CN105200821A - Dyeing method of biomass polyester and polyamide blend fiber fabric - Google Patents
Dyeing method of biomass polyester and polyamide blend fiber fabric Download PDFInfo
- Publication number
- CN105200821A CN105200821A CN201510777050.5A CN201510777050A CN105200821A CN 105200821 A CN105200821 A CN 105200821A CN 201510777050 A CN201510777050 A CN 201510777050A CN 105200821 A CN105200821 A CN 105200821A
- Authority
- CN
- China
- Prior art keywords
- dyeing
- biomass polyester
- polyamide blend
- fibre fabric
- blend fibre
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000004043 dyeing Methods 0.000 title claims abstract description 52
- 239000002028 Biomass Substances 0.000 title claims abstract description 49
- 239000004952 Polyamide Substances 0.000 title claims abstract description 48
- 229920002647 polyamide Polymers 0.000 title claims abstract description 48
- 239000004744 fabric Substances 0.000 title claims abstract description 45
- 239000000203 mixture Substances 0.000 title claims abstract description 41
- 239000000835 fiber Substances 0.000 title claims abstract description 39
- 238000000034 method Methods 0.000 title claims abstract description 30
- 229920006149 polyester-amide block copolymer Polymers 0.000 title claims abstract description 21
- 229920000728 polyester Polymers 0.000 claims abstract description 28
- 239000000975 dye Substances 0.000 claims description 22
- 238000004040 coloring Methods 0.000 claims description 18
- 238000004140 cleaning Methods 0.000 claims description 14
- 230000009467 reduction Effects 0.000 claims description 13
- 239000003795 chemical substances by application Substances 0.000 claims description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 9
- 230000004048 modification Effects 0.000 claims description 8
- 238000012986 modification Methods 0.000 claims description 8
- SJEYSFABYSGQBG-UHFFFAOYSA-M Patent blue Chemical compound [Na+].C1=CC(N(CC)CC)=CC=C1C(C=1C(=CC(=CC=1)S([O-])(=O)=O)S([O-])(=O)=O)=C1C=CC(=[N+](CC)CC)C=C1 SJEYSFABYSGQBG-UHFFFAOYSA-M 0.000 claims description 7
- 239000000980 acid dye Substances 0.000 claims description 7
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 6
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 6
- 239000007788 liquid Substances 0.000 claims description 6
- 230000008569 process Effects 0.000 claims description 6
- 230000014759 maintenance of location Effects 0.000 claims description 5
- JVBXVOWTABLYPX-UHFFFAOYSA-L sodium dithionite Chemical compound [Na+].[Na+].[O-]S(=O)S([O-])=O JVBXVOWTABLYPX-UHFFFAOYSA-L 0.000 claims description 5
- 239000000986 disperse dye Substances 0.000 claims description 4
- 229960000583 acetic acid Drugs 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 3
- 239000012362 glacial acetic acid Substances 0.000 claims description 3
- 239000003002 pH adjusting agent Substances 0.000 claims description 3
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 3
- 235000017550 sodium carbonate Nutrition 0.000 claims description 3
- 239000002253 acid Substances 0.000 claims description 2
- 238000004513 sizing Methods 0.000 claims description 2
- 239000002351 wastewater Substances 0.000 claims description 2
- 239000002932 luster Substances 0.000 abstract 1
- 230000000052 comparative effect Effects 0.000 description 3
- 230000007613 environmental effect Effects 0.000 description 2
- 210000000697 sensory organ Anatomy 0.000 description 2
- 239000004753 textile Substances 0.000 description 2
- 238000010792 warming Methods 0.000 description 2
- 239000002759 woven fabric Substances 0.000 description 2
- 239000003513 alkali Substances 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000000686 essence Substances 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000002000 scavenging effect Effects 0.000 description 1
Landscapes
- Coloring (AREA)
Abstract
The invention relates to a dyeing method of a biomass polyester and polyamide blend fiber fabric. The dyeing method comprises the following steps: carrying out first-time dyeing on the biomass polyester and polyamide blend fiber fabric by using a first dyeing solution, wherein the dyeing bath ratio is 1 to (3-7) and the dyeing temperature is 100-110 DEG C; and carrying out second-time dyeing on the biomass polyester and polyamide blend fiber fabric by using a second dyeing solution, wherein the dyeing bath ratio is 1 to (3-5) and the dyeing temperature is 90-100 DEG C. According to the dyeing method provided by the invention, by adopting a two-bath method to dye, biomass polyester components in the biomass polyester and polyamide blend fiber fabric are dyed; then polyamide components are dyed, so that the biomass polyester components and the polyamide components in the fabric are not damaged and the color fastness is good; and furthermore, by adjusting technological parameters, the bath ratio is reduced, so that the dyeing method is relatively environmentally friendly, and the produced fabric has relatively good hand feeling, color and luster, and sense.
