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CN105619848B - A kind of microwave heating equipment and method - Google Patents

A kind of microwave heating equipment and method Download PDF

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Publication number
CN105619848B
CN105619848B CN201610030557.9A CN201610030557A CN105619848B CN 105619848 B CN105619848 B CN 105619848B CN 201610030557 A CN201610030557 A CN 201610030557A CN 105619848 B CN105619848 B CN 105619848B
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microwave
absorbing material
cavity
heating equipment
gap
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CN105619848A (en
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湛利华
陈效平
韦东才
黄明辉
常腾飞
李树健
李自强
丁星星
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Central South University
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C70/00Shaping composites, i.e. plastics material comprising reinforcements, fillers or preformed parts, e.g. inserts
    • B29C70/04Shaping composites, i.e. plastics material comprising reinforcements, fillers or preformed parts, e.g. inserts comprising reinforcements only, e.g. self-reinforcing plastics
    • B29C70/28Shaping operations therefor
    • B29C70/54Component parts, details or accessories; Auxiliary operations, e.g. feeding or storage of prepregs or SMC after impregnation or during ageing
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C35/00Heating, cooling or curing, e.g. crosslinking or vulcanising; Apparatus therefor
    • B29C35/02Heating or curing, e.g. crosslinking or vulcanizing during moulding, e.g. in a mould
    • B29C35/08Heating or curing, e.g. crosslinking or vulcanizing during moulding, e.g. in a mould by wave energy or particle radiation
    • B29C35/0805Heating or curing, e.g. crosslinking or vulcanizing during moulding, e.g. in a mould by wave energy or particle radiation using electromagnetic radiation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C70/00Shaping composites, i.e. plastics material comprising reinforcements, fillers or preformed parts, e.g. inserts
    • B29C70/04Shaping composites, i.e. plastics material comprising reinforcements, fillers or preformed parts, e.g. inserts comprising reinforcements only, e.g. self-reinforcing plastics
    • B29C70/28Shaping operations therefor
    • B29C70/40Shaping or impregnating by compression not applied
    • B29C70/42Shaping or impregnating by compression not applied for producing articles of definite length, i.e. discrete articles
    • B29C70/44Shaping or impregnating by compression not applied for producing articles of definite length, i.e. discrete articles using isostatic pressure, e.g. pressure difference-moulding, vacuum bag-moulding, autoclave-moulding or expanding rubber-moulding
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C35/00Heating, cooling or curing, e.g. crosslinking or vulcanising; Apparatus therefor
    • B29C35/02Heating or curing, e.g. crosslinking or vulcanizing during moulding, e.g. in a mould
    • B29C35/08Heating or curing, e.g. crosslinking or vulcanizing during moulding, e.g. in a mould by wave energy or particle radiation
    • B29C35/0805Heating or curing, e.g. crosslinking or vulcanizing during moulding, e.g. in a mould by wave energy or particle radiation using electromagnetic radiation
    • B29C2035/0855Heating or curing, e.g. crosslinking or vulcanizing during moulding, e.g. in a mould by wave energy or particle radiation using electromagnetic radiation using microwave

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  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Electromagnetism (AREA)
  • Toxicology (AREA)
  • Oral & Maxillofacial Surgery (AREA)
  • Thermal Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Composite Materials (AREA)
  • Mechanical Engineering (AREA)
  • Constitution Of High-Frequency Heating (AREA)

Abstract

The present invention provides a kind of microwave heating equipment, including microwave generator, microwave cavity and microwave shadow shield part, the microwave generator sends microwave into microwave cavity, it is used to place absorbing material in microwave cavity, the microwave shadow shield part is located in microwave cavity and is used for the outer surface for being covered in absorbing material, the microwave shadow shield part forms by shield microwaves area and through microwave region, described comprising one or more gap the microwave energy in microwave cavity to be entered in absorbing material at gap through microwave region and be absorbed.Heating can be pinpointed and/or oriented to absorbing material using microwave heating equipment provided by the invention.

Description

一种微波加热装置及方法A microwave heating device and method

技术领域technical field

本发明涉及微波领域,具体涉及一种微波加热装置及方法。The invention relates to the field of microwaves, in particular to a microwave heating device and method.

背景技术Background technique

微波具有对某些材料进行选择性加热、加热速度快、加热均匀、穿透性强、热惯性小等优点,将微波技术应用于复合材料固化领域,能显著减少固化时间,降低生产成本,获得优异的制品性能,具有巨大的发展潜力。Microwave has the advantages of selective heating of certain materials, fast heating speed, uniform heating, strong penetration, and small thermal inertia. Applying microwave technology to the field of composite material curing can significantly reduce curing time, reduce production costs, and obtain Excellent product performance, with great development potential.

国内外已在复合材料固化领域展开了大量研究,并取得了丰硕的成果。但这些研究存在一个共同的特征,复合材料均是直接暴露于微波场中完成固化。如中国专利申请CN201410295387提供一种微波-压力固化复合材料的温度均匀分布方法及成套固化装置,所述方法是在压力容器罐体中采用多边形腔体使得微波在腔体中发生多次反射,提高微波入射到复合材料的均匀性。同时在腔体的前后设置波导窗,气体介质可流动到腔体中,与复合材料发生对流换热,进一步提高材料的温度均匀性,并可实现压力容器内的气体在复合材料加热固化时施加压力。所述的装置主要包括多边形腔体和电磁屏蔽窗。本发明可提高复合材料构件的温度均匀性,降低微波固化复合材料构件的翘曲变形。A lot of research has been carried out in the field of composite material curing at home and abroad, and fruitful results have been obtained. However, these studies have a common feature, the composite materials are all directly exposed to the microwave field to complete the curing. For example, Chinese patent application CN201410295387 provides a method for uniform temperature distribution of microwave-pressure-cured composite materials and a complete set of curing device. The method is to use a polygonal cavity in the pressure vessel body so that microwaves are reflected multiple times in the cavity to improve Uniformity of microwave incidence on composite materials. At the same time, waveguide windows are set at the front and back of the cavity, the gas medium can flow into the cavity, and convective heat exchange occurs with the composite material, which further improves the temperature uniformity of the material, and can realize the gas in the pressure vessel when the composite material is heated and solidified. pressure. The device mainly includes a polygonal cavity and an electromagnetic shielding window. The invention can improve the temperature uniformity of the composite material component and reduce the warping deformation of the microwave solidified composite material component.

