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CN105315861A - Water-based ultraviolet-curing paint for door and preparing method thereof - Google Patents

Water-based ultraviolet-curing paint for door and preparing method thereof Download PDF

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Publication number
CN105315861A
CN105315861A CN201510837041.0A CN201510837041A CN105315861A CN 105315861 A CN105315861 A CN 105315861A CN 201510837041 A CN201510837041 A CN 201510837041A CN 105315861 A CN105315861 A CN 105315861A
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CN
China
Prior art keywords
parts
mill base
acrylate resin
prescription
filling
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201510837041.0A
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Chinese (zh)
Inventor
陆正齐
任太春
陈飞
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Anhui Wang Jia Yuan Door Co Ltd
Original Assignee
Anhui Wang Jia Yuan Door Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Anhui Wang Jia Yuan Door Co Ltd filed Critical Anhui Wang Jia Yuan Door Co Ltd
Priority to CN201510837041.0A priority Critical patent/CN105315861A/en
Publication of CN105315861A publication Critical patent/CN105315861A/en
Pending legal-status Critical Current

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Abstract

Water-based ultraviolet-curing paint for a door is prepared from 50-70 parts of polyether acrylic resin, 5-12 parts of polyester acrylic resin, 8-15 parts of urea resin, 15-20 parts of non-floating aluminum powder, 1-2 parts of 2,4,6-trimethybenzoyl-diphenylphosphine oxide, 3-6 parts of simethicone, 1-2 parts of p-toluene sulfonic acid, 2-4 parts of calcium naphthenate, 3-4 parts of lithopone, 5-8 parts of bentonite, 2-5 parts of dioctyl stearate, 15-20 parts of deionized water, 4-5 parts of butyl acetate, 10-15 parts of ethyl alcohol and 2-8 parts of isobutanol. A preparing method is simple in process, and the water-based ultraviolet-curing paint is high in curing speed, high in adhesive force and resistant to ageing.

