CN105462373A - Ultraviolet-resistant paint and preparation method thereof - Google Patents
Ultraviolet-resistant paint and preparation method thereof Download PDFInfo
- Publication number
- CN105462373A CN105462373A CN201511015543.1A CN201511015543A CN105462373A CN 105462373 A CN105462373 A CN 105462373A CN 201511015543 A CN201511015543 A CN 201511015543A CN 105462373 A CN105462373 A CN 105462373A
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- parts
- coating
- sulfonate
- antioxidant
- aging agent
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/32—Radiation-absorbing paints
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D105/00—Coating compositions based on polysaccharides or on their derivatives, not provided for in groups C09D101/00 or C09D103/00
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/48—Stabilisers against degradation by oxygen, light or heat
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Coating Of Shaped Articles Made Of Macromolecular Substances (AREA)
- Paints Or Removers (AREA)
- Polarising Elements (AREA)
Abstract
The invention discloses an ultraviolet-resistant paint which is prepared from the following raw materials in parts by weight: 0.75-2.15 parts of anti-aging agent, 1.2-2.3 parts of ethylene glycol monophenyl ether, 4-6.7 parts of triethanolamine oleate saponin, 0.23-0.76 part of antioxidant, 0.12-0.25 part of nekal formaldehyde condensate, 3.5-5.5 parts of 2,6-tert-butyl-4-methylphenol, 4-7.5 parts of sodium petroleum sulfonate and 2.45-4.36 parts of palm oil sodium fatty acid methyl ester sulfonate. The ultraviolet-resistant paint solves the technical problems of poor effects and single function when the existing like products are used in polarized lenses. When being coated on sunglasses and goggles, the prepared paint has the multiple functions of increasing hardness, resisting ultraviolet rays, eliminating glare, preventing vapor and absorbing infrared rays. The paint is suitable for polaroid substrates of sunglasses, goggles and the like, solves the actual demands, and is convenient for popularization and use.
Description
Technical field
The present invention relates to a kind of coating, especially relate to coating of a kind of antiultraviolet and preparation method thereof, belong to paint field.
Background technology
As everyone knows, polaroid is a kind of optical thin film being formed by layer high molecule Material cladding, have generation polarized light function, and it has important use in industries such as spectacles industry, optical instrument and display industry.But the simple polarized lenses that uses still has a lot of deficiency as sun glasses, as shielded ultraviolet, dazzle, the intensity of light polarizing film own cannot be eliminated completely, hardness is not high, scratch resistance is bad, easy water suction and make returning of polarization characteristic etc., therefore need with other materials with the use of.People require to include sun glasses or safety goggles: lower light intensity, shielding ultraviolet rays, elimination dazzle, not easily occur the requirements such as scratch, and this needs coating on polarized sunglasses to be applicable to coating, to reach above-mentioned multiple effect.But a lot of coating for eyeglass mainly concentrates at present increases eyeglass hardness, improve scratch resistance, and to eyeglass ultraviolet shielded, eliminate the aspects such as dazzle and do not have help.
Summary of the invention
For the deficiencies in the prior art, technical problem to be solved by this invention is, coating of a kind of antiultraviolet and preparation method thereof is provided, the transparency good, hardness is high, rub resistance, film Hardening, antiultraviolet, elimination dazzle, solve the technical problem of existing like product for polarized lenses less effective, function singleness.
For solving the problems of the technologies described above, the technical scheme that the present invention takes is, a kind of coating of antiultraviolet, and it is made up of the raw material of following parts by weight:
Anti-aging agent 0.75-2.15 part, ethylene glycol phenyl ether 1.2-2.3 part, triethanolamine oleate glycosides 4-6.7 part, antioxidant 0.23-0.76 part, sodium dibutyl naphthalene sulfonate formaldehyde condensation products 0.12-0.25 part, 2,6-, tri-grades of butyl-4-methylphenol 3.5-5.5 parts, petroleum sodium sulfonate 4-7.5 part, palm oil fatty acid methyl ester sulfonate 2.45-4.36 part.
