CN105125475A - Cosmetic film-forming moisture preserving additive - Google Patents
Cosmetic film-forming moisture preserving additive Download PDFInfo
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- CN105125475A CN105125475A CN201510620696.2A CN201510620696A CN105125475A CN 105125475 A CN105125475 A CN 105125475A CN 201510620696 A CN201510620696 A CN 201510620696A CN 105125475 A CN105125475 A CN 105125475A
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- 239000002537 cosmetic Substances 0.000 title claims abstract description 47
- 239000000654 additive Substances 0.000 title claims abstract description 11
- 230000000996 additive effect Effects 0.000 title claims abstract description 11
- 238000000855 fermentation Methods 0.000 claims abstract description 43
- 230000004151 fermentation Effects 0.000 claims abstract description 43
- 230000000968 intestinal effect Effects 0.000 claims abstract description 14
- 210000000813 small intestine Anatomy 0.000 claims abstract description 14
- FNAQSUUGMSOBHW-UHFFFAOYSA-H calcium citrate Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O.[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O FNAQSUUGMSOBHW-UHFFFAOYSA-H 0.000 claims abstract description 8
- 239000001354 calcium citrate Substances 0.000 claims abstract description 8
- 238000002156 mixing Methods 0.000 claims abstract description 8
- 235000013337 tricalcium citrate Nutrition 0.000 claims abstract description 8
- 239000000080 wetting agent Substances 0.000 claims description 30
- 239000007788 liquid Substances 0.000 claims description 26
- 239000012528 membrane Substances 0.000 claims description 18
- 238000003756 stirring Methods 0.000 claims description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 16
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 12
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 12
- 239000001963 growth medium Substances 0.000 claims description 12
- 239000003921 oil Substances 0.000 claims description 12
- 238000010298 pulverizing process Methods 0.000 claims description 12
- 238000007789 sealing Methods 0.000 claims description 12
- DCKVNWZUADLDEH-UHFFFAOYSA-N sec-butyl acetate Chemical compound CCC(C)OC(C)=O DCKVNWZUADLDEH-UHFFFAOYSA-N 0.000 claims description 12
- 230000001954 sterilising effect Effects 0.000 claims description 12
- 238000004659 sterilization and disinfection Methods 0.000 claims description 12
- 239000000203 mixture Substances 0.000 claims description 11
- 230000003203 everyday effect Effects 0.000 claims description 10
- 230000003020 moisturizing effect Effects 0.000 claims description 10
- 238000005406 washing Methods 0.000 claims description 7
- 241001116389 Aloe Species 0.000 claims description 6
- 241000717739 Boswellia sacra Species 0.000 claims description 6
- DKPFZGUDAPQIHT-UHFFFAOYSA-N Butyl acetate Natural products CCCCOC(C)=O DKPFZGUDAPQIHT-UHFFFAOYSA-N 0.000 claims description 6
- 239000004863 Frankincense Substances 0.000 claims description 6
- 239000002253 acid Substances 0.000 claims description 6
- 235000011399 aloe vera Nutrition 0.000 claims description 6
- 239000012531 culture fluid Substances 0.000 claims description 6
- 239000008367 deionised water Substances 0.000 claims description 6
- 229910021641 deionized water Inorganic materials 0.000 claims description 6
- 238000004821 distillation Methods 0.000 claims description 6
- 238000000605 extraction Methods 0.000 claims description 6
- 239000011521 glass Substances 0.000 claims description 6
- FUZZWVXGSFPDMH-UHFFFAOYSA-N hexanoic acid Chemical compound CCCCCC(O)=O FUZZWVXGSFPDMH-UHFFFAOYSA-N 0.000 claims description 6
- 238000011081 inoculation Methods 0.000 claims description 6
- 239000002609 medium Substances 0.000 claims description 6
- 239000002243 precursor Substances 0.000 claims description 6
- 230000001105 regulatory effect Effects 0.000 claims description 6
- 238000011218 seed culture Methods 0.000 claims description 6
- 210000000582 semen Anatomy 0.000 claims description 6
- 239000007787 solid Substances 0.000 claims description 6
- 239000000725 suspension Substances 0.000 claims description 6
