CN105581926B - Women privates conditioning liquid and preparation method thereof - Google Patents

Abstract

The invention relates to a women's private parts care solution and a preparation method thereof, comprising the following raw materials in proportion by weight: 1-4 parts of lavender essential oil; 1-4 parts of rose essential oil; 1-3 parts of fir essential oil; 89-97 parts of base liquid . The preparation method is as follows: (1) mixing the lavender essential oil, rose essential oil and fir essential oil in the above parts by weight and stirring evenly to obtain the essential oil mixture; (2) pouring the essential oil mixture obtained in step (1) into the base containing the above parts by weight Stir in the liquid container, fully dilute and fuse, and obtain the female private parts care liquid. The beneficial effects of the present invention are: moisturizing and cleaning women's private parts, improving the color of female private parts, having cleaning and whitening effects, long-term use, delaying the aging of private parts skin and increasing the elasticity of private parts skin, safe and non-irritating, without allergic reactions, and without toxic and side effects , can be applied to women of all ages, restore women's youth, and enhance married life.

Description

Nursing solution for female private parts and preparation method thereof

technical field

The invention belongs to the field of health care and medicine and health care products, and in particular relates to a female private parts care solution and a preparation method thereof.

Background technique

At present, there are many kinds of lotions for women's private parts on the market. Most of them use organic matter or traditional Chinese medicine formulas as bactericidal and antibacterial agents.

Some women are prone to negative phenomena such as darkening of the skin of the private parts, aging and lack of elasticity of the skin of the private parts due to factors such as sexual intercourse, childbirth or endocrine disorders. These conditions are not only detrimental to health, but may also lead to a decline in the quality of sexual life, and even affect family harmony.

Contents of the invention

In order to solve the above-mentioned problems in the prior art, the present invention provides a women's private parts care solution that has the function of a common lotion and can also whiten private parts skin, delay private parts skin aging, and increase private parts skin elasticity and its preparation method.

The technical scheme adopted in the present invention is:

A care solution for women's private parts, comprising the following raw materials in proportions by weight:

1-4 parts of lavender essential oil; 1-4 parts of rose essential oil; 1-3 parts of fir essential oil; 89-97 parts of base liquid.

Further: a women's private parts care solution, comprising the following raw materials in proportions by weight:

2 parts of lavender essential oil; 2 parts of rose essential oil; 2 parts of fir essential oil; 94 parts of base liquid.

Preferably: the base liquid is food-grade olive oil.

Preferably: the preparation method of above-mentioned lavender essential oil, comprises the following steps:

(1) Add fresh lavender inflorescences to soak in sodium chloride solution for 2-3 hours to obtain pretreatment raw materials;

(2) Place the pretreated raw material in a distillation device for atmospheric distillation at 100-105°C, and condense after atmospheric distillation to obtain a condensate;

(3) carrying out multiple leaching by the condensate through an adsorption column equipped with ethanol solution and activated carbon to obtain an extract;

(4) carry out decompression distillation to described extract solution, obtain lavender essential oil.

The preparation method of fir essential oil comprises the following steps:

(I) adding fresh fir leaves to water for soaking for 2-3 hours to obtain pretreated raw materials;

(II) Place the pretreated raw material in a distillation device for atmospheric distillation at 100-105°C, and condense after atmospheric distillation to obtain a condensate;

(Ⅲ) carrying out multiple leaching of the condensate through an adsorption column equipped with ethanol solution and activated carbon to obtain an extract;

(IV) Distilling the extract under reduced pressure to obtain fir essential oil.

Further: the concentration of the sodium chloride solution described in step (1) is 20%-25%.

Further: the pressure of vacuum distillation described in step (4) and step (IV) is 0.1-1.0kPa.

Preferably: the preparation method of above-mentioned rose essential oil, comprises the following steps:

(1) After crushing 400-600 parts by weight of fresh rose petals, add 2000-3000 parts by weight of distilled water, and then add 0.4-0.6 parts by weight of acid cellulase for the first enzymolysis, and the first enzymolysis is completed Finally, add 1-3 parts by weight of pectinase and 0.5-2 parts by weight of composite protease to carry out the second hydrolysis to obtain the initial product of enzymolysis;

(2) Put the initial product of enzymolysis in a fermenter for fermentation reaction, obtain a fermentation product after the reaction is completed, and heat the fermentation product to 80°C for use;

(3) The heated fermentation product is filtered in a constant flow in a plate frame, concentrated in a 25L rotary evaporator under a pressure of 0.1Mpa after filtration, concentrated 1000 times, and then added with 0.22-0.32 parts by weight of alcohol to obtain rose essential oil.