Optimize, the coating of above-mentioned antiultraviolet, it is made up of the raw material of following parts by weight:
0.75 part, anti-aging agent, ethylene glycol phenyl ether 1.2 parts, triethanolamine oleate glycosides 4 parts, antioxidant 0.23 part, sodium dibutyl naphthalene sulfonate formaldehyde condensation products 0.12 part, 2,6-tri-grades of butyl-4-methylphenols 3.5 parts, petroleum sodium sulfonate 4 parts, palm oil fatty acid methyl ester sulfonate 2.45 parts.
Optimize, the coating of above-mentioned antiultraviolet, its anti-aging agent is octylated diphenylamine.
Optimize, the coating of above-mentioned antiultraviolet, its antioxidant is butylated hydroxytoluene.
A preparation method for the coating of antiultraviolet, comprises the following steps:
1) take anti-aging agent and ethylene glycol phenyl ether by above-mentioned formula ratio, after adding triethanolamine oleate glycosides and antioxidant, one piece is placed in reactor, is heated to 50-60 DEG C, is incubated and leaves standstill 2-3 hour after 1-2 hour stirs;
2) the sodium dibutyl naphthalene sulfonate formaldehyde condensation products of formula ratio and 2,6-, tri-grades of butyl-4-methylphenols are added reactor, carry out dispersion with 500-600r/min and stir 15-20min, be then heated to 65-70 DEG C;
3) mixed emulsion is cooled to 15-20 DEG C, takes petroleum sodium sulfonate by formula ratio, add in the mixture in previous step, carry out dispersion with 400-500r/min and stir 20-25min;
4) take the palm oil fatty acid methyl ester sulfonate of formula ratio, carry out dispersion with 500-600r/min and stir 10-15min,
Be heated to 40-45 DEG C, be cooled to room temperature after insulation 10-20min, then pack, stamp, inspection, gets product.
The present invention has following positive effect: solve the technical problem of existing like product for polarized lenses less effective and function singleness, obtained coating material has Hardening, antiultraviolet, elimination dazzle, anti-steam, the ultrared multi-functional of absorption after sun glasses and safety goggles, be applicable to the polarizer substrate material such as sun glasses and safety goggles, solve actual demand, be convenient to promote the use of.
Embodiment
Below in conjunction with embodiment, invention is further described.
Embodiment 1
The present invention is a kind of coating of antiultraviolet, it is made up of the raw material of following parts by weight: anti-aging agent and octylated diphenylamine 0.75 part, ethylene glycol phenyl ether 1.2 parts, triethanolamine oleate glycosides 4 parts, antioxidant 0.23 part, sodium dibutyl naphthalene sulfonate formaldehyde condensation products 0.12 part, 2,6-tri-grades of butyl-4-methylphenols 3.5 parts, petroleum sodium sulfonate 4 parts, palm oil fatty acid methyl ester sulfonate 2.45 parts.Antioxidant is butylated hydroxytoluene.
The preparation method of the above-mentioned coating for antiultraviolet, comprises the following steps:
1) take anti-aging agent and ethylene glycol phenyl ether by above-mentioned formula ratio, after adding triethanolamine oleate glycosides and antioxidant, one piece is placed in reactor, is heated to 50 DEG C, is incubated and leaves standstill 2 hours after 1 hour stirs;
2) the sodium dibutyl naphthalene sulfonate formaldehyde condensation products of formula ratio and 2,6-, tri-grades of butyl-4-methylphenols are added reactor, carry out dispersion with 500r/min and stir 15min, be then heated to 65 DEG C;
3) mixed emulsion is cooled to 15 DEG C, takes petroleum sodium sulfonate by formula ratio, add in the mixture in previous step, carry out dispersion with 400r/min and stir 20min;
4) take the palm oil fatty acid methyl ester sulfonate of formula ratio, carry out dispersion with 500r/min and stir 10min,
Be heated to 4 DEG C, be cooled to room temperature after insulation 10min, then pack, stamp, inspection, gets product.Embodiment 2
The present invention is a kind of coating of antiultraviolet, it is made up of the raw material of following parts by weight: anti-aging agent and octylated diphenylamine 2.15 parts, ethylene glycol phenyl ether 2.3 parts, triethanolamine oleate glycosides 6.7 parts, antioxidant 0.76 part, sodium dibutyl naphthalene sulfonate formaldehyde condensation products 0.25 part, 2,6-tri-grades of butyl-4-methylphenols 5.5 parts, petroleum sodium sulfonate 7.5 parts, palm oil fatty acid methyl ester sulfonate 4.36 parts.Antioxidant is butylated hydroxytoluene.
