CN105457575B - Chloride final product quality control technique - Google Patents
Chloride final product quality control technique Download PDFInfo
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- CN105457575B CN105457575B CN201410463324.9A CN201410463324A CN105457575B CN 105457575 B CN105457575 B CN 105457575B CN 201410463324 A CN201410463324 A CN 201410463324A CN 105457575 B CN105457575 B CN 105457575B
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- Prior art keywords
- medium
- pipeline
- thermostatic
- condenser
- temperature
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- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 title claims abstract description 16
- 239000012467 final product Substances 0.000 title claims abstract description 8
- 238000003908 quality control method Methods 0.000 title claims abstract description 6
- 238000005660 chlorination reaction Methods 0.000 claims abstract description 22
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims abstract description 21
- 229910052801 chlorine Inorganic materials 0.000 claims abstract description 21
- 239000000460 chlorine Substances 0.000 claims abstract description 21
- 239000000463 material Substances 0.000 claims abstract description 20
- 238000000034 method Methods 0.000 claims abstract description 13
- 238000006243 chemical reaction Methods 0.000 claims abstract description 12
- 238000004519 manufacturing process Methods 0.000 claims abstract description 10
- 239000002609 medium Substances 0.000 claims description 148
- 239000011521 glass Substances 0.000 claims description 43
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 33
- 238000001816 cooling Methods 0.000 claims description 18
- 238000010438 heat treatment Methods 0.000 claims description 10
- 238000010521 absorption reaction Methods 0.000 claims description 6
- 238000007664 blowing Methods 0.000 claims description 6
- 239000012913 medium supplement Substances 0.000 claims description 6
- 230000007774 longterm Effects 0.000 claims description 3
- 239000002994 raw material Substances 0.000 claims description 3
- 230000006641 stabilisation Effects 0.000 abstract description 6
- 238000011105 stabilization Methods 0.000 abstract description 6
- 239000000047 product Substances 0.000 abstract description 5
- 239000012535 impurity Substances 0.000 abstract description 3
- 238000004880 explosion Methods 0.000 description 4
- OISVCGZHLKNMSJ-UHFFFAOYSA-N 2,6-dimethylpyridine Chemical class CC1=CC=CC(C)=N1 OISVCGZHLKNMSJ-UHFFFAOYSA-N 0.000 description 2
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 235000019628 coolness Nutrition 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
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- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The present invention relates to a kind of chloride final product quality control technique, it is that material is put into chlorination tank, start thermostatic medium, thermostatic medium flows to thermostatic medium heat exchanger and thermostatic medium condenser by chlorination tank chuck, thermostatic medium heat exchange station is flowed to again, reusable heat medium is heated to thermostatic medium, when temperature reaches needs temperature, stop being heated to thermostatic medium, reactor starts logical chlorine, is circulated using the reaction liberated heat of reactor, the heat being more than that reactor is released, partial heat is absorbed by cycle condenser, temperature adjustment is carried out with circulation heat exchanger.The invention is once heated using external heat source in the logical chlorine process of chloride production to thermostatic medium, be not required to be switched with cold and hot medium control the temperature of reactor, medium is in certain temperature range interior circulation, it is ensured that chlorination temperature in the kettle it is constant, the temperature difference is small, thermal loss is constant, reduces impurity wind, the flat permanent and conversion ratio stabilization of chemistry, improve product quality, process is simple, it is easy to operate, it is pollution-free.
Description
Technical field
The present invention relates to a kind of chloride final product quality control technique.
Background technology
At present, the temperature of reactor is heated and chuck using electrical heating and coil pipe mostly in the logical chlorine process of chloride production
The mode of heating, is switched to control the temperature of reactor with cold and hot medium, and the temperature easily caused in reactor is unstable, is heated
Uneven, fast near heating sources heat transfer, slow away from thermal source heat transfer, difference variation is big, causes chemical balance and reaction rate unstable
Fixed, temperature control medium when chloride is generated uses water and conduction oil, and because the specific heat of water and conduction oil is excessive, flow velocity is too fast, makes
Unstable into thermal loss, flow takes away greatly that heat is more, and the small heat of taking away of flow is few, and thermal loss is more, under causing temperature in the kettle
Drop is fast, is unfavorable for chlorination reaction, changes chloride slow, influences yield, and thermal loss is few, causes temperature in the kettle high, chloride
Easily there is impurity wind, influence the content of product, tail gas generally intercepts material with glass condenser in chlorination reaction, due to
The freezing point of material is higher, wall built-up phenomenon easily occurs, and material hangs over and caused on the outer wall of coiled pipe and the inwall of condenser condensation
Device is blocked, and makes pressure rise in kettle, occurs blast when serious, and water, one are used the temperature-reducing medium in glass condenser coiled pipe more
The explosion of denier coiled pipe has substantial amounts of water into reactor, and the quality to material is impacted, such as temperature in the kettle more than 100 degree with
On, once being broken, water can become water vapour, set off an explosion coiled pipe, cause potential safety hazard, the normal production of influence.