Description

A kind of door use ultraviolet-cured paint and preparation method thereof
Technical field
The present invention relates to technical field of coatings, particularly a kind of door use ultraviolet-cured paint and preparation method thereof.
Background technology
In current door processing industry, the technique for the paint of door external coating is more complicated, and curing speed is slow, and production difficulty is high, surface effect and sticking power poor.
For the problems referred to above, the invention provides a kind of door use ultraviolet-cured paint and preparation method thereof, technique is simple, and curing speed is fast, and product strong adhesion is ageing-resistant.
Summary of the invention
Technical problem to be solved by this invention is to provide a kind of door use ultraviolet-cured paint and preparation method thereof.Effectively can solving existing door, to paint technical recipe more complicated, and curing speed is slow, and production difficulty is high, surface effect and the poor problem of sticking power.
Polyoxyalkylene acrylate resin 50-70 part, polyester acrylate resin 5-12 part, non-floating type aluminium powder 15-20 part, 2; 4,6-trimethylbenzoy-dipheny phosphine oxide 1-2 part, dimethyl silicone oil 3-6 part, p-methyl benzenesulfonic acid 1-2 part, calcium naphthenate 2-4 part, zinc sulfide white 3-4 part, wilkinite 5-8 part, stearic acid dioctyl ester 2-5 part, deionized water 15-20 part, butylacetate 4-5 part, ethanol 10-15 part, isopropylcarbinol 2-8 part.
Further, described door use ultraviolet-cured paint also comprises color material 1-3 part.
Present invention also offers the preparation method of described door use ultraviolet-cured paint:
1. take wilkinite and deionized water by formula, at use stirrer moderate-speed mixer 15min after mixing, form native cream;
2. by 50% of polyoxyalkylene acrylate resin liquid measure and 50% of polyester acrylate resin liquid measure that take of filling a prescription, mix with the native cream 1. produced to step, add by the non-floating type aluminium powder, the zinc sulfide white and 2 that take of filling a prescription, 4,6-trimethylbenzoy-dipheny phosphine oxide, then stirrer is started, high-speed stirring 15min;
3. the mill base that 2. step produces is added shredder and start grinding, regulate mill base flow, controlling grinding temperature not higher than 50 DEG C, after fineness reaches 20 μm, with the residue polyoxyalkylene acrylate resin taken by filling a prescription and polyester acrylate resin, the mill base in shredder being ejected;
4. mill base step 3. produced is introduced in paint mixing tank and is stirred, and adds by the dimethyl silicone oil taken of filling a prescription, moderate-speed mixer 30min;
5. mill base step 4. produced is introduced in paint mixing tank and is stirred, and then adds by other components taken of filling a prescription, moderate-speed mixer 30min;
6. mill base specification 180 mesh filter screen step 5. produced filters, packaging.
Beneficial effect of the present invention is, provides a kind of door use ultraviolet-cured paint and preparation method thereof, and technique is simple, and curing speed is fast, and product strong adhesion is ageing-resistant.
Embodiment
Be further described the specific embodiment of the present invention below in conjunction with embodiment, following examples only for technical scheme of the present invention is clearly described, and can not limit the scope of the invention with this.
Embodiment 1
The concrete technical scheme of the present invention is as follows:
A kind of door use ultraviolet-cured paint, it is characterized in that, by weight, it is made up of following component:
Polyoxyalkylene acrylate resin 55 parts, polyester acrylate resin 10 parts, urea-formaldehyde resin 13 parts, non-floating type aluminium powder 19 parts, 2; 4,6-trimethylbenzoy-dipheny phosphine oxide 1 part, dimethyl silicone oil 5 parts, p-methyl benzenesulfonic acid 1 part, calcium naphthenate 3 parts, 4 parts, zinc sulfide white, wilkinite 6 parts, stearic acid dioctyl ester 4 parts, deionized water 13 parts, butylacetate 4 parts, ethanol 13 parts, isopropylcarbinol 6 parts.
Present invention also offers the preparation method of described door use ultraviolet-cured paint:
1. take wilkinite and deionized water by formula, at use stirrer moderate-speed mixer 15min after mixing, form native cream;
2. take by filling a prescription 50% of polyoxyalkylene acrylate resin liquid measure, 50% of 50% of polyester acrylate resin liquid measure and urea-formaldehyde resin liquid measure, mix with the native cream 1. produced to step, add by the non-floating type aluminium powder, the zinc sulfide white and 2 that take of filling a prescription, 4,6-trimethylbenzoy-dipheny phosphine oxide, then stirrer is started, high-speed stirring 15min;
3. the mill base that 2. step produces is added shredder and start grinding, regulate mill base flow, control grinding temperature not higher than 50 DEG C, after fineness reaches 20 μm, with by residue polyoxyalkylene acrylate resin, polyester acrylate resin and the urea-formaldehyde resin taken of filling a prescription, the mill base in shredder is ejected;