Description
Technical field
The present invention relates to the colouring method of a kind of biomass polyester and polyamide blend fibre fabric.
Background technology
In prior art, the preparation method of biomass polyester and polyamide blend fibre fabric comprises raw material and prepares, warping, weave, Alkali reduction, the steps such as dyeing, wherein, during dyeing, adopt and now the polyamide component in biomass polyester and polyamide blend fibre fabric is dyeed, and then biomass polyester composition is dyeed, and adopt bath raio to be 1:10, because the dyeing temperature of polyamide is lower than the dyeing temperature of biomass polyester, therefore, the Color of polyamide can be destroyed during high temperature dye biomass polyester, make the COLOR FASTNESS of polyamide poor, and the gloss of the biomass polyester produced in prior art and polyamide blend fibre fabric and sense organ are not all fine.
Summary of the invention
Technical problem to be solved by this invention is to provide the good and colouring method of the biomass polyester of more environmental protection and polyamide blend fibre fabric of a kind of COLOR FASTNESS.
For solving above technical problem, the present invention takes following technical scheme:
A colouring method for biomass polyester and polyamide blend fibre fabric, it comprises the following steps of carrying out successively:
Step (1), adopt the first dyeing liquor to carry out first time to biomass polyester and polyamide blend fibre fabric to dye, dye bath ratio is 1:3 ~ 7, and dyeing temperature is 100 ~ 110 DEG C;
Step (2), adopt the second dyeing liquor that the biomass polyester after step (1) dyeing and polyamide blend fibre fabric are carried out to second time and dye, dye bath ratio is 1:3 ~ 5, and dyeing temperature is 90 ~ 100 DEG C.
Particularly, the dyeing temperature of step (1) is 104 ~ 106 DEG C.
Particularly, the bath raio of step (1) is 1:4 ~ 6.
Particularly, the dyeing temperature of step (2) is 94 ~ 96 DEG C.
Particularly, the detailed description of the invention of step (1) is:
Described biomass polyester and polyamide blend fibre fabric are carried out preliminary treatment 5 ~ 15min in the dye bath of the levelling agent containing pH adjusting agent and 1 ~ 3g/L, and the pH of described dye bath is 7 ~ 8, and pretreatment temperature is 55 ~ 65 DEG C;
After preliminary treatment completes, carry out described first time dyeing, control temperature retention time is 30 ~ 40min, and after having dyeed, adopt reduction cleaning liquid to carry out reduction cleaning 30 ~ 50min, reduction cleaning temperature is 55 ~ 65 DEG C.
More specifically, described reduction cleaning liquid is made up of sodium hydrosulfite, soda ash and water, and the concentration of described sodium hydrosulfite is 2 ~ 4g/L, and described pure paper mill wastewater is 1 ~ 3g/L.
More specifically, when carrying out described first time dyeing, controlling programming rate is 0.5 ~ 1.5 DEG C/min, and when carrying out described reduction cleaning, controlling cooling rate is 0.5 ~ 1.5 DEG C/min.
Particularly, the formula of the first described dyeing liquor is as follows: the DISPERSE DYES of 0.3 ~ 1% (o.w.f), the glacial acetic acid of 0.5 ~ 0.15% (o.w.f), surplus are water.
Particularly, the detailed description of the invention of step (2) is as follows: the biomass polyester after step (1) dyeing and polyamide blend fibre fabric are carried out described second time and dyes, control temperature retention time is 30 ~ 40min, after dyeing, adopting containing mass percent is that process 20 ~ 30min is with fixation under the condition of pH4.5 ~ 5.5 and 70 ~ 80 DEG C for the process bath of the DomafixACL of 2% ~ 3%, and then carrying out shapes obtains the biomass polyester after dyeing and polyamide blend fibre fabric.
More specifically, the temperature of the sizing described in control is 125 ~ 135 DEG C, and the speed of a motor vehicle is 15 ~ 25m/min.
Particularly, the second described dyeing liquor is made up of modification ACID DYES, levelling agent and water, and the concentration of described modification ACID DYES is 0.5 ~ 5% (o.w.f), and the concentration of described levelling agent is 0.5 ~ 3g/L.
