CN105496883A - Application of cinnamomum burmanii fruit extract to personal care product - Google Patents
Application of cinnamomum burmanii fruit extract to personal care product Download PDFInfo
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- CN105496883A CN105496883A CN201511005004.XA CN201511005004A CN105496883A CN 105496883 A CN105496883 A CN 105496883A CN 201511005004 A CN201511005004 A CN 201511005004A CN 105496883 A CN105496883 A CN 105496883A
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- personal care
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- 241000723347 Cinnamomum Species 0.000 title abstract 5
- 235000010208 anthocyanin Nutrition 0.000 claims abstract description 17
- 229930002877 anthocyanin Natural products 0.000 claims abstract description 17
- 239000004410 anthocyanin Substances 0.000 claims abstract description 17
- 150000004636 anthocyanins Chemical class 0.000 claims abstract description 17
- 239000000463 material Substances 0.000 claims description 21
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 18
- 239000000706 filtrate Substances 0.000 claims description 17
- XFZJEEAOWLFHDH-UHFFFAOYSA-N (2R,2'R,3R,3'R,4R)-3,3',4',5,7-Pentahydroxyflavan(48)-3,3',4',5,7-pentahydroxyflavan Natural products C=12OC(C=3C=C(O)C(O)=CC=3)C(O)CC2=C(O)C=C(O)C=1C(C1=C(O)C=C(O)C=C1O1)C(O)C1C1=CC=C(O)C(O)=C1 XFZJEEAOWLFHDH-UHFFFAOYSA-N 0.000 claims description 15
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- HGVVOUNEGQIPMS-UHFFFAOYSA-N procyanidin Chemical compound O1C2=CC(O)=CC(O)=C2C(O)C(O)C1(C=1C=C(O)C(O)=CC=1)OC1CC2=C(O)C=C(O)C=C2OC1C1=CC=C(O)C(O)=C1 HGVVOUNEGQIPMS-UHFFFAOYSA-N 0.000 claims description 15
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- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 description 2
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- 230000002292 Radical scavenging effect Effects 0.000 description 2
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- 102000019197 Superoxide Dismutase Human genes 0.000 description 2
- 108010012715 Superoxide dismutase Proteins 0.000 description 2
- BGNXCDMCOKJUMV-UHFFFAOYSA-N Tert-Butylhydroquinone Chemical compound CC(C)(C)C1=CC(O)=CC=C1O BGNXCDMCOKJUMV-UHFFFAOYSA-N 0.000 description 2
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- KIUKXJAPPMFGSW-DNGZLQJQSA-N (2S,3S,4S,5R,6R)-6-[(2S,3R,4R,5S,6R)-3-Acetamido-2-[(2S,3S,4R,5R,6R)-6-[(2R,3R,4R,5S,6R)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2-carboxylic acid Chemical compound CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 KIUKXJAPPMFGSW-DNGZLQJQSA-N 0.000 description 1
- NIXOWILDQLNWCW-UHFFFAOYSA-N Acrylic acid Chemical compound OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 1
- 239000004255 Butylated hydroxyanisole Substances 0.000 description 1
- 239000004322 Butylated hydroxytoluene Substances 0.000 description 1
- NLZUEZXRPGMBCV-UHFFFAOYSA-N Butylhydroxytoluene Chemical compound CC1=CC(C(C)(C)C)=C(O)C(C(C)(C)C)=C1 NLZUEZXRPGMBCV-UHFFFAOYSA-N 0.000 description 1
- 244000281594 Cassia siamea Species 0.000 description 1
- 240000004528 Catalpa ovata Species 0.000 description 1
- 235000010005 Catalpa ovata Nutrition 0.000 description 1
- 241000723346 Cinnamomum camphora Species 0.000 description 1
- 206010064571 Gene mutation Diseases 0.000 description 1
- 241000218195 Lauraceae Species 0.000 description 1
- 229920002125 Sokalan® Polymers 0.000 description 1
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- 230000003064 anti-oxidating effect Effects 0.000 description 1
- 230000003005 anti-senility effect Effects 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000000975 bioactive effect Effects 0.000 description 1
- 239000007853 buffer solution Substances 0.000 description 1
- 235000019282 butylated hydroxyanisole Nutrition 0.000 description 1
- CZBZUDVBLSSABA-UHFFFAOYSA-N butylated hydroxyanisole Chemical compound COC1=CC=C(O)C(C(C)(C)C)=C1.COC1=CC=C(O)C=C1C(C)(C)C CZBZUDVBLSSABA-UHFFFAOYSA-N 0.000 description 1
- 229940043253 butylated hydroxyanisole Drugs 0.000 description 1
- 235000010354 butylated hydroxytoluene Nutrition 0.000 description 1
- 229960001631 carbomer Drugs 0.000 description 1
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- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