- 238000009423 ventilation Methods 0.000 claims description 6
- 238000000034 method Methods 0.000 abstract description 9
- 239000000126 substance Substances 0.000 abstract description 5
- 239000000463 material Substances 0.000 abstract description 3
- 239000003814 drug Substances 0.000 abstract description 2
- 239000002994 raw material Substances 0.000 abstract description 2
- 230000003712 anti-aging effect Effects 0.000 abstract 1
- 238000002386 leaching Methods 0.000 abstract 1
- 230000007774 longterm Effects 0.000 abstract 1
- 239000003925 fat Substances 0.000 description 47
- 230000000694 effects Effects 0.000 description 7
- 230000032683 aging Effects 0.000 description 4
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 3
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 3
- 230000002159 abnormal effect Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 230000005764 inhibitory process Effects 0.000 description 2
- 230000007102 metabolic function Effects 0.000 description 2
- 230000035479 physiological effects, processes and functions Effects 0.000 description 2
- 230000004215 skin function Effects 0.000 description 2
- 230000035943 smell Effects 0.000 description 2
- CYDQOEWLBCCFJZ-UHFFFAOYSA-N 4-(4-fluorophenyl)oxane-4-carboxylic acid Chemical compound C=1C=C(F)C=CC=1C1(C(=O)O)CCOCC1 CYDQOEWLBCCFJZ-UHFFFAOYSA-N 0.000 description 1
- 206010020649 Hyperkeratosis Diseases 0.000 description 1
- 206010020751 Hypersensitivity Diseases 0.000 description 1
- 239000004909 Moisturizer Substances 0.000 description 1
- 239000002202 Polyethylene glycol Substances 0.000 description 1
- 208000026935 allergic disease Diseases 0.000 description 1
- 230000000172 allergic effect Effects 0.000 description 1
- 230000007815 allergy Effects 0.000 description 1
- 208000010668 atopic eczema Diseases 0.000 description 1
- 230000004888 barrier function Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- CDQSJQSWAWPGKG-UHFFFAOYSA-N butane-1,1-diol Chemical compound CCCC(O)O CDQSJQSWAWPGKG-UHFFFAOYSA-N 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000001276 controlling effect Effects 0.000 description 1
- 230000002354 daily effect Effects 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 239000003845 household chemical Substances 0.000 description 1
- 230000001333 moisturizer Effects 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 235000014593 oils and fats Nutrition 0.000 description 1
- 229920001223 polyethylene glycol Polymers 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 230000001835 salubrious effect Effects 0.000 description 1
- 239000001540 sodium lactate Substances 0.000 description 1
- 229940005581 sodium lactate Drugs 0.000 description 1
- 235000011088 sodium lactate Nutrition 0.000 description 1
- 230000004936 stimulating effect Effects 0.000 description 1
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- Cosmetics (AREA)
Abstract
The invention discloses a cosmetic film-forming moisture preserving additive, belonging to the daily use chemical field and pharmaceuticals industry. The cosmetic film-forming moisture preserving additive takes the small intestine of a pig as a raw material, is obtained by the steps of taking intestinal oil, performing fermentation on the intestinal oil, then then leaching by a calcium citrate solution and mildewing, extracting a mycin solution in mycete after the mycete grows up, and mixing the mycin solution with cosmetic materials at last. An embodiment proves that the cosmetic film-forming moisture preserving additive is simple and easy to implement,a method is unique and novel, after being used for a long term, the moisture level of the cosmetic added the cosmetic film-forming moisture preserving additive is higher than that of a cosmetic without the cosmetic film-forming moisture preserving additive by more than 75 percent including 75 percent, anti-aging is realized, and any harm to skin does not exist.
Description
Technical field
The invention discloses a kind of cosmetics film forming moisturizing additive, belong to household chemicals field and pharmaceuticals industry.