More specifically, described modification ACID DYES is DorasynXL type dye, and described levelling agent is DoregalXL levelling agent.
Particularly, the biomass polyester in described biomass polyester and polyamide blend fibre fabric is PLA-acid fiber by polylactic.
Described biomass polyester and the commercially available acquisition of polyamide blend fibre fabric.
Due to the enforcement of above technical scheme, the present invention compared with prior art tool has the following advantages:
The present invention adopts two-bath process to dye, first the biomass polyester composition in biomass polyester and polyamide blend fibre fabric is dyeed, then polyamide component is dyeed, biomass polyester composition in fabric and polyamide component all can not be damaged, and COLOR FASTNESS is good, in addition, by the adjustment to technological parameter, bath raio is reduced, thus makes colouring method environmental protection more, and fabric feel, gloss and the sense organ produced are better.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention will be further described in detail, but the invention is not restricted to following examples.
Embodiment 1
A colouring method for biomass polyester and polyamide blend fibre fabric, it comprises the following steps of carrying out successively:
Step one a: bath, first dyes to the biomass polyester composition in biomass polyester and polyamide blended yarn woven fabric:
(1), by fabric preliminary treatment 10min is carried out in the dye bath of putting into containing pH adjusting agent and 2g/L levelling agent, and the pH value of wherein pretreated dye bath is adjusted to 7.5, temperature is 60 DEG C.
(2), then first time dyeing is carried out to fabric, the formula of the first dyeing liquor: DISPERSE DYES 0.5% (o.w.f), glacial acetic acid 0.8% (o.w.f), water; Bath raio 1:5, controls programming rate 1 DEG C/min and is warming up to 105 DEG C, temperature retention time 35min.
(3), then adopt cooling rate 1 DEG C/min to be cooled to 65 DEG C, adopt the cleaning of reduction cleaning liquid, remove the DISPERSE DYES that grey cloth is infected with, cleaning temperature is 60 DEG C, and scavenging period is 40min, reduction cleaning formula of liquid: sodium hydrosulfite 3g/L, soda ash 2g/L, water.
Step 2: two baths, then the polyamide component in biomass polyester and polyamide blended yarn woven fabric is dyeed.
(1), be warming up to 95 DEG C, insulation 35min carries out second time dyeing, the formula of the second dyeing liquor: modification ACID DYES (DorasynXL type dye) 1.5% (o.w.f), DoregalXL levelling agent 1g/L, water; Bath raio 1:4.
(2), under pH5 and 75 DEG C condition, 25min is processed with fixation with the process bath containing 2.5%DomafixACL after dyeing.
(3), then shape, setting temperature: 130 DEG C, the speed of a motor vehicle: 20m/min.
Comparative example 1
Colouring method is substantially the same manner as Example 1, unlike, dyeing temperature is 115 DEG C for the first time, and the second dyeing temperature is 105 DEG C.
Comparative example 2
Colouring method is substantially the same manner as Example 1, unlike, dyeing temperature is 95 DEG C for the first time, and the second dyeing temperature is 80 DEG C.
The technical indicators such as the dyefastness of the fabric that embodiment 1 and comparative example 1 and 2 obtain are see table 1.
Table 1
Note: detect according to GB18401-2010 " National Textile basic security technical specification ", institute's inspection project meets the category-B requirement that GB18401-2010 " National Textile basic security technical specification " standard specifies.
Above to invention has been detailed description; its object is to allow the personage being familiar with this art can understand content of the present invention and be implemented; can not limit the scope of the invention with this; the equivalence change that all Spirit Essences according to the present invention are done or modification, all should be encompassed in protection scope of the present invention.
Claims (10)
1. a colouring method for biomass polyester and polyamide blend fibre fabric, is characterized in that: it comprises the following steps of carrying out successively:
Step (1), adopt the first dyeing liquor to carry out first time to biomass polyester and polyamide blend fibre fabric to dye, dye bath ratio is 1:3 ~ 7, and dyeing temperature is 100 ~ 110 DEG C;
Step (2), adopt the second dyeing liquor that the biomass polyester after step (1) dyeing and polyamide blend fibre fabric are carried out to second time and dye, dye bath ratio is 1:3 ~ 5, and dyeing temperature is 90 ~ 100 DEG C.