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- MGJZITXUQXWAKY-UHFFFAOYSA-N diphenyl-(2,4,6-trinitrophenyl)iminoazanium Chemical compound [O-][N+](=O)C1=CC([N+](=O)[O-])=CC([N+]([O-])=O)=C1N=[N+](C=1C=CC=CC=1)C1=CC=CC=C1 MGJZITXUQXWAKY-UHFFFAOYSA-N 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
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- 239000000839 emulsion Substances 0.000 description 1
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- 230000003203 everyday effect Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 230000007760 free radical scavenging Effects 0.000 description 1
- 235000021022 fresh fruits Nutrition 0.000 description 1
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 230000003648 hair appearance Effects 0.000 description 1
- 229920002674 hyaluronan Polymers 0.000 description 1
- 229960003160 hyaluronic acid Drugs 0.000 description 1
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- 229910052757 nitrogen Inorganic materials 0.000 description 1
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- 239000000473 propyl gallate Substances 0.000 description 1
- 235000010388 propyl gallate Nutrition 0.000 description 1
- 229940075579 propyl gallate Drugs 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 238000012207 quantitative assay Methods 0.000 description 1
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- 230000005855 radiation Effects 0.000 description 1
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- 239000002562 thickening agent Substances 0.000 description 1
- 235000019165 vitamin E Nutrition 0.000 description 1
- 229940046009 vitamin E Drugs 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Dermatology (AREA)
- Biotechnology (AREA)
- Engineering & Computer Science (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Cosmetics (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention relates to application of cinnamomum burmanii fruit extract to a personal care product. The addition amount of the cinnamomum burmanii fruit extract to active matter of the personal care product ranges from 0.001wt% to 20wt%. Cinnamomum burmanii fruits contain rich antioxidant substances such as anthocyanin and procyanidine, and have the good function of scavenging free radicals. Active ingredients in the cinnamomum burmanii fruits are directly used in the personal care product in direct contact with the skin, and have no irritation to the skin.
Description
Technical field
The invention belongs to personal care articles field, relate to the application of a kind of cloudy Oleum Linderae extract in personal care articles particularly.
Background technology
Propose free radical theory according to Harman when studying Aging Mechanism, he thinks that the metabolic process of body all can produce various active oxygen species, contacts electromagenetic wave radiation, environmental pollution, chemicals in addition and also can generate a large amount of harmful free radical.Although organism has the system of defense maintaining poised state between oxidative and anti-oxidative, maintain the normal level of interior free yl, with advancing age, the pollution of environment, then a large amount of free radical produced in human body.Antioxidant system is not enough to scavenging free radicals, and balance will be destroyed, and causes free radical to be accumulated.These free radicals, especially reactive oxygen free radical, bring out lipid peroxidation, damage biological film; Cause protein-crosslinking to increase, enzymatic activity reduces; Damage dna, causes gene mutation, causes protein and enzymatic synthesis mistake, actively to reduce, finally cause cellular morphology, dysfunction, and even body aging, death.Antioxidant has the material catching free radical ability, can remove the living radical in skin, alleviate the skin oxidative stress damage that free radical causes, thus improve the skin aging caused by oxidative stress etc.There will be a known the scavenging free radicals type antioxidant in the organisms such as superoxide dismutase (SOD), vitamin E, vitamin C at present, in addition, also have the antioxidant propyl gallate of synthetic, TBHQ, BHT and Butylated hydroxyanisole, but because safety problem, the antioxidant of these synthesis is in use subject to the various restrictions of addition, scope of application aspect, therefore, develop to human-body safety, the antioxidant of natural origin more and more comes into one's own.