Background technology
Along with growth in the living standard, cosmetics have become the indispensable the articles for daily use of people, to the requirement of cosmetics also in raising, day by day tend to natural, nutrition and safe and non-stimulating property etc.Wetting agent is a class can absorb moisture hygroscopic compound from humid air, and wetting agent is by absorbing and keeping moisture to reach moisturizing, moisten, recover the effects such as elasticity of skin, because xerodermatic true cause is water deficient in horny layer; Keratodermatitis works the barrier effect controlling crust moisture loss, for keeping the balance of moisture of skin, keratose should keep certain moisture to change with the humidity resisting external environment, that is, make skin smooth, softness and high resilience, the water content of skin mesocuticle must be made to keep optimum state, it is generally acknowledged, cuticular water content should between 12 ~ 20%, lower than 10%, skin will be dry, coarsely even chap, therefore, we can keep again the material of keratodermatitis moisture to be referred to as wetting agent.
In recent years, people had had brand-new understanding for skin moisture-keeping, no longer met oils and fats skin protection in the past, but some salubrious replenishing water and preserving moisture products are shown special preference to, therefore, various wetting agent and moisturizer just arise at the historic moment, and its market prospect is considerable.Traditional wetting agent mainly contains glycerol, propylene glycol, butanediol, Polyethylene Glycol, sodium lactate etc., they synthesize by chemical method, although moistening effect is good, but for life-time service, certain harm can be caused for skin, and although wetting agent can absorb moisture and reaches moistening effect from air, must, under high humidity environment, make skin drier when moisture can be absorbed from the nexine of skin on the contrary under dry arctic weather condition.Although add conventional sealer moistening effect in addition in wetting agent to be improved, but sealer abnormal smells from the patient is special, airtight, certain inhibition is had for the physiology of skin and metabolic function, life-time service can cause allergy and redness, therefore, research is a kind of pins the moisture content of skin own, and the wetting agent absorbing outside moisture is the direction of researching and developing from now on.
Summary of the invention
The technical problem that the present invention mainly solves: for current wetting agent mostly containing chemical composition, although moistening effect is good, but life-time service can cause certain harm to skin, wetting agent conventional in addition just must can play effect under high humidity environment, and the sealer abnormal smells from the patient wherein contained is special, airtight, there is certain inhibition for the physiology of skin and metabolic function, life-time service can cause irritated and red and swollen problem, provides a kind of cosmetics film forming moisturizing additive.The method take pig small intestine as raw material, after getting loose fat, loose fat is fermented, mouldy by calcium citrate solutions drip washing afterwards, the mycin liquid in mycete is extracted after mycete grows, finally by mycin liquid and cosmetic material mixing, thus make a kind of cosmetics film forming of the present invention moisturizing additive.The wetting agent that the method is made is not only containing chemical substance; skin is not injured, and natural protecting film can be formed for skin after using, pin skin internal moisture on the one hand; from external environment, absorb moisture content on the other hand, make skin ambient relative humidity reach more than 75%.
