CN105519819A - Method for producing fish feed with collagen - Google Patents
Method for producing fish feed with collagen Download PDFInfo
- Publication number
- CN105519819A CN105519819A CN201510985598.9A CN201510985598A CN105519819A CN 105519819 A CN105519819 A CN 105519819A CN 201510985598 A CN201510985598 A CN 201510985598A CN 105519819 A CN105519819 A CN 105519819A
- Authority
- CN
- China
- Prior art keywords
- parts
- material solution
- vitamin
- wall material
- mass fraction
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 102000008186 Collagen Human genes 0.000 title claims abstract description 33
- 108010035532 Collagen Proteins 0.000 title claims abstract description 33
- 229920001436 collagen Polymers 0.000 title claims abstract description 33
- 241000251468 Actinopterygii Species 0.000 title abstract description 14
- 238000004519 manufacturing process Methods 0.000 title abstract description 8
- 239000000243 solution Substances 0.000 claims abstract description 89
- 239000011162 core material Substances 0.000 claims abstract description 67
- 239000000463 material Substances 0.000 claims abstract description 63
- 239000003094 microcapsule Substances 0.000 claims abstract description 42
- 239000011259 mixed solution Substances 0.000 claims abstract description 41
- 238000001035 drying Methods 0.000 claims abstract description 11
- 239000000203 mixture Substances 0.000 claims description 58
- 239000000839 emulsion Substances 0.000 claims description 45
- 238000003756 stirring Methods 0.000 claims description 45
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 41
- 239000008187 granular material Substances 0.000 claims description 40
- 235000019733 Fish meal Nutrition 0.000 claims description 30
- 239000004467 fishmeal Substances 0.000 claims description 30
- 238000000034 method Methods 0.000 claims description 22
- 239000011782 vitamin Substances 0.000 claims description 20
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 18
- 229940088594 vitamin Drugs 0.000 claims description 17
- 229930003231 vitamin Natural products 0.000 claims description 17
- 235000013343 vitamin Nutrition 0.000 claims description 17
- 150000003722 vitamin derivatives Chemical class 0.000 claims description 17
- -1 115 parts Chemical compound 0.000 claims description 15
- 229910052500 inorganic mineral Inorganic materials 0.000 claims description 15
- 235000010755 mineral Nutrition 0.000 claims description 15
- 239000011707 mineral Substances 0.000 claims description 15
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 claims description 14
- CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 claims description 14
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 claims description 14
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 14
- OVBPIULPVIDEAO-LBPRGKRZSA-N folic acid Chemical compound C=1N=C2NC(N)=NC(=O)C2=NC=1CNC1=CC=C(C(=O)N[C@@H](CCC(O)=O)C(O)=O)C=C1 OVBPIULPVIDEAO-LBPRGKRZSA-N 0.000 claims description 14
- 239000002994 raw material Substances 0.000 claims description 14
- 150000001875 compounds Chemical class 0.000 claims description 12
- 239000006041 probiotic Substances 0.000 claims description 12
- 230000000529 probiotic effect Effects 0.000 claims description 12
- 235000018291 probiotics Nutrition 0.000 claims description 12
- 238000010438 heat treatment Methods 0.000 claims description 10
- 238000002360 preparation method Methods 0.000 claims description 10
- ZZSNKZQZMQGXPY-UHFFFAOYSA-N Ethyl cellulose Chemical compound CCOCC1OC(OC)C(OCC)C(OCC)C1OC1C(O)C(O)C(OC)C(CO)O1 ZZSNKZQZMQGXPY-UHFFFAOYSA-N 0.000 claims description 9
- 239000004372 Polyvinyl alcohol Substances 0.000 claims description 9
- 235000011187 glycerol Nutrition 0.000 claims description 9
- 235000012054 meals Nutrition 0.000 claims description 9
- 229920002451 polyvinyl alcohol Polymers 0.000 claims description 9
- 229920001285 xanthan gum Polymers 0.000 claims description 9
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 claims description 8
- FPIPGXGPPPQFEQ-UHFFFAOYSA-N 13-cis retinol Natural products OCC=C(C)C=CC=C(C)C=CC1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-UHFFFAOYSA-N 0.000 claims description 7
- 239000001763 2-hydroxyethyl(trimethyl)azanium Substances 0.000 claims description 7
- GHOKWGTUZJEAQD-UHFFFAOYSA-N Chick antidermatitis factor Natural products OCC(C)(C)C(O)C(=O)NCCC(O)=O GHOKWGTUZJEAQD-UHFFFAOYSA-N 0.000 claims description 7
- 235000019743 Choline chloride Nutrition 0.000 claims description 7
- SQUHHTBVTRBESD-UHFFFAOYSA-N Hexa-Ac-myo-Inositol Natural products CC(=O)OC1C(OC(C)=O)C(OC(C)=O)C(OC(C)=O)C(OC(C)=O)C1OC(C)=O SQUHHTBVTRBESD-UHFFFAOYSA-N 0.000 claims description 7
- OVBPIULPVIDEAO-UHFFFAOYSA-N N-Pteroyl-L-glutaminsaeure Natural products C=1N=C2NC(N)=NC(=O)C2=NC=1CNC1=CC=C(C(=O)NC(CCC(O)=O)C(O)=O)C=C1 OVBPIULPVIDEAO-UHFFFAOYSA-N 0.000 claims description 7
- 235000019764 Soybean Meal Nutrition 0.000 claims description 7
- 229920002472 Starch Polymers 0.000 claims description 7
- JZRWCGZRTZMZEH-UHFFFAOYSA-N Thiamine Natural products CC1=C(CCO)SC=[N+]1CC1=CN=C(C)N=C1N JZRWCGZRTZMZEH-UHFFFAOYSA-N 0.000 claims description 7
- FPIPGXGPPPQFEQ-BOOMUCAASA-N Vitamin A Natural products OC/C=C(/C)\C=C\C=C(\C)/C=C/C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-BOOMUCAASA-N 0.000 claims description 7
- 229930003779 Vitamin B12 Natural products 0.000 claims description 7
- 229930003571 Vitamin B5 Natural products 0.000 claims description 7
- 229930003427 Vitamin E Natural products 0.000 claims description 7
- FPIPGXGPPPQFEQ-OVSJKPMPSA-N all-trans-retinol Chemical compound OC\C=C(/C)\C=C\C=C(/C)\C=C\C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-OVSJKPMPSA-N 0.000 claims description 7
- FAPWYRCQGJNNSJ-UBKPKTQASA-L calcium D-pantothenic acid Chemical compound [Ca+2].OCC(C)(C)[C@@H](O)C(=O)NCCC([O-])=O.OCC(C)(C)[C@@H](O)C(=O)NCCC([O-])=O FAPWYRCQGJNNSJ-UBKPKTQASA-L 0.000 claims description 7