Further: the time of the first enzymatic hydrolysis and the second enzymatic hydrolysis described in step (1) is 1 hour, wherein the pH value is adjusted to 3.8-4.5 with citric acid before the first enzymatic hydrolysis.

Further: the time for the fermentation reaction in step (2) is 24 hours, the pH value is 6.0 when the fermentation is adjusted with citric acid, and the fermentation temperature is 26-30°C.

A method for preparing the above-mentioned women's private parts care solution, comprising the following steps:

(1) Stir evenly after mixing the lavender essential oil, rose essential oil and fir essential oil of the above weight parts, to obtain the essential oil mixture;

(2) Pour the essential oil mixture obtained in step (1) into a container containing the above-mentioned base liquid by weight, stir, fully dilute and fuse, and obtain the private parts care liquid for women.

Lavender essential oil is extracted from lavender. It can clear away heat and detoxify, clean the skin, control oil content, remove freckles, whiten skin, remove wrinkles and rejuvenate skin, remove eye bags and dark circles, and promote skin care functions such as regeneration and recovery of damaged tissues. It can purify and soothe the mind, relieve anger and exhaustion, and enable people to face life with peace of mind.

Rose essential oil can stimulate and coordinate the human immune and nervous system, and at the same time help to improve the secretion of endocrine glands, remove organ sclerosis, repair cells, adjust female endocrine, nourish the uterus, relieve dysmenorrhea, improve frigidity and menopausal discomfort. In particular, it has a very good beauty and skin care effect. It can lighten spots from the inside and outside, promote the decomposition of melanin, improve skin dryness, restore skin elasticity, and let women have white, elastic and healthy skin. It is an aromatic essential oil suitable for women's health care.

Fir, scientific name (Abies fabri(Mast.) Craib), fir essential oil is extracted from fir leaves, has moisturizing, moisturizing, antibacterial and anti-inflammatory properties, shrinks pores, detoxifies and nourishes skin, removes wrinkles and lines, relaxes and activates collaterals, improves insomnia, promotes metabolism, anti-wrinkle and anti-aging Effects of aging.

Olive oil is directly cold-pressed from fresh olives, without heating and chemical treatment, and retains natural nutrients. Edible high-grade olive oil is a natural fruit juice extracted from first-ripe or mature olive fresh fruit through physical cold pressing process. Olive oil is rich in monounsaturated fatty acid-oleic acid, as well as vitamin A, vitamin B, Vitamin D, vitamin E, vitamin K and antioxidants, etc. Women often consume olive oil, which can enhance skin elasticity and receive the effect of moisturizing and beautifying the skin.

The beneficial effects of the present invention are as follows: the present invention utilizes a variety of plant essential oils for scientific cooperation to synergistically exert the effects of plant essential oils. The specific mechanism of action is as follows: 1. Lavender essential oil can be matched with a variety of pure plant essential oil active factors to complement each other and quickly penetrate hair follicles for disinfection and antibacterial , promote cell regeneration, restore skin connective tissue, balance skin surface oil secretion, soothe sensitive skin, restore skin self-repair function, and strengthen skin's resistance to the outside world; 2. Pure lavender essential oil can be used as a versatile oil, or a variety of essential oils for deployment, after deployment, its efficacy will increase exponentially, but the ratio of essential oils is very important, requiring very high technical parameters. In the present invention, lavender essential oil, rose essential oil and fir essential oil are combined The scientifically perfect golden ratio is blended into the compound essential oil, which abandons the disadvantages of unilateral essential oils, and the multiple functions cooperate with each other, which greatly improves the effect of deep repair; 3. The present invention adds three kinds of essential oils to the scientific blending effect to cleanse and moisturize the skin The excellent olive oil base oil can quickly penetrate into the skin to absorb, moisturize and clean women's private parts, improve the color of women's private parts, and has the effect of cleaning and whitening. Long-term use can delay the aging of private parts skin and increase the elasticity of private parts skin, safe and non-toxic Stimulation, no allergic reaction, no toxic side effects, can be used by women of all ages, restore women's youth, and improve married life.

Detailed ways

Provide 3 specific examples below, the present invention is further explained and illustrated, it should be pointed out that: the present invention is not limited to following best implementation mode, any skilled in the art can draw other under the inspiration of the present invention Products in various forms, but no matter any changes are made in their shapes or structures, any technical solutions that are the same as or similar to the present application all fall within the protection scope of the present invention.