4. mill base step 3. produced is introduced in paint mixing tank and is stirred, and adds by the dimethyl silicone oil taken of filling a prescription, moderate-speed mixer 30min;
5. mill base step 4. produced is introduced in paint mixing tank and is stirred, and then adds by other components taken of filling a prescription, moderate-speed mixer 30min;
6. mill base specification 180 mesh filter screen step 5. produced filters, packaging.
Embodiment 2
The concrete technical scheme of the present invention is as follows:
A kind of door use ultraviolet-cured paint, it is characterized in that, by weight, it is made up of following component:
Polyoxyalkylene acrylate resin 50 parts, polyester acrylate resin 5 parts, urea-formaldehyde resin 15 parts, non-floating type aluminium powder 15 parts, 2; 4,6-trimethylbenzoy-dipheny phosphine oxide 2 parts, dimethyl silicone oil 3 parts, p-methyl benzenesulfonic acid 1 part, calcium naphthenate 4 parts, 4 parts, zinc sulfide white, wilkinite 5 parts, stearic acid dioctyl ester 2 parts, deionized water 20 parts, butylacetate 5 parts, ethanol 15 parts, isopropylcarbinol 2 parts, 1 part, color material.
Present invention also offers the preparation method of described door use ultraviolet-cured paint:
1. take wilkinite and deionized water by formula, at use stirrer moderate-speed mixer 15min after mixing, form native cream;
2. take by filling a prescription 50% of polyoxyalkylene acrylate resin liquid measure, 50% of 50% of polyester acrylate resin liquid measure and urea-formaldehyde resin liquid measure, mix with the native cream 1. produced to step, add by the non-floating type aluminium powder, the zinc sulfide white and 2 that take of filling a prescription, 4,6-trimethylbenzoy-dipheny phosphine oxide, then stirrer is started, high-speed stirring 15min;
3. the mill base that 2. step produces is added shredder and start grinding, regulate mill base flow, control grinding temperature not higher than 50 DEG C, after fineness reaches 20 μm, with by residue polyoxyalkylene acrylate resin, polyester acrylate resin and the urea-formaldehyde resin taken of filling a prescription, the mill base in shredder is ejected;
4. mill base step 3. produced is introduced in paint mixing tank and is stirred, and adds by the dimethyl silicone oil taken of filling a prescription, moderate-speed mixer 30min;
5. mill base step 4. produced is introduced in paint mixing tank and is stirred, and then adds by other components taken of filling a prescription, moderate-speed mixer 30min;
6. mill base specification 180 mesh filter screen step 5. produced filters, packaging.
Embodiment 3
The concrete technical scheme of the present invention is as follows:
Polyoxyalkylene acrylate resin 70 parts, polyester acrylate resin 12 parts, urea-formaldehyde resin 8 parts, non-floating type aluminium powder 20 parts, 2; 4,6-trimethylbenzoy-dipheny phosphine oxide 1 part, dimethyl silicone oil 6 parts, p-methyl benzenesulfonic acid 2 parts, calcium naphthenate 2 parts, 3 parts, zinc sulfide white, wilkinite 8 parts, stearic acid dioctyl ester 2 parts, deionized water 15 parts, butylacetate 4 parts, ethanol 10 parts, isopropylcarbinol 2 parts, 3 parts, color material.
Present invention also offers the preparation method of described door use ultraviolet-cured paint:
1. take wilkinite and deionized water by formula, at use stirrer moderate-speed mixer 15min after mixing, form native cream;
2. take by filling a prescription 50% of polyoxyalkylene acrylate resin liquid measure, 50% of 50% of polyester acrylate resin liquid measure and urea-formaldehyde resin liquid measure, mix with the native cream 1. produced to step, add by the non-floating type aluminium powder, the zinc sulfide white and 2 that take of filling a prescription, 4,6-trimethylbenzoy-dipheny phosphine oxide, then stirrer is started, high-speed stirring 15min;
3. the mill base that 2. step produces is added shredder and start grinding, regulate mill base flow, control grinding temperature not higher than 50 DEG C, after fineness reaches 20 μm, with by residue polyoxyalkylene acrylate resin, polyester acrylate resin and the urea-formaldehyde resin taken of filling a prescription, the mill base in shredder is ejected;
4. mill base step 3. produced is introduced in paint mixing tank and is stirred, and adds by the dimethyl silicone oil taken of filling a prescription, moderate-speed mixer 30min;
5. mill base step 4. produced is introduced in paint mixing tank and is stirred, and then adds by other components taken of filling a prescription, moderate-speed mixer 30min;
6. mill base specification 180 mesh filter screen step 5. produced filters, packaging.
The above is only preferred embodiments of the present invention; it should be pointed out that for those skilled in the art, under the prerequisite not departing from the technology of the present invention principle; can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.