- 229960002079 calcium pantothenate Drugs 0.000 claims description 7
- 229960003178 choline chloride Drugs 0.000 claims description 7
- SGMZJAMFUVOLNK-UHFFFAOYSA-M choline chloride Chemical compound [Cl-].C[N+](C)(C)CCO SGMZJAMFUVOLNK-UHFFFAOYSA-M 0.000 claims description 7
- GVPFVAHMJGGAJG-UHFFFAOYSA-L cobalt dichloride Chemical compound [Cl-].[Cl-].[Co+2] GVPFVAHMJGGAJG-UHFFFAOYSA-L 0.000 claims description 7
- FDJOLVPMNUYSCM-WZHZPDAFSA-L cobalt(3+);[(2r,3s,4r,5s)-5-(5,6-dimethylbenzimidazol-1-yl)-4-hydroxy-2-(hydroxymethyl)oxolan-3-yl] [(2r)-1-[3-[(1r,2r,3r,4z,7s,9z,12s,13s,14z,17s,18s,19r)-2,13,18-tris(2-amino-2-oxoethyl)-7,12,17-tris(3-amino-3-oxopropyl)-3,5,8,8,13,15,18,19-octamethyl-2 Chemical compound [Co+3].N#[C-].N([C@@H]([C@]1(C)[N-]\C([C@H]([C@@]1(CC(N)=O)C)CCC(N)=O)=C(\C)/C1=N/C([C@H]([C@@]1(CC(N)=O)C)CCC(N)=O)=C\C1=N\C([C@H](C1(C)C)CCC(N)=O)=C/1C)[C@@H]2CC(N)=O)=C\1[C@]2(C)CCC(=O)NC[C@@H](C)OP([O-])(=O)O[C@H]1[C@@H](O)[C@@H](N2C3=CC(C)=C(C)C=C3N=C2)O[C@@H]1CO FDJOLVPMNUYSCM-WZHZPDAFSA-L 0.000 claims description 7
- ARUVKPQLZAKDPS-UHFFFAOYSA-L copper(II) sulfate Chemical compound [Cu+2].[O-][S+2]([O-])([O-])[O-] ARUVKPQLZAKDPS-UHFFFAOYSA-L 0.000 claims description 7
- 239000011790 ferrous sulphate Substances 0.000 claims description 7
- 235000003891 ferrous sulphate Nutrition 0.000 claims description 7
- 229960000304 folic acid Drugs 0.000 claims description 7
- 235000019152 folic acid Nutrition 0.000 claims description 7
- 239000011724 folic acid Substances 0.000 claims description 7
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 claims description 7
- 229960000367 inositol Drugs 0.000 claims description 7
- CDAISMWEOUEBRE-GPIVLXJGSA-N inositol Chemical compound O[C@H]1[C@H](O)[C@@H](O)[C@H](O)[C@H](O)[C@@H]1O CDAISMWEOUEBRE-GPIVLXJGSA-N 0.000 claims description 7
- BAUYGSIQEAFULO-UHFFFAOYSA-L iron(2+) sulfate (anhydrous) Chemical compound [Fe+2].[O-]S([O-])(=O)=O BAUYGSIQEAFULO-UHFFFAOYSA-L 0.000 claims description 7
- 229910000359 iron(II) sulfate Inorganic materials 0.000 claims description 7
- 229910052943 magnesium sulfate Inorganic materials 0.000 claims description 7
- 235000019341 magnesium sulphate Nutrition 0.000 claims description 7
- 229940099596 manganese sulfate Drugs 0.000 claims description 7
- 239000011702 manganese sulphate Substances 0.000 claims description 7
- 235000007079 manganese sulphate Nutrition 0.000 claims description 7
- SQQMAOCOWKFBNP-UHFFFAOYSA-L manganese(II) sulfate Chemical compound [Mn+2].[O-]S([O-])(=O)=O SQQMAOCOWKFBNP-UHFFFAOYSA-L 0.000 claims description 7
- 229910000403 monosodium phosphate Inorganic materials 0.000 claims description 7
- 235000019799 monosodium phosphate Nutrition 0.000 claims description 7
- 239000001103 potassium chloride Substances 0.000 claims description 7
- 235000011164 potassium chloride Nutrition 0.000 claims description 7
- CDAISMWEOUEBRE-UHFFFAOYSA-N scyllo-inosotol Natural products OC1C(O)C(O)C(O)C(O)C1O CDAISMWEOUEBRE-UHFFFAOYSA-N 0.000 claims description 7
- 239000011780 sodium chloride Substances 0.000 claims description 7
- AJPJDKMHJJGVTQ-UHFFFAOYSA-M sodium dihydrogen phosphate Chemical compound [Na+].OP(O)([O-])=O AJPJDKMHJJGVTQ-UHFFFAOYSA-M 0.000 claims description 7
- 239000004455 soybean meal Substances 0.000 claims description 7
- 235000019698 starch Nutrition 0.000 claims description 7
- 239000008107 starch Substances 0.000 claims description 7
- 235000019157 thiamine Nutrition 0.000 claims description 7
- KYMBYSLLVAOCFI-UHFFFAOYSA-N thiamine Chemical compound CC1=C(CCO)SCN1CC1=CN=C(C)N=C1N KYMBYSLLVAOCFI-UHFFFAOYSA-N 0.000 claims description 7
- 229960003495 thiamine Drugs 0.000 claims description 7
- 239000011721 thiamine Substances 0.000 claims description 7
- 235000019155 vitamin A Nutrition 0.000 claims description 7
- 239000011719 vitamin A Substances 0.000 claims description 7
- 235000019163 vitamin B12 Nutrition 0.000 claims description 7
- 239000011715 vitamin B12 Substances 0.000 claims description 7
- 235000009492 vitamin B5 Nutrition 0.000 claims description 7
- 239000011675 vitamin B5 Substances 0.000 claims description 7
- 235000019165 vitamin E Nutrition 0.000 claims description 7
- 229940046009 vitamin E Drugs 0.000 claims description 7
- 239000011709 vitamin E Substances 0.000 claims description 7
- 229940045997 vitamin a Drugs 0.000 claims description 7
- NWONKYPBYAMBJT-UHFFFAOYSA-L zinc sulfate Chemical compound [Zn+2].[O-]S([O-])(=O)=O NWONKYPBYAMBJT-UHFFFAOYSA-L 0.000 claims description 7
- 229960001763 zinc sulfate Drugs 0.000 claims description 7
- 229910000368 zinc sulfate Inorganic materials 0.000 claims description 7
- 239000006185 dispersion Substances 0.000 claims description 5
- 238000005538 encapsulation Methods 0.000 claims description 5
- 239000008236 heating water Substances 0.000 claims description 5
- 238000000265 homogenisation Methods 0.000 claims description 5
- 238000002156 mixing Methods 0.000 claims description 5
- 238000001694 spray drying Methods 0.000 claims description 5
- 230000008961 swelling Effects 0.000 claims description 5
- 241000193749 Bacillus coagulans Species 0.000 claims description 4
- 241000894006 Bacteria Species 0.000 claims description 4
- 241000186000 Bifidobacterium Species 0.000 claims description 4
- 229940054340 bacillus coagulans Drugs 0.000 claims description 4
- 235000014655 lactic acid Nutrition 0.000 claims description 4
- 239000004310 lactic acid Substances 0.000 claims description 4
- 235000013557 nattō Nutrition 0.000 claims description 4
- WIGIZIANZCJQQY-UHFFFAOYSA-N 4-ethyl-3-methyl-N-[2-[4-[[[(4-methylcyclohexyl)amino]-oxomethyl]sulfamoyl]phenyl]ethyl]-5-oxo-2H-pyrrole-1-carboxamide Chemical compound O=C1C(CC)=C(C)CN1C(=O)NCCC1=CC=C(S(=O)(=O)NC(=O)NC2CCC(C)CC2)C=C1 WIGIZIANZCJQQY-UHFFFAOYSA-N 0.000 claims description 3
- 241000193171 Clostridium butyricum Species 0.000 claims description 3
- 240000001046 Lactobacillus acidophilus Species 0.000 claims description 3
- 235000013956 Lactobacillus acidophilus Nutrition 0.000 claims description 3