在对复合材料制件进行加热时,因其本身属于热的不良导体,因而若采用传统加热方式则制件的中心升温慢而周边升温快,而若采用传统的微波方式进行均匀加热则极有可能导致制件中心散热慢而过热,而即使同时使用微波方式和传统方式对复合材料进行加热,也都会使得加热固化情况不能良好的受控。因此,本领域需要针对这种情况而开发一种特别的微波加热装置及微波加热方法。When heating a composite material part, because it is a poor conductor of heat, if the traditional heating method is used, the center of the part will heat up slowly and the surrounding area will heat up quickly, but if the traditional microwave method is used for uniform heating, it will be extremely effective. It may lead to slow heat dissipation in the center of the part and overheating, and even if the composite material is heated by microwave and traditional methods at the same time, the heating and curing conditions cannot be well controlled. Therefore, there is a need in the art to develop a special microwave heating device and microwave heating method for this situation.

发明内容Contents of the invention

因此,本发明提供一种微波加热装置,包括微波发生器、微波腔、微波局部屏蔽件和测温装置,所述微波发生器向微波腔内发送微波,微波腔内用于放置吸波材料,所述微波局部屏蔽件位于微波腔内且用于覆盖在吸波材料的外表面,所述微波局部屏蔽件由屏蔽微波区和透过微波区组成,所述透过微波区包含一条或多条缝隙使得微波腔内的微波能从缝隙处进入吸波材料中而被其吸收;所述测温装置包含测温头和测温传输线,所述测温头设置在微波局部屏蔽件内侧的吸波材料中,所述测温传输线一端与测温头连接,另一端引出至所述微波腔外侧。Therefore, the present invention provides a microwave heating device, including a microwave generator, a microwave cavity, a microwave partial shield and a temperature measuring device, the microwave generator sends microwaves into the microwave cavity, and the microwave cavity is used to place microwave-absorbing materials. The microwave partial shield is located in the microwave cavity and is used to cover the outer surface of the absorbing material. The microwave partial shield is composed of a microwave shielding area and a microwave transmission area. The microwave transmission area includes one or more The gap allows the microwave energy in the microwave cavity to enter the microwave absorbing material from the gap and be absorbed by it; the temperature measuring device includes a temperature measuring head and a temperature measuring transmission line, and the temperature measuring head is arranged on the microwave absorbing material inside the microwave partial shield. In the material, one end of the temperature measurement transmission line is connected to the temperature measurement head, and the other end is led out to the outside of the microwave cavity.

本发明方案中,在对吸波材料的加热性能以及本发明所述微波加热装置(微波局部屏蔽件)的性能熟悉之前,均需要使用测温装置4来研究和探求一个合适的吸波材料的加热或固化方法。而在研发人员对上述性能均掌握清楚后,则无需再在吸波材料中设置测温头,此时通过及时调节微波功率即可实现对吸波材料的可控的定点加热和固化。本发明中,在所述吸波材料(如碳纤维与树脂的复合材料)加热固化后,因测温头无法再取出而会在产品中形成一个小的瑕疵点。因而在实验室探究出各测温点与本发明中微波加热装置的对应关系后形成经验参数;工业生产过程中,均通过所述经验参数调控微波频率即可,而不再需要在所述复合材料中设置测温头,从而避免在产品中形成小的瑕疵点。In the scheme of the present invention, before the heating performance of the microwave-absorbing material and the performance of the microwave heating device (microwave partial shield) of the present invention are familiar, it is necessary to use the temperature measuring device 4 to research and search for a suitable microwave-absorbing material. heating or curing method. After the R&D personnel have a clear understanding of the above properties, there is no need to install a temperature measuring head in the absorbing material. At this time, the controllable fixed-point heating and curing of the absorbing material can be realized by adjusting the microwave power in time. In the present invention, after the wave-absorbing material (such as a composite material of carbon fiber and resin) is heated and solidified, a small defect will be formed in the product because the temperature measuring head cannot be taken out again. Thereby in the laboratory explores each temperature measuring point and the corresponding relation of microwave heating device in the present invention and forms empirical parameter; The temperature measuring head is set in the material, so as to avoid the formation of small flaws in the product.

本发明还提供一种微波加热装置,包括微波发生器、微波腔和微波局部屏蔽件,所述微波发生器向微波腔内发送微波,微波腔内用于放置吸波材料,所述微波局部屏蔽件位于微波腔内且用于覆盖在吸波材料的外表面,所述微波局部屏蔽件由屏蔽微波区和透过微波区组成,所述透过微波区包含一条或多条缝隙使得微波腔内的微波能从缝隙处进入吸波材料中而被其吸收;所述透过微波区的面积占整个微波局部屏蔽件面积的30%或以下。The present invention also provides a microwave heating device, which includes a microwave generator, a microwave cavity and a partial microwave shielding member. The microwave generator sends microwaves into the microwave cavity, and the microwave cavity is used to place absorbing materials. The part is located in the microwave cavity and is used to cover the outer surface of the microwave-absorbing material. The microwave partial shielding part is composed of a microwave-shielding area and a microwave-transmitting area. The microwave-transmitting area contains one or more gaps so that the microwave cavity The microwave energy enters the wave-absorbing material from the gap and is absorbed by it; the area of the microwave-penetrating region accounts for 30% or less of the area of the entire microwave partial shielding member.

