CN105568302A - Aluminum material surface treatment process - Google Patents
Aluminum material surface treatment process Download PDFInfo
- Publication number
- CN105568302A CN105568302A CN201511013079.2A CN201511013079A CN105568302A CN 105568302 A CN105568302 A CN 105568302A CN 201511013079 A CN201511013079 A CN 201511013079A CN 105568302 A CN105568302 A CN 105568302A
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- CN
- China
- Prior art keywords
- parts
- aluminum material
- water
- minutes
- aluminium
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 title claims abstract description 37
- 229910052782 aluminium Inorganic materials 0.000 title claims abstract description 37
- 239000000463 material Substances 0.000 title claims abstract description 20
- 238000004381 surface treatment Methods 0.000 title claims abstract description 14
- 238000000034 method Methods 0.000 title claims abstract description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 29
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 20
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 12
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims abstract description 8
- SHZGCJCMOBCMKK-UHFFFAOYSA-N D-mannomethylose Natural products CC1OC(O)C(O)C(O)C1O SHZGCJCMOBCMKK-UHFFFAOYSA-N 0.000 claims abstract description 8
- 150000008265 rhamnosides Chemical class 0.000 claims abstract description 8
- 238000002360 preparation method Methods 0.000 claims abstract description 6
- 239000004411 aluminium Substances 0.000 claims description 24
- 238000003756 stirring Methods 0.000 claims description 24
- 230000002000 scavenging effect Effects 0.000 claims description 15
- 238000005516 engineering process Methods 0.000 claims description 7
- 239000002253 acid Substances 0.000 claims description 6
- 239000000428 dust Substances 0.000 claims description 6
- 238000005530 etching Methods 0.000 claims description 3
- 238000005260 corrosion Methods 0.000 abstract description 4
- 230000007797 corrosion Effects 0.000 abstract description 4
- 238000004140 cleaning Methods 0.000 abstract 6
- 239000007788 liquid Substances 0.000 abstract 4
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 abstract 3
- 238000007598 dipping method Methods 0.000 abstract 2
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 abstract 1
- 239000003513 alkali Substances 0.000 abstract 1
- -1 aromatic hydroxy acid Chemical class 0.000 abstract 1
- 230000015572 biosynthetic process Effects 0.000 abstract 1
- 235000011187 glycerol Nutrition 0.000 abstract 1
- 230000007935 neutral effect Effects 0.000 abstract 1
- 229910017604 nitric acid Inorganic materials 0.000 abstract 1
- 238000005406 washing Methods 0.000 abstract 1
- 230000001681 protective effect Effects 0.000 description 3
- 238000005054 agglomeration Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000001125 extrusion Methods 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 238000011017 operating method Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000007493 shaping process Methods 0.000 description 1
- 238000002791 soaking Methods 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- 230000003245 working effect Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23G—CLEANING OR DE-GREASING OF METALLIC MATERIAL BY CHEMICAL METHODS OTHER THAN ELECTROLYSIS
- C23G1/00—Cleaning or pickling metallic material with solutions or molten salts
- C23G1/02—Cleaning or pickling metallic material with solutions or molten salts with acid solutions
- C23G1/12—Light metals
- C23G1/125—Light metals aluminium
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Cleaning And De-Greasing Of Metallic Materials By Chemical Methods (AREA)
- Chemical Treatment Of Metals (AREA)
Abstract
The invention relates to the technical field of aluminum material processing, in particular to an aluminum material surface treatment process. Acetone is used for cleaning the surface of an aluminum material; then, clear water is used for cleaning the surface of the aluminum material until residues on the surface of the aluminum material are totally removed; the aluminum material is put in NaOH solution of 80 g/L for alkali corrosion, and is washed by the clear water after being taken out; the aluminum material is put in cleaning liquid for dipping; the cleaning liquid is prepared by 25 parts of aromatic hydroxy acid, 15 parts of N, N-dimethylformamide, 5 parts of dilute nitric acid, 0.5 part of rhamnoside, 10 parts of glycerin and 40 parts of water; the aluminum material is washed by water after being fished out until the pH value of the washing water becomes neutral; and the aluminum material is dried. The surface treatment process is simple in operation process, adds a cleaning liquid dipping step, reasonably designs a formula and a preparation method of the cleaning liquid, and realizes formation of one layer of effective protection film on the surface of the aluminum material; the protection film is longer in service life and higher in corrosion resistance; and the surface performance of the aluminum material is greatly improved.