In order to solve the problems of the technologies described above, the technical solution adopted in the present invention is:
(1) get fresh pig small intestinal 5 ~ 10kg, after dirt inside and outside clean water pig small intestine and external skin fat, pig small intestine are put into archenteron-scrapping machine, remove intestinal skin, casing, obtain loose fat;
(2) after loose fat obtained above being put into pulverizer pulverizing, put in the fermentation tank after sterilization, be placed in the place of ventilation, lucifuge, the deionized water adding loose fat weight 3 ~ 5 times afterwards carries out fermentation process to it, first regulates fermentation temperature to be 30 ~ 45 DEG C, sealing and fermenting 10 ~ 12 days, then fermentation temperature to 38 ~ 55 DEG C are heightened, sealing and fermenting 13 ~ 15 days, after its loose fat complete fermentation terminates, must mix turbid liquid;
(3) turbid for mixing obtained above liquid is put into the glass container after sterilization, hide with gauze, set temperature is 25 ~ 32 DEG C, relative air humidity is 60 ~ 75%, places 5 ~ 8 days, after making himself mouldy, working concentration is the calcium citrate solutions of 0.9mol/L, adjust ph is after 5.8 ~ 6.5, and every day carries out drip washing 1 ~ 3 time, till mycete grows completely to mycete;
(4) the loose fat mycete of generation is inoculated on solid medium, cultivate 5 ~ 7 days at temperature 25 DEG C, obtain loose fat mycotic spore culture, then to be made in inoculation of suspension liquid to seed tank in sterilized culture medium, pass into filtrated air afterwards, cultivate 20 ~ 25h at 26 DEG C after, seed culture fluid is inoculated into fermentation tank sterilized containing in the culture medium of ALPHA Tolylic acid precursor, again pass into filtrated air, stir, cultivate 3 ~ 5 days at 24 DEG C, afterwards fermentation liquid is cooled, filter, pH to 2 ~ 2.5 are regulated with the hydrochloric acid solution that concentration is 0.4mol/L, and carry out multi-stage counter current extraction with butyl acetate, obtain butyl ester extract, by this butyl ester extract through activated carbon decolorizing, after distillation loose fat mycete extracting solution,
(5) a 3L sealed container is got, separate from centre with a semipermeable membrane, be divided into two-layer up and down, the loose fat mycete extracting solution obtained in above-mentioned steps is poured on semipermeable membrane upper strata, afterwards container top is pressurizeed, pressure is set to 1 ~ 3MPa, gets semipermeable membrane upper strata concentrated solution after pressurization 15 ~ 20min;
(6) according to the mass fraction, get 15 ~ 25 parts of roseleafs, 2 ~ 6 parts of Folium Aloes are put into jet mill and are carried out micron-class superfine pulverizing, obtain 10 ~ 20 μm of superfines, slowly add part 20 ~ 25 parts of Semen Cucumidis sativi oil and 30 ~ 50 parts of Olibanum quintessence oils afterwards again, stir clockwise, add 4 ~ 7 parts of above-mentioned obtained concentrated solutions subsequently again, after again stirring, a kind of cosmetics film forming wetting agent can be obtained.
Application process of the present invention is: the 1 ~ 3mL cosmetics film forming wetting agent got made by the present invention puts into 30 ~ 50mL cosmetics, abundant mix homogeneously, after every day sooner or later clean, get 2 ~ 4mL and spread upon each position on the face, pat till absorbing completely gently, life-time service, records the cosmetics adding cosmetic film formers wetting agent higher by more than 75% than the cosmetics moisturizing degree not adding cosmetic film formers wetting agent, and slow down aging, for skin without any harm.
The invention has the beneficial effects as follows:
(1) wetting agent that the method is made not only does not contain chemical substance, does not injure, can not cause redness, allergic phenomena for skin;
(2) natural protecting film can be formed for skin after using, pin skin internal moisture on the one hand, from external environment, absorb moisture content on the other hand, make skin ambient relative humidity reach more than 70%.