In the following examples, 1 part by weight refers to 1 g.

Example 1

A women's private parts care solution, comprising the following raw materials in parts by weight:

1 part of lavender essential oil; 1 part of rose essential oil; 1 part of fir essential oil; 89 parts of food grade olive oil.

Wherein the preparation method of lavender essential oil comprises the following steps:

(1) adding fresh lavender inflorescences to a concentration of 20% sodium chloride solution and soaking for 2 hours to obtain pretreatment raw materials;

(2) Place the pretreated raw material in a distillation device to carry out atmospheric distillation at 100° C., and condense after atmospheric distillation to obtain a condensate;

(3) carrying out multiple leaching by the condensate through an adsorption column equipped with ethanol solution and activated carbon to obtain an extract;

(4) carrying out vacuum distillation under pressure of 0.1kPa to obtain lavender essential oil by said extract solution.

The preparation method of rose essential oil comprises the following steps:

(1) 400 parts by weight of fresh rose petals are pulverized, 2000 parts by weight of distilled water are added, after the pH of the distilled water is adjusted to 3.8 with citric acid, 0.5 parts by weight of acid cellulase is added to carry out enzymolysis for the first time. The time of the first enzymolysis is 1 hour, and then the second enzymolysis is carried out with 1 weight part of pectinase and 0.5 weight part of the compound protease, the second time of enzymolysis is 1 hour, and the initial product of enzymolysis is obtained;

(2) Put the initial product of enzymolysis in a fermenter for 24 hours to ferment to obtain a fermented product. Before fermentation, use citric acid to adjust the pH value of the fermentation to 6.0, and the fermentation temperature is 26°C. After the fermentation is completed, the fermented product is heated to 80°C. stand-by;

(3) The fermentation product is filtered at a constant flow in a plate frame, and then concentrated in a 25L rotary evaporator under a pressure of 0.1Mpa. After concentration of 1000 times, 0.22 parts by weight of alcohol is added to obtain rose essential oil.

The preparation method of fir essential oil comprises the following steps:

(1) Add fresh fir leaves to water and soak for 2 hours to obtain pretreated raw materials;

(2) Place the pretreated raw material in a distillation device to carry out atmospheric distillation at 100° C., and condense after atmospheric distillation to obtain a condensate;

(3) carrying out multiple leaching by the condensate through an adsorption column equipped with ethanol solution and activated carbon to obtain an extract;

(4) carry out vacuum distillation under the pressure of 0.1kPa to obtain fir essential oil.

The method for preparing the above-mentioned women's private parts care solution includes the following preparation steps:

(1) Stir evenly after the obtained lavender essential oil, rose essential oil and fir essential oil are mixed according to the above-mentioned proportioning by weight, to obtain the essential oil mixture;

(2) Pour the essential oil mixture obtained in the step (1) into a container containing the above-mentioned food-grade olive oil in parts by weight, stir, fully dilute and fuse, and serve as a women's private parts care solution.

Example 2

A women's private parts care solution, comprising the following raw materials in parts by weight:

2 parts of lavender essential oil; 2 parts of rose essential oil; 2 parts of fir essential oil; 93 parts of food grade olive oil.

Wherein the preparation method of lavender essential oil comprises the following steps:

(1) adding fresh lavender inflorescences to a concentration of 23% sodium chloride solution and soaking for 2.5 hours to obtain pretreated raw materials;

(2) Place the pretreated raw material in a distillation device for atmospheric distillation at 103° C., and condense after atmospheric distillation to obtain a condensate;

(3) carrying out multiple leaching by the condensate through an adsorption column equipped with ethanol solution and activated carbon to obtain an extract;

(4) carrying out vacuum distillation under pressure of 0.5kPa with described extract solution, obtains lavender essential oil.

The preparation method of rose essential oil comprises the following steps:

(1) 500 parts by weight of fresh rose petals are pulverized, 2500 parts by weight of distilled water are added, after the pH of the distilled water is adjusted to 4.1 with citric acid, 0.5 parts by weight of acid cellulase is added to carry out the first enzymolysis, the first The time for the first enzymolysis is 1 hour, and the second enzymolysis is carried out with 2 parts by weight of pectinase and 1.2 parts by weight of compound protease, and the time for the second enzymolysis is 1 hour to obtain the initial product of the enzymolysis;

(2) Put the initial product of enzymolysis in a fermenter for 24 hours to ferment to obtain a fermented product. Before fermentation, use citric acid to adjust the pH value of the fermentation to 6.0, and the fermentation temperature is 28°C. After the fermentation is completed, the fermented product is heated to 80°C. stand-by;

(3) The fermentation product is filtered with a ceramic membrane, concentrated in a 25L rotary evaporator under a pressure of 0.1Mpa, concentrated 1000 times, and then added with 0.27 parts by weight of alcohol to obtain rose essential oil.