The content of the invention
It is an object of the invention to overcome disadvantages mentioned above, there is provided a kind of chloride final product quality control technique, it is mainly solved
Determined the side that the temperature of reactor is heated using electrical heating and coil pipe heating and chuck mostly in the logical chlorine process of chloride production
Formula, is switched to control the temperature of reactor with cold and hot medium, and the temperature easily caused in reactor is unstable, is heated uneven,
Difference variation is big, causes that chemical balance and reaction rate are unstable, and condenser is easily blocked, and is set off an explosion, and safety in production is made
The problems such as being impacted to product quality after into influence and coiled pipe fracture.The object of the present invention is achieved like this, 1, first will
In raw material input chlorinating container, start thermostatic medium circulating pump and start the cycle over thermostatic medium, thermostatic medium is connected by pipeline
To the thermostatic medium outlet valve outflow that the thermostatic medium inlet valve of chlorinating container, thermostatic medium pass through chlorinating container chuck,
Thermostatic medium outlet valve and pipeline are connected, and are confluxed after flowing to thermostatic medium condenser and thermostatic medium air heat exchanger, by pipe
Road flows to thermostatic medium heat exchange station, and the thermostatic medium inlet valve and thermostatic medium outlet valve on kettle are normally opened；2nd, thermostatic medium is opened
Medium entrance valve on heat exchange station, gives thermostatic medium heat exchange station heat temperature raising, and thermal medium enters house steward and provides by thermal medium, by pipe
Road enters thermostatic medium heat exchange station, and house steward is returned by pipeline flow-direction thermal medium by medium after hot-cast socket, thermostatic medium heat exchange station
Medium supplement is supplemented by pipeline, when temperature reaches reaction requires temperature, stops heating thermostatic medium heat exchange station, is started
Self-loopa, constant temperature circulating medium heat is provided by reactor；3rd, the heat that chlorinating container is produced is in thermostatic medium air heat-exchange
Drive air to carry out hot-cast socket with blower fan at device to disperse heat, temp control indicator is housed on pipeline, control thermostatic medium is empty
The fan operation of gas heat exchanger, thermostatic medium condenser is that the auxiliary equipment of constant temperature is used to start when temperature rises too fast, permanent
Warm medium condenser enters house steward and flows to pipeline equipped with circulating water cooling pipeline by recirculated water, has been exchanged heat by thermostatic medium condenser
Pipeline recirculated water is connected to by pipeline after and returns house steward, thermostatic medium heat exchange station is furnished with auxiliary temperature-reducing pipeline, be constant temperature during parking
Media for heat exchange station lower the temperature, house steward's flow ipe is entered by cold medium, flow to thermostatic medium heat exchange station heat exchange after the completion of, by pipeline flow-direction
Pipeline cold medium returns house steward；4th, when occurring maloperation in production process, can cause temperature rise it is too fast, constant temperature circulating medium without
When method takes away heat, start cold medium circulation and lowered the temperature, cold medium is squeezed into by cold medium heat exchange station cold medium circulating pump
Pipeline, flows to pipeline cold medium and enters house steward, by pipeline flow-direction chlorinating container, through cold Jie of pipeline flow-direction pipeline after heat exchange completion
Matter returns house steward, then through pipeline flow-direction cold medium condenser, by flowing to cold medium heat exchange station after hot-cast socket, cold medium condenser is matched somebody with somebody
There is circulating water cooling, entering house steward by pipeline recirculated water flows to pipeline, after being exchanged heat through cold medium condenser, followed by pipeline flow-direction pipeline
Ring water returns house steward, and cold medium heat exchange station is furnished with circulating water cooling, enters house steward by pipeline recirculated water and flow to pipeline, is exchanged heat through cold medium
Stand after the completion of heat exchange, house steward is returned by pipeline flow-direction pipeline recirculated water, the medium supplement of cold medium heat exchange station returns house steward by thermal medium
Supplemented by pipeline；5th, continous way chlorination only needs long-term circulation constant temperature medium, and batch (-type) chlorination reaches end when reaction
Start cold medium during point to be lowered the temperature, cooling blowing is stopped when reaching blowing temperature；6th, in tail gas in logical chlorine process entrainment of
Substantial amounts of material, need to be intercepted with glass condenser, and tail gas enters glass condenser by chlorinating container by gas phase pipe, warp