- 229940039695 lactobacillus acidophilus Drugs 0.000 claims description 3
- 150000003718 vitamin K5 derivatives Chemical group 0.000 claims description 3
- 238000009360 aquaculture Methods 0.000 abstract description 8
- 244000144974 aquaculture Species 0.000 abstract description 8
- 239000002245 particle Substances 0.000 abstract 2
- 238000003912 environmental pollution Methods 0.000 abstract 1
- 235000018102 proteins Nutrition 0.000 description 7
- 102000004169 proteins and genes Human genes 0.000 description 7
- 108090000623 proteins and genes Proteins 0.000 description 7
- 241000404975 Synchiropus splendidus Species 0.000 description 5
- 241001465754 Metazoa Species 0.000 description 4
- 230000037396 body weight Effects 0.000 description 4
- 102000010834 Extracellular Matrix Proteins Human genes 0.000 description 3
- 108010037362 Extracellular Matrix Proteins Proteins 0.000 description 3
- 210000002744 extracellular matrix Anatomy 0.000 description 3
- 108010082495 Dietary Plant Proteins Proteins 0.000 description 2
- 210000004027 cell Anatomy 0.000 description 2
- 238000012258 culturing Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000003925 fat Substances 0.000 description 2
- 235000019197 fats Nutrition 0.000 description 2
- 235000019786 weight gain Nutrition 0.000 description 2
- 241000143060 Americamysis bahia Species 0.000 description 1
- 241000238557 Decapoda Species 0.000 description 1
- 102000002322 Egg Proteins Human genes 0.000 description 1
- 108010000912 Egg Proteins Proteins 0.000 description 1
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 1
- 241000124008 Mammalia Species 0.000 description 1
- 101710172711 Structural protein Proteins 0.000 description 1
- 238000005273 aeration Methods 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 235000021120 animal protein Nutrition 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 230000023555 blood coagulation Effects 0.000 description 1
- 238000007664 blowing Methods 0.000 description 1
- 210000000988 bone and bone Anatomy 0.000 description 1
- 210000000481 breast Anatomy 0.000 description 1
- 244000144987 brood Species 0.000 description 1
- 230000002308 calcification Effects 0.000 description 1
- 150000001720 carbohydrates Chemical class 0.000 description 1
- 235000014633 carbohydrates Nutrition 0.000 description 1
- 210000000845 cartilage Anatomy 0.000 description 1
- 235000013339 cereals Nutrition 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 210000002808 connective tissue Anatomy 0.000 description 1
- 235000019621 digestibility Nutrition 0.000 description 1
- 210000002249 digestive system Anatomy 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- MECHNRXZTMCUDQ-RKHKHRCZSA-N ergocalciferol group Chemical group CC(C)[C@@H](C)\C=C\[C@@H](C)[C@H]1CC[C@H]2\C(\CCC[C@]12C)=C\C=C/1\C[C@@H](O)CCC1=C MECHNRXZTMCUDQ-RKHKHRCZSA-N 0.000 description 1
- 235000020776 essential amino acid Nutrition 0.000 description 1
- 239000003797 essential amino acid Substances 0.000 description 1
- 230000003203 everyday effect Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000008103 glucose Substances 0.000 description 1
- 239000003102 growth factor Substances 0.000 description 1
- 235000012907 honey Nutrition 0.000 description 1
- 238000001727 in vivo Methods 0.000 description 1
- 239000003446 ligand Substances 0.000 description 1
- 238000005461 lubrication Methods 0.000 description 1
- 230000035800 maturation Effects 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 210000000056 organ Anatomy 0.000 description 1
- 210000004681 ovum Anatomy 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 230000019491 signal transduction Effects 0.000 description 1
- 210000003491 skin Anatomy 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 210000002784 stomach Anatomy 0.000 description 1
- 210000002435 tendon Anatomy 0.000 description 1
- 210000001519 tissue Anatomy 0.000 description 1
- 239000011573 trace mineral Substances 0.000 description 1
- 235000013619 trace mineral Nutrition 0.000 description 1
- AVBGNFCMKJOFIN-UHFFFAOYSA-N triethylammonium acetate Chemical compound CC(O)=O.CCN(CC)CC AVBGNFCMKJOFIN-UHFFFAOYSA-N 0.000 description 1
- 210000001835 viscera Anatomy 0.000 description 1
- 150000003717 vitamin K4 derivatives Chemical group 0.000 description 1
- 150000003720 vitamin K7 derivatives Chemical group 0.000 description 1
- RMDJVOZETBHEAR-GHTRHTQZSA-N vitamin d5 Chemical group C1(/[C@@H]2CC[C@@H]([C@]2(CCC1)C)[C@H](C)CC[C@H](CC)C(C)C)=C\C=C1\C[C@@H](O)CCC1=C RMDJVOZETBHEAR-GHTRHTQZSA-N 0.000 description 1
- 230000029663 wound healing Effects 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
- Y02A40/80—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in fisheries management
- Y02A40/81—Aquaculture, e.g. of fish
- Y02A40/818—Alternative feeds for fish, e.g. in aquacultures
Landscapes
- Fodder In General (AREA)
Abstract
本发明公开了一种利用胶原蛋白生产鱼饲料的方法，包括：芯材溶液制备；壁材溶液制备；将芯材溶液分别加入到壁材溶液中，得到混合溶液；干燥，得到微胶囊颗粒；将不同的微胶囊颗粒按比例混匀，得到鱼饲料。本发明结构简单，易于制造，制作成本低，经济效益高；利用胶原蛋白制作微囊化饲料后，可改善水产养殖的情况，节约了饲料并提高生产效率，降低水产养殖对环境的污染。The invention discloses a method for producing fish feed by using collagen, comprising: preparing a core material solution; preparing a wall material solution; respectively adding the core material solution into the wall material solution to obtain a mixed solution; drying to obtain microcapsule particles; Different microcapsule particles are mixed in proportion to obtain fish feed. The invention is simple in structure, easy to manufacture, low in production cost and high in economic benefit; after making microencapsulated feed with collagen, the situation of aquaculture can be improved, feed can be saved, production efficiency can be improved, and environmental pollution of aquaculture can be reduced.
Description
Technical field
The present invention relates to fish meal preparing technical field, specifically a kind of method utilizing collagen to produce fish meal.
