CN105396635A - Single-mode stationary cooling simple equipment of high-temperature crucible - Google Patents
Single-mode stationary cooling simple equipment of high-temperature crucible Download PDFInfo
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- CN105396635A CN105396635A CN201510981746.XA CN201510981746A CN105396635A CN 105396635 A CN105396635 A CN 105396635A CN 201510981746 A CN201510981746 A CN 201510981746A CN 105396635 A CN105396635 A CN 105396635A
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- container
- solid ice
- temperature crucible
- ice container
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- 238000001816 cooling Methods 0.000 title claims abstract description 25
- 239000007787 solid Substances 0.000 claims abstract description 28
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 12
- 230000003068 static effect Effects 0.000 claims abstract description 9
- 230000002706 hydrostatic effect Effects 0.000 claims 2
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 abstract description 10
- 229910052717 sulfur Inorganic materials 0.000 abstract description 10
- 239000011593 sulfur Substances 0.000 abstract description 10
- 239000000463 material Substances 0.000 abstract description 4
- 239000002802 bituminous coal Substances 0.000 abstract description 2
- 239000000110 cooling liquid Substances 0.000 abstract description 2
- 239000000126 substance Substances 0.000 abstract description 2
- 238000002485 combustion reaction Methods 0.000 abstract 1
- 239000003245 coal Substances 0.000 description 4
- 230000009931 harmful effect Effects 0.000 description 3
- 238000005259 measurement Methods 0.000 description 3
- RAHZWNYVWXNFOC-UHFFFAOYSA-N Sulphur dioxide Chemical compound O=S=O RAHZWNYVWXNFOC-UHFFFAOYSA-N 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 238000003915 air pollution Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000000523 sample Substances 0.000 description 1
- 238000010561 standard procedure Methods 0.000 description 1
Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01L—CHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
- B01L7/00—Heating or cooling apparatus; Heat insulating devices
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N31/00—Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods
- G01N31/12—Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods using combustion
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- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Engineering & Computer Science (AREA)
- Combustion & Propulsion (AREA)
- Molecular Biology (AREA)
- Clinical Laboratory Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
Abstract
本发明公开了一种高温坩埚单一模式静止冷却简易设备，属于涉及到烟煤可燃物质中含硫量的分析设备领域。它包括支柱、装设于支柱上的底座、装设于底座内部的固体冰容器；支柱的中心设有一个圆形的引水道；底座上设有容器孔，固体冰容器放置于容器孔内；底座还设有与引水道相连通的过水道；固体冰容器为液态水经过冷却成型形成的圆柱形容器，圆柱形容器的横截面外径等于容器孔的直径；固体冰容器内装设有高温坩埚，高温坩埚内装有燃烧物；固体冰容器的内部形状与高温坩埚的外部形状完全相同。本发明是一种结构简单、采用固态冰容器对高温坩埚实施快速冷却的单一模式静止冷却简易设备。
The invention discloses a single-mode static cooling simple equipment for a high-temperature crucible, which belongs to the field of analysis equipment related to sulfur content in combustible substances of bituminous coal. It includes a pillar, a base installed on the pillar, and a solid ice container installed inside the base; a circular water diversion channel is arranged in the center of the pillar; a container hole is arranged on the base, and the solid ice container is placed in the container hole; The base is also provided with a water channel connected with the water diversion channel; the solid ice container is a cylindrical container formed by cooling liquid water, and the outer diameter of the cross section of the cylindrical container is equal to the diameter of the container hole; the solid ice container is equipped with a high-temperature crucible , the high-temperature crucible contains combustion materials; the inner shape of the solid ice container is exactly the same as the outer shape of the high-temperature crucible. The invention is a single-mode static cooling simple device with simple structure and adopting a solid ice container to rapidly cool a high-temperature crucible.
Description
技术领域technical field
本发明主要涉及到烟煤可燃物质中含硫量的分析设备领域，特指一种高温坩埚单一模式静止冷却简易设备。The invention mainly relates to the field of analysis equipment for the sulfur content in the combustible substances of bituminous coal, in particular to a simple equipment for single-mode static cooling of a high-temperature crucible.
