CN105174907A - 3D printing clay material and preparation method thereof - Google Patents
3D printing clay material and preparation method thereof Download PDFInfo
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- CN105174907A CN105174907A CN201510369622.6A CN201510369622A CN105174907A CN 105174907 A CN105174907 A CN 105174907A CN 201510369622 A CN201510369622 A CN 201510369622A CN 105174907 A CN105174907 A CN 105174907A
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- 239000004927 clay Substances 0.000 title claims abstract description 58
- 239000000463 material Substances 0.000 title claims abstract description 44
- 238000010146 3D printing Methods 0.000 title claims abstract description 38
- 238000002360 preparation method Methods 0.000 title claims abstract description 9
- 230000004048 modification Effects 0.000 claims abstract description 15
- 238000012986 modification Methods 0.000 claims abstract description 15
- 238000000034 method Methods 0.000 claims description 42
- 239000000203 mixture Substances 0.000 claims description 30
- 239000000843 powder Substances 0.000 claims description 15
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 14
- 238000001816 cooling Methods 0.000 claims description 8
- 239000013078 crystal Substances 0.000 claims description 8
- 238000010298 pulverizing process Methods 0.000 claims description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- 150000001875 compounds Chemical class 0.000 claims description 7
- 238000007599 discharging Methods 0.000 claims description 7
- 238000000227 grinding Methods 0.000 claims description 7
- 238000004898 kneading Methods 0.000 claims description 7
- 239000005995 Aluminium silicate Substances 0.000 claims description 5
- 239000004698 Polyethylene Substances 0.000 claims description 5
- 235000012211 aluminium silicate Nutrition 0.000 claims description 5
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims description 5
- -1 polyethylene Polymers 0.000 claims description 5
- 229920000573 polyethylene Polymers 0.000 claims description 5
- 239000001993 wax Substances 0.000 claims description 5
- OSGAYBCDTDRGGQ-UHFFFAOYSA-L calcium sulfate Chemical compound [Ca+2].[O-]S([O-])(=O)=O OSGAYBCDTDRGGQ-UHFFFAOYSA-L 0.000 claims description 4
- GUJOJGAPFQRJSV-UHFFFAOYSA-N dialuminum;dioxosilane;oxygen(2-);hydrate Chemical compound O.[O-2].[O-2].[O-2].[Al+3].[Al+3].O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O GUJOJGAPFQRJSV-UHFFFAOYSA-N 0.000 claims description 4
- 229910052901 montmorillonite Inorganic materials 0.000 claims description 4
- 239000012188 paraffin wax Substances 0.000 claims description 4
- 229910052581 Si3N4 Inorganic materials 0.000 claims description 3
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 3
- NJLLQSBAHIKGKF-UHFFFAOYSA-N dipotassium dioxido(oxo)titanium Chemical compound [K+].[K+].[O-][Ti]([O-])=O NJLLQSBAHIKGKF-UHFFFAOYSA-N 0.000 claims description 3
- 239000010433 feldspar Substances 0.000 claims description 3
- 239000010453 quartz Substances 0.000 claims description 3
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 claims description 3
- 229910010271 silicon carbide Inorganic materials 0.000 claims description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 3
- HQVNEWCFYHHQES-UHFFFAOYSA-N silicon nitride Chemical compound N12[Si]34N5[Si]62N3[Si]51N64 HQVNEWCFYHHQES-UHFFFAOYSA-N 0.000 claims description 3
- OJMOMXZKOWKUTA-UHFFFAOYSA-N aluminum;borate Chemical compound [Al+3].[O-]B([O-])[O-] OJMOMXZKOWKUTA-UHFFFAOYSA-N 0.000 claims description 2
- 238000003837 high-temperature calcination Methods 0.000 claims description 2
- 238000005516 engineering process Methods 0.000 abstract description 10
- 238000000465 moulding Methods 0.000 abstract description 6
- 238000007493 shaping process Methods 0.000 description 8
- 239000000919 ceramic Substances 0.000 description 7
- 238000007639 printing Methods 0.000 description 4
- 230000007547 defect Effects 0.000 description 2
- 229910010272 inorganic material Inorganic materials 0.000 description 2
- 239000011147 inorganic material Substances 0.000 description 2
- 238000002844 melting Methods 0.000 description 2
- 230000008018 melting Effects 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 238000003723 Smelting Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229940036811 bone meal Drugs 0.000 description 1
- 239000002374 bone meal Substances 0.000 description 1
- 229920006351 engineering plastic Polymers 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 238000010304 firing Methods 0.000 description 1
- 235000021552 granulated sugar Nutrition 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000007769 metal material Substances 0.000 description 1
- 239000011505 plaster Substances 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 238000005245 sintering Methods 0.000 description 1
- 238000004513 sizing Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
Abstract
The invention relates to a 3D printing clay material and a preparation method thereof. According to the present invention, in order to obtain the clay material suitable for 3D printing technology, the clay is subjected to the modification treatment so as to obtain the clay material, wherein the clay material has advantages of good plasticity, easy molding, good mechanical property and high precision, is suitable for the 3D printing molding technology, promotes the promotion application of the 3D printing molding technology, and has broad market prospects.