Background technology
Collagen, also collagen is claimed, it is a kind of structural protein of extracellular matrix, English name " collagen ", is developed by Greek, GL-PP, in white, containing a small amount of galactolipin and glucose, be the main component of extracellular matrix (ECM), account for 85% of collagenous fibres solids.Collagen is ubiquitous a kind of high molecular weight protein in animal body, mainly be present in the connective tissue (bone, cartilage, skin, tendon, tough etc.) of animal, it is the functional protein that mammal in-vivo content is maximum, distribution is the widest, account for 25% ~ 30% of mammalian body internal protein, be equivalent to 6% of body weight.Many marine organisms, as the skin of fish, account for its protein content even up to more than 80%.To body and internal organs play support, protection, combine and formed boundary every etc. effect.With the transmission of the formation organized, maturation, cell-tocell, and joint lubrication, wound healing, calcification, blood clotting and aging etc. have close relationship.Except biomethanics aspect, also there is the functions such as the transport of such as signal transduction, growth factor and cell factor.
The main component of fish meal is protein, fat, vitamin and mineral matter etc., and protein is the important nutrient of fishes and shrimps existence, is the important composition material forming body cell, tissue, organ.The protein that fish normal growth needs have quantity enough, easily to digest and assimilate in feed, various amino acid ligand ratio is suitable.In general, contained by animal protein, essential amino acid ratio is all close with animal product, and thus biologic valence is high, quality better, and most cereal and other vegetable proteins are few containing TEAA, ratio does not meet animal needs, biological value is low, the at present conventional many employings of fish meal be vegetable protein, the assimilation effect after fish feed is poor, poor growth, therefore feed coefficient is large, need the fish meal amount of input large, may also can pollute water quality, feeding cost is higher.
Summary of the invention
The object of the present invention is to provide a kind of method utilizing collagen to produce fish meal, the situation of aquaculture can be improved, saved feed and enhanced productivity, reduce aquaculture to the pollution of environment.
For achieving the above object, the invention provides following technical scheme:
Utilize collagen to produce the method for fish meal, comprise the following steps:
(1) core material solution preparation: take collagen 40-55 part according to mass fraction, add suitable quantity of water, stir until dissolved to emulsion form, obtained first core material solution; Take phosphatide oil 1-2.5 part and dehulled soybean meal 5-8 part according to mass fraction, add suitable quantity of water, after heating, stir until dissolved to emulsion form, obtained second core material solution; Take alphalise starch 18-25 part and Choline Chloride 0.5-0.8 part according to mass fraction, add suitable quantity of water, heating stirs until dissolved to emulsion form, obtained 3rd core material solution; Take vitamin mixtures 1.5-1.8 part, mineral mixture 0.5-1.2 part and compound probiotic 0.02-0.03 part according to mass fraction, add suitable quantity of water, stir until dissolved to emulsion form, obtained 4th core material solution;
(2) wall material solution preparation: get seawood meal, xanthans and glycerine, mix, add suitable quantity of water, make its swelling, dispersion, 45-50 DEG C of heating water bath makes it fully be dissolved to emulsion form, obtained first wall material solution; Get polyvinyl alcohol, under 90-95 DEG C of water bath condition, be dissolved in water, high-speed stirred, to fully dissolving, obtains the second wall material solution; Get Aquacoat, add water and stir 20-50min, obtained 3rd wall material solution;
(3) according to mass ratio be the wall material core ratio of 8-10:1, the first core material solution in step (1) joined in the 3rd wall material solution in step (2), fully stir, mix to emulsion form, then homogenize, obtain the first mixed solution; According to the wall material core ratio that mass ratio is 6-8:1, the second core material solution in step (1) is joined in the second wall material solution in step (2), fully stir, mix to emulsion form, then homogenize, obtain the second mixed solution; According to the wall material core ratio that mass ratio is 8-10:1, the 3rd core material solution in step (1) is joined in the first wall material solution in step (2), fully stir, mix to emulsion form, then homogenize, obtain the 3rd mixed solution; According to the wall material core ratio that mass ratio is 8-10:1, the 4th core material solution in step (1) is joined in the first wall material solution in step (2), fully stir, mix to emulsion form, then homogenize, obtain the 4th mixed solution;
(4) spray drying process is then adopted to carry out drying to the first mixed solution, the second mixed solution, the 3rd mixed solution and the 4th mixed solution respectively, EAT time dry is 160-180 DEG C, leaving air temp is 70-85 DEG C, feed rate is 1-1.5ml/min, obtains the first microcapsule granule, the second microcapsule granule, the 3rd microcapsule granule and the 4th microcapsule granule after drying respectively;
(5) by the first microcapsule granule, the second microcapsule granule, the 3rd microcapsule granule and the 4th microcapsule granule in mass ratio for 8-10:3-7:5-10:1 mixes, mixing after encapsulation, obtain fish meal.
As the further scheme of the present invention: in described step (1), take collagen 48 parts according to mass fraction, phosphatide oil 1.8 parts, dehulled soybean meal 7 parts, alphalise starch be 22 parts, Choline Chloride is 0.65 part, vitamin mixtures is 1.7 parts, mineral mixture is 0.8 part and compound probiotic 0.025 part.
As the further scheme of the present invention: described compound probiotic is one or more and saccharomycetic mixture in bafillus natto, bacillus coagulans, clostridium butyricum, lactic acid bacteria, Bifidobacterium and lactobacillus acidophilus.
As the further scheme of the present invention: in described step (1), described vitamin mixtures is made up of vitamin A 4-8 part, vitamin B5 5-15 part, vitamin B12 0.02-0.028 part, calciferol-5 parts, vitamin E 60-80 part, Vitamin K4-7 parts, folic acid 0.2-0.5 part, thiamine 12-18 part and inositol 120-160 part according to the raw material of mass fraction.
As the further scheme of the present invention: in described step (1), described vitamin mixtures is made up of vitamin A 6 parts, vitamin B5 10 parts, vitamin B12 0.025 part, vitamine D3 part, vitamin E 70 parts, vitamin K5 part, 0.4 part, folic acid, thiamine 15 parts and inositol 140 parts according to the raw material of mass fraction.
As the further scheme of the present invention: in described step (1), described mineral mixture is made up of sodium chloride 40-80 part, KI 0.01-0.03 part, sodium dihydrogen phosphate 150-180 part, magnesium sulfate 50-65 part, potassium chloride 80-120 part, ferrous sulfate 20-40 part, zinc sulfate 2-3 part, manganese sulfate 0.2-0.3 part, copper sulphate 0.2-0.3 part and cobalt chloride 0.3-0.8 part according to the raw material of mass fraction.
As the further scheme of the present invention: in described step (1), described mineral mixture is made up of 60 parts, sodium chloride, KI 0.02 part, sodium dihydrogen phosphate 160 parts, 60 parts, magnesium sulfate, 115 parts, potassium chloride, 30 parts, ferrous sulfate, 2.5 parts, zinc sulfate, manganese sulfate 0.25 part, 0.25 part, copper sulphate and cobalt chloride 0.5 part according to the raw material of mass fraction.