本发明还提供一种微波加热装置,包括微波发生器、微波腔和微波局部屏蔽件,所述微波发生器向微波腔内发送微波,微波腔内用于放置吸波材料,所述微波局部屏蔽件位于微波腔内且用于覆盖在吸波材料的外表面,所述微波局部屏蔽件由屏蔽微波区和透过微波区组成,所述透过微波区包含一条或多条缝隙使得微波腔内的微波能从缝隙处进入吸波材料中而被其吸收;所述微波腔上含有一个或多个由金属蜂窝板构成的通风窗或通风墙,用于在屏蔽微波的同时可使得微波腔内外侧气流畅通。所述通风窗是指微波腔的侧壁、底板和顶板上面积的一部分由金属蜂窝板构成。而所述通风墙是指微波腔的侧壁、底板和顶板中至少有一面全部由金属蜂窝板构成,例如微波腔的侧壁、底板和顶板整体全部由金属蜂窝板构成。The present invention also provides a microwave heating device, which includes a microwave generator, a microwave cavity and a partial microwave shielding member. The microwave generator sends microwaves into the microwave cavity, and the microwave cavity is used to place absorbing materials. The part is located in the microwave cavity and is used to cover the outer surface of the microwave-absorbing material. The microwave partial shielding part is composed of a microwave-shielding area and a microwave-transmitting area. The microwave-transmitting area contains one or more gaps so that the microwave cavity The microwave energy enters the microwave-absorbing material from the gap and is absorbed by it; the microwave cavity contains one or more ventilation windows or ventilation walls made of metal honeycomb panels, which are used to shield the microwave while making the microwave cavity Outer airflow is unobstructed. The ventilation window means that a part of the area of the side wall, the bottom plate and the top plate of the microwave cavity is made of metal honeycomb panels. The ventilation wall means that at least one side wall, bottom plate and top plate of the microwave cavity are all made of metal honeycomb panels, for example, the side walls, bottom plate and top plate of the microwave cavity are all made of metal honeycomb panels.

当微波腔内的吸波材料不仅需要定点或定向加热固化,还需要同时进行热压整体同步加热固化时,使用该装置可以实现微波定点加热与热压罐整体加热同时进行的加热或固化效果。When the microwave-absorbing material in the microwave cavity not only needs fixed-point or directional heating and curing, but also needs to be simultaneously heated and cured by hot pressing as a whole, this device can realize the simultaneous heating or curing effect of microwave fixed-point heating and overall heating of the autoclave.

因此,本发明提供一种新的微波加热装置及微波加热固化方法,使得微波可以针对复合材料制件的局部进行优先加热和固化,使得加热固化过程整体均匀可控,从而得到高性能的制件产品。Therefore, the present invention provides a new microwave heating device and a microwave heating and curing method, so that microwaves can preferentially heat and cure parts of composite material parts, so that the overall heating and curing process is uniform and controllable, thereby obtaining high-performance parts product.

本领域技术人员知晓地,微波通常呈现穿透、反射和吸收三个基本特性。对于玻璃、部分塑料和陶瓷,微波几乎是穿越而不被吸收;对于水和食物等吸波材料就会吸收微波而使其自身发热;而对金属类物质,则会反射微波。自然界中到处都有微波,但存在于自然界的微波,因为分散不集中,故不能用于加热物品。微波炉是利用其内部的磁控管,将电能转变成微波,例如以2450MHZ的振荡频率穿透食物,当微波被吸波材料吸收时,吸波材料内的极性分子(如水、脂肪、蛋白质、糖等)即被吸引以每秒24亿5千万次的速度快速振荡,这种震荡的宏观表现就是吸波材料被加热了;这就是微波加热的大致原理。Those skilled in the art know that microwaves usually exhibit three basic characteristics: penetration, reflection and absorption. For glass, some plastics and ceramics, microwaves almost pass through without being absorbed; for absorbing materials such as water and food, they will absorb microwaves and make themselves heat; and for metal substances, they will reflect microwaves. There are microwaves everywhere in nature, but the microwaves that exist in nature cannot be used to heat objects because they are scattered and not concentrated. Microwave ovens use their internal magnetrons to convert electrical energy into microwaves, such as penetrating food at an oscillation frequency of 2450MHZ. When microwaves are absorbed by microwave-absorbing materials, polar molecules (such as water, fat, protein, Sugar, etc.) are attracted to vibrate rapidly at a speed of 2.45 billion times per second. The macroscopic manifestation of this oscillation is that the absorbing material is heated; this is the general principle of microwave heating.

本发明中,所述吸波材料是指该材料中至少有一种组分能吸收一定频率的微波。本领域技术人员能理解的,本发明中,微波能从缝隙处进入吸波材料中而被吸波材料定点吸收,所述定点吸收的概念是宏观的定点概念,也就是使用本发明中提供的装置对吸波材料加热时,并不会只对某个点进行加热,而是对某个指定的区域进行加热。In the present invention, the microwave-absorbing material means that at least one component in the material can absorb microwaves of a certain frequency. Those skilled in the art can understand that in the present invention, microwave energy enters the wave-absorbing material from the gap and is absorbed by the wave-absorbing material at a fixed point. The concept of fixed-point absorption is a macroscopic fixed-point concept, that is, using the When the device heats the absorbing material, it does not only heat a certain point, but heats a designated area.

在一种具体的实施方式中,所述微波发生器的功率可调节,优选其功率线性可调,例如在100~600w间均线性可调。所述微波发生器的功率例如可以在1500w以内均可调节,在一种具体的实施方式中,所述微波发生器的功率在100~600w间为更常用的功率。In a specific implementation manner, the power of the microwave generator is adjustable, preferably its power is linearly adjustable, for example, it is linearly adjustable between 100-600W. The power of the microwave generator can be adjusted within 1500w, for example. In a specific implementation, the power of the microwave generator is more commonly used between 100-600w.