Detailed description of the invention
First get fresh pig small intestinal 5 ~ 10kg, after dirt inside and outside clean water pig small intestine and external skin fat, pig small intestine are put into archenteron-scrapping machine, remove intestinal skin, casing, obtain loose fat, then after loose fat obtained above being put into pulverizer pulverizing, put in the fermentation tank after sterilization, be placed in the place of ventilation, lucifuge, the deionized water adding loose fat weight 3 ~ 5 times afterwards carries out fermentation process to it, first regulates fermentation temperature to be 30 ~ 45 DEG C, sealing and fermenting 10 ~ 12 days, then fermentation temperature to 38 ~ 55 DEG C are heightened, sealing and fermenting 13 ~ 15 days, after its loose fat complete fermentation terminates, must mix turbid liquid, next turbid for mixing obtained above liquid is put into the glass container after sterilization, hide with gauze, set temperature is 25 ~ 32 DEG C, relative air humidity is 60 ~ 75%, places 5 ~ 8 days, after making himself mouldy, working concentration is the calcium citrate solutions of 0.9mol/L, adjust ph is after 5.8 ~ 6.5, and every day carries out drip washing 1 ~ 3 time, till mycete grows completely to mycete, afterwards the loose fat mycete of generation is inoculated on solid medium, cultivate 5 ~ 7 days at temperature 25 DEG C, obtain loose fat mycotic spore culture, then to be made in inoculation of suspension liquid to seed tank in sterilized culture medium, pass into filtrated air afterwards, cultivate 20 ~ 25h at 26 DEG C after, seed culture fluid is inoculated into fermentation tank sterilized containing in the culture medium of ALPHA Tolylic acid precursor, again pass into filtrated air, stir, cultivate 3 ~ 5 days at 24 DEG C, afterwards fermentation liquid is cooled, filter, pH to 2 ~ 2.5 are regulated with the hydrochloric acid solution that concentration is 0.4mol/L, and carry out multi-stage counter current extraction with butyl acetate, obtain butyl ester extract, by this butyl ester extract through activated carbon decolorizing, after distillation loose fat mycete extracting solution, get a 3L sealed container subsequently, separate from centre with a semipermeable membrane, be divided into two-layer up and down, the loose fat mycete extracting solution obtained in above-mentioned steps is poured on semipermeable membrane upper strata, afterwards container top is pressurizeed, pressure is set to 1 ~ 3MPa, gets semipermeable membrane upper strata concentrated solution after pressurization 15 ~ 20min, according to the mass fraction finally, get 15 ~ 25 parts of roseleafs, 2 ~ 6 parts of Folium Aloes are put into jet mill and are carried out micron-class superfine pulverizing, obtain 10 ~ 20 μm of superfines, slowly add part 20 ~ 25 parts of Semen Cucumidis sativi oil and 30 ~ 50 parts of Olibanum quintessence oils afterwards again, stir clockwise, add 4 ~ 7 parts of above-mentioned obtained concentrated solutions subsequently again, after again stirring, a kind of cosmetics film forming wetting agent can be obtained.
Example 1
First get fresh pig small intestinal 5kg, after dirt inside and outside clean water pig small intestine and external skin fat, pig small intestine are put into archenteron-scrapping machine, remove intestinal skin, casing, obtain loose fat, then after loose fat obtained above being put into pulverizer pulverizing, put in the fermentation tank after sterilization, be placed in the place of ventilation, lucifuge, the deionized water adding loose fat weight 3 times afterwards carries out fermentation process to it, first regulates fermentation temperature to be 30 DEG C, sealing and fermenting 10 days, then fermentation temperature to 38 DEG C is heightened, sealing and fermenting 13 days, after its loose fat complete fermentation terminates, must mix turbid liquid, next turbid for mixing obtained above liquid is put into the glass container after sterilization, hide with gauze, set temperature is 25 DEG C, relative air humidity is 60%, places 5 days, after making himself mouldy, working concentration is the calcium citrate solutions of 0.9mol/L, adjust ph is after 5.8, and every day carries out drip washing 1 time, till mycete grows completely to mycete, afterwards the loose fat mycete of generation is inoculated on solid medium, cultivate 5 days at temperature 25 DEG C, obtain loose fat mycotic spore culture, then to be made in inoculation of suspension liquid to seed tank in sterilized culture medium, pass into filtrated air afterwards, cultivate 20h at 26 DEG C after, seed culture fluid is inoculated into fermentation tank sterilized containing in the culture medium of ALPHA Tolylic acid precursor, again pass into filtrated air, stir, cultivate 3 days at 24 DEG C, afterwards fermentation liquid is cooled, filter, pH to 2 is regulated with the hydrochloric acid solution that concentration is 0.4mol/L, and carry out multi-stage counter current extraction with butyl acetate, obtain butyl ester extract, by this butyl ester extract through activated carbon decolorizing, after distillation loose fat mycete extracting solution, get a 3L sealed container subsequently, separate from centre with a semipermeable membrane, be divided into two-layer up and down, the loose fat mycete extracting solution obtained in above-mentioned steps is poured on semipermeable membrane upper strata, pressurize to container top afterwards, pressure is set to 1MPa, gets semipermeable membrane upper strata concentrated solution after pressurization 15min, according to the mass fraction finally, get 15 parts of roseleafs, 2 parts of Folium Aloes are put into jet mill and are carried out micron-class superfine pulverizing, obtain 10 μm of superfines, slowly add part 20 parts of Semen Cucumidis sativi oil and 30 parts of Olibanum quintessence oils afterwards again, stir clockwise, add 4 parts of above-mentioned obtained concentrated solutions subsequently again, after again stirring, a kind of cosmetics film forming wetting agent can be obtained.