2. the colouring method of biomass polyester according to claim 1 and polyamide blend fibre fabric, is characterized in that: the detailed description of the invention of step (1) is:
Described biomass polyester and polyamide blend fibre fabric are carried out preliminary treatment 5 ~ 15min in the dye bath of the levelling agent containing pH adjusting agent and 1 ~ 3g/L, and the pH of described dye bath is 7 ~ 8, and pretreatment temperature is 55 ~ 65 DEG C;
After preliminary treatment completes, carry out described first time dyeing, control temperature retention time is 30 ~ 40min, and after having dyeed, adopt reduction cleaning liquid to carry out reduction cleaning 30 ~ 50min, reduction cleaning temperature is 55 ~ 65 DEG C.
3. the colouring method of biomass polyester according to claim 2 and polyamide blend fibre fabric, it is characterized in that: described reduction cleaning liquid is made up of sodium hydrosulfite, soda ash and water, the concentration of described sodium hydrosulfite is 2 ~ 4g/L, and described pure paper mill wastewater is 1 ~ 3g/L.
4. the colouring method of biomass polyester according to claim 2 and polyamide blend fibre fabric, it is characterized in that: when carrying out described first time dyeing, controlling programming rate is 0.5 ~ 1.5 DEG C/min, and when carrying out described reduction cleaning, controlling cooling rate is 0.5 ~ 1.5 DEG C/min.
5. the colouring method of biomass polyester according to claim 1 and polyamide blend fibre fabric, is characterized in that: the formula of the first described dyeing liquor is as follows: DISPERSE DYES 0.3 ~ 1%(o.w.f), 0.5 ~ 0.15%(o.w.f) glacial acetic acid, surplus be water.
6. the colouring method of biomass polyester according to claim 1 and polyamide blend fibre fabric, it is characterized in that: the detailed description of the invention of step (2) is as follows: the biomass polyester after step (1) dyeing and polyamide blend fibre fabric are carried out described second time and dyes, control temperature retention time is 30 ~ 40min, after dyeing, adopt containing mass percent be the process bath of the DomafixACL of 2% ~ 3% under the condition of pH4.5 ~ 5.5 and 70 ~ 80 DEG C process 20 ~ 30min with fixation, then carrying out shapes obtains the biomass polyester after dyeing and polyamide blend fibre fabric.
7. the colouring method of biomass polyester according to claim 6 and polyamide blend fibre fabric, is characterized in that: the temperature of the sizing described in control is 125 ~ 135 DEG C, and the speed of a motor vehicle is 15 ~ 25m/min.
8. the colouring method of biomass polyester according to claim 1 and polyamide blend fibre fabric, it is characterized in that: the second described dyeing liquor is made up of modification ACID DYES, levelling agent and water, the concentration of described modification ACID DYES is 0.5 ~ 5%(o.w.f), the concentration of described levelling agent is 0.5 ~ 3g/L.
9. the colouring method of biomass polyester according to claim 8 and polyamide blend fibre fabric, is characterized in that: described modification ACID DYES is DorasynXL type dye, and described levelling agent is DoregalXL levelling agent.
10. the colouring method of biomass polyester according to claim 1 and polyamide blend fibre fabric, is characterized in that: the biomass polyester in described biomass polyester and polyamide blend fibre fabric is PLA-acid fiber by polylactic.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510777050.5A CN105200821B8 (en) | 2015-11-13 | 2015-11-13 | A kind of colouring method of biomass polyester and polyamide blend fibre fabric |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510777050.5A CN105200821B8 (en) | 2015-11-13 | 2015-11-13 | A kind of colouring method of biomass polyester and polyamide blend fibre fabric |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| CN105200821A true CN105200821A (en) | 2015-12-30 |
| CN105200821B CN105200821B (en) | 2017-08-25 |
| CN105200821B8 CN105200821B8 (en) | 2017-10-17 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201510777050.5A Active CN105200821B8 (en) | 2015-11-13 | 2015-11-13 | A kind of colouring method of biomass polyester and polyamide blend fibre fabric |
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| CN (1) | CN105200821B8 (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109295751A (en) * | 2018-09-20 | 2019-02-01 | 罗曼罗兰创意设计（苏州）有限公司 | A kind of colouring method of biomass polyester and biomass polyester amine blend fibre fabric |