As the further scheme of the present invention: in described step (2), take seawood meal 80-150 part, xanthans 600-800 part and glycerine 80-100 part according to mass fraction; Polyvinyl alcohol 150-600 part, Aquacoat 850-1000 part.
As the further scheme of the present invention: in described step (2), take seawood meal 120 parts according to mass fraction, xanthans 700 parts and glycerine 90 parts; Polyvinyl alcohol is 350 parts, and Aquacoat is 900 parts.
As the further scheme of the present invention: in described step (3), what homogenize employing is twice homogenization, and the rotating speed of homogeneous is 5000-6000r/min for the first time, and the duration is 8-10min; The rotating speed of second time homogeneous is 9000-9500r/min, and the duration is 20-25min.
Compared with prior art, the invention has the beneficial effects as follows:
Structure of the present invention is simple, is easy to manufacture, and cost of manufacture is low, high financial profit.The content of material equilibriums such as obtained fish meal protein, fat, carbohydrate and trace element can carry out rational allocation according to grow period desired nutritional of different cultivars and difference, after fish and shrimp are edible, absorbability is better, promote that fish grow fast, promote digestibility, reduce digestive system load, reduce DD incidence, feed coefficient is low, and cost of manufacture reduces; Shorten kind of a fish bosom ovum time, improve fish brood amount, promote kind of a fish-egg quality.The present invention can improve the situation of aquaculture, saved feed and enhanced productivity after utilizing collagen to make microencapsulation feed, reduces aquaculture to the pollution of environment.
Detailed description of the invention
Below in conjunction with the embodiment of the present invention, be clearly and completely described the technical scheme in the embodiment of the present invention, obviously, described embodiment is only the present invention's part embodiment, instead of whole embodiments.Based on the embodiment in the present invention, those of ordinary skill in the art, not making the every other embodiment obtained under creative work prerequisite, belong to the scope of protection of the invention.
Embodiment 1(most preferred embodiment)
In the embodiment of the present invention, utilize collagen to produce the method for fish meal, comprise the following steps:
(1) core material solution preparation: take collagen 48 parts according to mass fraction, add suitable quantity of water, stir until dissolved to emulsion form, obtained first core material solution; Take phosphatide oil 1.8 parts and dehulled soybean meal 7 parts according to mass fraction, add suitable quantity of water, after heating, stir until dissolved to emulsion form, obtained second core material solution; Take alphalise starch 22 parts and Choline Chloride 0.65 part according to mass fraction, add suitable quantity of water, heating stirs until dissolved to emulsion form, obtained 3rd core material solution; Take vitamin mixtures 1.7 parts, mineral mixture 0.8 part and compound probiotic 0.025 part according to mass fraction, add suitable quantity of water, stir until dissolved to emulsion form, obtained 4th core material solution; Vitamin mixtures is made up of vitamin A 6 parts, vitamin B5 10 parts, vitamin B12 0.025 part, vitamine D3 part, vitamin E 70 parts, vitamin K5 part, 0.4 part, folic acid, thiamine 15 parts and inositol 140 parts according to the raw material of mass fraction; Mineral mixture is made up of 60 parts, sodium chloride, KI 0.02 part, sodium dihydrogen phosphate 160 parts, 60 parts, magnesium sulfate, 115 parts, potassium chloride, 30 parts, ferrous sulfate, 2.5 parts, zinc sulfate, manganese sulfate 0.25 part, 0.25 part, copper sulphate and cobalt chloride 0.5 part according to the raw material of mass fraction; Compound probiotic is bafillus natto, bacillus coagulans, clostridium butyricum, lactic acid bacteria, Bifidobacterium, lactobacillus acidophilus and saccharomycetic mixture;
(2) wall material solution preparation: get seawood meal 120 parts, xanthans 700 parts and glycerine 90 parts according to mass fraction, mix, add suitable quantity of water, make its swelling, dispersion, 48 DEG C of heating water baths make it fully be dissolved to emulsion form, obtained first wall material solution; Get polyvinyl alcohol 350 parts, under 95 DEG C of water bath condition, be dissolved in water, high-speed stirred, to fully dissolving, obtains the second wall material solution; Get Aquacoat 900 parts, add water and stir 30min, obtained 3rd wall material solution;
(3) according to mass ratio be the wall material core ratio of 9:1, the first core material solution in step (1) joined in the 3rd wall material solution in step (2), fully stir, mix to emulsion form, then homogenize, obtain the first mixed solution; According to the wall material core ratio that mass ratio is 7:1, the second core material solution in step (1) is joined in the second wall material solution in step (2), fully stir, mix to emulsion form, then homogenize, obtain the second mixed solution; According to the wall material core ratio that mass ratio is 9:1, the 3rd core material solution in step (1) is joined in the first wall material solution in step (2), fully stir, mix to emulsion form, then homogenize, obtain the 3rd mixed solution; According to the wall material core ratio that mass ratio is 9:1, the 4th core material solution in step (1) is joined in the first wall material solution in step (2), fully stir, mix to emulsion form, then homogenize, obtain the 4th mixed solution; Wherein, what homogenize employing is twice homogenization, and the rotating speed of homogeneous is 5500r/min for the first time, and the duration is 9min; The rotating speed of second time homogeneous is 9200r/min, and the duration is 22min;
(4) spray drying process is then adopted to carry out drying to the first mixed solution, the second mixed solution, the 3rd mixed solution and the 4th mixed solution respectively, EAT time dry is 170 DEG C, leaving air temp is 80 DEG C, feed rate is 1.2ml/min, obtains the first microcapsule granule, the second microcapsule granule, the 3rd microcapsule granule and the 4th microcapsule granule after drying respectively;
(5) by the first microcapsule granule, the second microcapsule granule, the 3rd microcapsule granule and the 4th microcapsule granule in mass ratio for 9:5:8:1 mixes, mixing after encapsulation, obtain fish meal.