This case method is unique novel, the 1mL cosmetics film forming wetting agent got during use made by the present invention puts into 30mL cosmetics, abundant mix homogeneously, after every day sooner or later clean, get 2mL and spread upon each position on the face, pat gently till absorbing completely, life-time service, record the cosmetics adding cosmetic film formers wetting agent higher by 75% than the cosmetics moisturizing degree not adding cosmetic film formers wetting agent, and slow down aging, for skin without any harm.
Example 2
First get fresh pig small intestinal 8kg, after dirt inside and outside clean water pig small intestine and external skin fat, pig small intestine are put into archenteron-scrapping machine, remove intestinal skin, casing, obtain loose fat, then after loose fat obtained above being put into pulverizer pulverizing, put in the fermentation tank after sterilization, be placed in the place of ventilation, lucifuge, the deionized water adding loose fat weight 4 times afterwards carries out fermentation process to it, first regulates fermentation temperature to be 40 DEG C, sealing and fermenting 11 days, then fermentation temperature to 50 DEG C is heightened, sealing and fermenting 14 days, after its loose fat complete fermentation terminates, must mix turbid liquid, next turbid for mixing obtained above liquid is put into the glass container after sterilization, hide with gauze, set temperature is 30 DEG C, relative air humidity is 70%, places 7 days, after making himself mouldy, working concentration is the calcium citrate solutions of 0.9mol/L, adjust ph is after 6.2, and every day carries out drip washing 2 times, till mycete grows completely to mycete, afterwards the loose fat mycete of generation is inoculated on solid medium, cultivate 6 days at temperature 25 DEG C, obtain loose fat mycotic spore culture, then to be made in inoculation of suspension liquid to seed tank in sterilized culture medium, pass into filtrated air afterwards, cultivate 23h at 26 DEG C after, seed culture fluid is inoculated into fermentation tank sterilized containing in the culture medium of ALPHA Tolylic acid precursor, again pass into filtrated air, stir, cultivate 4 days at 24 DEG C, afterwards fermentation liquid is cooled, filter, pH to 2.3 is regulated with the hydrochloric acid solution that concentration is 0.4mol/L, and carry out multi-stage counter current extraction with butyl acetate, obtain butyl ester extract, by this butyl ester extract through activated carbon decolorizing, after distillation loose fat mycete extracting solution, get a 3L sealed container subsequently, separate from centre with a semipermeable membrane, be divided into two-layer up and down, the loose fat mycete extracting solution obtained in above-mentioned steps is poured on semipermeable membrane upper strata, pressurize to container top afterwards, pressure is set to 2MPa, gets semipermeable membrane upper strata concentrated solution after pressurization 18min, according to the mass fraction finally, get 22 parts of roseleafs, 4 parts of Folium Aloes are put into jet mill and are carried out micron-class superfine pulverizing, obtain 15 μm of superfines, slowly add part 23 parts of Semen Cucumidis sativi oil and 40 parts of Olibanum quintessence oils afterwards again, stir clockwise, add 5 parts of above-mentioned obtained concentrated solutions subsequently again, after again stirring, a kind of cosmetics film forming wetting agent can be obtained.