Cloudy fragrant, another name adhesion tree, Chinese catalpa Camphor tree, fragrant cassia tree, belong to Lauraceae xylophyta, mainly distribute the ground such as Guangdong, Fujian and Southeast Asia.Cloudy XIANGSHU aiphyllium, growing way is prosperous, strong stress resistance.Cloudy XIANGSHU ties a large amount of oval fruits every year, and be rich in anthocyanin procyanidin in cloudy Oleum Linderae meat, and fresh fruit sarcocarp water content is lower, storage tolerance is good.And cloudy Oleum Linderae is that be not utilized, valuable natural resources in fact always.Anthocyanin and procyanidin are all scavenging free radicals and antioxidative bioactive substance.Up to now, there is not yet the investigation and application of cloudy Oleum Linderae extract in personal care articles.Early stage, patent CN102276455A report utilized ultrasonic wave extraction to extract the real active ingredient of cloudy Oleum Linderae, but without subsequent treatment.Do not find the patent of cloudy fragrant extract for personal care articles aspect so far.
Summary of the invention
In order to solve the above-mentioned problems in the prior art, the invention provides the application of a kind of cloudy Oleum Linderae extract in personal care articles.
As follows in order to realize the technical scheme that above-mentioned technical purpose adopts:
The application of a kind of cloudy Oleum Linderae extract of the present invention in personal care articles, the addition of the active matter of described cloudy Oleum Linderae extract in personal care articles is 0.001 ~ 20wt%.
Particularly, described personal care articles comprises skin care item or daily article for washing.Preferably, described skin care item comprise facial treatment milk, cold cream frost, elite; Described daily article for washing comprises shampoo, clean product.
As one embodiment of the present invention, described personal care articles is skin care item, calculates comprise following component according to percentage by weight:
Further, described skin care item calculate according to percentage by weight and comprise following component in the present invention:
As another embodiment of the present invention, described personal care articles is articles for washing, calculates comprise following component according to percentage by weight:
Further, described personal care articles is articles for washing, calculates comprise following component according to percentage by weight:
All skin care item substrate of the present invention is selected as biological polyoses glue, surfactant, thickening suspending agent, emulsifing thickener, polyalcohols wetting agent, chelating agen, conditioner etc. all belong to conventional.
As preferred version of the present invention, described cloudy Oleum Linderae extract is prepared from by the following method:
1) by the oils and fats that cloudy smoked bean curd fruit granule squeezes out, through the remaining lipid material of petroleum ether backflow lixiviate 2 ~ 10 hours, then distilling under reduced pressure removing petroleum ether, distilling under reduced pressure removing petroleum ether, obtains fat free matter material powder;
2) by step 1) the fat free matter material powder of gained mixes by quality 1:5 ~ 20 with deionized water, carries out ultrasonic Treatment, colloid is liquefied, filter, and collects filtrate;
3) by step 2) gained filtrate loading chromatographic column, the ethanol water with 95% is stripping liquid, flow velocity 0.3 ~ 4 times of bed volume/hour, the anthocyanin that desorbing resin adsorbs and procyanidin, collect the stripping liquid containing anthocyanin and procyanidin; Filtrate is carried out distilling under reduced pressure and is reclaimed alcoholic solvent, is reclaimed by alcoholic solvent in stripping liquid, dry, obtains anthocyanin and procyanidin mixing powdery.
As preferably, step 1) in, the condition of lixiviate is: temperature 90 DEG C, time 60min, citric acid 0.6%, solid-liquid ratio 1: 3, and the filtrate obtained is at 30 ~ 60 DEG C, distilling under reduced pressure removing petroleum ether under vacuum-0.07 ~-0.09MPa.