The preparation method of fir essential oil comprises the following steps:

(1) Add fresh fir leaves to water and soak for 2.5 hours to obtain pretreated raw materials;

(2) Place the pretreated raw material in a distillation device for atmospheric distillation at 103° C., and condense after atmospheric distillation to obtain a condensate;

(3) carrying out multiple leaching by the condensate through an adsorption column equipped with ethanol solution and activated carbon to obtain an extract;

(4) carry out vacuum distillation under the pressure of 0.5kPa with described extract solution, obtain fir essential oil.

The method for preparing the above-mentioned women's private parts care solution includes the following preparation steps:

(1) Stir evenly after the obtained lavender essential oil, rose essential oil and fir essential oil are mixed according to the above-mentioned proportioning by weight, to obtain the essential oil mixture;

(2) Pour the essential oil mixture obtained in the step (1) into a container containing the above-mentioned food-grade olive oil in parts by weight, stir, fully dilute and fuse, and serve as a women's private parts care solution.

Example 3

A women's private parts care solution, comprising the following raw materials in parts by weight:

4 parts of lavender essential oil; 4 parts of rose essential oil; 3 parts of fir essential oil; 97 parts of food grade olive oil.

Wherein the preparation method of lavender essential oil comprises the following steps:

(1) adding fresh lavender inflorescences to a concentration of 25% sodium chloride solution and soaking for 3 hours to obtain pretreatment raw materials;

(2) Place the pretreated raw material in a distillation device to carry out atmospheric distillation at 105° C., and condense after atmospheric distillation to obtain a condensate;

(3) carrying out multiple leaching by the condensate through an adsorption column equipped with ethanol solution and activated carbon to obtain an extract;

(4) carrying out vacuum distillation under pressure of 1.0kPa with described extract solution, obtains lavender essential oil.

The preparation method of rose essential oil comprises the following steps:

(1) 600 parts by weight of fresh rose petals are pulverized, 3000 parts by weight of distilled water are added, after the pH of the distilled water is adjusted to 4.5 with citric acid, 0.5 parts by weight of acid cellulase is added to carry out enzymolysis for the first time, the first time The time of the first enzymolysis is 1 hour, and then the second enzymolysis is carried out with 3 parts by weight of pectinase and 2 parts by weight of compound protease, and the time of the second enzymolysis is 1 hour to obtain the initial product of the enzymolysis;

(2) Put the initial product of enzymolysis in a fermenter for 24 hours to ferment to obtain a fermented product. Before fermentation, adjust the pH value of the fermentation to 6.0 with citric acid, and the fermentation temperature is 30°C. After the fermentation is completed, the fermented product is heated to 80°C. stand-by;

(3) The fermentation product is filtered at a constant flow in a plate frame, and then concentrated in a 25L rotary evaporator under a pressure of 0.1Mpa. After concentration of 1000 times, 0.32 parts by weight of alcohol is added to obtain rose essential oil.

The preparation method of fir essential oil comprises the following steps:

(1) Add fresh fir leaves to water and soak for 3 hours to obtain pretreated raw materials;

(2) Place the pretreated raw material in a distillation device to carry out atmospheric distillation at 105° C., and condense after atmospheric distillation to obtain a condensate;

(3) carrying out multiple leaching by the condensate through an adsorption column equipped with ethanol solution and activated carbon to obtain an extract;

(4) carry out vacuum distillation under the pressure of 1.0kPa to obtain fir essential oil by the extract.

The method for preparing the above-mentioned women's private parts care solution includes the following preparation steps:

(1) Stir evenly after the obtained lavender essential oil, rose essential oil and fir essential oil are mixed according to the above-mentioned proportioning by weight, to obtain the essential oil mixture;

(2) Pour the essential oil mixture obtained in the step (1) into a container containing the above-mentioned food-grade olive oil in parts by weight, stir, fully dilute and fuse, and serve as a women's private parts care solution.