This case method is unique novel, the 2mL cosmetics film forming wetting agent got during use made by the present invention puts into 40mL cosmetics, abundant mix homogeneously, after every day sooner or later clean, get 3mL and spread upon each position on the face, pat gently till absorbing completely, life-time service, record the cosmetics adding cosmetic film formers wetting agent higher by 76% than the cosmetics moisturizing degree not adding cosmetic film formers wetting agent, and slow down aging, for skin without any harm.
Example 3
First get fresh pig small intestinal 10kg, after dirt inside and outside clean water pig small intestine and external skin fat, pig small intestine are put into archenteron-scrapping machine, remove intestinal skin, casing, obtain loose fat, then after loose fat obtained above being put into pulverizer pulverizing, put in the fermentation tank after sterilization, be placed in the place of ventilation, lucifuge, the deionized water adding loose fat weight 5 times afterwards carries out fermentation process to it, first regulates fermentation temperature to be 45 DEG C, sealing and fermenting 12 days, then fermentation temperature to 55 DEG C is heightened, sealing and fermenting 15 days, after its loose fat complete fermentation terminates, must mix turbid liquid, next turbid for mixing obtained above liquid is put into the glass container after sterilization, hide with gauze, set temperature is 32 DEG C, relative air humidity is 75%, places 8 days, after making himself mouldy, working concentration is the calcium citrate solutions of 0.9mol/L, adjust ph is after 6.5, and every day carries out drip washing 3 times, till mycete grows completely to mycete, afterwards the loose fat mycete of generation is inoculated on solid medium, cultivate 7 days at temperature 25 DEG C, obtain loose fat mycotic spore culture, then to be made in inoculation of suspension liquid to seed tank in sterilized culture medium, pass into filtrated air afterwards, cultivate 25h at 26 DEG C after, seed culture fluid is inoculated into fermentation tank sterilized containing in the culture medium of ALPHA Tolylic acid precursor, again pass into filtrated air, stir, cultivate 5 days at 24 DEG C, afterwards fermentation liquid is cooled, filter, pH to 2.5 is regulated with the hydrochloric acid solution that concentration is 0.4mol/L, and carry out multi-stage counter current extraction with butyl acetate, obtain butyl ester extract, by this butyl ester extract through activated carbon decolorizing, after distillation loose fat mycete extracting solution, get a 3L sealed container subsequently, separate from centre with a semipermeable membrane, be divided into two-layer up and down, the loose fat mycete extracting solution obtained in above-mentioned steps is poured on semipermeable membrane upper strata, pressurize to container top afterwards, pressure is set to 3MPa, gets semipermeable membrane upper strata concentrated solution after pressurization 20min, according to the mass fraction finally, get 25 parts of roseleafs, 6 parts of Folium Aloes are put into jet mill and are carried out micron-class superfine pulverizing, obtain 20 μm of superfines, slowly add part 25 parts of Semen Cucumidis sativi oil and 50 parts of Olibanum quintessence oils afterwards again, stir clockwise, add 7 parts of above-mentioned obtained concentrated solutions subsequently again, after again stirring, a kind of cosmetics film forming wetting agent can be obtained.
This case method is unique novel, the 3mL cosmetics film forming wetting agent got during use made by the present invention puts into 50mL cosmetics, abundant mix homogeneously, after every day sooner or later clean, get 4mL and spread upon each position on the face, pat gently till absorbing completely, life-time service, record the cosmetics adding cosmetic film formers wetting agent higher by 77% than the cosmetics moisturizing degree not adding cosmetic film formers wetting agent, and slow down aging, for skin without any harm.
