[go: up one dir, main page]

CN105109830A - Packaging method for adult monochamus alternatus attractant lure core - Google Patents

Packaging method for adult monochamus alternatus attractant lure core Download PDF

Info

Publication number
CN105109830A
CN105109830A CN201510487775.0A CN201510487775A CN105109830A CN 105109830 A CN105109830 A CN 105109830A CN 201510487775 A CN201510487775 A CN 201510487775A CN 105109830 A CN105109830 A CN 105109830A
Authority
CN
China
Prior art keywords
microns
thickness
polyethylene
packaging
attractant
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201510487775.0A
Other languages
Chinese (zh)
Inventor
张飞萍
李俊楠
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Fujian Agriculture and Forestry University
Original Assignee
Fujian Agriculture and Forestry University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Fujian Agriculture and Forestry University filed Critical Fujian Agriculture and Forestry University
Priority to CN201510487775.0A priority Critical patent/CN105109830A/en
Publication of CN105109830A publication Critical patent/CN105109830A/en
Pending legal-status Critical Current

Links

Landscapes

  • Catching Or Destruction (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

本发明针对现有松褐天牛成虫引诱剂诱芯需要低温保存的缺陷,提供一种松褐天牛成虫引诱剂诱芯的包装方法。具体为:采用PA/PE共挤膜密封包装,或采用PA/EVOH/PA/PE共挤膜密封包装,或采用PE/PVDC/PE共挤膜密封包装,或采用PE/PVDC/PA/EVOH/PA/PE共挤膜密封包装,或先采用PA/EVOH/PA/PE共挤膜密封包装,然后再用PE/PVDC/PE共挤膜进行二次密封包装。通过该方法包装的诱芯不需要低温保存,且室内室温下存储的有效期不少于10个月,且包装方法简单,成本低,十分便于引诱剂诱芯的长途运输和长期存储,大大降低了诱捕防治松褐天牛的成本。

Aiming at the defect that the existing chrysalis adult attractant lure core needs to be stored at low temperature, the invention provides a packaging method for the monochamus adult attractant lure core. Specifically: sealed packaging with PA/PE co-extruded film, or sealed packaging with PA/EVOH/PA/PE co-extruded film, or sealed packaging with PE/PVDC/PE co-extruded film, or sealed packaging with PE/PVDC/PA/EVOH /PA/PE co-extruded film for sealed packaging, or first use PA/EVOH/PA/PE co-extruded film for sealed packaging, and then use PE/PVDC/PE co-extruded film for secondary sealed packaging. The lures packaged by this method do not need low-temperature preservation, and the validity period of storage at room temperature is not less than 10 months, and the packaging method is simple and low in cost, which is very convenient for long-distance transportation and long-term storage of attractant lures, greatly reducing the Costs of trapping and controlling Monochamus alternata.

Description

一种松褐天牛成虫引诱剂诱芯的包装方法A kind of packing method of attractant lure core of monochamus alternatus adult

技术领域 technical field

本发明涉及昆虫引诱剂诱芯的包装方法,更具体涉及一种松褐天牛成虫引诱剂诱芯的包装方法。 The invention relates to a packaging method for an insect attractant lure core, and more particularly relates to a packaging method for an adult montina monochamus adult attractant lure core.

背景技术 Background technique

松材线虫病又称“松树的癌症”,是松树的毁灭性病害,能使受害松树在短期内枯萎、死亡。据统计,自1982年以来,我国因松材线虫病造成的直接经济损失就超过500亿元。迄今为止,松材线虫病已在我国长江流域及其以南的大多数省份造成严重危害,且呈现快速扩散蔓延的趋势,对我国森林生态环境安全形成巨大威胁。 Pine wood nematode disease, also known as "pine cancer", is a devastating disease of pine trees, which can cause the affected pine trees to wither and die in a short period of time. According to statistics, since 1982, the direct economic loss caused by pine wood nematode in my country has exceeded 50 billion yuan. So far, pine wood nematode disease has caused serious harm in the Yangtze River Basin and most provinces south of my country, and it is spreading rapidly, posing a huge threat to the safety of my country's forest ecological environment.

