CN105381886B - It is a kind of to be used for the floating agent containing golden thiocyanation castaway slag - Google Patents
It is a kind of to be used for the floating agent containing golden thiocyanation castaway slag Download PDFInfo
- Publication number
- CN105381886B CN105381886B CN201510918613.8A CN201510918613A CN105381886B CN 105381886 B CN105381886 B CN 105381886B CN 201510918613 A CN201510918613 A CN 201510918613A CN 105381886 B CN105381886 B CN 105381886B
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- China
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- parts
- xanthate
- thiocyanation
- floating
- floating agent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 239000003795 chemical substances by application Substances 0.000 title claims abstract description 28
- 238000007667 floating Methods 0.000 title claims abstract description 24
- 239000002893 slag Substances 0.000 title claims abstract description 15
- 238000006365 thiocyanation reaction Methods 0.000 title claims abstract description 15
- TUZCOAQWCRRVIP-UHFFFAOYSA-N butoxymethanedithioic acid Chemical compound CCCCOC(S)=S TUZCOAQWCRRVIP-UHFFFAOYSA-N 0.000 claims abstract description 14
- CONMNFZLRNYHIQ-UHFFFAOYSA-N 3-methylbutoxymethanedithioic acid Chemical compound CC(C)CCOC(S)=S CONMNFZLRNYHIQ-UHFFFAOYSA-N 0.000 claims abstract description 13
- ARUVKPQLZAKDPS-UHFFFAOYSA-L copper(II) sulfate Chemical compound [Cu+2].[O-][S+2]([O-])([O-])[O-] ARUVKPQLZAKDPS-UHFFFAOYSA-L 0.000 claims abstract description 13
- OXVXWUDYARFPLN-UHFFFAOYSA-N ethylazanium;hydron;sulfate Chemical compound CC[NH3+].OS([O-])(=O)=O OXVXWUDYARFPLN-UHFFFAOYSA-N 0.000 claims abstract description 11
- GCLGEJMYGQKIIW-UHFFFAOYSA-H sodium hexametaphosphate Chemical compound [Na]OP1(=O)OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])O1 GCLGEJMYGQKIIW-UHFFFAOYSA-H 0.000 claims abstract description 11
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000004115 Sodium Silicate Substances 0.000 claims abstract description 5
- 235000019795 sodium metasilicate Nutrition 0.000 claims abstract description 5
- 229910052911 sodium silicate Inorganic materials 0.000 claims abstract description 5
- 239000012991 xanthate Substances 0.000 claims description 3
- MOMKYJPSVWEWPM-UHFFFAOYSA-N 4-(chloromethyl)-2-(4-methylphenyl)-1,3-thiazole Chemical compound C1=CC(C)=CC=C1C1=NC(CCl)=CS1 MOMKYJPSVWEWPM-UHFFFAOYSA-N 0.000 claims description 2
- ZOOODBUHSVUZEM-UHFFFAOYSA-N ethoxymethanedithioic acid Chemical compound CCOC(S)=S ZOOODBUHSVUZEM-UHFFFAOYSA-N 0.000 claims description 2
- 235000019983 sodium metaphosphate Nutrition 0.000 claims description 2
- 125000000740 n-pentyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 claims 1
- 238000005188 flotation Methods 0.000 abstract description 19
- 239000012141 concentrate Substances 0.000 abstract description 10
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 abstract description 10
- 229910052737 gold Inorganic materials 0.000 abstract description 10
- 239000010931 gold Substances 0.000 abstract description 10
- 238000011084 recovery Methods 0.000 abstract description 7
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 abstract description 5
- 239000000843 powder Substances 0.000 abstract description 5
- 239000011593 sulfur Substances 0.000 abstract description 4
- 229910052717 sulfur Inorganic materials 0.000 abstract description 4
- WURBVZBTWMNKQT-UHFFFAOYSA-N 1-(4-chlorophenoxy)-3,3-dimethyl-1-(1,2,4-triazol-1-yl)butan-2-one Chemical compound C1=NC=NN1C(C(=O)C(C)(C)C)OC1=CC=C(Cl)C=C1 WURBVZBTWMNKQT-UHFFFAOYSA-N 0.000 abstract description 3
- 239000012190 activator Substances 0.000 abstract description 2
- OMZSGWSJDCOLKM-UHFFFAOYSA-N copper(II) sulfide Chemical compound [S-2].[Cu+2] OMZSGWSJDCOLKM-UHFFFAOYSA-N 0.000 abstract description 2
- 229910001608 iron mineral Inorganic materials 0.000 abstract description 2
- 235000019353 potassium silicate Nutrition 0.000 abstract description 2
- 239000004088 foaming agent Substances 0.000 abstract 1
- 239000003921 oil Substances 0.000 description 10
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 6
- 229910052710 silicon Inorganic materials 0.000 description 6
- 239000010703 silicon Substances 0.000 description 6
- 239000011734 sodium Substances 0.000 description 6
- 229910052708 sodium Inorganic materials 0.000 description 6
- 238000000034 method Methods 0.000 description 3
- 238000003723 Smelting Methods 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 229910052500 inorganic mineral Inorganic materials 0.000 description 2
- 239000011707 mineral Substances 0.000 description 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 1
- XLJYGTUUQWFFGT-UHFFFAOYSA-N CC(C)CC[Na] Chemical group CC(C)CC[Na] XLJYGTUUQWFFGT-UHFFFAOYSA-N 0.000 description 1
- 235000008733 Citrus aurantifolia Nutrition 0.000 description 1