The preparation method of the coating of above-mentioned antiultraviolet, comprises the following steps:
1) take anti-aging agent and ethylene glycol phenyl ether by above-mentioned formula ratio, after adding triethanolamine oleate glycosides and antioxidant, one piece is placed in reactor, is heated to 55 DEG C, is incubated and leaves standstill 2.5 hours after 1.5 hours stir;
2) the sodium dibutyl naphthalene sulfonate formaldehyde condensation products of formula ratio and 2,6-, tri-grades of butyl-4-methylphenols are added reactor, carry out dispersion with 550r/min and stir 17min, be then heated to 67 DEG C;
3) mixed emulsion is cooled to 16 DEG C, takes petroleum sodium sulfonate by formula ratio, add in the mixture in previous step, carry out dispersion with 440r/min and stir 22min;
4) take the palm oil fatty acid methyl ester sulfonate of formula ratio, carry out dispersion with 540r/min and stir 12min,
Be heated to 402 DEG C, be cooled to room temperature after insulation 13min, then pack, stamp, inspection, gets product.
Embodiment 3
The present invention is a kind of coating of antiultraviolet, it is made up of the raw material of following parts by weight: anti-aging agent and octylated diphenylamine 1.15 parts, ethylene glycol phenyl ether 1.8 parts, triethanolamine oleate glycosides 5.7 parts, antioxidant 0.46 part, sodium dibutyl naphthalene sulfonate formaldehyde condensation products 0.18 part, 2,6-tri-grades of butyl-4-methylphenols 4.6 parts, petroleum sodium sulfonate 5.5 parts, palm oil fatty acid methyl ester sulfonate 3.05 parts.Antioxidant is butylated hydroxytoluene.
The preparation method of the coating of above-mentioned antiultraviolet, comprises the following steps:
1) take anti-aging agent and ethylene glycol phenyl ether by above-mentioned formula ratio, after adding triethanolamine oleate glycosides and antioxidant, one piece is placed in reactor, is heated to 60 DEG C, is incubated and leaves standstill 3 hours after 2 hours stir;
2) the sodium dibutyl naphthalene sulfonate formaldehyde condensation products of formula ratio and 2,6-, tri-grades of butyl-4-methylphenols are added reactor, carry out dispersion with 600r/min and stir 20min, be then heated to 70 DEG C;
3) mixed emulsion is cooled to 20 DEG C, takes petroleum sodium sulfonate by formula ratio, add in the mixture in previous step, carry out dispersion with 500r/min and stir 25min;
4) take the palm oil fatty acid methyl ester sulfonate of formula ratio, carry out dispersion with 600r/min and stir 15min,
Be heated to 45 DEG C, be cooled to room temperature after insulation 20min, then pack, stamp is checked, and gets product.
The finished product prepared by embodiment 1-3 carries out the test of following table properties, the results are shown in Table 1:
Can find out, indices all conformance with standard of coating of the present invention, have very strong abrasion resistance and wear resistance etc.The invention solves the technical problem of existing like product for polarized lenses less effective and function singleness, obtained coating material has Hardening, antiultraviolet, elimination dazzle, anti-steam, the ultrared multi-functional of absorption after sun glasses and safety goggles, be applicable to the polarizer substrate material such as sun glasses and safety goggles, solve actual demand, be convenient to promote the use of.
To the above-mentioned explanation of the disclosed embodiments, professional and technical personnel in the field are realized or uses the present invention.To be apparent for those skilled in the art to the multiple amendment of these embodiments, General Principle as defined herein can without departing from the spirit or scope of the present invention, realize in other embodiments.Therefore, the present invention can not be restricted to these embodiments shown in this article, but will meet the widest scope consistent with principle disclosed herein and features of novelty.
