
(4) it detects the agalloch eaglewood essence and assigns running water, it is filling after qualified.
Comparative example 5
Take following raw material：Water 100g, 1,3-PD 12.5g, Phenoxyethanol 0.75g, Lignum Aquilariae Resinatum extract 0.6g, sea are become silted up
Mud extract 11.0g.
It is operated according to following steps：
(1) water is first added in into the emulsification pot cleaned up, then 1,3-PD is added in into emulsification pot, with 35r/min
Speed continue mixed solution in stirring and emulsifying pot, and 85 DEG C are to slowly warm up to the speed of 5 DEG C/min, stop heating, obtain
Obtain mixed liquor I；
(2) mixed liquor I is cooled to 45 DEG C, is slowly added to Phenoxyethanol, persistently stirred with the speed of 25r/min, uniformly
Stirring is clear to mixed liquor, obtains mixed liquor I I；
(3) after Lignum Aquilariae Resinatum extract, extra large sludge extract are sequentially added into mixed liquor I I again, after stirring 10min, filtering,
Supernatant is taken, the agalloch eaglewood essence is obtained and assigns running water；
(4) it detects the agalloch eaglewood essence and assigns running water, it is filling after qualified.
Comparative example 6
Take following raw material：Water 100g, 1,3-PD 12.5g, Phenoxyethanol 0.75g, Lignum Aquilariae Resinatum extract 0.6g, sea are become silted up
Mud extract 11.0g.
It is operated according to following steps：
(1) water is first added in into the emulsification pot cleaned up, then 1,3-PD is added in into emulsification pot, with 35r/min
Speed continue mixed solution in stirring and emulsifying pot, and 85 DEG C are to slowly warm up to the speed of 5 DEG C/min, stop heating, obtain
Obtain mixed liquor I；
(2) mixed liquor I is cooled to 55 DEG C, is slowly added to Phenoxyethanol, persistently stirred with the speed of 25r/min, uniformly
Stirring is clear to mixed liquor, obtains mixed liquor I I；
(3) after Lignum Aquilariae Resinatum extract, extra large sludge extract are sequentially added into mixed liquor I I again, after stirring 10min, filtering,
Supernatant is taken, the agalloch eaglewood essence is obtained and assigns running water；
(4) it detects the agalloch eaglewood essence and assigns running water, it is filling after qualified.
Experimental example
Examples 1 to 7 and comparative example 1~6 are repeated, agalloch eaglewood essence is made and assigns running water or assigns running water；According to《Cosmetics health
Specification》, above-mentioned agalloch eaglewood essence is assigned into running water or assigns running water progress wholesomeness inspection, testing result is as shown in Table 1 and Table 2：
1. Micro biological Tests result of table
2. health chemical testing result of table
Through microorganism detection, total plate count, yeast and mold, pseudomonas aeruginosa, staphylococcus aureus, excrement large intestine
Bacteria detection result meets the requirements；Through health chemical testing, lead, arsenic, mercury inspection result meet the requirements.
Volunteer is recruited, selection skin quality is coarse, dim and volunteer heavier color spot is tested, with above-described embodiment 1
~7 and comparative example 1~6 made from agalloch eaglewood essence assign running water or assign running water be sample, using clear water for control, allow experimenter (test
Person is divided into 14 groups, every group of 30 people, totally 420 people) it is each using primary daily morning and evening, and assist other skin care item, other shields of experimenter
Skin product all same, 15 days are a test period, and observation improves situation using rear experimenter's skin quality, and record skin quality improves and color spot
The number of desalination, as a result such as table 3：
3. experimenter's skin quality of table improves situation survey graft.
As shown in the above results, the agalloch eaglewood essence tax running water prepared using embodiment 1 can most effectively improve subject
Skin quality, lighten the stain；Agalloch eaglewood essence prepared by embodiment 2~5 is assigned running water and is slightly different in amounts of components with embodiment 1,
Effect is slightly worse than embodiment 1, but still can effectively improve the skin quality of subject, lightens the stain.
Embodiment 6~7 is matched using raw material components same as Example 1, but condition and embodiment 1 in preparation process
Difference, finally, effect are slightly worse than example；The preparation process for illustrating agalloch eaglewood essence tax running water of the present invention can influence agalloch eaglewood essence
The effect of running water, is assigned by China, it should stringent control.
Lack extra large sludge extract in the tax running water prepared in comparative example 1, although the skin quality of part subject can be improved,
But for most subjects, to no effect.
Lack Lignum Aquilariae Resinatum extract in the tax running water prepared in comparative example 2, it is apparent that effect is than comparison from result
Example 1 is worse, illustrates that Lignum Aquilariae Resinatum extract assigns improvement of the component of running water to subject's skin quality as agalloch eaglewood essence of the present invention, color spot
Desalination, plays the role of very important.
In the tax running water prepared in comparative example 3~4, because the dosage of raw material components is not reasonable, hence it is evident that reduce subject
The successful number that skin quality improves；Comparative example 5~6, although employing raw material components same as Example 1 and dosage, because
Preparation process has differences, and also results in the successful number of subject's skin quality improvement and reduces.In clear water control group, the skin quality of subject
And color spot does not improve.