松褐天牛又名松墨天牛,是我国松材线虫病的主要媒介昆虫,该虫主要通过成虫携带松材线虫取食等行为传播松材线虫病。到目前为止,控制松褐天牛,切断病害传播途经,仍然是我国控制松材线虫病最有效的方法之一。长期以来,利用松褐天牛成虫引诱剂监测和控制松褐天牛,是我国松材线虫病防控的主要措施之一。将引诱剂诱芯安装在诱捕器上,并挂设在松林中诱捕松褐天牛成虫,能起到有效监测和防治松褐天牛的效果,抑制松材线虫病的扩散蔓延。 Monochamus alternata, also known as Monochamus monochamus, is the main vector insect of pine wood nematode in my country. So far, controlling the monochamus and cutting off the transmission route of the disease is still one of the most effective methods for controlling pine wood nematode in my country. For a long time, monitoring and controlling Monochamus alternatus with adult attractants has been one of the main measures for the prevention and control of pine wood nematode disease in my country. Installing the attractant lure core on the trap and hanging it in the pine forest to trap the adult chrysalis monochamus can effectively monitor and control the pine brown monochamus, and inhibit the spread of pine wood nematode disease.

由于松褐天牛成虫引诱剂活性成分均具有极强的挥发性,且单个诱芯的引诱剂诱液剂量大,因此在诱芯的运输和存储过程中很容易产生引诱剂活性成分损失的现象,导致诱芯的野外诱虫效果降低,甚至失效。目前解决这一问题的方法主要有以下两种:一是在运输和存储过程中,始终将引诱剂诱芯冷冻保存,该法能够有效保持引诱剂诱芯的诱虫效果,但存在运输和贮存成本高,需要专用冷冻设备等缺陷,一些偏远山区由于没有专用冷冻设备而无法有效储存和使用引诱剂防治松褐天牛;二是采用铝塑复合材料如PA/AL/PE、PET/AL/CPP、PA/AL/RCP等复合膜包装诱芯,但在实践中发现,由于引诱剂诱芯中的萜烯类物质具有极强的穿透能力,且单个诱芯剂量大,采用铝塑复合材料包装,并在室内室温下存储一段时间后,铝层和塑料层很容易相互脱离,同时复合膜出现严重皱褶的现象,引诱剂活性成分流失严重,导致诱芯使用效果显著下降,甚至失效;因此即使是采用铝塑复合材料包装,仍然需要专用设备冷冻保存,存储成本高。 Since the active ingredients of the adult attractants of Monochamus alternata are highly volatile, and the dosage of the attractant liquid for a single lure is large, the loss of the active ingredients of the attractant is easy to occur during the transportation and storage of the lure , leading to the reduction of the field insect trapping effect of the lure core, or even failure. At present, there are mainly two methods to solve this problem: one is to keep the attractant lures frozen during the transportation and storage process. This method can effectively maintain the insect-attracting effect of the attractant lures. The cost is high, and special refrigeration equipment is needed. Some remote mountainous areas cannot effectively store and use attractants to prevent and control pine beetle due to the lack of special refrigeration equipment; the second is to use aluminum-plastic composite materials such as PA/AL/PE, PET/AL/ CPP, PA/AL/RCP and other composite film packaging lures, but in practice, it is found that because the terpenes in the attractant lure have a strong penetrating ability, and the dosage of a single lure is large, aluminum-plastic composite Material packaging and storage at room temperature for a period of time, the aluminum layer and the plastic layer are easily separated from each other, and the composite film is severely wrinkled, and the active ingredients of the attractant are seriously lost, resulting in a significant decline in the use of the lure, or even failure ; Therefore, even if it is packaged with aluminum-plastic composite materials, it still needs special equipment for frozen storage, and the storage cost is high.