Anti-inflammatory and bactericidal effects:

Operate according to the national standard GB15797-2002:

Adding Staphylococcus aureus to the women's private parts care solution made in Example 1 and the bacteriostatic rate reached 65% after 2min; adding Candida albicans to the female care solution made in Example 1 and the bacteriostatic rate reached after 2min 70%;

Adding Staphylococcus aureus to the women's private parts care solution made in Example 2 reached 67% after 2min; In the women's care solution made in Example 2, adding Candida albicans strain reached 2min after 2min. 78%.

Adding Staphylococcus aureus to the women's private parts care solution made in Example 3 reached 68% after 2min; Added Candida albicans to the women's care solution made in Example 3 and the bacteriostasis rate reached 2min after 2min 80%.

How to use: When using this female private parts care solution, dilute it with warm water and wash it, take 10-15ml each time, usually use it every night before going to bed for care.

Claims (9)

1. A women's private parts care solution is characterized in that it is made up of the following raw materials in parts by weight: 1-4 parts of lavender essential oil; 1-4 parts of rose essential oil; 1-3 parts of fir essential oil; 89-97 parts of base liquid . 2. The care liquid for women's private parts according to claim 1, characterized in that it is made up of the following raw materials in parts by weight: 2 parts of lavender essential oil; 2 parts of rose essential oil; 2 parts of fir essential oil; 94 parts of base liquid. 3. women's private parts care solution according to claim 1, characterized in that, said base liquid is food-grade olive oil. 4. female private parts care solution according to claim 1, is characterized in that, described lavender essential oil preparation method, comprises the following steps: (1) Add fresh lavender inflorescences to soak in sodium chloride solution for 2-3 hours to obtain pretreatment raw materials; (2) Place the pretreated raw material in a distillation device for atmospheric distillation at 100-105°C, and condense after atmospheric distillation to obtain a condensate; (3) carrying out multiple leaching by the condensate through an adsorption column equipped with ethanol solution and activated carbon to obtain an extract; (4) carry out decompression distillation to described extract solution, obtain lavender essential oil; The preparation method of described fir essential oil comprises the following preparation steps: (I) adding fresh fir leaves to water for soaking for 2-3 hours to obtain pretreated raw materials; (II) Place the pretreated raw material in a distillation device for atmospheric distillation at 100-105° C., and condense to obtain a condensate after atmospheric distillation; (Ⅲ) carrying out multiple leaching of the condensate through an adsorption column equipped with ethanol solution and activated carbon to obtain an extract; (IV) Distilling the extract under reduced pressure to obtain fir essential oil. 5. The care solution for women's private parts according to claim 4, characterized in that the concentration of the sodium chloride solution in step (1) is 20%-25%. 6. The women's private parts care solution according to claim 4, characterized in that, the pressure of the vacuum distillation described in step (4) and step (IV) is 0.1-1.0kPa. 7. women's private parts care solution according to claim 1, is characterized in that, the preparation method of described rose essential oil, comprises the following steps: (1) After crushing 400-600 parts by weight of fresh rose petals, add 2000-3000 parts by weight of distilled water, and then add 0.4-0.6 parts by weight of acid cellulase for the first enzymolysis, and the first enzymolysis is completed Finally, add 1-3 parts by weight of pectinase and 0.5-2 parts by weight of composite protease to carry out the second hydrolysis to obtain the initial product of enzymolysis; (2) Put the initial product of enzymolysis in a fermenter for fermentation reaction, obtain a fermentation product after the reaction is completed, and heat the fermentation product to 80°C for use; (3) The heated fermentation product is filtered in a constant flow in a plate frame, concentrated in a 25L rotary evaporator under a pressure of 0.1Mpa after filtration, concentrated 1000 times, and then added with 0.22-0.32 parts by weight of alcohol to obtain rose essential oil. 8. The women's private parts care solution according to claim 7, characterized in that, the first enzymolysis and the second enzymolysis time described in step (1) are 1h, wherein before the first enzymolysis Use citric acid to adjust the pH value to 3.8-4.5; the fermentation reaction time in step (2) is 24 hours, use citric acid to adjust the pH value during fermentation to 6.0, and the fermentation temperature is 26-30°C. 9. A method for preparing the women's private parts care solution as described in any one of claims 1-8, is characterized in that, comprises the following steps: (1) Stir evenly after mixing the lavender essential oil, rose essential oil and fir essential oil of the above weight parts, to obtain the essential oil mixture; (2) Pour the essential oil mixture obtained in step (1) into a container containing the above-mentioned base liquid by weight, stir, fully dilute and fuse, and obtain the private parts care liquid for women.