在一种具体的实施方式中,微波腔内还设置有悬空固定在微波腔的侧壁、底板或顶板上且用于放置吸波材料的透波板,所述缝隙开在所述微波局部屏蔽件的底部,且微波发生器位于微波腔内的顶部。如此设置方式使得来自于微波发生器1中的微波并不直接从缝隙处进入吸波材料中,而是经过在微波腔内的均匀分散后再从缝隙进入吸波材料中;使得本发明提供的微波定点加热方法更为稳定可控;且微波发生器置于微波腔顶部还便于操作。In a specific implementation, the microwave cavity is also provided with a wave-transmitting plate suspended and fixed on the side wall, bottom plate or top plate of the microwave cavity and used to place the absorbing material. The bottom of the component, and the microwave generator is located at the top of the microwave cavity. Such an arrangement makes the microwaves from the microwave generator 1 not directly enter the microwave-absorbing material from the gap, but enter the microwave-absorbing material from the gap after being uniformly dispersed in the microwave cavity; The microwave fixed-point heating method is more stable and controllable; and the microwave generator is placed on the top of the microwave cavity for easy operation.

在一种具体的实施方式中,微波频率为2450±50兆赫或915±25兆赫,且所述缝隙的长宽比为≥2:1,优选≥5:1,更优选≥10:1。当然,所述微波频率还可以是433兆赫或5800兆赫等用于工业加热的常用频率。优选地,所述缝隙的长度为≥20mm,优选≥40mm,更优选≥80mm,且缝隙的宽度为1~30mm。本发明中,微波频率为2450兆赫或915兆赫时,二者的波长分别为12.245cm和32.8cm。本发明中,微波能穿过比微波波长更短的所述缝隙,但微波不能透过直径小至一定程度的孔,例如孔直径在微波波长的1/4以下时,微波难以透过,或者微波透过该孔后的能量大幅衰减。本发明中,使用长宽比比值较高的缝隙透过微波时,对吸波材料的定点加热效果越好。In a specific embodiment, the microwave frequency is 2450±50 MHz or 915±25 MHz, and the aspect ratio of the slit is ≥2:1, preferably ≥5:1, more preferably ≥10:1. Of course, the microwave frequency can also be 433 MHz or 5800 MHz and other common frequencies used for industrial heating. Preferably, the length of the slit is ≥ 20 mm, preferably ≥ 40 mm, more preferably ≥ 80 mm, and the width of the slit is 1-30 mm. In the present invention, when the microwave frequency is 2450 MHz or 915 MHz, the wavelengths of the two are 12.245 cm and 32.8 cm respectively. In the present invention, the microwave can pass through the gap shorter than the microwave wavelength, but the microwave cannot pass through the hole whose diameter is small to a certain extent, for example, when the hole diameter is below 1/4 of the microwave wavelength, the microwave is difficult to pass through, or After the microwave passes through the hole, the energy is greatly attenuated. In the present invention, when the microwave is transmitted through the slit with a higher aspect ratio, the fixed-point heating effect on the microwave-absorbing material is better.

本发明中,所述缝隙为矩形、菱形、梯形、弧线形或异形,这在本发明中不受限制,优选所述缝隙为瘦长矩形、菱形或梯形。本发明中,所述缝隙的长宽比是指其长度与缝隙最窄处的比值。本发明中,所述缝隙可以单独存在,每条缝隙均被屏蔽微波区31隔开,也可以是所述缝隙以孔或缺口等其它形式连接在一起,这在本发明中均不受限制。本发明中,微波局部屏蔽件中的屏蔽微波区31可以为金属板、金属箔、金属蜂窝孔板等形式或其组合,例如为铝板、铝箔或蜂窝铝板。但优选本发明中形成屏蔽微波区的材质中包含铝箔、铜箔或锡箔,且其厚度为0.01mm以上。In the present invention, the slit is rectangular, rhombus, trapezoidal, arc-shaped or special-shaped, which is not limited in the present invention. Preferably, the slit is elongated rectangular, rhombus or trapezoidal. In the present invention, the aspect ratio of the slit refers to the ratio of its length to the narrowest part of the slit. In the present invention, the slits may exist independently, and each slit is separated by the shielded microwave region 31 , or the slits may be connected together in other forms such as holes or gaps, which are not limited in the present invention. In the present invention, the microwave shielding area 31 in the partial microwave shielding member can be in the form of metal plate, metal foil, metal honeycomb hole plate or a combination thereof, such as aluminum plate, aluminum foil or honeycomb aluminum plate. However, it is preferable that the material forming the microwave shielding region in the present invention includes aluminum foil, copper foil or tin foil, and its thickness is more than 0.01 mm.

本发明中,所述测温装置包括热电偶、热敏电阻、红外传感器、光纤荧光传感器和光纤光栅传感器中的一种或多种。若测温装置中包括金属电线,则需要对该金属电线进行微波屏蔽处理。而若采用光纤线,则无需对测温装置进行微波屏蔽。In the present invention, the temperature measuring device includes one or more of thermocouples, thermistors, infrared sensors, optical fiber fluorescence sensors and optical fiber grating sensors. If the temperature measuring device includes metal wires, microwave shielding treatment needs to be performed on the metal wires. However, if the optical fiber line is used, there is no need to shield the temperature measuring device from microwaves.

本发明中,所述微波腔接受来自微波发生器中的微波且在工作过程中将微波能全部屏蔽在微波腔中。所述微波腔包括炉门,所述炉门设置在微波腔的侧壁、底板或顶板上,这在本发明中均不受限制。In the present invention, the microwave cavity receives the microwaves from the microwave generator and completely shields the microwave energy in the microwave cavity during the working process. The microwave cavity includes an oven door, and the oven door is arranged on a side wall, a bottom plate or a top plate of the microwave cavity, which are not limited in the present invention.

在一种具体的实施方式中,有测温头设置在吸波材料中的定点吸波处,且所述测温头与微波局部屏蔽件上缝隙间的距离为≥2mm。In a specific embodiment, a temperature measuring head is arranged at a fixed-point absorbing place in the wave-absorbing material, and the distance between the temperature measuring head and the gap on the partial microwave shielding member is ≥ 2mm.