发明内容 Contents of the invention

为了解决上述问题,本发明提供了一种松褐天牛成虫引诱剂诱芯的包装方法,该包装方法所用材料简单、包装程序简便、成本低,能使引诱剂诱芯在室内室温下存储的有效期达到10个月以上,具有成本低、效果好和使用方便等优点。 In order to solve the above-mentioned problems, the present invention provides a kind of packing method of the attractant lure core of monochamus alternatus adult, the material used in this packing method is simple, the packing procedure is simple and convenient, and cost is low, can make the attractant lure core store at room temperature. The validity period reaches more than 10 months, and has the advantages of low cost, good effect and convenient use.

为实现上述目的,本发明采取的技术方案如下: In order to achieve the above object, the technical scheme that the present invention takes is as follows:

一种松褐天牛成虫引诱剂诱芯的包装方法,采用PA/PE(聚酰胺/聚乙烯)共挤膜、PA/EVOH/PA/PE(聚酰胺/乙烯-乙烯醇共聚物/聚酰胺/聚乙烯)共挤膜、PE/PVDC/PE(聚乙烯/聚偏二氯乙烯/聚乙烯)共挤膜、PE/PVDC/PA/EVOH/PA/PE(聚乙烯/聚偏二氯乙烯/聚酰胺/乙烯-乙烯醇共聚物/聚酰胺/聚乙烯)共挤膜中的一种或两种密封包装松褐天牛成虫引诱剂诱芯。 A packaging method for the lure core of the adult pine beetle attractant, using PA/PE (polyamide/polyethylene) co-extrusion film, PA/EVOH/PA/PE (polyamide/ethylene-vinyl alcohol copolymer/polyamide /polyethylene) co-extrusion film, PE/PVDC/PE (polyethylene/polyvinylidene chloride/polyethylene) co-extrusion film, PE/PVDC/PA/EVOH/PA/PE (polyethylene/polyvinylidene chloride /polyamide/ethylene-vinyl alcohol copolymer/polyamide/polyethylene) co-extrusion film in one or two kinds of hermetically packaged monochamus adult attractant lures.

优选方法一,将引诱剂诱芯先用PA/EVOH/PA/PE共挤膜密封包装,然后再用PE/PVDC/PE共挤膜进行二次密封包装。 Preferred method 1 is to seal and package the attractant core with PA/EVOH/PA/PE co-extruded film first, and then use PE/PVDC/PE co-extruded film for secondary sealed packaging.

优选方法二,将引诱剂诱芯用PE/PVDC/PA/EVOH/PA/PE共挤膜密封包装。 The second preferred method is to seal and package the attractant core with PE/PVDC/PA/EVOH/PA/PE co-extrusion film.

所述PE/PVDC/PE共挤膜中PVDC层的厚度为5~25微米,所述PE/PVDC/PA/EVOH/PA/PE共挤膜中PVDC层的厚度为5~25微米,PA层的厚度为15~30微米。 The thickness of the PVDC layer in the PE/PVDC/PE co-extrusion film is 5-25 microns, the thickness of the PVDC layer in the PE/PVDC/PA/EVOH/PA/PE co-extrusion film is 5-25 microns, and the PA layer The thickness is 15-30 microns.

优选的,所述PE/PVDC/PE共挤膜中PVDC层的厚度为15~25微米,所述PE/PVDC/PA/EVOH/PA/PE共挤膜中PVDC层的厚度为15~25微米,PA层的厚度为15~30微米。 Preferably, the thickness of the PVDC layer in the PE/PVDC/PE co-extrusion film is 15-25 microns, and the thickness of the PVDC layer in the PE/PVDC/PA/EVOH/PA/PE co-extrusion film is 15-25 microns , the thickness of the PA layer is 15-30 microns.