Embodiment 2
In the embodiment of the present invention, utilize collagen to produce the method for fish meal, comprise the following steps:
(1) core material solution preparation: take collagen 40 parts according to mass fraction, add suitable quantity of water, stir until dissolved to emulsion form, obtained first core material solution; Take phosphatide oil 1 part and dehulled soybean meal 5 parts according to mass fraction, add suitable quantity of water, after heating, stir until dissolved to emulsion form, obtained second core material solution; Take alphalise starch 18 parts and Choline Chloride 0.5 part according to mass fraction, add suitable quantity of water, heating stirs until dissolved to emulsion form, obtained 3rd core material solution; Take vitamin mixtures 1.5 parts, mineral mixture 0.5 part and compound probiotic 0.02 part according to mass fraction, add suitable quantity of water, stir until dissolved to emulsion form, obtained 4th core material solution; Vitamin mixtures is made up of vitamin A 4 parts, vitamin B5 5 parts, vitamin B12 0.02 part, calciferol part, vitamin E 60 parts, Vitamin K4 part, 0.2 part, folic acid, thiamine 12 parts and inositol 120 parts according to the raw material of mass fraction; Mineral mixture is made up of 40 parts, sodium chloride, KI 0.01 part, sodium dihydrogen phosphate 150 parts, 50 parts, magnesium sulfate, 80 parts, potassium chloride, 20 parts, ferrous sulfate, 2 parts, zinc sulfate, manganese sulfate 0.2 part, 0.2 part, copper sulphate and cobalt chloride 0.3 part according to the raw material of mass fraction; Compound probiotic is lactic acid bacteria, Bifidobacterium and saccharomycetic mixture;
(2) wall material solution preparation: get seawood meal 80 parts, xanthans 600 parts and glycerine 80 parts according to mass fraction, mix, add suitable quantity of water, make its swelling, dispersion, 45 DEG C of heating water baths make it fully be dissolved to emulsion form, obtained first wall material solution; Get polyvinyl alcohol 150 parts, under 90 DEG C of water bath condition, be dissolved in water, high-speed stirred, to fully dissolving, obtains the second wall material solution; Get Aquacoat 850 parts, add water and stir 20min, obtained 3rd wall material solution;
(3) according to mass ratio be the wall material core ratio of 8:1, the first core material solution in step (1) joined in the 3rd wall material solution in step (2), fully stir, mix to emulsion form, then homogenize, obtain the first mixed solution; According to the wall material core ratio that mass ratio is 6:1, the second core material solution in step (1) is joined in the second wall material solution in step (2), fully stir, mix to emulsion form, then homogenize, obtain the second mixed solution; According to the wall material core ratio that mass ratio is 8:1, the 3rd core material solution in step (1) is joined in the first wall material solution in step (2), fully stir, mix to emulsion form, then homogenize, obtain the 3rd mixed solution; According to the wall material core ratio that mass ratio is 8:1, the 4th core material solution in step (1) is joined in the first wall material solution in step (2), fully stir, mix to emulsion form, then homogenize, obtain the 4th mixed solution; Wherein, what homogenize employing is twice homogenization, and the rotating speed of homogeneous is 5000r/min for the first time, and the duration is 10min; The rotating speed of second time homogeneous is 9000r/min, and the duration is 25min;
(4) spray drying process is then adopted to carry out drying to the first mixed solution, the second mixed solution, the 3rd mixed solution and the 4th mixed solution respectively, EAT time dry is 160 DEG C, leaving air temp is 70 DEG C, feed rate is 1ml/min, obtains the first microcapsule granule, the second microcapsule granule, the 3rd microcapsule granule and the 4th microcapsule granule after drying respectively;
(5) by the first microcapsule granule, the second microcapsule granule, the 3rd microcapsule granule and the 4th microcapsule granule in mass ratio for 8:3:5:1 mixes, mixing after encapsulation, obtain fish meal.
Embodiment 3
In the embodiment of the present invention, utilize collagen to produce the method for fish meal, comprise the following steps:
(1) core material solution preparation: take collagen 55 parts according to mass fraction, add suitable quantity of water, stir until dissolved to emulsion form, obtained first core material solution; Take phosphatide oil 2.5 parts and dehulled soybean meal 8 parts according to mass fraction, add suitable quantity of water, after heating, stir until dissolved to emulsion form, obtained second core material solution; Take alphalise starch 18 parts and Choline Chloride 0.8 part according to mass fraction, add suitable quantity of water, heating stirs until dissolved to emulsion form, obtained 3rd core material solution; Take vitamin mixtures 1.8 parts, mineral mixture 1.2 parts and compound probiotic 0.03 part according to mass fraction, add suitable quantity of water, stir until dissolved to emulsion form, obtained 4th core material solution; Vitamin mixtures is made up of vitamin A 8 parts, vitamin B5 15 parts, vitamin B12 0.028 part, Vitamin D5 part, vitamin E 80 parts, vitamin K7 part, 0.5 part, folic acid, thiamine 18 parts and inositol 160 parts according to the raw material of mass fraction; Mineral mixture is made up of 80 parts, sodium chloride, KI 0.03 part, sodium dihydrogen phosphate 180 parts, 65 parts, magnesium sulfate, 120 parts, potassium chloride, 40 parts, ferrous sulfate, 3 parts, zinc sulfate, manganese sulfate 0.3 part, 0.3 part, copper sulphate and cobalt chloride 0.8 part according to the raw material of mass fraction; Compound probiotic is bafillus natto, bacillus coagulans and saccharomycetic mixture;
(2) wall material solution preparation: get seawood meal 150 parts, xanthans 800 parts and glycerine 100 parts according to mass fraction, mix, add suitable quantity of water, make its swelling, dispersion, 50 DEG C of heating water baths make it fully be dissolved to emulsion form, obtained first wall material solution; Get polyvinyl alcohol 600 parts, under 95 DEG C of water bath condition, be dissolved in water, high-speed stirred, to fully dissolving, obtains the second wall material solution; Get Aquacoat 1000 parts, add water and stir 50min, obtained 3rd wall material solution;
(3) according to mass ratio be the wall material core ratio of 10:1, the first core material solution in step (1) joined in the 3rd wall material solution in step (2), fully stir, mix to emulsion form, then homogenize, obtain the first mixed solution; According to the wall material core ratio that mass ratio is 8:1, the second core material solution in step (1) is joined in the second wall material solution in step (2), fully stir, mix to emulsion form, then homogenize, obtain the second mixed solution; According to the wall material core ratio that mass ratio is 10:1, the 3rd core material solution in step (1) is joined in the first wall material solution in step (2), fully stir, mix to emulsion form, then homogenize, obtain the 3rd mixed solution; According to the wall material core ratio that mass ratio is 10:1, the 4th core material solution in step (1) is joined in the first wall material solution in step (2), fully stir, mix to emulsion form, then homogenize, obtain the 4th mixed solution; Wherein, what homogenize employing is twice homogenization, and the rotating speed of homogeneous is 6000r/min for the first time, and the duration is 8min; The rotating speed of second time homogeneous is 9500r/min, and the duration is 20min;
(4) spray drying process is then adopted to carry out drying to the first mixed solution, the second mixed solution, the 3rd mixed solution and the 4th mixed solution respectively, EAT time dry is 180 DEG C, leaving air temp is 85 DEG C, feed rate is 1.5ml/min, obtains the first microcapsule granule, the second microcapsule granule, the 3rd microcapsule granule and the 4th microcapsule granule after drying respectively;
(5) by the first microcapsule granule, the second microcapsule granule, the 3rd microcapsule granule and the 4th microcapsule granule in mass ratio for 10:7:10:1 mixes, mixing after encapsulation, obtain fish meal.
Buy with market
Fish meal foregoing invention embodiment prepared, as feed of throwing something and feeding, separately adopts small fish feed in contrast.Experimentation is as follows:
Mandarin fish is supported temporarily and chooses physique stalwartness after 20 days immediately, the fry of honey stomach uses fish as test, feeding experiment is carried out in ecological culture pond, linked network case in culturing pool, often organizes feed and establishes 3 repetitions, respectively select the mandarin fish that 100 tail specifications are close, point to support in the consistent net cage of 12 specifications.Continuous 24 hours blowing aerations in culturing pool, dissolved oxygen remains on more than 6mg/L, and morning every day, evening are respectively satiated with food and throw something and feed once, continue half an hour at every turn, once find dead fish, pull out in time and weigh.Cultivate after three months, measure the body weight of the mandarin fish of DIFFERENT FEED group of ingesting respectively.Data mean+SD represents.Result of the test is as shown in table 1 below, and as can be seen from the table, the feed coefficient of experimental group is lower than control group, and rate of body weight gain is higher than control group, and show that this fish meal can promote growing of mandarin fish, the utilization rate of feed is high.Therefore, the present invention can improve the situation of aquaculture, saved feed and enhanced productivity after utilizing collagen to make microencapsulation feed, reduces aquaculture to the pollution of environment.