Description
Technical field
The present invention relates to a kind of 3D printed material and preparation method thereof, be specifically related to a kind of 3D printing clay material and preparation method thereof.
Background technology
3D printing technique, also known as increasing material manufacturing technology, is a kind of emerging technology in rapid shaping field, and it is a kind of based on digital model file, uses powdery metal or plastics etc. can jointing material, is carried out the technology of constructed object by the mode successively printed.Along with development and the application of 3D printing technique, can the development of material decide 3D and print have and apply widely, and material becomes one of key factor of restriction 3D printing technique future trend.At present, 3D printed material mainly comprises engineering plastics, photosensitive resin, rubber type of material, metallic substance and stupalith etc., in addition, the foodstuffs material such as coloured plaster material, artificial bone meal, cell biological raw material, wood materials and granulated sugar also prints field at 3D and obtains application.
Clay is as one of mankind's application inorganic materials the earliest, have that storage is enriched, advantage with low cost, so far be still apply maximum inorganic materials during people live, clay not only can be used for firing of stupalith, house is built, laying road etc., industry can also be used for, as the process of the filler in macromolecular material, waste water, the smelting etc. of metal.Along with the development of 3D printing technique, various material is applied to 3D and prints, and the using method of traditional material also there occurs change, the appearance of 3D printing technique, and the using method being similarly clay provides new thinking.When utilizing 3D printing technique forming ceramic products, the 3D printed material that people use is all the ceramic powder fired by clay, then ceramic product is obtained by direct or indirect method, but the preparation method of ceramic powder is complicated and with high costs, seriously hinder the development of 3D printing technique on forming process of ceramics and application.Clay itself has excellent viscosity and plasticity-, ceramic body can be made by straight forming, then sintering obtains pottery, but due to the defect of technique, technology, it is simple that shaping ceramic idiosome has structure, the shortcomings such as poor dimensional precision, seriously limit clay and the application of goods in life thereof, if 3D printing technique be used for clay and then shapingly obtain pottery, can improve completely and solve above-mentioned defect, therefore, clay is used for 3D printing shaping to clay and the application of goods in life is significant and marketable value.
Clay material without modification is not suitable for 3D printing shaping, the clay mechanical property of high-ductility is poor, be unfavorable for the support in moulding process and moulding, and the good clay cohesiveness of mechanical property and plasticity poor, be unfavorable for bonding in moulding process and extrude, thus, needing to carry out modification to clay, obtaining the clay material being suitable for 3D printing technique, is the precondition that clay can be used for 3D printing technique.
Summary of the invention
The present invention, in order to expand the range of application of 3D printing technique in life, makes clay material can be used for 3D printing technique, carries out modification to clay, thus proposes a kind of 3D printing clay material and preparation method thereof.
A kind of 3D printing of the present invention clay material, it is characterized in that pulverous clay mixture, its material weight part is composed as follows:
Clay 50-65 part,
Aggregate 1-20 part,
Carrier 20-35 part,
Treating compound 10-20 part,
Toughner 3-8 part,
Wherein said clay is that to eliminate organic fineness through high-temperature calcination be one or both in 800-2000 object kaolin, polynite; Described aggregate to be fineness be in 500-2000 object hydromuscovite powder, montmorillonite powder, quartz powder and feldspar powder one or more; Described carrier is one or both in paraffin, polyethylene wax; Described treating compound is that water and ethanol are by 1: 2 miscible ethanolic soln; Described toughner is one or more in silicon carbide whisker, silicon nitride crystal whisker, potassium titanate crystal whisker, aluminium borate whisker, alumina whisker, ZnOw, calcium sulfate crystal whiskers.