Although illustrate and describing the present invention with specific embodiment, it will be appreciated that without departing substantially from the present invention's
Many other change and modification can be made in the case of spirit and scope.It is, therefore, intended that in the following claims
Including belonging to all such changes and modifications in the scope of the invention.
Claims (10)
1. a kind of agalloch eaglewood essence assigns running water, which is characterized in that by weight, is mainly made of following raw material：100 parts of water, 1,
8~15 parts of 3-propanediol, 0.6~0.8 part of Phenoxyethanol, 0.5~1.5 part of Lignum Aquilariae Resinatum extract, extra large sludge extract 5.0~12.0
Part；
Wherein, the preparation method of the Lignum Aquilariae Resinatum extract is：(1) agalloch eaglewood of Edgeworthia chrysantha is taken, is crushed to the agalloch eaglewood powder of 15 mesh；
(2) water is added in into agalloch eaglewood powder, is heated to 100 DEG C, and keep temperature 12h, then carry out refrigerated separation, obtain agalloch eaglewood extraction
Object；
It is described sea sludge extract extracting method be：Green mud and black mud are taken, after 30 DEG C of drying, is cooled to room temperature, by mass ratio
It is 1:1 green mud and the mixture of black mud, which are placed in ethanol solution, to be extracted for 24 hours, and the mass fraction of ethanol solution is 75%, ethyl alcohol
The volume of solution is 8 times of volume of mixture, centrifuges 30min with the speed of 2500r/min, takes supernatant, obtains extra large mud and carries
Take object.
2. agalloch eaglewood essence according to claim 1 assigns running water, which is characterized in that by weight, mainly by following raw material
It is made：100 parts of water, 9.3~12.6 parts of 1,3-PD, 0.70~0.76 part of Phenoxyethanol, 0.6~1.3 part of Lignum Aquilariae Resinatum extract,
Extra large 5.8~11.3 parts of sludge extract.
3. agalloch eaglewood essence according to claim 1 assigns running water, which is characterized in that by weight, mainly by following raw material
It is made：100 parts of water, 12.5 parts of 1,3-PD, 0.75 part of Phenoxyethanol, 0.6 part of Lignum Aquilariae Resinatum extract, extra large sludge extract 11.0
Part.
4. the preparation method of running water is assigned according to any one of claims 1 to 3 agalloch eaglewood essence, which is characterized in that including following
Step：
(1) 1,3-PD is added in into water, it is lasting to stir, and heating is slowly heated with the heating rate of 1-5 DEG C/min, it obtains
Mixed liquor I；
(2) after mixed liquor I being cooled to 40-50 DEG C, Phenoxyethanol is slowly added to, uniform stirring is clear to mixed liquor, is mixed
Close liquid II；
(3) Lignum Aquilariae Resinatum extract, extra large sludge extract are sequentially added into mixed liquor I I, stirring after filtering, obtains the agalloch eaglewood essence
Running water is assigned by China.
5. preparation method according to claim 4, which is characterized in that in step (1), the speed of the stirring for 20~
30r/min。
6. preparation method according to claim 4, which is characterized in that in step (1), the heating of the slow heating heating
Rate is 1~3 DEG C/min.
7. preparation method according to claim 4, which is characterized in that in step (1), slow heating is warming up to 80~85
℃。
8. preparation method according to claim 4, which is characterized in that in step (2), mixed liquor I is cooled to 40~45 DEG C.
9. preparation method according to claim 4, which is characterized in that in step (2), the speed of the stirring for 20~
30r/min。
10. preparation method according to claim 4, which is characterized in that in step (3), the time of the stirring is 5~15
Minute.
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| CN106361684A (en) * | 2016-08-31 | 2017-02-01 | 广东芭薇生物科技股份有限公司 | Active composition for adjusting microorganism ecological balance of skin surface |
| CN106727035A (en) * | 2017-01-23 | 2017-05-31 | 珠海市玖鑫化妆品有限公司 | The preparation technology and antiallergic of a kind of Lignum Aquilariae Resinatum extract repair facial mask |
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|---|---|---|---|---|
| CN103054777A (en) * | 2013-01-14 | 2013-04-24 | 中山市国林沉香科学研究所 | Agarwood Chinese Medicine Shampoo and Its Preparation Method |
| CN104523520A (en) * | 2014-12-19 | 2015-04-22 | 韩嘉 | Application of Aquilaria sinensis extract used as effective constituent for whitening |
| CN104940050A (en) * | 2015-05-07 | 2015-09-30 | 孙广娥 | Use of agilawood volatile oil stoste in preparation of skin-care product |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103054777A (en) * | 2013-01-14 | 2013-04-24 | 中山市国林沉香科学研究所 | Agarwood Chinese Medicine Shampoo and Its Preparation Method |
| CN104523520A (en) * | 2014-12-19 | 2015-04-22 | 韩嘉 | Application of Aquilaria sinensis extract used as effective constituent for whitening |
| CN104940050A (en) * | 2015-05-07 | 2015-09-30 | 孙广娥 | Use of agilawood volatile oil stoste in preparation of skin-care product |
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| "海泥美容功效体系制备条件的研究";罗红宇等;《浙江海洋学院学报（自然科学版）》;20091231;第28卷(第4期);415-418 * |
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