Fish meal prepared by table 1 embodiment 1-3 and the mandarin fish growing state that control feed is fed
| Group | Initial weight (g) | Eventually heavy (g) | Rate of body weight gain | Feed coefficient |
| Embodiment 1 | 5.494 | 89.49 | 16.29 | 3.20 |
| Embodiment 2 | 5.505 | 78.96 | 14.34 | 3.65 |
| Embodiment 3 | 5.495 | 83.15 | 13.97 | 3.74 |
| Control feed | 5.502 | 62.85 | 11.42 | 4.58 |
To those skilled in the art, obviously the invention is not restricted to the details of above-mentioned one exemplary embodiment, and when not deviating from spirit of the present invention or essential characteristic, the present invention can be realized in other specific forms.Therefore, no matter from which point, all should embodiment be regarded as exemplary, and be nonrestrictive, scope of the present invention is limited by claims instead of above-mentioned explanation, and all changes be therefore intended in the implication of the equivalency by dropping on claim and scope are included in the present invention.
In addition, be to be understood that, although this description is described according to embodiment, but not each embodiment only comprises an independently technical scheme, this narrating mode of description is only for clarity sake, those skilled in the art should by description integrally, and the technical scheme in each embodiment also through appropriately combined, can form other embodiments that it will be appreciated by those skilled in the art that.
Claims (10)
1. utilize collagen to produce the method for fish meal, it is characterized in that, comprise the following steps:
(1) core material solution preparation: take collagen 40-55 part according to mass fraction, add suitable quantity of water, stir until dissolved to emulsion form, obtained first core material solution; Take phosphatide oil 1-2.5 part and dehulled soybean meal 5-8 part according to mass fraction, add suitable quantity of water, after heating, stir until dissolved to emulsion form, obtained second core material solution; Take alphalise starch 18-25 part and Choline Chloride 0.5-0.8 part according to mass fraction, add suitable quantity of water, heating stirs until dissolved to emulsion form, obtained 3rd core material solution; Take vitamin mixtures 1.5-1.8 part, mineral mixture 0.5-1.2 part and compound probiotic 0.02-0.03 part according to mass fraction, add suitable quantity of water, stir until dissolved to emulsion form, obtained 4th core material solution;
(2) wall material solution preparation: get seawood meal, xanthans and glycerine, mix, add suitable quantity of water, make its swelling, dispersion, 45-50 DEG C of heating water bath makes it fully be dissolved to emulsion form, obtained first wall material solution; Get polyvinyl alcohol, under 90-95 DEG C of water bath condition, be dissolved in water, high-speed stirred, to fully dissolving, obtains the second wall material solution; Get Aquacoat, add water and stir 20-50min, obtained 3rd wall material solution;
(3) according to mass ratio be the wall material core ratio of 8-10:1, the first core material solution in step (1) joined in the 3rd wall material solution in step (2), fully stir, mix to emulsion form, then homogenize, obtain the first mixed solution; According to the wall material core ratio that mass ratio is 6-8:1, the second core material solution in step (1) is joined in the second wall material solution in step (2), fully stir, mix to emulsion form, then homogenize, obtain the second mixed solution; According to the wall material core ratio that mass ratio is 8-10:1, the 3rd core material solution in step (1) is joined in the first wall material solution in step (2), fully stir, mix to emulsion form, then homogenize, obtain the 3rd mixed solution; According to the wall material core ratio that mass ratio is 8-10:1, the 4th core material solution in step (1) is joined in the first wall material solution in step (2), fully stir, mix to emulsion form, then homogenize, obtain the 4th mixed solution;
(4) spray drying process is then adopted to carry out drying to the first mixed solution, the second mixed solution, the 3rd mixed solution and the 4th mixed solution respectively, EAT time dry is 160-180 DEG C, leaving air temp is 70-85 DEG C, feed rate is 1-1.5ml/min, obtains the first microcapsule granule, the second microcapsule granule, the 3rd microcapsule granule and the 4th microcapsule granule after drying respectively;
(5) by the first microcapsule granule, the second microcapsule granule, the 3rd microcapsule granule and the 4th microcapsule granule in mass ratio for 8-10:3-7:5-10:1 mixes, mixing after encapsulation, obtain fish meal.
2. the method utilizing collagen to produce fish meal according to claim 1, it is characterized in that, in described step (1), take collagen 48 parts according to mass fraction, phosphatide oil 1.8 parts, dehulled soybean meal 7 parts, alphalise starch be 22 parts, Choline Chloride is 0.65 part, vitamin mixtures is 1.7 parts, mineral mixture is 0.8 part and compound probiotic 0.025 part.
3. the method utilizing collagen to produce fish meal according to claim 1, it is characterized in that, described compound probiotic is one or more and saccharomycetic mixture in bafillus natto, bacillus coagulans, clostridium butyricum, lactic acid bacteria, Bifidobacterium and lactobacillus acidophilus.
4. the method utilizing collagen to produce fish meal according to claim 1, it is characterized in that, in described step (1), described vitamin mixtures is made up of vitamin A 4-8 part, vitamin B5 5-15 part, vitamin B12 0.02-0.028 part, calciferol-5 parts, vitamin E 60-80 part, Vitamin K4-7 parts, folic acid 0.2-0.5 part, thiamine 12-18 part and inositol 120-160 part according to the raw material of mass fraction.
5. the method utilizing collagen to produce fish meal according to claim 4, it is characterized in that, in described step (1), described vitamin mixtures is made up of vitamin A 6 parts, vitamin B5 10 parts, vitamin B12 0.025 part, vitamine D3 part, vitamin E 70 parts, vitamin K5 part, 0.4 part, folic acid, thiamine 15 parts and inositol 140 parts according to the raw material of mass fraction.
6. the method utilizing collagen to produce fish meal according to claim 1, it is characterized in that, in described step (1), described mineral mixture is made up of sodium chloride 40-80 part, KI 0.01-0.03 part, sodium dihydrogen phosphate 150-180 part, magnesium sulfate 50-65 part, potassium chloride 80-120 part, ferrous sulfate 20-40 part, zinc sulfate 2-3 part, manganese sulfate 0.2-0.3 part, copper sulphate 0.2-0.3 part and cobalt chloride 0.3-0.8 part according to the raw material of mass fraction.
7. the method utilizing collagen to produce fish meal according to claim 6, it is characterized in that, in described step (1), described mineral mixture is made up of 60 parts, sodium chloride, KI 0.02 part, sodium dihydrogen phosphate 160 parts, 60 parts, magnesium sulfate, 115 parts, potassium chloride, 30 parts, ferrous sulfate, 2.5 parts, zinc sulfate, manganese sulfate 0.25 part, 0.25 part, copper sulphate and cobalt chloride 0.5 part according to the raw material of mass fraction.