Gas after glass condenser cooling is intercepted enters tail gas absorption, and vavuum pump and air-cooler, air warp are started before logical chlorine is started
After crossing air heat exchanger cooling, glass condenser is sent into by pipeline, vavuum pump is entered by pipeline after glass condenser hot-cast socket,
Amplify gas through vavuum pump heel row, switch when the coiled pipe outer wall and glass condenser inwall of glass condenser have material wall built-up phenomenon
Pipeline, starts air-heater, and air sends into glass condenser after hot-air heat exchanger is heated by pipeline, through glass condenser heat
Vavuum pump is entered by pipeline after conversion, gas is amplified through vavuum pump heel row, hot-air is molten the material of wall built-up by glass condenser
Change is back to and continues chlorination in kettle；7th, the hot-air of glass condenser discharge can also be utilized to coil tube heating by the material of wall built-up
Dissolve, return chlorination tank and continue chlorination, when glass condenser coiled pipe is broken, because the pressure in kettle is more than the pressure in coiled pipe
Power, tail gas can take away absorption by vavuum pump, and the coiled pipe in glass condenser is divided to two groups, and condenser has two or more sets.The invention
Thermostatic medium is once heated using external heat source in the logical chlorine process of chloride production, is not required to be switched with cold and hot medium control
The temperature of reactor, medium is in certain temperature range interior circulation, it is ensured that chlorination temperature in the kettle it is constant, the temperature difference is small, heat damage
Mistake is constant, because temperature can be transferred to most preferably logical chlorine temperature by the stabilization of temperature, due to optimal logical chlorine temperature stabilization, reduces impurity
Wind, the flat permanent and conversion ratio stabilization of chemistry, improves the quality of product, due to the stabilization of temperature, the thermostatic medium inlet valve on kettle
It is normally opened with thermostatic medium outlet valve, reduce manipulation strength, the coiled pipe in glass condenser is divided into two groups, condenser have two groups or
It is multigroup, can be difficult condenser condenser inner wall and the material melting of the outer wall hanging of condenser coiled pipe using air's switching
Block, the temperature-reducing medium in condenser coiled pipe is air, only has gas to discharge when coiled pipe is broken, and does not interfere with the product of chloride
Quality, will not set off an explosion, and improve safety in production coefficient, and its technical process is simple, it is easy to operate, pollution-free, is conducive to
Promotion and application.
Brief description of the drawings：
Accompanying drawing 1 is the flow chart that chloride final product quality of the present invention controls process system.
Accompanying drawing 2 is the process flow diagram that chloride final product quality of the present invention controls technique.
Highly preferred embodiment of the present invention：
1st, start in raw material input chlorinating container R-01 P-02 thermostatic medium circulating pumps and start the cycle over constant temperature Jie first
Matter, thermostatic medium is connected to the thermostatic medium inlet valve of chlorinating container R-01 by pipeline HWS-023-H, and thermostatic medium passes through
The thermostatic medium outlet valve outflow of chlorinating container R-01 chucks, thermostatic medium outlet valve and pipeline HWR-024 are connected, and flow direction is permanent
Conflux after warm medium condenser E-02 and thermostatic medium air heat exchanger E-03, flowing to thermostatic medium by pipeline HWR-028 changes
Heat stations R-02, the thermostatic medium inlet valve and thermostatic medium outlet valve on kettle is normally opened；
2nd, the medium entrance valve on thermostatic medium heat exchange station R-02 is opened, thermostatic medium heat exchange station heat temperature raising is given, is heated
Intensification can be carried out according to the temperature that is actually needed of material, and such as phenol leads to chlorine, lead to chlorine temperature in 65-75 degree, and lutidines leads to chlorine
In 190-200 degree, thermal medium enters house steward HOS-005-H and provides temperature by thermal medium, is situated between into constant temperature by pipeline HOS-017-H
Matter heat exchange station R-02, flows to thermal medium and returns house steward HOR-006-H by medium after hot-cast socket by pipeline HOR-015-H, and constant temperature is situated between
The medium supplement of matter heat exchange station is supplemented by pipeline HOS-016-H, when temperature reaches reaction requires temperature, is stopped to constant temperature
Media for heat exchange station R-02 is heated, and starts self-loopa, and constant temperature circulating medium heat is provided by reactor R-01；
3rd, the heat that chlorinating container R-01 is produced drives air to enter at thermostatic medium air heat exchanger E-03 with blower fan