在一种具体的实施方式中,所述吸波材料为包括碳纤维与树脂的复合材料,且在所述微波局部屏蔽件的外侧还设置有用于将微波加热所述吸波材料过程中产生的气体及时抽出的真空袋,优选在所述真空袋的内侧以及微波局部屏蔽件的外侧还设置有透气毡用于抽真空时气体的导流;所述测温装置还包括显示屏,其设置在微波腔外侧用于及时显示所述测温头测得的温度。在一种具体的实施方式中,根据显示屏中即时显示的所测温度,手动控制所述微波发生器的功率,使得其对吸波材料的加热达到所需要求。In a specific embodiment, the microwave absorbing material is a composite material including carbon fiber and resin, and a gas generated during microwave heating of the microwave absorbing material is also provided on the outside of the microwave partial shield. The vacuum bag extracted in time is preferably also provided with an air felt on the inner side of the vacuum bag and the outer side of the microwave partial shield for the diversion of gas during vacuuming; the temperature measuring device also includes a display screen, which is arranged on the microwave The outside of the cavity is used to display the temperature measured by the temperature measuring head in time. In a specific embodiment, the power of the microwave generator is manually controlled according to the measured temperature instantly displayed on the display screen, so that the heating of the microwave-absorbing material can meet the required requirements.

在一种具体的实施方式中,所述透过微波区32的面积占整个微波局部屏蔽件面积的15%以下,更优选在5%以下。In a specific implementation manner, the area of the microwave-permeable region 32 accounts for less than 15% of the area of the entire partial microwave shielding member, more preferably less than 5%.

在一种具体的实施方式中,所述微波局部屏蔽件中至少部分屏蔽微波区的结构粘贴覆盖在所述吸波材料的外表面上。In a specific implementation manner, the structure of at least partially shielding the microwave region in the partial microwave shielding member is pasted and covered on the outer surface of the microwave absorbing material.

本发明还提供一种微波加热方法,包括使用上述微波加热装置对吸波材料进行定点和或定向加热。The present invention also provides a microwave heating method, including using the above-mentioned microwave heating device to conduct fixed-point and or directional heating on the microwave-absorbing material.

本发明能带来如下有益效果:本发明利用微波具有材料选择性加热、能快速均匀地加热吸波材料、并且热惯性小、易于控制的特点,通过采用对吸波材料的部分表面进行微波屏蔽处理,从而使微波只能对材料上需要加热的区域进行定向加热和固化,本发明为需要对吸波材料制件进行局部升温或者局部固化的要求提供了一种解决办法和思路。本发明缩短了复合材料类吸波材料的加热时间,并降低了能耗。The present invention can bring the following beneficial effects: the present invention utilizes the characteristics that microwaves have material selective heating, can heat absorbing materials rapidly and evenly, and have small thermal inertia and are easy to control. treatment, so that the microwave can only perform directional heating and curing on the area that needs to be heated on the material. The present invention provides a solution and idea for the requirement of local heating or local curing of microwave-absorbing material parts. The invention shortens the heating time of the composite wave-absorbing material and reduces energy consumption.

附图说明Description of drawings

图1为本发明提供的一种微波加热装置示意图,Fig. 1 is a schematic diagram of a microwave heating device provided by the present invention,

图2为本发明提供的另一种微波加热装置示意图,Figure 2 is a schematic diagram of another microwave heating device provided by the present invention,

图3为本发明提供的另一种微波加热装置示意图,Fig. 3 is a schematic diagram of another microwave heating device provided by the present invention,

图4为本发明提供的又一种微波加热装置示意图;Fig. 4 is a schematic diagram of another microwave heating device provided by the present invention;

其中,1、微波发生器,2、微波腔,3、微波局部屏蔽件,31、屏蔽微波区,32、透过微波区,4、测温装置,41、测温头,42、显示屏,43、测温传输线,5、真空袋,6、透气毡,7、透波板,8、真空管,9、快接接头,10、密封胶带,01、吸波材料。Among them, 1. Microwave generator, 2. Microwave cavity, 3. Partial microwave shielding member, 31. Shielding microwave area, 32. Through microwave area, 4. Temperature measuring device, 41. Temperature measuring head, 42. Display screen, 43. Temperature measurement transmission line, 5. Vacuum bag, 6. Breathable felt, 7. Wave-permeable plate, 8. Vacuum tube, 9. Quick connector, 10. Sealing tape, 01. Wave-absorbing material.

具体实施方式detailed description

图1提供了一种微波加热装置,包括微波发生器1、微波腔2、微波局部屏蔽件3和测温装置4,所述微波发生器向微波腔内发送微波,微波腔内用于放置吸波材料01,所述微波局部屏蔽件位于微波腔内且用于覆盖在吸波材料的外表面,所述微波局部屏蔽件由屏蔽微波区和透过微波区组成,所述透过微波区包含一条或多条缝隙使得微波腔内的微波能从缝隙处进入吸波材料中而被其吸收;所述测温装置包含测温头41和测温传输线43,所述测温头设置在微波局部屏蔽件内侧的吸波材料中,所述测温传输线一端与测温头连接,另一端引出至所述微波腔外侧。本例中,所述微波腔为未设通风窗的封闭式微波腔。Figure 1 provides a microwave heating device, including a microwave generator 1, a microwave cavity 2, a microwave partial shield 3 and a temperature measuring device 4, the microwave generator sends microwaves into the microwave cavity, and the microwave cavity is used to place absorbing Wave material 01, the microwave partial shield is located in the microwave cavity and is used to cover the outer surface of the microwave absorbing material, the microwave partial shield is composed of a microwave shielding area and a microwave transmission area, and the microwave transmission area includes One or more slits allow the microwave energy in the microwave cavity to enter the microwave-absorbing material from the slit and be absorbed by it; the temperature measuring device includes a temperature measuring head 41 and a temperature measuring transmission line 43, and the temperature measuring head is arranged on the microwave part In the microwave-absorbing material inside the shielding member, one end of the temperature measurement transmission line is connected to the temperature measurement head, and the other end is led out to the outside of the microwave cavity. In this example, the microwave cavity is a closed microwave cavity without ventilation windows.