| CN110565403A (en) * | 2019-09-12 | 2019-12-13 | 杭州卓达染整有限公司 | polyester-nylon composite yarn fabric dyeing method |
| CN111058149A (en) * | 2019-12-18 | 2020-04-24 | 晋江市远祥服装织造有限公司 | Biomass polyester and polyamide blended fabric and preparation method and product thereof |
| CN115387138A (en) * | 2022-09-30 | 2022-11-25 | 舒普林印染有限公司 | Disperse dyeing process of super cotton-like polyester fiber knitted fabric |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1391623A (en) * | 1999-11-25 | 2003-01-15 | 卡尔·弗罗伊登伯格公司 | Method for producing dyed textile materials consisting of polyester and polyamide |
| CN1993515A (en) * | 2004-08-04 | 2007-07-04 | 崔诚训 | A method for dyeing microfibers and fabric woven with microfibers dyed thereby |
| CN103628267A (en) * | 2013-12-04 | 2014-03-12 | 北京富泰革基布股份有限公司 | Polyamide fiber and polyester fiber composite synthetic leather and processing technology |
-
2015
- 2015-11-13 CN CN201510777050.5A patent/CN105200821B8/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1391623A (en) * | 1999-11-25 | 2003-01-15 | 卡尔·弗罗伊登伯格公司 | Method for producing dyed textile materials consisting of polyester and polyamide |
| CN1993515A (en) * | 2004-08-04 | 2007-07-04 | 崔诚训 | A method for dyeing microfibers and fabric woven with microfibers dyed thereby |
| CN103628267A (en) * | 2013-12-04 | 2014-03-12 | 北京富泰革基布股份有限公司 | Polyamide fiber and polyester fiber composite synthetic leather and processing technology |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109295751A (en) * | 2018-09-20 | 2019-02-01 | 罗曼罗兰创意设计（苏州）有限公司 | A kind of colouring method of biomass polyester and biomass polyester amine blend fibre fabric |
| CN110565403A (en) * | 2019-09-12 | 2019-12-13 | 杭州卓达染整有限公司 | polyester-nylon composite yarn fabric dyeing method |
| CN110565403B (en) * | 2019-09-12 | 2022-03-22 | 杭州卓达染整有限公司 | Polyester-nylon composite yarn fabric dyeing method |
| CN111058149A (en) * | 2019-12-18 | 2020-04-24 | 晋江市远祥服装织造有限公司 | Biomass polyester and polyamide blended fabric and preparation method and product thereof |
| CN115387138A (en) * | 2022-09-30 | 2022-11-25 | 舒普林印染有限公司 | Disperse dyeing process of super cotton-like polyester fiber knitted fabric |
Also Published As
| Publication number | Publication date |
|---|---|
| CN105200821B8 (en) | 2017-10-17 |
| CN105200821B (en) | 2017-08-25 |
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| CB03 | Change of inventor or designer information |
Inventor after: Zhai Tao Inventor after: Zhou Yan Inventor after: Cao Guolan Inventor after: Niu Yanyan Inventor before: Zhou Yan Inventor before: Sun Xiankang Inventor before: Zhai Tao Inventor before: Cao Guolan Inventor before: Niu Yanyan |
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Effective date of registration: 20170817 Address after: 215228, No. 10, building 1188, west two ring road, Shengze Town, Wujiang District, Jiangsu, Suzhou Patentee after: SUZHOU RUIZHONG NEW MATERIAL TECHNOLOGY CO.,LTD. Address before: 215228 No. 7, No., Central Avenue, Shengze town textile technology demonstration zone, Wujiang District, Jiangsu, China Patentee before: Suzhou CINC Textile Technologies Stock Corp. |
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| TR01 | Transfer of patent right | ||
| CI03 | Correction of invention patent |
Correction item: Patentee|Address|Inventor Correct: Suzhou Ruizhong New Material Technology Co., Ltd.|215228, No. 10, building 1188, west two ring road, Shengze Town, Wujiang District, Jiangsu, Suzhou|Di Tao|Zhou Yan|Cao Guolan|Niu Yanyan False: Suzhou CINC Textile Technologies Stock Corp.|215228 No. 7, No., Central Avenue, Shengze town textile technology demonstration zone, Wujiang District, Jiangsu, China|Zhou Yan|Sun Xiankang|Di Tao|Cao Guolan|Niu Yanyan Number: 34-02 Page: The title page Volume: 33 Correction item: Patentee|Address|Inventor Correct: Suzhou Ruizhong New Material Technology Co., Ltd.|215228, No. 10, building 1188, west two ring road, Shengze Town, Wujiang District, Jiangsu, Suzhou|Di Tao|Zhou Yan|Cao Guolan|Niu Yanyan False: Suzhou CINC Textile Technologies Stock Corp.|215228 No. 7, No., Central Avenue, Shengze town textile technology demonstration zone, Wujiang District, Jiangsu, China|Zhou Yan|Sun Xiankang|Di Tao|Cao Guolan|Niu Yanyan Number: 34-02 Volume: 33 |
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| CI03 | Correction of invention patent |