Row hot-cast socket disperses heat, and temp control indicator is housed on pipeline HWR-028, control thermostatic medium air heat exchanger E-03's
Fan operation, because the specific heat of air is small, moment loss heat it is easily-controllable, it is ensured that temperature it is constant, due to the stabilization of temperature,
Temperature can be transferred into most preferably logical chlorine temperature carries out constant, and such as phenol leads to chlorine, leads to that chlorine temperature is constant at 70 degree, and lutidines leads to chlorine
At 195 degree, thermostatic medium condenser E-02 is that the auxiliary equipment of constant temperature is used to start when temperature rises too fast to temperature, and constant temperature is situated between
Matter condenser E-02 enters house steward CWS-002 and flows to pipeline CWS-020 equipped with circulating water cooling pipeline by recirculated water, is situated between by constant temperature
Pipeline recirculated water is connected to by pipeline CWR-019 after the completion of matter condenser E-02 heat exchange and returns house steward CWR-001, thermostatic medium heat exchange
The R-02 that stands is furnished with auxiliary temperature-reducing pipeline, for thermostatic medium heat exchange station R-02 lowers the temperature during parking, enters house steward LOS-003 by cold medium and flows
Enter pipeline LOS-018, flow to after the completion of thermostatic medium heat exchange station R-02 heat exchange, pipeline cold medium is flowed to by pipeline LOR-014 and is returned
House steward LOR-004；
4th, when occurring maloperation in production process, temperature can be caused to rise too fast, constant temperature circulating medium cannot be by heat
When taking away, start cold medium circulation and lowered the temperature, cold medium is squeezed into by cold medium heat exchange station R-03 cold medium circulating pumps P-01
Pipeline LOS-007, flows to pipeline cold medium and enters house steward LOS-003, and chlorinating container R-01 is flowed to through piping LOS-022, changes
Heat flows to pipeline cold medium and returns house steward LOR-004 after completing through pipeline LOR-021, then to flow to cold medium through pipeline LOR-013 cold
Condenser E-01, by flowing to cold medium heat exchange station R-03 after hot-cast socket, cold medium condenser E-01 is furnished with circulating water cooling, by managing
Road recirculated water enters house steward CWS-002 and flows to pipeline CWS-012, after being exchanged heat through cold medium condenser E-01, is flowed by pipeline CWR-011
House steward CWR-001 is returned to pipeline recirculated water, cold medium heat exchange station R-03 is furnished with circulating water cooling, house steward is entered by pipeline recirculated water
CWS-002 flows to pipeline CWS-010, after the completion of being exchanged heat through cold medium heat exchange station R-03, flows to pipeline by pipeline CWR-008 and circulates
Water returns house steward CWR-001, and the medium supplement of cold medium heat exchange station R-03 is returned house steward HOR-006-H and passes through pipeline by thermal medium
HOR-009-H is supplemented；
5th, continous way chlorination only needs long-term circulation constant temperature medium, and batch (-type) chlorination starts cold when reaction reaches terminal
Medium is lowered the temperature, and cooling blowing is stopped when reaching blowing temperature；
6th, need to be intercepted with glass condenser entrainment of substantial amounts of material in tail gas in logical chlorine process, tail gas is by chlorine
Change reactor R-01 and glass condenser E-06 is entered by gas phase pipe PG-025, the gas after being intercepted through glass condenser E-06 coolings
Body enters tail gas absorption, and vavuum pump P-03 and air-cooler C-01 is started before logical chlorine is started, and air is by air heat exchanger E-04
After cooling, glass condenser E-06 is sent into by pipeline PG-027, entered by pipeline PG-029 after glass condenser E-06 hot-cast sockets
Enter vavuum pump P-03, amplify gas through vavuum pump P-03 heel row, when the coiled pipe outer wall and glass condenser E- of glass condenser E-06
06 inwall switches pipeline when having material wall built-up phenomenon, start air-heater C-02, and air is after hot-air heat exchanger E-05 is heated
Glass condenser E-06 is sent into by pipeline PG-026, vavuum pump is entered by pipeline PG-029 after glass condenser E-06 hot-cast sockets
P-03, gas is amplified through vavuum pump P-03 heel row, and hot-air dissolves the material of wall built-up by glass condenser E-06 and is back to kettle
Interior continuation chlorination；
7th, the hot-air of glass condenser E-06 discharges can also be utilized to dissolve the material of wall built-up to coil tube heating, is returned
Chlorination tank continues chlorination, and when glass condenser coiled pipe is broken, because the pressure in kettle is more than the pressure in coiled pipe, tail gas can quilt
P-03 vavuum pumps take away absorption, do not result in pollution and security incident, and the coiled pipe in glass condenser is divided to two groups, and condenser has many
Group, preferably to intercept the material of gas entrainment when air switches.