图1和2中的所述吸波材料为碳纤维与树脂组成的复合材料制件,所述复合材料制件的制备方式例如为:先将碳纤维织成织物,再将吸波的材料树脂浸润到碳纤维织物中,形成未固化的复合材料制件,该未固化的复合材料制件可以使用透波材料(如玻璃)制成的模具盛装。所述制件包括在下的底座和在上的两个L型件,在两个L型件的底部相接处产生近似三角形的狭缝,因而使用一种预料搓成条(填充物)后填进该狭缝以最终填满该区域,使得终产品没有裂纹。这个狭缝区域无论采用传统加热方式还是使用普通的微波加热均会存在问题,传统加热方式使制件中心处的升温速度比外面部分的升温速度慢,而传统的微波方式中心散热困难,且二者都难以实现对加热进行定点控制。采用本发明提供的装置和方法对该处进行定点加热,例如微波局部屏蔽件上的缝隙长度和宽度分别为70mm和2mm,吸波材料制件的总高度为40cm,底板的厚度为5mm,测温头设置在底板上,微波局部屏蔽件上的缝隙设置在该狭缝的正下方,因而测温头与微波局部屏蔽件上的缝隙间的最小距离为2mm。当打开本发明所述微波加热装置后,来自于微波发生器1中的微波输入微波腔2,且微波能均匀分布在微波腔2中。所述吸波材料的大部分外表面均被微波局部屏蔽件3屏蔽反射,因而微波能只能从所述狭缝处进入微波局部屏蔽件内侧的吸波材料中,因为微波能量有限,因而被某处的吸波材料将微波能几乎吸收殆尽,所述定点吸波处例如为图1和2中所示的圆形区域。微波加热具有热惯性小的特点,因而对吸波材料定点或定向加热的可控性极高。本发明中,因为微波发生器产生的微波功率不高,例如控制功率在600w以下,因而并不会出现金属屏蔽件反射微波而打火的情况。常用的情况下,所述微波的功率在600w以内连续可调,例如在500w以内可调,更多的情况下,所述微波的功率为150~600w。所述测温装置中包括有设置在吸波材料中的定点吸波处的测温头,与显示屏配合使用用于及时显示该定点加热处的温度变化情况,如果加热程度超过预期,则可以实时通过调整微波功率而调整制件升温速度的快慢。The absorbing material in Figures 1 and 2 is a composite material made of carbon fiber and resin. The preparation method of the composite material is, for example, weaving carbon fiber into a fabric, and then soaking the absorbing material resin into the In the carbon fiber fabric, an uncured composite part is formed which can be contained using a mold made of a wave-transparent material such as glass. The product includes a base at the bottom and two L-shaped pieces at the top, and an approximately triangular slit is formed at the junction of the bottoms of the two L-shaped pieces, so a pre-rolled strip (filler) is used to fill into the slit to eventually fill the area so that the final product is free of cracks. There will be problems in this slit area regardless of the traditional heating method or the ordinary microwave heating method. The traditional heating method makes the heating rate of the center of the workpiece slower than that of the outer part, while the traditional microwave method has difficulty in dissipating heat from the center, and the two Both are difficult to realize fixed-point control of heating. Adopt device and method provided by the present invention to carry out fixed-point heating to this place, for example the slit length and the width on the partial microwave shielding part are respectively 70mm and 2mm, the total height of the wave-absorbing material parts is 40cm, and the thickness of the bottom plate is 5mm, measure The temperature head is set on the bottom plate, and the gap on the microwave partial shield is set directly below the slit, so the minimum distance between the temperature measuring head and the gap on the microwave partial shield is 2mm. When the microwave heating device of the present invention is turned on, microwaves from the microwave generator 1 are input into the microwave cavity 2, and the microwave energy is evenly distributed in the microwave cavity 2. Most of the outer surface of the microwave-absorbing material is shielded and reflected by the microwave partial shield 3, so microwave energy can only enter the microwave-absorbing material inside the microwave partial shield from the slit, because the microwave energy is limited, so it is absorbed The microwave energy is almost completely absorbed by the microwave-absorbing material at a certain place, and the fixed-point wave-absorbing place is, for example, the circular area shown in FIGS. 1 and 2 . Microwave heating has the characteristics of small thermal inertia, so the controllability of fixed-point or directional heating of microwave-absorbing materials is extremely high. In the present invention, because the microwave power generated by the microwave generator is not high, for example, the control power is below 600w, and thus the situation that the metal shield reflects microwaves and sparks does not occur. In common cases, the power of the microwave is continuously adjustable within 600w, for example, within 500w, and in more cases, the power of the microwave is 150-600w. The temperature measuring device includes a temperature measuring head set at a fixed-point absorbing place in the wave-absorbing material, which is used in conjunction with the display to display the temperature change of the fixed-point heating place in time. If the heating degree exceeds expectations, it can be Adjust the heating speed of the workpiece by adjusting the microwave power in real time.

图2提供了一种更为具体的微波加热装置,装置中还包括透波板7,透波板设置在微波腔2内,具体是悬空固定在微波腔的侧壁上,用于放置吸波材料;所述缝隙开在所述微波局部屏蔽件的底部,且微波发生器位于微波腔内的顶壁上;装置中还包括用于将微波加热所述吸波材料过程中产生的气体及时抽出的真空袋5,以及在所述真空袋的内侧以及微波局部屏蔽件的外侧还设置有透气毡6用于抽真空时气体的导流;所述测温装置还包括显示屏42,其设置在微波腔外侧用于及时显示所述测温头测得的温度。与真空袋5配合的部件还包括用于抽真空的真空管8和快接接头9,以及用于将真空袋粘贴在所述透波板7上的密封胶带10。Figure 2 provides a more specific microwave heating device, which also includes a wave-transmitting plate 7, the wave-transmitting plate is arranged in the microwave cavity 2, specifically suspended and fixed on the side wall of the microwave cavity, for placing the microwave absorbing material; the slit is opened at the bottom of the microwave partial shield, and the microwave generator is located on the top wall of the microwave cavity; the device also includes a device for extracting the gas generated during the microwave heating of the absorbing material in time The vacuum bag 5, and the inside of the vacuum bag and the outside of the partial microwave shield are also provided with an air felt 6 for guiding the gas when vacuuming; the temperature measuring device also includes a display screen 42, which is arranged on The outside of the microwave cavity is used to display the temperature measured by the temperature measuring head in time. The components that cooperate with the vacuum bag 5 also include a vacuum tube 8 and a quick connector 9 for vacuuming, and a sealing tape 10 for pasting the vacuum bag on the wave-transmitting plate 7 .