As preferably, step 3) in, the ethanol water with 95% is stripping liquid, filtrate 60 DEG C, under vacuum-0.09MPa distilling under reduced pressure reclaim alcoholic solvent, make the determining alcohol of filtrate be down to 9.5%, anthocyanin and procyanidin mixing powdery can be obtained obtaining.
Beneficial effect of the present invention is as described below:
Cloudy Oleum Linderae of the present invention contains abundant antioxidant as anthocyanin, procyanidin etc., has the function of good scavenging free radicals.Anthocyanin during cloudy Oleum Linderae is real is to the suppression ratio IC of free radical
50=2.7 μ g/mL are that vitamin C is to 3 of free radical suppression ratio times.Active component (active component is anthocyanin, these two kinds of compositions of procyanidin mainly) in cloudy Oleum Linderae is directly used in directly and in the personal care articles of contact skin, has no stimulation to skin by the present invention.
figure of description
Fig. 1 is that the cloudy Oleum Linderae extract of variable concentrations of the present invention is to the design sketch of the scavenging capacity of DPPH free radical.
Detailed description of the invention
Set forth the present invention further below by specific embodiment, but the use of these embodiments only for being described in more detail, and shall not be applied to and limit the present invention in any form.
The preparation of cloudy Oleum Linderae extract
1, by the oils and fats that cloudy smoked bean curd fruit granule squeezes out, through the remaining lipid material of petroleum ether backflow lixiviate 2 ~ 10 hours, then by the filtrate that obtains at 30 ~ 60 DEG C, distilling under reduced pressure removing petroleum ether under vacuum-0.07 ~-0.09MPa, obtain fat free matter material powder;
2, the fat free matter material powder of step 1 gained is mixed by quality 1:5 ~ 20 with deionized water, carry out ultrasonic Treatment, colloid is liquefied, filter, collect filtrate;
3, step 2 gained filtrate is loaded chromatographic column, the ethanol water with 95% is stripping liquid, flow velocity 0.3 ~ 4 times of bed volume/hour, the anthocyanin that desorbing resin adsorbs and procyanidin, collect the stripping liquid containing anthocyanin and procyanidin; Filtrate 60 DEG C, under vacuum-0.09MPa distilling under reduced pressure reclaim alcoholic solvent, make the determining alcohol of filtrate be down to 9.5%, alcoholic solvent in stripping liquid reclaimed, dry, obtain anthocyanin and procyanidin mixing powdery.
Embodiment one, facial treatment milk containing cloudy Oleum Linderae extract
The raw material components table of the facial treatment milk of table 1 containing cloudy Oleum Linderae extract
Processing technology is as follows:
1, the feed components preparing facial treatment milk is weighed according to table 1, by A, B phase raw material, (wherein in B phase, xanthan gum should be pre-mixed evenly, add other component in B phase again) be heated to 75-80 DEG C respectively, be uniformly mixed, obtain A phase and B phase respectively.
2, start when stirring, A phase is slowly added B phase, with the speed homogenizing 1 minute of 2600rpa/min.
3, the stirring of step 2 gained material is cooled to 45 DEG C, adds each material in C phase, be cooled to room temperature, be up to the standards, discharging.
Embodiment two, containing cloudy Oleum Linderae extract cold cream frost
The raw material components table of the cold cream frost of table 2 containing cloudy Oleum Linderae extract
Processing technology is as follows:
1, each raw material components preparing cold cream frost is weighed according to table 2, by A, B phase raw material, (wherein the hyaluronic acid of A phase, xanthan gum and carbomer should be pre-mixed evenly, add other component of A phase again) be heated to 75-80 DEG C respectively, be uniformly mixed, obtain A phase and B phase respectively.
2, under startup stirring state, B phase is slowly added in A phase, then with 2800rpa/min speed homogenizing 2 minutes.