优选的,本发明的引诱剂诱芯是采用公开号为CN102986739A的专利披露的技术制得的诱液,然后用脱脂棉吸附,后用聚乙烯薄膜密封制得。 Preferably, the attractant lure of the present invention is prepared by adopting the technique disclosed in the patent with publication number CN102986739A, then absorbing it with absorbent cotton, and then sealing it with a polyethylene film.

本发明的有益效果在于: The beneficial effects of the present invention are:

(1)本发明引诱剂诱芯的包装过程简单,所用材料成本低,包装存储效果好;包装材料中所用的PA和EVOH成分对引诱剂活性成分中的信息素混合物和萜烯类化合物具有极高的阻隔性能,能够有效阻止上述两类活性成分损失;包装材料中所用的PVDC成分对水蒸气和乙醇等极性化合物具有极高的阻隔性能,既能够防止空气中的水蒸气进入诱芯,又能够较好地阻隔诱芯中的乙醇流失;包装材料中所用的PE成分能够提供较好的热封性能;将由上述包装材料不同成分制成的共挤膜单独或组合使用,能够有效地避免引诱剂活性成分在运输和存储过程中流失,并避免包装材料不同成分层间相互脱离,优势明显; (1) The packaging process of the attractant lure core of the present invention is simple, the cost of materials used is low, and the packaging and storage effect is good; the PA and EVOH components used in the packaging materials have a very strong effect on the pheromone mixture and terpene compounds in the active components of the attractant. High barrier performance can effectively prevent the loss of the above two types of active ingredients; the PVDC component used in packaging materials has extremely high barrier performance to polar compounds such as water vapor and ethanol, which can prevent water vapor in the air from entering the lure, It can also better block the loss of ethanol in the lure; the PE component used in the packaging material can provide better heat sealing performance; the co-extrusion film made of the different components of the above packaging material can be used alone or in combination, which can effectively avoid The active ingredients of the attractant are lost during transportation and storage, and the separation of different component layers of the packaging material is avoided, which has obvious advantages;

(2)采用本发明包装的松褐天牛成虫引诱剂诱芯在运输和存储过程中不需要专用设备冷冻保存,可在室内室温下存储,存储有效期不少于10个月,使用时撕去诱芯外包装,将诱芯直接悬挂安装在松褐天牛诱捕器挡虫板中央的中空部位,能够诱捕大量的松褐天牛成虫,降低疫区松枯死木数量,抑制松材线虫病传播蔓延,且具有成本低,便于运输和存储等优点。 (2) The attractant lure cores packaged by the present invention do not require special equipment for frozen storage during transportation and storage, and can be stored at room temperature, with a storage validity period of not less than 10 months, and are torn off when used. The outer packaging of the lure, the lure is directly hung and installed in the hollow part of the center of the chrysanthemum trap, which can trap a large number of adult chrysalis, reduce the number of dead pine trees in the epidemic area, and inhibit the spread of pine wood nematode disease Spread, and has the advantages of low cost, convenient transportation and storage.

附图说明 Description of drawings

图1不同包装材料引诱剂组分的质量损失(g),A指对照(无包装);B指用PA/纯铝/PE复合膜包装;C指用PA/PE共挤膜包装;D指用PA/EVOH/PA/PE共挤膜包装;E指用PE/PVDC/PE共挤膜包装;F指先用PA/EVOH/PA/PE共挤膜包装,再用PE/PVDC/PE共挤膜包装;G指用PE/PVDC/PA/EVOH/PA/PE共挤膜包装; Figure 1 Mass loss (g) of attractant components in different packaging materials, A refers to the control (no packaging); B refers to packaging with PA/pure aluminum/PE composite film; C refers to packaging with PA/PE co-extrusion film; D refers to Packed with PA/EVOH/PA/PE co-extruded film; E means packed with PE/PVDC/PE co-extruded film; F means packed with PA/EVOH/PA/PE co-extruded film first, and then co-extruded with PE/PVDC/PE Film packaging; G refers to PE/PVDC/PA/EVOH/PA/PE co-extrusion film packaging;