图3中还提供了另一种微波加热装置,装置中的透过微波区32包括三条缝隙,这三条缝隙分布在吸波材料的上侧和下侧,三条缝隙间以屏蔽微波区31隔开或三条缝隙相连皆可。实现发现,这种方案与图1中所示的一条缝隙的方案一样,均能对吸波材料起到定点或定向加热效果。此外,图3中的微波腔的四周侧壁上均开有通风窗,蜂窝孔金属板通风窗在确保将微波屏蔽在微波腔内的同时使得微波腔内可以与外部进行良好通风。Another microwave heating device is provided in Fig. 3. The microwave-transmitting area 32 in the device includes three slits, which are distributed on the upper and lower sides of the absorbing material, and the three slits are separated by a microwave-shielding area 31. Or three slits can be connected. It has been found that this solution is the same as the one slit solution shown in Fig. 1, and both can exert a fixed-point or directional heating effect on the wave-absorbing material. In addition, there are ventilation windows on the surrounding side walls of the microwave cavity in Fig. 3, and the ventilation windows of the honeycomb metal plate ensure that the microwave is shielded in the microwave cavity and at the same time, the microwave cavity can be well ventilated with the outside.

图4中提供了又一种微波加热装置,该装置中不涉及测温装置,因而适合用于在工艺参数研究清楚后对吸波材料进行工业化大规模的加工(包括加热和固化)。Another microwave heating device is provided in Fig. 4, which does not involve a temperature measuring device, so it is suitable for industrial large-scale processing (including heating and curing) of microwave absorbing materials after the process parameters are clearly studied.

在图1~4的方案中,圆形虚线区域为微波定向加热固化区域,而除圆形虚线区域以外的吸波材料上的其它区域均为该步骤中不需要加热或固化的区域,在对定点加热区域进行加热时,其它区域的温度无明显上升或者其温度升高缓慢。In the schemes of Figures 1 to 4, the circular dotted line area is the microwave directional heating and curing area, and other areas on the absorbing material except the circular dotted line area are all areas that do not need to be heated or cured in this step. When the fixed-point heating area is heated, the temperature of other areas does not rise significantly or its temperature rises slowly.

本发明中,所述微波局部屏蔽件的屏蔽微波区是指其至少可以反射一些频率的微波,所述吸波材料是指其至少可以吸收一些频率的微波,而所述透波板是指其至少可以透过一些频率的微波。In the present invention, the shielded microwave region of the microwave partial shield means that it can at least reflect microwaves of some frequencies, and the microwave-absorbing material means that it can absorb microwaves of At least some frequencies of microwaves are permeable.

如图1~4所示,本发明提供一种利用微波加热吸波材料,使吸波材料制件局部温度升高或者固化的装置和方法。该方法为将吸波材料制件中不需要加热或者固化的区域先用微波屏蔽材料进行覆盖,对吸波材料制件需要加热或者固化的区域则不覆盖微波屏蔽材料(留一条或多条缝隙),使得所述微波局部屏蔽件3由屏蔽微波区31和透过微波区32组成。然后,把粘贴好微波屏蔽材料的吸波材料制件置于微波腔中。微波发生器产生微波进入并均匀分散在微波腔中,对吸波材料制件没有贴微波屏蔽材料的区域(透过微波区32)内部进行加热或者固化。吸波材料制件上贴了微波屏蔽材料的区域(屏蔽微波区31)由于微波不能进入其中,所以这些区域吸收不到微波能量,其可以基本保持原来的温度基本不变。因此,使用本发明提供的装置和方法可以对吸波材料制件上需要加热的某些特定区域进行有针对性的加热或固化。As shown in Figures 1 to 4, the present invention provides a device and method for heating a wave-absorbing material with microwaves to raise or solidify the local temperature of a wave-absorbing material. The method is to cover the area of the microwave-absorbing material part that does not need to be heated or cured with microwave shielding material first, and the area of the wave-absorbing material part that needs to be heated or cured is not covered with the microwave shielding material (leaving one or more gaps). ), so that the microwave partial shield 3 is composed of a microwave-shielding region 31 and a microwave-transmitting region 32. Then, the microwave-absorbing material product pasted with the microwave shielding material is placed in the microwave cavity. The microwave generator generates microwaves to enter and evenly disperse in the microwave cavity, and heat or solidify the area of the microwave-absorbing material product without the microwave shielding material (through the microwave area 32 ). The area (shielded microwave area 31 ) pasted with microwave shielding material on the absorbing material product cannot absorb microwave energy because microwaves cannot enter it, and it can basically keep the original temperature substantially unchanged. Therefore, the device and method provided by the present invention can be used to carry out targeted heating or curing on some specific areas on the absorbing material that need to be heated.

本发明通过对吸波材料制件的外面覆盖微波屏蔽材料,然后留下需要加热或固化的区域不覆盖微波屏蔽材料。当微波源开启后,微波腔中充满微波能场,微波从图1~3中的微波定点照射区域进入吸波材料制件中,对吸波材料制件需要加热的区域进行升温或者固化。同时,操作员可以通过放置在该吸波材料制件中微波定点照射区域的测温头41、测温传输线43和显示屏42实时知晓吸波材料制件中微波定点照射区域的温度,并通过手动调整微波发生器的输入功率来调整吸波材料制件的被微波照射区域的温度;防止温度过高或者过低的情况发生。In the present invention, the microwave shielding material is covered on the outer surface of the wave-absorbing material, and then the area to be heated or solidified is not covered with the microwave shielding material. When the microwave source is turned on, the microwave cavity is filled with a microwave energy field, and the microwave enters the microwave-absorbing material part from the microwave fixed-point irradiation area in Figures 1 to 3, and heats up or solidifies the area of the microwave-absorbing material part that needs to be heated. At the same time, the operator can know the temperature of the microwave fixed-point irradiation area in the microwave-absorbing material part in real time through the temperature measuring head 41, the temperature measurement transmission line 43 and the display screen 42 placed in the microwave-absorbing material part. Manually adjust the input power of the microwave generator to adjust the temperature of the microwave-irradiated area of the absorbing material; prevent the temperature from being too high or too low.