Claims (1)
1. a cosmetics film forming moisturizing additive, is characterized in that concrete operation step is:
(1) get fresh pig small intestinal 5 ~ 10kg, after dirt inside and outside clean water pig small intestine and external skin fat, pig small intestine are put into archenteron-scrapping machine, remove intestinal skin, casing, obtain loose fat;
(2) after loose fat obtained above being put into pulverizer pulverizing, put in the fermentation tank after sterilization, be placed in the place of ventilation, lucifuge, the deionized water adding loose fat weight 3 ~ 5 times afterwards carries out fermentation process to it, first regulates fermentation temperature to be 30 ~ 45 DEG C, sealing and fermenting 10 ~ 12 days, then fermentation temperature to 38 ~ 55 DEG C are heightened, sealing and fermenting 13 ~ 15 days, after its loose fat complete fermentation terminates, must mix turbid liquid;
(3) turbid for mixing obtained above liquid is put into the glass container after sterilization, hide with gauze, set temperature is 25 ~ 32 DEG C, relative air humidity is 60 ~ 75%, places 5 ~ 8 days, after making himself mouldy, working concentration is the calcium citrate solutions of 0.9mol/L, adjust ph is after 5.8 ~ 6.5, and every day carries out drip washing 1 ~ 3 time, till mycete grows completely to mycete;
(4) the loose fat mycete of generation is inoculated on solid medium, cultivate 5 ~ 7 days at temperature 25 DEG C, obtain loose fat mycotic spore culture, then to be made in inoculation of suspension liquid to seed tank in sterilized culture medium, pass into filtrated air afterwards, cultivate 20 ~ 25h at 26 DEG C after, seed culture fluid is inoculated into fermentation tank sterilized containing in the culture medium of ALPHA Tolylic acid precursor, again pass into filtrated air, stir, cultivate 3 ~ 5 days at 24 DEG C, afterwards fermentation liquid is cooled, filter, pH to 2 ~ 2.5 are regulated with the hydrochloric acid solution that concentration is 0.4mol/L, and carry out multi-stage counter current extraction with butyl acetate, obtain butyl ester extract, by this butyl ester extract through activated carbon decolorizing, after distillation loose fat mycete extracting solution,
(5) a 3L sealed container is got, separate from centre with a semipermeable membrane, be divided into two-layer up and down, the loose fat mycete extracting solution obtained in above-mentioned steps is poured on semipermeable membrane upper strata, afterwards container top is pressurizeed, pressure is set to 1 ~ 3MPa, gets semipermeable membrane upper strata concentrated solution after pressurization 15 ~ 20min;
(6) according to the mass fraction, get 15 ~ 25 parts of roseleafs, 2 ~ 6 parts of Folium Aloes are put into jet mill and are carried out micron-class superfine pulverizing, obtain 10 ~ 20 μm of superfines, slowly add part 20 ~ 25 parts of Semen Cucumidis sativi oil and 30 ~ 50 parts of Olibanum quintessence oils afterwards again, stir clockwise, add 4 ~ 7 parts of above-mentioned obtained concentrated solutions subsequently again, after again stirring, a kind of cosmetics film forming wetting agent can be obtained.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510620696.2A CN105125475A (en) | 2015-09-27 | 2015-09-27 | Cosmetic film-forming moisture preserving additive |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510620696.2A CN105125475A (en) | 2015-09-27 | 2015-09-27 | Cosmetic film-forming moisture preserving additive |
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| CN105125475A true CN105125475A (en) | 2015-12-09 |
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| CN201510620696.2A Pending CN105125475A (en) | 2015-09-27 | 2015-09-27 | Cosmetic film-forming moisture preserving additive |
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1072588A (en) * | 1991-11-29 | 1993-06-02 | 株式会社塔尼沙克 | Hair nourishing agent and production method thereof |
| CN103957997A (en) * | 2011-10-25 | 2014-07-30 | 奥麒个人护理产品公司 | Composition containing an extract of a sequential or simultaneous fermentation |
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2015
- 2015-09-27 CN CN201510620696.2A patent/CN105125475A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1072588A (en) * | 1991-11-29 | 1993-06-02 | 株式会社塔尼沙克 | Hair nourishing agent and production method thereof |
| CN103957997A (en) * | 2011-10-25 | 2014-07-30 | 奥麒个人护理产品公司 | Composition containing an extract of a sequential or simultaneous fermentation |
Non-Patent Citations (1)
| Title |
|---|
| 邓毛程 等: "《发酵工艺原理》", 30 September 2007, 中国轻工业出版社 * |
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