Claims (5)
1. a coating for antiultraviolet, is characterized in that:
Be made up of the raw material of following parts by weight: anti-aging agent 0.75-2.15 part, ethylene glycol phenyl ether 1.2-2.3 part, triethanolamine oleate glycosides 4-6.7 part, antioxidant 0.23-0.76 part, sodium dibutyl naphthalene sulfonate formaldehyde condensation products 0.12-0.25 part, 2,6-, tri-grades of butyl-4-methylphenol 3.5-5.5 parts, petroleum sodium sulfonate 4-7.5 part, palm oil fatty acid methyl ester sulfonate 2.45-4.36 part.
2. the coating of antiultraviolet according to claim 1, is characterized in that:
Be made up of the raw material of following parts by weight: 0.75 part, anti-aging agent, ethylene glycol phenyl ether 1.2 parts, triethanolamine oleate glycosides 4 parts, antioxidant 0.23 part, sodium dibutyl naphthalene sulfonate formaldehyde condensation products 0.12 part, 2,6-, tri-grades of butyl-4-methylphenols 3.5 parts, petroleum sodium sulfonate 4 parts, palm oil fatty acid methyl ester sulfonate 2.45 parts.
3. the coating of antiultraviolet according to claim 1, is characterized in that: described anti-aging agent is octylated diphenylamine.
4. the coating of antiultraviolet according to claim 1, is characterized in that: described antioxidant is butylated hydroxytoluene.
5. the preparation method of the coating of the antiultraviolet according to any one of claim 1-4, comprises the following steps:
1) take anti-aging agent and ethylene glycol phenyl ether by above-mentioned formula ratio, after adding triethanolamine oleate glycosides and antioxidant, one piece is placed in reactor, is heated to 50-60 DEG C, is incubated and leaves standstill 2-3 hour after 1-2 hour stirs;
2) the sodium dibutyl naphthalene sulfonate formaldehyde condensation products of formula ratio and 2,6-, tri-grades of butyl-4-methylphenols are added reactor, carry out dispersion with 500-600r/min and stir 15-20min, be then heated to 65-70 DEG C;
3) mixed emulsion is cooled to 15-20 DEG C, takes petroleum sodium sulfonate by formula ratio, add in the mixture in previous step, carry out dispersion with 400-500r/min and stir 20-25min;
4) take the palm oil fatty acid methyl ester sulfonate of formula ratio, carry out dispersion with 500-600r/min and stir 10-15min,
Be heated to 40-45 DEG C, be cooled to room temperature after insulation 10-20min, then pack, stamp, inspection, gets product.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201511015543.1A CN105462373A (en) | 2015-12-30 | 2015-12-30 | Ultraviolet-resistant paint and preparation method thereof |
| PCT/CN2016/112043 WO2017114343A1 (en) | 2015-12-30 | 2016-12-26 | Anti-ultraviolet coating and preparation method therefor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201511015543.1A CN105462373A (en) | 2015-12-30 | 2015-12-30 | Ultraviolet-resistant paint and preparation method thereof |
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| Publication Number | Publication Date |
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| CN105462373A true CN105462373A (en) | 2016-04-06 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201511015543.1A Pending CN105462373A (en) | 2015-12-30 | 2015-12-30 | Ultraviolet-resistant paint and preparation method thereof |
Country Status (2)
| Country | Link |
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| CN (1) | CN105462373A (en) |
| WO (1) | WO2017114343A1 (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2017114343A1 (en) * | 2015-12-30 | 2017-07-06 | 曲少春 | Anti-ultraviolet coating and preparation method therefor |
| CN108003668A (en) * | 2017-12-15 | 2018-05-08 | 江苏黄金屋光学眼镜股份有限公司 | A kind of yellowing-resistant ultraviolet-proof |
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2016
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2017114343A1 (en) * | 2015-12-30 | 2017-07-06 | 曲少春 | Anti-ultraviolet coating and preparation method therefor |
| CN108003668A (en) * | 2017-12-15 | 2018-05-08 | 江苏黄金屋光学眼镜股份有限公司 | A kind of yellowing-resistant ultraviolet-proof |
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| Publication number | Publication date |
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| WO2017114343A1 (en) | 2017-07-06 |
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Application publication date: 20160406 |