以上所述仅为本发明的优选实施例而已,并不用于限制本发明,对于本领域的技术人员来说,本发明可以有各种更改和变化。凡在本发明的精神和原则之内,所作的任何修改、等同替换、改进等,均应包含在本发明的保护范围之内。The above descriptions are only preferred embodiments of the present invention, and are not intended to limit the present invention. For those skilled in the art, the present invention may have various modifications and changes. Any modifications, equivalent replacements, improvements, etc. made within the spirit and principles of the present invention shall be included within the protection scope of the present invention.

Claims (17)

1. a kind of microwave heating equipment, including microwave generator (1), microwave cavity (2), microwave shadow shield part (3) and thermometric dress Put (4), the microwave generator sends microwave into microwave cavity, is used to place absorbing material (01), the microwave in microwave cavity Shadow shield part is located in microwave cavity and is used for the outer surface for being covered in absorbing material, and the microwave shadow shield part (3) is by shielding Cover microwave region (31) and formed through microwave region (32), it is described to cause microwave comprising one or more gap through microwave region (32) The microwave energy of intracavitary enters in absorbing material and is absorbed at gap;The temperature measuring equipment includes temperature measuring head (41) and thermometric Transmission line (43), the temperature measuring head are arranged in the absorbing material on the inside of microwave shadow shield part, described thermometric transmission line one end It is connected with temperature measuring head, the other end is led on the outside of the microwave cavity.
2. a kind of microwave heating equipment, including microwave generator (1), microwave cavity (2) and microwave shadow shield part (3), described micro- Wave producer sends microwave into microwave cavity, is used to place absorbing material (01), the microwave shadow shield part position in microwave cavity In in microwave cavity and for being covered in the outer surface of absorbing material, the microwave shadow shield part (3) is by shield microwaves area (31) Formed with through microwave region (32), the microwave energy caused through microwave region (32) comprising one or more gap in microwave cavity Enter at gap in absorbing material and be absorbed;The area through microwave region (32) accounts for whole microwave shadow shield part 30% or less of area.
3. a kind of microwave heating equipment, including microwave generator (1), microwave cavity (2) and microwave shadow shield part (3), described micro- Wave producer sends microwave into microwave cavity, is used to place absorbing material (01), the microwave shadow shield part position in microwave cavity In in microwave cavity and for being covered in the outer surface of absorbing material, the microwave shadow shield part (3) is by shield microwaves area (31) Formed with through microwave region (32), the microwave energy caused through microwave region (32) comprising one or more gap in microwave cavity Enter at gap in absorbing material and be absorbed;It is made up of on the microwave cavity containing one or more metal honeycomb plate Vent window or ventilation wall, for may be such that sidewind is unimpeded inside and outside microwave cavity while shield microwaves.
4. the microwave heating equipment according to any one in claims 1 to 3, it is characterised in that the microwave generator Power adjustable section.
5. microwave heating equipment according to claim 4, it is characterised in that the power linear of the microwave generator can Adjust.
6. the microwave heating equipment according to any one in claims 1 to 3, it is characterised in that also set up in microwave cavity There is the wave transparent plate (7) being suspended vacantly in the side wall, bottom plate or top plate of microwave cavity and for placing absorbing material, the gap is opened In the bottom of the microwave shadow shield part, and microwave generator is located at the top of microwave cavity.
7. the microwave heating equipment according to any one in claims 1 to 3, it is characterised in that microwave frequency 2450 ± 50 megahertzs or 915 ± 25 megahertzs, and the length-width ratio in the gap is >=2:1.
8. microwave heating equipment according to claim 7, it is characterised in that the length-width ratio in the gap is >=5:1.
9. microwave heating equipment according to claim 8, it is characterised in that the length-width ratio in the gap is >=10:1.
10. microwave heating equipment according to claim 7, it is characterised in that the length in the gap is >=20mm, and is stitched The width of gap is 1~30mm.
11. microwave heating equipment according to claim 10, it is characterised in that the length in the gap is >=40mm.
12. microwave heating equipment according to claim 11, it is characterised in that the length in the gap is >=80mm.
13. microwave heating equipment according to claim 1, it is characterised in that the absorbing material be include carbon fiber with The composite of resin, and be additionally provided with the outside of the microwave shadow shield part for microwave to be heated into the absorbing material During the vacuum bag (5) extracted out in time of caused gas;The temperature measuring equipment also includes display screen (42), and it is arranged on microwave It is used to show the temperature that the temperature measuring head measures in time on the outside of chamber.
14. microwave heating equipment according to claim 13, it is characterised in that in the inner side of the vacuum bag and microwave The water conservancy diversion that airfelt (6) is used for gas when vacuumizing is additionally provided with the outside of shadow shield part, in the microwave shadow shield part The structure at least part shield microwaves area, which is pasted, to be covered on the outer surface of the absorbing material.
15. the microwave heating equipment according to any one in claims 1 to 3, it is characterised in that described to pass through microwave region (32) area accounts for less than the 15% of whole microwave shadow shield part area.
16. microwave heating equipment according to claim 15, it is characterised in that the area through microwave region (32) accounts for Less than the 5% of whole microwave shadow shield part area.
17. a kind of microwave heating method, including the use of as described in any one in claim 1~16 microwave heating equipment to inhaling Wave material is pinpointed and/or oriented heating.
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