Description
Technical field
The present invention relates to aluminum profile extrusion technical field, specifically relate to a kind of process of surface treatment of aluminium.
Background technology
Aluminium is used widely because it has good corrosion resistance nature, and aluminium needs when machine-shaping to carry out surface treatment to it, to form protective membrane.
Summary of the invention
For the technical problem existed in prior art, the object of the present invention is to provide a kind of process of surface treatment of aluminium, for achieving the above object, present invention employs following technical scheme:
A process of surface treatment for aluminium, step is as follows:
Step 1., use acetone aluminium material surface is cleaned, then with clear water rinse, until aluminium material surface residue cleans up;
Step 2., aluminium is put into the NaOH solution alkaline etching 5 minutes of 80g/L, rinse with clear water after taking-up;
Step 3., aluminium put into the scavenging solution being heated to 50 DEG C in advance and soaks 10 minutes, scavenging solution is made up of 25 parts of aromatic hydroxyl acid, 15 parts of DMFs, 5 parts of dust technology, 0.5 part of rhamnoside, 10 parts of glycerol and 40 parts of water;
Step 4., pull rear water out and rinse until the pH value of wash-down water returns to neutrality, dry at 150 DEG C.
Preferably, the preparation method of the scavenging solution that 3. described step uses is: in container, first add 25 parts of aromatic hydroxyl acid and 15 parts of water, stir 5 minutes; Then slowly add 5 parts of dust technology, limit edged stirs, and stirs 5 minutes after interpolation; Then slowly add 15 parts of DMFs and 15 parts of water, limit edged stirs, and stirs 5 minutes after interpolation; Then slowly add 0.5 part of rhamnoside, limit edged stirs, and stirs 5 minutes after interpolation; Finally add 10 parts of glycerol and 10 parts of water fast, stir 5 minutes.
Beneficial effect of the present invention shows:
1), the scavenging solution that uses in process of surface treatment, its formulating of recipe is reasonable, novel, particularly with the addition of a small amount of rhamnoside, can significantly improve the processing efficiency of scavenging solution, then improves the surface treatment properties of aluminium.
2), the preparation method of scavenging solution, by progressively adding and different order of addition(of ingredients), the solubility property between each material can not only be improved, the possibility of particle agglomeration can also be avoided, thus surface processing efficiency is promoted significantly.
3), process of surface treatment, operating procedure is succinct, set up scavenging solution soaking step, the formula of appropriate design scavenging solution and the preparation method of scavenging solution, thus realize forming one deck effective " protective film " at aluminium material surface, and the work-ing life of this protective film is longer, corrosion resistance nature is high, significantly improves the surface property of aluminium.
Embodiment
Below with reference to embodiment, the present invention is described in detail.But; embodiment content is only citing made for the present invention and explanation; affiliated those skilled in the art make various amendment to described specific embodiment or supplement or adopt similar mode to substitute; only otherwise depart from the design of invention or surmount this scope as defined in the claims, protection scope of the present invention all should be belonged to.
One, the composition of scavenging solution
25 parts of aromatic hydroxyl acid, 15 parts of DMFs, 5 parts of dust technology, 0.5 part of rhamnoside, 10 parts of glycerol and 40 parts of water.
Two, the preparation method of scavenging solution is:
First in container, add 25 parts of aromatic hydroxyl acid and 15 parts of water, stir 5 minutes; Then slowly add 5 parts of dust technology, limit edged stirs, and stirs 5 minutes after interpolation; Then slowly add 15 parts of DMFs and 15 parts of water, limit edged stirs, and stirs 5 minutes after interpolation; Then slowly add 0.5 part of rhamnoside, limit edged stirs, and stirs 5 minutes after interpolation; Finally add 10 parts of glycerol and 10 parts of water fast, stir 5 minutes.