- QUSNBJAOOMFDIB-UHFFFAOYSA-N Ethylamine Chemical compound CCN QUSNBJAOOMFDIB-UHFFFAOYSA-N 0.000 description 1
- AQGDXJQRVOCUQX-UHFFFAOYSA-N N.[S] Chemical compound N.[S] AQGDXJQRVOCUQX-UHFFFAOYSA-N 0.000 description 1
- 241001062472 Stokellia anisodon Species 0.000 description 1
- 239000005864 Sulphur Substances 0.000 description 1
- 235000011941 Tilia x europaea Nutrition 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 238000000498 ball milling Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 239000004571 lime Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000005065 mining Methods 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- MNWBNISUBARLIT-UHFFFAOYSA-N sodium cyanide Chemical compound [Na+].N#[C-] MNWBNISUBARLIT-UHFFFAOYSA-N 0.000 description 1
- AAJRIJBGDLLRAE-UHFFFAOYSA-M sodium;butoxymethanedithioate Chemical group [Na+].CCCCOC([S-])=S AAJRIJBGDLLRAE-UHFFFAOYSA-M 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03D—FLOTATION; DIFFERENTIAL SEDIMENTATION
- B03D1/00—Flotation
- B03D1/001—Flotation agents
- B03D1/018—Mixtures of inorganic and organic compounds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03D—FLOTATION; DIFFERENTIAL SEDIMENTATION
- B03D2201/00—Specified effects produced by the flotation agents
- B03D2201/02—Collectors
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03D—FLOTATION; DIFFERENTIAL SEDIMENTATION
- B03D2201/00—Specified effects produced by the flotation agents
- B03D2201/04—Frothers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03D—FLOTATION; DIFFERENTIAL SEDIMENTATION
- B03D2201/00—Specified effects produced by the flotation agents
- B03D2201/06—Depressants
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03D—FLOTATION; DIFFERENTIAL SEDIMENTATION
- B03D2203/00—Specified materials treated by the flotation agents; Specified applications
- B03D2203/02—Ores
- B03D2203/025—Precious metal ores
Landscapes
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Manufacture And Refinement Of Metals (AREA)
Abstract
It is a kind of to be used for the floating agent containing golden thiocyanation castaway slag, by weight, including following component：200~320 parts of calgon, 1500 ~ 2500 parts of sodium metasilicate, 40 ~ 60 parts of ethyl ammonia sulfate, 30~55 parts of copper sulphate, 66 ~ 110 parts of butyl xanthate, 133 ~ 220 parts of isoamyl xanthate, 50~110 parts of 2# oil.Gangue is suppressed using calgon, waterglass suppresses iron mineral, and ethyl ammonia sulfate Z 200 makees the collecting agent of copper sulfide, and copper sulphate makees activator, and butyl xanthate, isoamyl xanthate make collecting agent, and 2# oil makees foaming agent；Greatly improved using the concentrate grade powder after the floating agent floating and enriching of the present invention, the tenor of flotation dreg is low, and the rate of recovery is up to 80%, and concentrate Gold grade is improved to 20g/t after enrichment, and silver-colored grade, which is improved to 220g/t, sulfur content, reaches 33%.Flotation cost declines to a great extent, and has effectively reclaimed resource, protects environment.
Description
Technical field
The invention belongs to mineral floating field, and in particular to a kind of to be used for the floating agent containing golden thiocyanation castaway slag.
Background technology
China has just carried out the large scale mining of gold since the seventies in last century and has selected smelting.But by gold smelting at that time
The limitation of industry processing techniques, the recovery process technology of gold are substantially gold containing ore by broken, ball milling, table concentration or added
Cymag carries out the complex compound of reaction generation gold through techniques such as zinc dust precipitations under conditions of lime does protection alkali, is finally melted
Gold is smelt, element sulphur is not almost reclaimed, and the golden rate of recovery is given up only between 65~70% after largely carrying gold containing golden tailings
Abandon and heap is stored in Tailings Dam.These, through analyzing sulfur-bearing, Jin Heyin, cause the wasting of resources and environmental pollution containing golden tailings.Flotation medicine
Agent is the important component of flotation, is to solve mineral difficulty to select problem by improving floating agent and Development of Novel floating agent
One of important means.It is existing it is most widely used containing golden tailings collecting agent have xanthate, black powder, ammonium black powder etc., but these collecting agents
Collecting ability is although good, but its selectivity is all universal relatively low and CN in by slag-Influence, Floatation Concentrate Grade is low, flotation into
This height, resource cannot be reclaimed fully, cause the wasting of resources.