图2不同厚度PVDC共挤膜包装下诱芯的质量损失(g),A指先用PA/EVOH/PA/PE共挤膜包装,再用PE/PVDC/PE共挤膜包装;B指用PE/PVDC/PA/EVOH/PA/PE共挤膜包装。膜厚度指聚偏二氯乙烯层的厚度(微米)。 Figure 2 The mass loss (g) of lures packaged with different thicknesses of PVDC co-extrusion film, A refers to packaging with PA/EVOH/PA/PE co-extrusion film first, and then PE/PVDC/PE co-extrusion film; B refers to PE /PVDC/PA/EVOH/PA/PE co-extrusion film packaging. Film thickness refers to the thickness (microns) of the polyvinylidene chloride layer.

图3不同厚度PA共挤膜包装下诱芯的质量损失(g),A指先用PA/EVOH/PA/PE共挤膜包装,再用PE/PVDC/PE共挤膜包装;B指用PE/PVDC/PA/EVOH/PA/PE共挤膜包装。膜厚度指聚酰胺层的厚度(微米)。 Figure 3 Mass loss (g) of the lure under different thicknesses of PA co-extrusion film packaging, A refers to packaging with PA/EVOH/PA/PE co-extrusion film first, and then PE/PVDC/PE co-extrusion film packaging; B refers to PE /PVDC/PA/EVOH/PA/PE co-extrusion film packaging. Film thickness refers to the thickness (microns) of the polyamide layer.

具体实施方式 Detailed ways

本发明用下列实施例来进一步说明本发明,但本发明的保护范围并不限于下列实施例。 The present invention further illustrates the present invention with following examples, but protection scope of the present invention is not limited to following examples.

实施例1Example 1

一、不同包装方法下松褐天牛成虫引诱剂各组分质量损失测定1. Determination of the mass loss of each component of the adult attractant of Monochamus alternatus under different packaging methods

引诱剂组分的准备:松褐天牛成虫引诱剂组分根据专利“一种松褐天牛成虫引诱剂(公开号:CN102986739A)”确定,包括信息素混合物、萜烯类和无水乙醇。按照松褐天牛成虫引诱剂的释放方法,将各组分分别用脱脂棉吸附,后分别用聚乙烯薄膜密封。信息素混合物、萜烯和无水乙醇3个组分的加入量分别为2克、20克和5克。 Preparation of attractant components: The attractant components of Monochamus alternata adults are determined according to the patent "An Attractant for Monochamus monochamus adults (publication number: CN102986739A)", including pheromone mixture, terpenes and absolute ethanol. According to the release method of the adult attractant of the monochamus alternatus, each component is absorbed with absorbent cotton, and then sealed with polyethylene film respectively. The addition amounts of the three components of pheromone mixture, terpene and absolute ethanol are 2 grams, 20 grams and 5 grams respectively.