3, the stirring of step 2 gained material is cooled to 60 DEG C, adds C phase, stir.
4, be cooled to 45 DEG C, add D phase, stir and be cooled to room temperature, be up to the standards, discharging.
Embodiment three, shampoo containing cloudy Oleum Linderae extract
The raw material components table of the shampoo of table 3 containing cloudy Oleum Linderae extract
Processing technology is as follows:
1, weigh each raw material components preparing shampoo according to table 3, A phase material added reactor and disperse completely, stir simultaneously and add B phase material, be heated to 75-80 DEG C, be incubated 20-30 minutes, treat that material is uniformly dissolved completely.
2, open water quench, treat that temperature is down to about 50 DEG C, add C phase material, stir.
3, continue to be cooled to about 45 DEG C, add D phase material, stir.
4, be to be mixedly cooled to room temperature, be up to the standards, discharging.
Embodiment four, clean product containing cloudy Oleum Linderae extract
The raw material components table of clean the product of table 4 containing cloudy Oleum Linderae extract
Processing technology is as follows:
1, weigh each raw material components of preparation clean product according to table 4, A phase good for scale is added thermosol in water-bath, and bath temperature is about 85 DEG C, dissolves completely form homogeneous phase to A phase.
2, after the A phase in step 1 is dissolved completely, add sodium chloride (B phase), and start to lower the temperature 65 DEG C, stir with the speed of 1600rpa/min.
3, the material treating in step 2 is cooled to about 50 DEG C and adds C phase, even with the speed dispersed with stirring of 2000rpa/min.
4, treat step 3 obtain material and be cooled to about 45 DEG C and add D phase, be stirred to knot cream even, be up to the standards, discharging.
effect example
effect one, cloudy Oleum Linderae extract scavenging ability of DPPH free radical are tested
1,1-diphenyl-2-trinitrophenyl-hydrazine (1,1-Diphenyl-2-picrylhydrazylradical2,2-Diphenyl-1-(2,4,6-trinitrophenyl) hydrazyl, DPPH) is a kind of stable nitrogen center organic free radical.DPPH method was suggested in 1958, was widely used in the oxidation resistance of quantitative assay Biosample, classification material and food.
1, with the DPPH solution of dehydrated alcohol preparation 0.1mmol/L, keep in Dark Place.The detected solution of preparation 0.5mg/ml.
2,2ml is tested sample (test sample come from embodiment one) solution and 2mlDPPH solution adds in same test tube, shake up, room temperature measures its absorbance A 1 after leaving standstill 30min, Simultaneously test 2ml tests sample solution and the mixed absorbance A 2 of 2ml dehydrated alcohol, and the absorbance A 3 that 2mlDPPH solution mixes with 2ml solvent (distilled water or corresponding buffer solution).
3, the expression of radical scavenging activity:
Clearance rate (%)=[1-(A1-A2)/A3] × 100%
As seen from Figure 1, cloudy Oleum Linderae extract is to the IC of DPPH free radical scavenging
50value is 0.05%, has good DPPH radical scavenging activity, can be used as effective antioxidant, as preventing skin ageing, maintaining the antioxidant activity thing use of the skin state of young healthy, can strengthen hair quality, anti-jag etc. in hair products.
effect example two, senile-resistant efficacy are tested
The cloudy Oleum Linderae extract used in the present invention, can as the both effectiveness raw material of scavenging free radicals, antioxidation and anti-aging cosmetics, and its type of service does not have particular/special requirement, it may be used for water preparation, cream, emulsion, elite, shampoo, in the personal care articles of the various different dosage form such as cleansing milk.Use facial treatment milk in the present invention's application Antisenility Experiment, formula is the formula composition in application example one, and wherein cloudy Oleum Linderae extractive content is 10.0wt%.
Tested crowd: healthy volunteer 15 people, 35 ~ 50 years old age.
The method of appraisal procedure and judging quota: winter carries out body build-in test 20 ages between the women of 35 to 50 years old, experimenter uses given the test agent every day 2 times, continue 60 days, face uses the facial treatment milk of embodiment one, uses contrast facial treatment milk at another half of face.