背景技术Background technique
硫元素是煤样中最主要的有害成份，煤样中所含有的硫燃烧后会生成二氧化硫等有害气体，造成大气污染和环境污染；硫元素同时对煤的炼焦、气化、燃烧都会带来有害的影响，因此测量煤中硫元素的含量是一项非常重要的工作。艾氏测硫法是目前各国通用的测定煤中全硫含量的标准方法之一，具有准确度高、成批测定等优点。然而，由于艾氏测硫步骤较多，难以实现全程自动化，故测量效率较低。在艾氏测硫中，一个很重要的步骤是对燃烧物中取出的高温坩埚进行冷却，冷却后用玻璃棒搅碎坩埚中的灼烧物，制作溶液。现有技术中，对高温坩埚的冷却几乎都是自热冷却。现有技术的冷却具有一定的缺陷：冷却时间较长，冷却效率较低，从而导致测量硫的实验时间漫长。因此，设计一种能够快速冷却高温坩埚的装置具有一定的价值。Sulfur is the most important harmful component in coal samples. The sulfur contained in coal samples will produce harmful gases such as sulfur dioxide after burning, causing air pollution and environmental pollution; Harmful effects, so measuring the content of sulfur in coal is a very important work. The Ehrlich sulfur method is currently one of the standard methods for determining the total sulfur content in coal, which has the advantages of high accuracy and batch determination. However, due to the large number of steps in Ai’s sulfur measurement, it is difficult to realize full automation, so the measurement efficiency is low. In the measurement of sulfur by Ehrlich, a very important step is to cool the high-temperature crucible taken out of the burning material, and after cooling, use a glass rod to crush the burning material in the crucible to make a solution. In the prior art, the cooling of the high-temperature crucible is almost all self-thermal cooling. The cooling of the prior art has certain defects: the cooling time is long and the cooling efficiency is low, which results in a long experiment time for measuring sulfur. Therefore, it is of certain value to design a device that can rapidly cool the high-temperature crucible.
发明内容Contents of the invention
本发明需解决的技术问题是：针对现有技术存在的冷却时间较长等技术问题，本发明提供一种结构简单、采用固态冰容器对高温坩埚实施快速冷却的单一模式静止冷却简易设备。The technical problem to be solved by the present invention is: in view of the technical problems such as long cooling time in the prior art, the present invention provides a single-mode static cooling simple device with simple structure and fast cooling of high-temperature crucible by using a solid ice container.
为了解决上述问题，本发明提出的解决方案为：一种高温坩埚单一模式静止冷却简易设备，它包括支柱、装设于所述支柱上的底座、装设于所述底座内部的固体冰容器。In order to solve the above problems, the solution proposed by the present invention is: a single-mode static cooling simple equipment for a high-temperature crucible, which includes a pillar, a base installed on the pillar, and a solid ice container installed inside the base.
所述支柱的中心设有一个圆形的引水道；所述底座4上设有容器孔，所述固体冰容器放置于所述容器孔内。A circular water diversion channel is provided at the center of the pillar; a container hole is provided on the base 4, and the solid ice container is placed in the container hole.
所述底座还设有与所述引水道相连通的过水道；所述固体冰容器为液态水经过冷却成型形成的圆柱形容器，所述圆柱形容器的横截面外径等于所述容器孔的直径。The base is also provided with a water passage connected with the water diversion channel; the solid ice container is a cylindrical container formed by cooling liquid water, and the outer diameter of the cross section of the cylindrical container is equal to that of the container hole. diameter.
所述固体冰容器内装设有高温坩埚，所述高温坩埚内装有燃烧物；所述固体冰容器的内部形状与所述高温坩埚的外部形状完全相同。A high-temperature crucible is installed in the solid ice container, and combustibles are installed in the high-temperature crucible; the internal shape of the solid ice container is exactly the same as the external shape of the high-temperature crucible.
本发明与现有技术相比，具有如下优点和有益效果：Compared with the prior art, the present invention has the following advantages and beneficial effects:
(1)本发明的一种高温坩埚单一模式静止冷却简易设备设有固体冰容器，固体冰容器的内部结构与高温坩埚外部结构完全相同，可以最大面积的对高温坩埚实施降温，冰生成的水由过水道流入，再经引水道流出。(1) A kind of high-temperature crucible single-mode static cooling simple equipment of the present invention is provided with solid ice container, and the internal structure of solid ice container is exactly the same as the high-temperature crucible external structure, can implement cooling to high-temperature crucible with the largest area, and the water that ice produces It flows in through the water channel, and then flows out through the diversion channel.
(2)本发明结构简单、采用固态冰容器对高温坩埚实施了快速冷却，缩短了冷却时间，从而提高了冷却效率。(2) The invention has a simple structure, adopts a solid ice container to rapidly cool the high-temperature crucible, shortens the cooling time, and thus improves the cooling efficiency.
附图说明Description of drawings
图1是本发明的一种高温坩埚单一模式静止冷却简易设备的结构原理示意图。Fig. 1 is a schematic diagram of the structure and principle of a simple equipment for single-mode static cooling of a high-temperature crucible according to the present invention.
图中，1—高温坩埚；2—燃烧物；3—固态冰容器；4—底座；41—容器孔；42—过水道；5—支柱；51—引水道。In the figure, 1—high temperature crucible; 2—combustible material; 3—solid ice container; 4—base; 41—container hole; 42—aqueduct; 5—pillar; 51—aqueduct.