Above-mentioned a kind of 3D printing clay material is obtained by following preparation method, it is characterized in that concrete steps are as follows:
1, the treating compound of the carrier of the aggregate of the clay of 50-65 weight, 1-20 weight part, 20-35 weight part, 10-20 weight part, the toughner of 3-8 weight part are added in planetary ball mill carry out mixed grinding 1-2h and obtain mixture A;
2, mixture A step 1 obtained puts into high temperature modification kneader, temperature be 90-120 DEG C, speed carry out under being the condition of 20-30r/min kneading process 20-30min after discharging, room temperature cooling after obtain mixture B;
3, mixture B Lowtemperaturepulverizer step 2 obtained carries out pulverization process, and pulverize temperature and be-5-0 DEG C, smashing fineness is 800-1200 order, obtains a kind of 3D printing clay material.
The present invention, in order to obtain the clay material being applicable to 3D printing technique, has carried out modification to clay: the characteristic utilizing carrier at high temperature melting, by clay parcel in the carrier, can carry out shaping printing during printing after melting, the sizing of cooling after fixing; Adding treating compound makes clay plasticity better, can better be coated in carrier; Add toughner, improve the toughness of clay, during 3D printing shaping, mechanical property is better, prints the toughness of products obtained also more excellent; Have employed planetary ball mill and high temperature modification kneader processes clay, not only make carrier evenly wrap up clay material, and gap between each material is little, density is large, and thus shrinking percentage is little, and printing precision is high.It is good that the clay material adopting above-mentioned method of modifying to obtain has plasticity, easy-formation, and mechanical property is good, the advantage that precision is high, is applicable to 3D printing shaping technology, facilitates applying of 3D printing shaping technology, have wide market outlook.
The feature that the present invention gives prominence to and beneficial effect are:
1, the present invention is in order to be used for 3D printing technique by clay, has carried out modification to clay, obtains a kind of clay material being suitable for 3D and printing.
2, the present invention proposes the method for clay being carried out to modification, preparing one, to have plasticity good, and easy-formation, mechanical property is good, the clay material that precision is high.
3, the product size precision that the inventive method is obtained is good, and forming shape easily controls, and method is simple and reliable, with low cost.
Embodiment
Below by way of embodiment, the present invention is described in further detail, but this should be interpreted as scope of the present invention is only limitted to following example.When not departing from aforesaid method thought of the present invention, the various replacement made according to ordinary skill knowledge and customary means or change, all should be within the scope of the present invention.
embodiment 1
1,500 object hydromuscovite powder of 800 order kaolin of 50 weight, 10 weight parts, the paraffin of 20 weight parts, the water of 10 weight parts and ethanol are added in planetary ball mill by the silicon carbide whisker of 1: 2 miscible ethanolic soln, 3 weight parts carry out mixed grinding 1h and obtain mixture A;
2, mixture A step 1 obtained puts into high temperature modification kneader, temperature be 90 DEG C, speed carry out under being the condition of 30r/min kneading process 20min after discharging, room temperature cooling after obtain mixture B;
3, mixture B Lowtemperaturepulverizer step 2 obtained carries out pulverization process, and pulverizing temperature is 0 DEG C, and smashing fineness is 800 orders, obtains a kind of 3D printing clay material.
embodiment 2
1,2000 object montmorillonite powder of 2000 object kaolin of 65 weight, 20 weight parts, the polyethylene wax of 35 weight parts, the water of 20 weight parts and ethanol are added in planetary ball mill by the silicon nitride crystal whisker of 1: 2 miscible ethanolic soln, 8 weight parts carry out mixed grinding 1h and obtain mixture A;
2, mixture A step 1 obtained puts into high temperature modification kneader, temperature be 120 DEG C, speed carry out under being the condition of 20r/min kneading process 20min after discharging, room temperature cooling after obtain mixture B;
3, mixture B Lowtemperaturepulverizer step 2 obtained carries out pulverization process, and pulverize temperature and be-5 DEG C, smashing fineness is 800 orders, obtains a kind of 3D printing clay material.