8. the method utilizing collagen to produce fish meal according to claim 1, is characterized in that, in described step (2), take seawood meal 80-150 part, xanthans 600-800 part and glycerine 80-100 part according to mass fraction; Polyvinyl alcohol 150-600 part, Aquacoat 850-1000 part.
9. the method utilizing collagen to produce fish meal according to claim 8, is characterized in that, in described step (2), take seawood meal 120 parts according to mass fraction, xanthans 700 parts and glycerine 90 parts; Polyvinyl alcohol is 350 parts, and Aquacoat is 900 parts.
10. the method utilizing collagen to produce fish meal according to claim 1, is characterized in that, in described step (3), what homogenize employing is twice homogenization, and the rotating speed of homogeneous is 5000-6000r/min for the first time, and the duration is 8-10min; The rotating speed of second time homogeneous is 9000-9500r/min, and the duration is 20-25min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510985598.9A CN105519819A (en) | 2015-12-25 | 2015-12-25 | Method for producing fish feed with collagen |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510985598.9A CN105519819A (en) | 2015-12-25 | 2015-12-25 | Method for producing fish feed with collagen |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105519819A true CN105519819A (en) | 2016-04-27 |
Family
ID=55762732
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510985598.9A Pending CN105519819A (en) | 2015-12-25 | 2015-12-25 | Method for producing fish feed with collagen |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105519819A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106591195A (en) * | 2016-12-29 | 2017-04-26 | 中国科学院水生生物研究所 | Microbial immunopotentiator applicable to aquatic animals and application of microbial immunopotentiator |
| CN109548711A (en) * | 2018-11-19 | 2019-04-02 | 浙江海洋大学 | Dragon design spot green-house scale cultural method |
| CN112755924A (en) * | 2021-01-04 | 2021-05-07 | 陕西科技大学 | Preparation method of vinyl collagen microspheres |
| CN115606716A (en) * | 2022-09-30 | 2023-01-17 | 广东越群生物科技股份有限公司 | Microcapsule fry feed free of starch and preparation method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4217370A (en) * | 1977-08-25 | 1980-08-12 | Blue Wing Corporation | Lipid-containing feed supplements and foodstuffs |
| CN101766260A (en) * | 2010-01-12 | 2010-07-07 | 海南大学 | Powdered tilapia oil and production method thereof |
| CN104605142A (en) * | 2015-02-27 | 2015-05-13 | 浙江海洋学院 | Processing technology of microcapsule grouper microparticle feed |
| CN104824376A (en) * | 2015-05-06 | 2015-08-12 | 宁德市夏威食品有限公司 | Production technology of complex-agglomerated micro-capsule fermented aquatic feed additive and additive |
| CN105410455A (en) * | 2015-11-30 | 2016-03-23 | 孙序元 | Ornamental demersal fish feed and preparation method thereof |
-
2015
- 2015-12-25 CN CN201510985598.9A patent/CN105519819A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4217370A (en) * | 1977-08-25 | 1980-08-12 | Blue Wing Corporation | Lipid-containing feed supplements and foodstuffs |
| CN101766260A (en) * | 2010-01-12 | 2010-07-07 | 海南大学 | Powdered tilapia oil and production method thereof |
| CN104605142A (en) * | 2015-02-27 | 2015-05-13 | 浙江海洋学院 | Processing technology of microcapsule grouper microparticle feed |
| CN104824376A (en) * | 2015-05-06 | 2015-08-12 | 宁德市夏威食品有限公司 | Production technology of complex-agglomerated micro-capsule fermented aquatic feed additive and additive |
| CN105410455A (en) * | 2015-11-30 | 2016-03-23 | 孙序元 | Ornamental demersal fish feed and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 冷向军等: "胶原蛋白部分替代鱼粉饲养异育银鲫的试验", 《水产科学》 * |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106591195A (en) * | 2016-12-29 | 2017-04-26 | 中国科学院水生生物研究所 | Microbial immunopotentiator applicable to aquatic animals and application of microbial immunopotentiator |
| CN106591195B (en) * | 2016-12-29 | 2019-10-08 | 中国科学院水生生物研究所 | It is a kind of suitable for the microorganism immunopotentiator of aquatic livestock and its application |
| CN109548711A (en) * | 2018-11-19 | 2019-04-02 | 浙江海洋大学 | Dragon design spot green-house scale cultural method |
| CN112755924A (en) * | 2021-01-04 | 2021-05-07 | 陕西科技大学 | Preparation method of vinyl collagen microspheres |
| CN115606716A (en) * | 2022-09-30 | 2023-01-17 | 广东越群生物科技股份有限公司 | Microcapsule fry feed free of starch and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103156092B (en) | Saltwater fish compound feed taking microalgae flour as fat source and processing method thereof | |
| CN102239968B (en) | Carnivorous fur-bearing animal feed and preparation method thereof | |
| CA2748979C (en) | Sodium stearoyl-2-lactylate derivatives as an animal feed additive for improving fat utilization efficiency | |
| CN103519007B (en) | A kind of pig farm special feed | |
| CN104719630A (en) | Poultry feed acidifier and preparation method thereof | |
| CN105519819A (en) | Method for producing fish feed with collagen | |
| CN102090540B (en) | Wenchang chicken feed containing corn starch and preparation method thereof | |
| CN108294191A (en) | A kind of sea cucumber fast growing period special compound feed and preparation method thereof | |
| CN104489405A (en) | Fish feed and production process thereof | |
| CN113115867A (en) | Rumen-bypass feed additive special for beef cattle and sheep in later fattening period and preparation method and application thereof | |
| CN102669478A (en) | Compound feed for piglets | |
| CN105166382A (en) | Powdered oil premix for feed | |
| CN103549163B (en) | Cherry Valley meat duck medium-stage feed | |
| CN105614028A (en) | Premixed feed for blue foxes in reproduction period and preparing method thereof | |
| CN102657300B (en) | Compound feed product for breastfeed suckling pigs | |
| CN106819472A (en) | One boar biological feedstuff and preparation method thereof, purposes | |
| CN104938863A (en) | Emulsified powdered oil and fat used for pig fodder and preparation method thereof | |
| CN118901900A (en) | Nutritional supplement for pet food | |
| CN104273385A (en) | Feed for young and female bamboo rats | |
| CN106721105A (en) | Expanded pellet feed of toad growth and preparation method thereof can be promoted | |
| CN111053162A (en) | Pet meal box mixed rice | |
| CN105076876A (en) | Schizothorax prenanti juvenile fish feed | |
| CN105961914A (en) | Eleutheronema tetradactylum low fish meal environment-friendly feed, and preparation and application method thereof | |
| CN104522325A (en) | A formula of sucking pig feed and a preparing method of the sucking pig feed | |
| CN108576467A (en) | It is a kind of using sweetgum leaf, chrysanthemum pears leaf, eaglewood leaf as chicken feed of raw material and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20160427 |
|
| RJ01 | Rejection of invention patent application after publication |