具体实施方式detailed description
以下将结合附图和具体实施例对本发明作进一步详细说明。The present invention will be further described in detail below in conjunction with the accompanying drawings and specific embodiments.
参见图1所示，本发明的一种高温坩埚单一模式静止冷却简易设备，包括支柱5、装设于支柱5上的底座4、装设于底座4内部的固体冰容器3；固体冰容器3通过与高温坩埚1的接触实施冷却。Referring to shown in Fig. 1, a kind of high-temperature crucible single-mode static cooling simple equipment of the present invention comprises a pillar 5, a base 4 installed on the pillar 5, a solid ice container 3 installed inside the base 4; the solid ice container 3 Cooling is performed by contact with the high-temperature crucible 1 .
参见图1所示，支柱5的中心设有一个圆形的引水道51；底座4上设有容器孔41，固体冰容器3放置于容器孔41内；底座4还设有与引水道51相连通的过水道42；固体冰容器3为液态水经过冷却成型形成的圆柱形容器，圆柱形容器的横截面外径等于容器孔41的直径；固体冰容器3内装设有高温坩埚1，高温坩埚1内装有燃烧物2；固体冰容器3的内部形状与高温坩埚1的外部形状完全相同；固体冰容器3从高温坩埚1中吸收热量，实施冷却功能；冰吸收热量后转变为水，生成的水由过水道42流入，经引水道51流出。Referring to Fig. 1, the center of the pillar 5 is provided with a circular water diversion channel 51; the base 4 is provided with a container hole 41, and the solid ice container 3 is placed in the container hole 41; Through the water channel 42; the solid ice container 3 is a cylindrical container formed by cooling and forming of liquid water, and the outer diameter of the cross section of the cylindrical container is equal to the diameter of the container hole 41; the solid ice container 3 is equipped with a high-temperature crucible 1, a high-temperature crucible 1 is equipped with combustibles 2; the internal shape of the solid ice container 3 is exactly the same as the external shape of the high-temperature crucible 1; the solid ice container 3 absorbs heat from the high-temperature crucible 1, and implements a cooling function; Water flows in from the water channel 42 and flows out through the water channel 51 .
Claims (1)
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510981746.XA CN105396635A (en) | 2015-12-23 | 2015-12-23 | Single-mode stationary cooling simple equipment of high-temperature crucible |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510981746.XA CN105396635A (en) | 2015-12-23 | 2015-12-23 | Single-mode stationary cooling simple equipment of high-temperature crucible |
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| CN105396635A true CN105396635A (en) | 2016-03-16 |
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| CN201510981746.XA Pending CN105396635A (en) | 2015-12-23 | 2015-12-23 | Single-mode stationary cooling simple equipment of high-temperature crucible |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103699202A (en) * | 2012-09-27 | 2014-04-02 | 三星电子株式会社 | System-on-chip with capability for controlling power supply according to data transaction and method of operating the same |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1071502A (en) * | 1992-11-23 | 1993-04-28 | 冶金工业部钢铁研究总院 | Cold crucible for induction furnace |
| JP2010043776A (en) * | 2008-08-11 | 2010-02-25 | Ulvac Japan Ltd | Water cooling crucible and electron beam melting furnace |
| CN203990708U (en) * | 2014-03-18 | 2014-12-10 | 中国农业科学院兰州畜牧与兽药研究所 | When a kind of application of sample, place the ice chest of centrifuge tube |
| CN204170748U (en) * | 2014-09-29 | 2015-02-25 | 湖北省银丰鼎诚生物工程有限公司 | A kind of molecule experiments EP pipe rack |
-
2015
- 2015-12-23 CN CN201510981746.XA patent/CN105396635A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1071502A (en) * | 1992-11-23 | 1993-04-28 | 冶金工业部钢铁研究总院 | Cold crucible for induction furnace |
| JP2010043776A (en) * | 2008-08-11 | 2010-02-25 | Ulvac Japan Ltd | Water cooling crucible and electron beam melting furnace |
| CN203990708U (en) * | 2014-03-18 | 2014-12-10 | 中国农业科学院兰州畜牧与兽药研究所 | When a kind of application of sample, place the ice chest of centrifuge tube |
| CN204170748U (en) * | 2014-09-29 | 2015-02-25 | 湖北省银丰鼎诚生物工程有限公司 | A kind of molecule experiments EP pipe rack |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103699202A (en) * | 2012-09-27 | 2014-04-02 | 三星电子株式会社 | System-on-chip with capability for controlling power supply according to data transaction and method of operating the same |
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Application publication date: 20160316 |
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