embodiment 3
1,2000 object quartz powders of 800 object polynites of 55 weight, 10 weight parts, the paraffin of 25 weight parts, the water of 15 weight parts and ethanol are added in planetary ball mill by the potassium titanate crystal whisker of 1: 2 miscible ethanolic soln, 5 weight parts carry out mixed grinding 1.5h and obtain mixture A;
2, mixture A step 1 obtained puts into high temperature modification kneader, temperature be 100 DEG C, speed carry out under being the condition of 25r/min kneading process 25min after discharging, room temperature cooling after obtain mixture B;
3, mixture B Lowtemperaturepulverizer step 2 obtained carries out pulverization process, and pulverize temperature and be-3 DEG C, smashing fineness is 800 orders, obtains a kind of 3D printing clay material.
embodiment 4
1,2000 object feldspar powder of 2000 object polynites of 60 weight, 15 weight parts, the polyethylene wax of 20 weight parts, the water of 10 weight parts and ethanol are added in planetary ball mill by the ZnOw of 1: 2 miscible ethanolic soln, 6 weight parts carry out mixed grinding 1h and obtain mixture A;
2, mixture A step 1 obtained puts into high temperature modification kneader, temperature be 110 DEG C, speed carry out under being the condition of 20r/min kneading process 20min after discharging, room temperature cooling after obtain mixture B;
3, mixture B Lowtemperaturepulverizer step 2 obtained carries out pulverization process, and pulverize temperature and be-4 DEG C, smashing fineness is 1000 orders, obtains a kind of 3D printing clay material.
embodiment 5
1,2000 object water montmorillonite powder of 1000 object kaolin of 50 weight, 30 weight parts, the polyethylene wax of 30 weight parts, the water of 15 weight parts and ethanol are added in planetary ball mill by the alumina whisker of 1: 2 miscible ethanolic soln, 8 weight parts carry out mixed grinding 2h and obtain mixture A;
2, mixture A step 1 obtained puts into high temperature modification kneader, temperature be 95 DEG C, speed carry out under being the condition of 25r/min kneading process 25min after discharging, room temperature cooling after obtain mixture B;
3, mixture B Lowtemperaturepulverizer step 2 obtained carries out pulverization process, and pulverize temperature and be-5 DEG C, smashing fineness is 800 orders, obtains a kind of 3D printing clay material.
Claims (2)
1. a 3D printing clay material, it is characterized in that pulverous clay mixture, and its material weight part is composed as follows:
Clay 50-65 part,
Aggregate 1-20 part,
Carrier 20-35 part,
Treating compound 10-20 part,
Toughner 3-8 part,
Wherein said clay is that to eliminate organic fineness through high-temperature calcination be one or both in 800-2000 object kaolin, polynite; Described aggregate to be fineness be in 500-2000 object hydromuscovite powder, montmorillonite powder, quartz powder and feldspar powder one or more; Described carrier is one or both in paraffin, polyethylene wax; Described treating compound is that water and ethanol are by 1: 2 miscible ethanolic soln; Described toughner is one or more in silicon carbide whisker, silicon nitride crystal whisker, potassium titanate crystal whisker, aluminium borate whisker, alumina whisker, ZnOw, calcium sulfate crystal whiskers.
2. a kind of 3D printing clay material according to claim 1, it is characterized in that being obtained by following preparation method, concrete steps are as follows:
1) treating compound of the carrier of the aggregate of the clay of 50-65 weight, 1-20 weight part, 20-35 weight part, 10-20 weight part, the toughner of 3-8 weight part are added in planetary ball mill carry out mixed grinding 1-2h and obtain mixture A;
2) by step 1) the mixture A that obtains puts into high temperature modification kneader, temperature be 90-120 DEG C, speed carry out kneading process 20-30min under being the condition of 20-30r/min after discharging, obtain mixture B after room temperature cooling;
3) by step 2) the mixture B Lowtemperaturepulverizer that obtains carries out pulverization process, and pulverize temperature and be-5-0 DEG C, smashing fineness is 800-1200 order, obtains a kind of 3D printing clay material.
Priority Applications (1)
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| CN201510369622.6A CN105174907A (en) | 2015-06-30 | 2015-06-30 | 3D printing clay material and preparation method thereof |
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| CN201510369622.6A CN105174907A (en) | 2015-06-30 | 2015-06-30 | 3D printing clay material and preparation method thereof |
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| CN105174907A true CN105174907A (en) | 2015-12-23 |
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