The content of the invention
Contain the shortcomings that golden tailings flotation recovery rate is low, concentrate grade is low present invention aim to address existing, there is provided one
Kind improves the floating agent containing golden tailings flotation recovery rate, concentrate grade.
To achieve the above object, the technical solution adopted by the present invention is, a kind of to be used for the flotation containing golden thiocyanation castaway slag
Medicament, by weight, including following component：200~320 parts of calgon, 1500 ~ 2500 parts of sodium metasilicate, ethyl ammonia sulfate（Z-
200）40 ~ 60 parts, 30~55 parts of copper sulphate, 66 ~ 110 parts of butyl xanthate, 133 ~ 220 parts of isoamyl xanthate, 2# oil（Terpenic oil）
50~110 parts.
Preferably, it is described to be used for the floating agent containing golden thiocyanation castaway slag, by weight, including following component：Six
250 parts of sodium metaphosphate, 2000 parts of sodium metasilicate, 50 parts of ethyl ammonia sulfate, 40 parts of copper sulphate, 90 parts of butyl xanthate, isoamyl xanthate 180
Part, 80 parts of 2# oil.
The butyl xanthate is sodium n-butyl xanthate, and the isoamyl xanthate is isopentyl sodium xanthate.
The beneficial effect comprise that：Gangue is suppressed using calgon, waterglass suppresses iron mineral, second sulphur ammonia
Ester Z-200 makees the collecting agent of copper sulfide, and copper sulphate makees activator, and butyl xanthate, isoamyl xanthate make collecting agent, and 2# oil bubbles
Agent；Greatly improved using the concentrate grade powder after the floating agent floating and enriching of the present invention, the tenor of flotation dreg is low, recovery
Rate is up to 80%, and concentrate Gold grade is improved to 20g/t after enrichment, and silver-colored grade, which is improved to 220g/t, sulfur content, reaches 33%.Flotation
Cost declines to a great extent, and has effectively reclaimed resource, protects environment.
Embodiment
Embodiment 1
By weight, calgon 250g, silicon are included for the flotation floating agent per ton containing golden thiocyanation castaway slag
Sour sodium 2000g, ethyl ammonia sulfate 50g, copper sulphate 40g, butyl xanthate 90g, isoamyl xanthate 180g, 2# oil 80g.
Embodiment 2
By weight, calgon 280g, silicon are included for the flotation floating agent per ton containing golden thiocyanation castaway slag
Sour sodium 1900g, ethyl ammonia sulfate 45g, copper sulphate 45g, butyl xanthate 95g, isoamyl xanthate 190g, 2# oil 90g.
Embodiment 3
By weight, calgon 230g, silicon are included for the flotation floating agent per ton containing golden thiocyanation castaway slag
Sour sodium 2100g, ethyl ammonia sulfate 50g, copper sulphate 35g, butyl xanthate 75g, isoamyl xanthate 150g, 2# oil 60g.
Embodiment 4
By weight, calgon 300g, silicon are included for the flotation floating agent per ton containing golden thiocyanation castaway slag
Sour sodium 1500g, ethyl ammonia sulfate 50g, copper sulphate 50g, butyl xanthate 100g, isoamyl xanthate 200g, 2# oil 100g.
Embodiment 5
By weight, calgon 200g, silicon are included for the flotation floating agent per ton containing golden thiocyanation castaway slag
Sour sodium 2000g, ethyl ammonia sulfate 40g, copper sulphate 30g, butyl xanthate 66g, isoamyl xanthate 140g, 2# oil 50g.
Embodiment 6
By weight, calgon 320g, silicon are included for the flotation floating agent per ton containing golden thiocyanation castaway slag
Sour sodium 2500g, ethyl ammonia sulfate 60g, copper sulphate 55g, butyl xanthate 110g, isoamyl xanthate 220g, 2# oil 110g.
Using 1-6 of embodiment of the present invention floating agent, according to the conventional flotation method containing golden thiocyanation castaway slag, obtain
The concentrate production target such as following table arrived：
。
Greatly improved using the concentrate grade powder after the floating agent floating and enriching of the present invention, the tenor of flotation dreg
Low, the rate of recovery is up to 70 ~ 80%, and concentrate Gold grade is improved to more than 18g/t after enrichment, and silver-colored grade is improved to more than 200g/t,
Sulfur content reaches more than 30%.Flotation cost declines to a great extent, and has effectively reclaimed resource, protects environment.