引诱剂各组分的包装:(1)不包装,作为对照;(2)PA/纯铝/PE膜包装,将引诱剂各组分分别用聚酰胺-纯铝-聚乙烯复合膜(PA/纯铝/PE)密封包装,其中聚酰胺厚度15微米,聚乙烯厚度55微米,纯铝厚度50微米;(3)PA/PE膜包装,将引诱剂各组分分别用聚酰胺-聚乙烯共挤膜(PA/PE)密封包装,其中聚酰胺厚度15微米,聚乙烯厚度55微米;(4)PA/EVOH/PA/PE膜包装,将引诱剂各个组分分别用聚酰胺-乙烯-乙烯醇共聚物-聚酰胺-聚乙烯共挤膜(PA/EVOH/PA/PE)密封包装,其中聚酰胺厚度15微米,乙烯-乙烯醇共聚物厚度15微米,聚乙烯厚度55微米;(5)PE/PVDC/PE膜包装,将引诱剂各个组分分别用聚乙烯-聚偏二氯乙烯-聚乙烯共挤膜(PE/PVDC/PE)密封包装,其中聚偏二氯乙烯厚度15微米,聚乙烯厚度55微米;(6)PA/EVOH/PA/PE膜和PE/PVDC/PE膜二次封装,将引诱剂各个组分先分别用聚酰胺-乙烯-乙烯醇共聚物-聚酰胺-聚乙烯共挤膜密封包装(聚酰胺厚度15微米,乙烯-乙烯醇共聚物厚度15微米,聚乙烯厚度55微米),然后再分别用聚乙烯-聚偏二氯乙烯-聚乙烯共挤膜密封包装(聚偏二氯乙烯厚度15微米,聚乙烯厚度55微米);(7)PE/PVDC/PA/EVOH/PA/PE膜包装,将引诱剂各个组分先分别用聚乙烯-聚偏二氯乙烯-聚酰胺-乙烯-乙烯醇共聚物-聚酰胺-聚乙烯共挤膜密封包装(PE/PVDC/PA/EVOH/PA/PE,聚乙烯厚度55微米,聚偏二氯乙烯厚度15微米,聚酰胺厚度15微米,乙烯-乙烯醇共聚物厚度15微米,聚乙烯厚度55微米)。 The packaging of each component of the attractant: (1) No packaging, as a control; (2) PA/pure aluminum/PE film packaging, each component of the attractant is respectively wrapped with a polyamide-pure aluminum-polyethylene composite film (PA/ Pure aluminum/PE) airtight packaging, in which polyamide thickness is 15 microns, polyethylene thickness is 55 microns, and pure aluminum thickness is 50 microns; (3) PA/PE film packaging, each component of the attractant is respectively coated with polyamide-polyethylene Extruded film (PA/PE) sealed packaging, in which the thickness of polyamide is 15 microns, and the thickness of polyethylene is 55 microns; (4) PA/EVOH/PA/PE film packaging, the components of the attractant are respectively polyamide-ethylene-ethylene Alcohol copolymer-polyamide-polyethylene co-extrusion film (PA/EVOH/PA/PE) sealed packaging, in which the thickness of polyamide is 15 microns, the thickness of ethylene-vinyl alcohol copolymer is 15 microns, and the thickness of polyethylene is 55 microns; (5) PE/PVDC/PE film packaging, each component of the attractant is sealed and packaged with polyethylene-polyvinylidene chloride-polyethylene co-extrusion film (PE/PVDC/PE), in which the thickness of polyvinylidene chloride is 15 microns, The thickness of polyethylene is 55 microns; (6) PA/EVOH/PA/PE film and PE/PVDC/PE film are encapsulated twice, and each component of the attractant is firstly coated with polyamide-ethylene-vinyl alcohol copolymer-polyamide- Polyethylene co-extrusion film sealing package (polyamide thickness 15 microns, ethylene-vinyl alcohol copolymer thickness 15 microns, polyethylene thickness 55 microns), and then respectively sealed with polyethylene-polyvinylidene chloride-polyethylene co-extrusion film Packaging (polyvinylidene chloride thickness 15 microns, polyethylene thickness 55 microns); (7) PE/PVDC/PA/EVOH/PA/PE film packaging, each component of the attractant is first coated with polyethylene-polyethylene Vinyl chloride-polyamide-ethylene-vinyl alcohol copolymer-polyamide-polyethylene co-extrusion film sealed packaging (PE/PVDC/PA/EVOH/PA/PE, polyethylene thickness 55 microns, polyvinylidene chloride thickness 15 microns , polyamide thickness 15 microns, ethylene-vinyl alcohol copolymer thickness 15 microns, polyethylene thickness 55 microns).