Evaluation criterion: 1, trier evaluates autologous skin change; 2, medical practitioner is contrasted the face-image that trier tries out front and back by graphical analysis instrument VISIA (German CK Company, Instrument), provides evaluation.
Evaluation result: 1, the trier of 95% has been evaluated as larger improvement to autologous skin, be specially and use the face of this anti-aging skin care product glossy, wrinkle of skin is improved.2, medical practitioner evaluation, trier's facial wrinkles of 90% is improved, and skin shine improves, and it is level and smooth that skin becomes, and anti-aging effects is more obvious.
Above result shows: the present invention is best result of use containing the personal care articles of the cloudy Oleum Linderae extract of 10.0wt%, specifies in content range, all effectively can improve skin shine, improve wrinkle, delay skin aging in the present invention.
Obviously, the above embodiment of the present invention is only for example of the present invention is clearly described, and is not the restriction to embodiments of the present invention.For those of ordinary skill in the field, can also make other changes in different forms on the basis of the above description.Here cannot give exhaustive to all embodiments.Every belong to technical scheme of the present invention the apparent change of extending out or variation be still in the row of protection scope of the present invention.
Claims (9)
1. the application of cloudy Oleum Linderae extract in personal care articles, is characterized in that, the addition of the active matter of described cloudy Oleum Linderae extract in personal care articles is 0.001 ~ 20wt%.
2. application according to claim 1, is characterized in that, described personal care articles comprises skin care item or daily article for washing.
3. application according to claim 2, is characterized in that, described personal care articles is skin care item, calculates comprise following component according to percentage by weight:
4. application according to claim 3, is characterized in that, described skin care item calculate according to percentage by weight and comprise following component:
5. application according to claim 2, is characterized in that, described personal care articles is articles for washing, calculates comprise following component according to percentage by weight:
6. application according to claim 5, is characterized in that, described personal care articles is articles for washing, calculates comprise following component according to percentage by weight:
7. according to the application in claim 1 ~ 6 described in any one, it is characterized in that, described cloudy Oleum Linderae extract is prepared from by the following method:
1) by the oils and fats that cloudy smoked bean curd fruit granule squeezes out, through the remaining lipid material of petroleum ether backflow lixiviate 2 ~ 10 hours, then distilling under reduced pressure removing petroleum ether, obtained fat free matter material powder;
2) by step 1) the fat free matter material powder of gained mixes by quality 1:5 ~ 20 with deionized water, carries out ultrasonic Treatment, colloid is liquefied, filter, and collects filtrate;
3) by step 2) gained filtrate loading chromatographic column, the ethanol water with 95% is stripping liquid, flow velocity 0.3 ~ 4 times of bed volume/hour, the anthocyanin that desorbing resin adsorbs and procyanidin, collect the stripping liquid containing anthocyanin and procyanidin; Filtrate is carried out distilling under reduced pressure and is reclaimed alcoholic solvent, is reclaimed by alcoholic solvent in stripping liquid, dry, obtains anthocyanin and procyanidin mixing powdery.
8. application according to claim 7, it is characterized in that: step 1) in, the condition of lixiviate is: temperature 90 DEG C, time 60min, citric acid 0.6%, solid-liquid ratio 1: 3, and the filtrate obtained is at 30 ~ 60 DEG C, distilling under reduced pressure removing petroleum ether under vacuum-0.07 ~-0.09MPa.
9. application according to claim 7, it is characterized in that: step 3) in, ethanol water with 95% is stripping liquid, filtrate 60 DEG C, under vacuum-0.09MPa distilling under reduced pressure reclaim alcoholic solvent, make the determining alcohol of filtrate be down to 9.5%, anthocyanin and procyanidin mixing powdery can be obtained obtaining.
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| CN118120871A (en) * | 2024-05-07 | 2024-06-04 | 云南省农业科学院农产品加工研究所 | Color protecting composition and preparation method thereof |
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