Claims (1)
1. a kind of chloride final product quality control technique, it is characterised in that：
（1）First by raw material input chlorinating container, start thermostatic medium circulating pump and start the cycle over thermostatic medium, thermostatic medium
The thermostatic medium inlet valve of chlorinating container, the thermostatic medium that thermostatic medium passes through chlorinating container chuck are connected to by pipeline
Outlet valve is flowed out, and thermostatic medium outlet valve and pipeline are connected, after flowing to thermostatic medium condenser and thermostatic medium air heat exchanger
Conflux, by pipeline flow-direction thermostatic medium heat exchange station, the thermostatic medium inlet valve and thermostatic medium outlet valve on kettle are normally opened；
（2）The medium entrance valve on thermostatic medium heat exchange station is opened, is situated between to thermostatic medium heat exchange station heat temperature raising, thermal medium by heat
Matter enters house steward's offer, and thermostatic medium heat exchange station is entered by pipeline, is returned by pipeline flow-direction thermal medium by medium after hot-cast socket total
Pipe, the medium supplement of thermostatic medium heat exchange station is supplemented by pipeline, when temperature reaches reaction requires temperature, is stopped to constant temperature
Media for heat exchange station is heated, and starts self-loopa, and constant temperature circulating medium heat is provided by reactor；
（3）The heat that chlorinating container is produced carries out hot-cast socket by heat at thermostatic medium air heat exchanger with blower fan drive air
Amount disperses, and temp control indicator is housed on pipeline, controls the fan operation of thermostatic medium air heat exchanger, thermostatic medium condenser
Be constant temperature auxiliary equipment be used for when temperature rise it is too fast when start, thermostatic medium condenser equipped with circulating water cooling pipeline by following
Ring water enters house steward and flows to pipeline, and being connected to pipeline recirculated water by pipeline after the completion of being exchanged heat by thermostatic medium condenser returns house steward,
Thermostatic medium heat exchange station is furnished with auxiliary temperature-reducing pipeline, for thermostatic medium heat exchange station is lowered the temperature during parking, enters house steward by cold medium and flows into
Pipeline, is flowed to after the completion of the heat exchange of thermostatic medium heat exchange station, and house steward is returned by pipeline flow-direction pipeline cold medium；
（4）When occurring maloperation in production process, temperature can be caused to rise too fast, constant temperature circulating medium cannot take away heat
When, starting cold medium circulation and lowered the temperature, cold medium squeezes into pipeline by cold medium heat exchange station cold medium circulating pump, flows to pipeline
Cold medium enters house steward, and by pipeline flow-direction chlorinating container, heat exchange returns house steward after completing through pipeline flow-direction pipeline cold medium, then passes through
Pipeline flow-direction cold medium condenser, by flowing to cold medium heat exchange station after hot-cast socket, cold medium condenser is furnished with circulating water cooling,
House steward is entered by pipeline recirculated water and flows to pipeline, after being exchanged heat through cold medium condenser, house steward is returned by pipeline flow-direction pipeline recirculated water, it is cold
Media for heat exchange station is furnished with circulating water cooling, enters house steward by pipeline recirculated water and flows to pipeline, after the completion of being exchanged heat through cold medium heat exchange station,
House steward is returned by pipeline flow-direction pipeline recirculated water, the medium supplement of cold medium heat exchange station is returned house steward and mended by pipeline by thermal medium
Fill；
（5）Continous way chlorination only needs long-term circulation constant temperature medium, and batch (-type) chlorination starts cold Jie when reaction reaches terminal
Matter is lowered the temperature, and cooling blowing is stopped when reaching blowing temperature；