Claims (2)
1. a kind of be used for the floating agent containing golden thiocyanation castaway slag, it is characterised in that by weight, including following component：Six
200~320 parts of sodium metaphosphate, 1500 ~ 2500 parts of sodium metasilicate, 40 ~ 60 parts of ethyl ammonia sulfate, 30~55 parts of copper sulphate, butyl xanthate
66 ~ 110 parts, 133 ~ 220 parts of isoamyl xanthate, 50~110 parts of 2# oil.
2. it is used for the floating agent containing golden thiocyanation castaway slag as claimed in claim 1, it is characterised in that by weight, including
Following component：250 parts of calgon, 2000 parts of sodium metasilicate, 50 parts of ethyl ammonia sulfate, 40 parts of copper sulphate are 90 parts of butyl xanthate, different
180 parts of amyl group xanthate, 80 parts of 2# oil.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510918613.8A CN105381886B (en) | 2015-12-14 | 2015-12-14 | It is a kind of to be used for the floating agent containing golden thiocyanation castaway slag |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510918613.8A CN105381886B (en) | 2015-12-14 | 2015-12-14 | It is a kind of to be used for the floating agent containing golden thiocyanation castaway slag |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN105381886A CN105381886A (en) | 2016-03-09 |
| CN105381886B true CN105381886B (en) | 2017-12-29 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510918613.8A Active CN105381886B (en) | 2015-12-14 | 2015-12-14 | It is a kind of to be used for the floating agent containing golden thiocyanation castaway slag |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105381886B (en) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107413532A (en) * | 2017-09-30 | 2017-12-01 | 徐州中泰能源科技有限公司 | A kind of copper ore floatation agent |
| CN114522806B (en) * | 2022-02-24 | 2024-08-09 | 矿冶科技集团有限公司 | Composite flotation collector, application and scheelite flotation method |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4710361A (en) * | 1983-01-14 | 1987-12-01 | Ostrea Antonio M | Gold recovery by sulhydric-fatty acid flotation as applied to gold ores/cyanidation tailings |
| CN101214470A (en) * | 2008-01-21 | 2008-07-09 | 北京科技大学 | A method for recovering copper, lead and zinc in cyanide tailings by flotation with poor cyanide solution |
| CN102513215A (en) * | 2011-12-09 | 2012-06-27 | 紫金矿业集团股份有限公司 | Method for separating gold, silver and other metals and sulfur from waste cyanide tailings by floatation |
| CN104073645A (en) * | 2014-06-30 | 2014-10-01 | 东北大学 | Method for floatation-recovering valuable metals in superfine cyanided tailings by using high-cyanogen backwater |
| CN104722408A (en) * | 2014-11-24 | 2015-06-24 | 贵州紫金矿业股份有限公司 | Method for recycling gold in cyanided tailings in ramified and series flotation mode |
-
2015
- 2015-12-14 CN CN201510918613.8A patent/CN105381886B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4710361A (en) * | 1983-01-14 | 1987-12-01 | Ostrea Antonio M | Gold recovery by sulhydric-fatty acid flotation as applied to gold ores/cyanidation tailings |
| CN101214470A (en) * | 2008-01-21 | 2008-07-09 | 北京科技大学 | A method for recovering copper, lead and zinc in cyanide tailings by flotation with poor cyanide solution |
| CN102513215A (en) * | 2011-12-09 | 2012-06-27 | 紫金矿业集团股份有限公司 | Method for separating gold, silver and other metals and sulfur from waste cyanide tailings by floatation |
| CN104073645A (en) * | 2014-06-30 | 2014-10-01 | 东北大学 | Method for floatation-recovering valuable metals in superfine cyanided tailings by using high-cyanogen backwater |
| CN104722408A (en) * | 2014-11-24 | 2015-06-24 | 贵州紫金矿业股份有限公司 | Method for recycling gold in cyanided tailings in ramified and series flotation mode |
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| Publication number | Publication date |
|---|---|
| CN105381886A (en) | 2016-03-09 |
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Effective date of registration: 20190304 Address after: 472500 North Section of North Building of Tonggou District, Southwest corner, at the intersection of Xinling Street and Hangu Road, East Lingbao City, Sanmenxia City, Henan Province Patentee after: Henan Gold Industry Technology Research Institute Co., Ltd. Address before: 472500 Middle Section of Dingyuan Road, Daonan Industrial Zone, Lingbao City, Sanmenxia City, Henan Province Patentee before: LINGBAO JINYUAN CHENGUANG NONFERROUS MINING CO., LTD. |
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