Claims (3)

1. a door use ultraviolet-cured paint, is characterized in that, by weight, it is made up of following component:
Polyoxyalkylene acrylate resin 50-70 part, polyester acrylate resin 5-12 part, urea-formaldehyde resin 8-15 part, non-floating type aluminium powder 15-20 part, 2; 4,6-trimethylbenzoy-dipheny phosphine oxide 1-2 part, dimethyl silicone oil 3-6 part, p-methyl benzenesulfonic acid 1-2 part, calcium naphthenate 2-4 part, zinc sulfide white 3-4 part, wilkinite 5-8 part, stearic acid dioctyl ester 2-5 part, deionized water 15-20 part, butylacetate 4-5 part, ethanol 10-15 part, isopropylcarbinol 2-8 part.
2. a kind of door use ultraviolet-cured paint as claimed in claim 1, is characterized in that, describedly also comprises color material 1-3 part.
3. a kind of door use ultraviolet-cured paint as claimed in claim 1 or 2, is characterized in that, the preparation method of described door use ultraviolet-cured paint is as follows:
1. take wilkinite and deionized water by formula, at use stirrer moderate-speed mixer 15min after mixing, form native cream;
2. take by filling a prescription 50% of polyoxyalkylene acrylate resin liquid measure, 50% of 50% of polyester acrylate resin liquid measure and urea-formaldehyde resin liquid measure, mix with the native cream 1. produced to step, add by the non-floating type aluminium powder, the zinc sulfide white and 2 that take of filling a prescription, 4,6-trimethylbenzoy-dipheny phosphine oxide, then stirrer is started, high-speed stirring 15min;
3. the mill base that 2. step produces is added shredder and start grinding, regulate mill base flow, control grinding temperature not higher than 50 DEG C, after fineness reaches 20 μm, with by residue polyoxyalkylene acrylate resin, polyester acrylate resin and the urea-formaldehyde resin taken of filling a prescription, the mill base in shredder is ejected;
4. mill base step 3. produced is introduced in paint mixing tank and is stirred, and adds by the dimethyl silicone oil taken of filling a prescription, moderate-speed mixer 30min;
5. mill base step 4. produced is introduced in paint mixing tank and is stirred, and then adds by other components taken of filling a prescription, moderate-speed mixer 30min;
6. mill base specification 180 mesh filter screen step 5. produced filters, packaging.
CN201510837041.0A 2015-11-24 2015-11-24 Water-based ultraviolet-curing paint for door and preparing method thereof Pending CN105315861A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201510837041.0A CN105315861A (en) 2015-11-24 2015-11-24 Water-based ultraviolet-curing paint for door and preparing method thereof

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Application Number Priority Date Filing Date Title
CN201510837041.0A CN105315861A (en) 2015-11-24 2015-11-24 Water-based ultraviolet-curing paint for door and preparing method thereof

Publications (1)

Publication Number Publication Date
CN105315861A true CN105315861A (en) 2016-02-10

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Country Link
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Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2002003750A (en) * 2000-06-23 2002-01-09 Sakura Color Prod Corp Acid-resistant masking coating composition
EP1516023B1 (en) * 2002-06-01 2009-02-18 BASF Coatings AG Coating substance, method for the production thereof, and use thereof for the production of adhesive coatings
CN101792636A (en) * 2010-03-10 2010-08-04 中国科学技术大学 Ultraviolet-light curable aqueous heat-insulating nano composite coating and preparation method thereof
CN102070981A (en) * 2010-12-02 2011-05-25 广州慧谷化学有限公司 Ultraviolet curing paint and preparation method and application thereof
CN102702957A (en) * 2012-06-21 2012-10-03 南京工业大学 Water-based light-cured composite glass fiber insulating sleeve coating and preparation method thereof
CN103980812A (en) * 2014-05-19 2014-08-13 上海正欧实业有限公司 UV-LED (ultraviolet-light emitting diode) photocureable coating and preparation method thereof

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2002003750A (en) * 2000-06-23 2002-01-09 Sakura Color Prod Corp Acid-resistant masking coating composition
EP1516023B1 (en) * 2002-06-01 2009-02-18 BASF Coatings AG Coating substance, method for the production thereof, and use thereof for the production of adhesive coatings
CN101792636A (en) * 2010-03-10 2010-08-04 中国科学技术大学 Ultraviolet-light curable aqueous heat-insulating nano composite coating and preparation method thereof
CN102070981A (en) * 2010-12-02 2011-05-25 广州慧谷化学有限公司 Ultraviolet curing paint and preparation method and application thereof
CN102702957A (en) * 2012-06-21 2012-10-03 南京工业大学 Water-based light-cured composite glass fiber insulating sleeve coating and preparation method thereof
CN103980812A (en) * 2014-05-19 2014-08-13 上海正欧实业有限公司 UV-LED (ultraviolet-light emitting diode) photocureable coating and preparation method thereof

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Application publication date: 20160210