（6）Entrainment of substantial amounts of material in tail gas in logical chlorine process, need to be intercepted with glass condenser, tail gas is anti-by chlorination
Answer kettle to enter glass condenser by gas phase pipe, the gas after being intercepted through glass condenser cooling enters tail gas absorption, starting
Start vavuum pump and air-cooler before logical chlorine, air by pipeline by after air heat exchanger cooling, sending into glass condenser, through glass
Vavuum pump is entered by pipeline after condenser hot-cast socket, amplifies gas through vavuum pump heel row, when the coiled pipe outer wall and glass of glass condenser
Glass condenser inner wall switches pipeline when having material wall built-up phenomenon, start air-heater, air by after hot-air heat exchanger heating by
Pipeline sends into glass condenser, and vavuum pump is entered by pipeline after glass condenser hot-cast socket, and gas, heat are amplified through vavuum pump heel row
Air dissolves the material of wall built-up to be back to and continues chlorination in kettle by glass condenser；
（7）The hot-air of glass condenser discharge can also be utilized to dissolve the material of wall built-up to coil tube heating, return chlorination tank
Continue chlorination, when glass condenser coiled pipe is broken, because the pressure in kettle is more than the pressure in coiled pipe, tail gas can be by vavuum pump
Absorption is taken away, the coiled pipe in glass condenser is divided to two groups, and condenser has multigroup.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410463324.9A CN105457575B (en) | 2014-09-12 | 2014-09-12 | Chloride final product quality control technique |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410463324.9A CN105457575B (en) | 2014-09-12 | 2014-09-12 | Chloride final product quality control technique |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN105457575A CN105457575A (en) | 2016-04-06 |
| CN105457575B true CN105457575B (en) | 2017-06-06 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410463324.9A Expired - Fee Related CN105457575B (en) | 2014-09-12 | 2014-09-12 | Chloride final product quality control technique |
Country Status (1)
| Country | Link |
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| CN (1) | CN105457575B (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN114471400B (en) * | 2021-12-30 | 2023-11-28 | 苏州市协力化工设备有限公司 | Temperature control method and control system for reactor |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6374907B1 (en) * | 1999-10-08 | 2002-04-23 | 3M Innovative Properties Company | Hydrofluoroether as a heat-transfer fluid |
| DE10241276A1 (en) * | 2002-09-06 | 2004-03-18 | Zentes Unitex Gmbh | Heat exchanger for maintaining constant temperature in polymers has a heated internal torpedo with ends matched to those of the exchanger body ends forming a polymer flow channel |
| CN101254451A (en) * | 2007-11-29 | 2008-09-03 | 苏州昆拓冷机有限公司 | Reactor constant temperature freezer |
| EP2096305A1 (en) * | 2008-02-27 | 2009-09-02 | Sophia Antipolis Energie Developpement | Facility for generating electricity from solar energy |
| CN202715402U (en) * | 2012-04-13 | 2013-02-06 | 广西巴帝食品有限责任公司 | Double pipe type circulation heat exchange matching system |
| CN203635190U (en) * | 2013-11-29 | 2014-06-11 | 广东中泽重工有限公司 | Jacketed type reaction kettle |
-
2014
- 2014-09-12 CN CN201410463324.9A patent/CN105457575B/en not_active Expired - Fee Related
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6374907B1 (en) * | 1999-10-08 | 2002-04-23 | 3M Innovative Properties Company | Hydrofluoroether as a heat-transfer fluid |
| DE10241276A1 (en) * | 2002-09-06 | 2004-03-18 | Zentes Unitex Gmbh | Heat exchanger for maintaining constant temperature in polymers has a heated internal torpedo with ends matched to those of the exchanger body ends forming a polymer flow channel |
| CN101254451A (en) * | 2007-11-29 | 2008-09-03 | 苏州昆拓冷机有限公司 | Reactor constant temperature freezer |
| EP2096305A1 (en) * | 2008-02-27 | 2009-09-02 | Sophia Antipolis Energie Developpement | Facility for generating electricity from solar energy |
| CN202715402U (en) * | 2012-04-13 | 2013-02-06 | 广西巴帝食品有限责任公司 | Double pipe type circulation heat exchange matching system |
| CN203635190U (en) * | 2013-11-29 | 2014-06-11 | 广东中泽重工有限公司 | Jacketed type reaction kettle |
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| Publication number | Publication date |
|---|---|
| CN105457575A (en) | 2016-04-06 |
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