Three, the process of surface treatment of aluminium
Step 1., use acetone aluminium material surface is cleaned, then with clear water rinse, until aluminium material surface residue cleans up;
Step 2., aluminium is put into the NaOH solution alkaline etching 5 minutes of 80g/L, rinse with clear water after taking-up;
Step 3., aluminium put into the scavenging solution being heated to 50 DEG C in advance and soaks 10 minutes;
Step 4., pull rear water out and rinse until the pH value of wash-down water returns to neutrality, dry at 150 DEG C.
Claims (2)
1. a process of surface treatment for aluminium, is characterized in that step is as follows:
Step 1., use acetone aluminium material surface is cleaned, then with clear water rinse, until aluminium material surface residue cleans up;
Step 2., aluminium is put into the NaOH solution alkaline etching 5 minutes of 80g/L, rinse with clear water after taking-up;
Step 3., aluminium put into the scavenging solution being heated to 50 DEG C in advance and soaks 10 minutes, scavenging solution is made up of 25 parts of aromatic hydroxyl acid, 15 parts of DMFs, 5 parts of dust technology, 0.5 part of rhamnoside, 10 parts of glycerol and 40 parts of water;
Step 4., pull rear water out and rinse until the pH value of wash-down water returns to neutrality, dry at 150 DEG C.
2. the process of surface treatment of aluminium as claimed in claim 1, is characterized in that the preparation method of the scavenging solution that 3. described step uses is: in container, first add 25 parts of aromatic hydroxyl acid and 15 parts of water, stir 5 minutes; Then slowly add 5 parts of dust technology, limit edged stirs, and stirs 5 minutes after interpolation; Then slowly add 15 parts of DMFs and 15 parts of water, limit edged stirs, and stirs 5 minutes after interpolation; Then slowly add 0.5 part of rhamnoside, limit edged stirs, and stirs 5 minutes after interpolation; Finally add 10 parts of glycerol and 10 parts of water fast, stir 5 minutes.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201511013079.2A CN105568302A (en) | 2015-12-31 | 2015-12-31 | Aluminum material surface treatment process |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201511013079.2A CN105568302A (en) | 2015-12-31 | 2015-12-31 | Aluminum material surface treatment process |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105568302A true CN105568302A (en) | 2016-05-11 |
Family
ID=55878908
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201511013079.2A Pending CN105568302A (en) | 2015-12-31 | 2015-12-31 | Aluminum material surface treatment process |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105568302A (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1900829A (en) * | 2002-01-09 | 2007-01-24 | 气体产品及化学制品公司 | Method for removing photoresist, etch and/or polymeric residues or contaminants from semiconductor substrates |
| CN101868563A (en) * | 2007-11-19 | 2010-10-20 | 日本帕卡濑精株式会社 | Base treatment agent for metal material and base treatment method for metal material |
| CN103668147A (en) * | 2012-09-26 | 2014-03-26 | 广州天至环保科技有限公司 | Chrome-free water-based protective agent capable of improving overall performance of tin and tin alloy clad layers |
| CN104555828A (en) * | 2015-01-05 | 2015-04-29 | 李经纬 | Automatic operating system of forklift |
-
2015
- 2015-12-31 CN CN201511013079.2A patent/CN105568302A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1900829A (en) * | 2002-01-09 | 2007-01-24 | 气体产品及化学制品公司 | Method for removing photoresist, etch and/or polymeric residues or contaminants from semiconductor substrates |
| CN101868563A (en) * | 2007-11-19 | 2010-10-20 | 日本帕卡濑精株式会社 | Base treatment agent for metal material and base treatment method for metal material |
| CN103668147A (en) * | 2012-09-26 | 2014-03-26 | 广州天至环保科技有限公司 | Chrome-free water-based protective agent capable of improving overall performance of tin and tin alloy clad layers |
| CN104555828A (en) * | 2015-01-05 | 2015-04-29 | 李经纬 | Automatic operating system of forklift |
Non-Patent Citations (3)
| Title |
|---|
| 史宏志等: "《烟草香味学》", 30 September 2011, 中国农业出版社 * |
| 郭静成: "《基础生物化学题解》", 30 September 1990, 北京农业大学出版社 * |
| 金黎: "鼠李糖脂作为清洗剂的应用研究", 《中国优秀硕士学位论文全文数据库（电子期刊）》 * |
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| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20160511 |
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| RJ01 | Rejection of invention patent application after publication |