将上述包装好的引诱剂各组分称重(含包装),后放在纸箱中并置于室内室温下保存10个月(2012年7月20日到2013年5月19日),10个月后再次测定各组分的质量(含包装),计算各组分的质量损失。试验设5重复。不同包装方法下引诱剂各组分存储10个月后的质量损失情况见图1。图1显示:(1)就信息素混合物而言,除对照外,所选择的几种包装方法的质量损失均较小,其中PA/纯铝/PE复合膜包装、PA/EVOH/PA/PE共挤膜和PE/PVDC/PE共挤膜二次封装、PE/PVDC/PA/EVOH/PA/PE共挤膜包装下几乎没有质量损失,而PA/PE共挤膜、PA/EVOH/PA/PE共挤膜包装下的质量略有增加,这与两种包装膜对水蒸气的阻隔性能弱有关;(2)就萜烯类而言,PA/EVOH/PA/PE共挤膜和PE/PVDC/PE共挤膜二次封装、PE/PVDC/PA/EVOH/PA/PE共挤膜包装下几乎没有质量损失,PA/PE共挤膜包装、PA/EVOH/PA/PE共挤膜包装下的质量略有增加,PA/纯铝/PE复合膜包装存储10个月后的铝层和聚乙烯层全部分离脱层,萜烯质量损失大;(3)就乙醇而言,PE/PVDC/PE共挤膜包装、PA/EVOH/PA/PE和PE/PVDC/PE共挤膜二次封装、PE/PVDC/PA/EVOH/PA/PE共挤膜包装、PA/纯铝/PE复合膜包装下的质量损失均小,其中PA/纯铝/PE复合膜包装下几乎没有质量损失。 Weigh each component of the above-mentioned packaged attractant (including packaging), put it in a carton and store it at room temperature for 10 months (from July 20, 2012 to May 19, 2013), 10 Measure the mass of each component (including packaging) again after 1 month, and calculate the mass loss of each component. The experiment was set to 5 repetitions. The mass loss of each component of the attractant after storage for 10 months under different packaging methods is shown in Figure 1. Figure 1 shows: (1) As far as the pheromone mixture is concerned, except for the control, the quality loss of the selected packaging methods is small, among which PA/pure aluminum/PE composite film packaging, PA/EVOH/PA/PE There is almost no quality loss under co-extrusion film and PE/PVDC/PE co-extrusion film secondary packaging, PE/PVDC/PA/EVOH/PA/PE co-extrusion film packaging, while PA/PE co-extrusion film, PA/EVOH/PA /PE co-extrusion film packaging has a slight increase in mass, which is related to the weak barrier properties of the two packaging films to water vapor; (2) As far as terpenes are concerned, PA/EVOH/PA/PE co-extrusion film and PE /PVDC/PE co-extrusion film secondary packaging, PE/PVDC/PA/EVOH/PA/PE co-extrusion film packaging with almost no quality loss, PA/PE co-extrusion film packaging, PA/EVOH/PA/PE co-extrusion film The mass under the package increased slightly, and the aluminum layer and polyethylene layer of the PA/pure aluminum/PE composite film package were all separated and delaminated after 10 months of storage, and the mass loss of terpene was large; (3) in terms of ethanol, PE/PE PVDC/PE co-extrusion film packaging, PA/EVOH/PA/PE and PE/PVDC/PE co-extrusion film secondary packaging, PE/PVDC/PA/EVOH/PA/PE co-extrusion film packaging, PA/pure aluminum/PE The quality loss under the composite film packaging is small, and there is almost no quality loss under the PA/pure aluminum/PE composite film packaging.

二、不同包装方法下松褐天牛成虫引诱剂诱芯的野外诱虫测试2. Field trap test of the attractant lures for adult chrysalis monochamus under different packaging methods

引诱剂诱芯的制备:根据专利“一种松褐天牛成虫引诱剂(公开号:CN102986739A)”制作松褐天牛成虫引诱剂诱液。将20克引诱剂诱液用脱脂棉吸附后用聚乙烯薄膜密封,即制得松褐天牛成虫引诱剂诱芯。 Preparation of attractant lure cores: According to the patent "An Attractant for Adult Monochamus monochamus (Publication No.: CN102986739A)", the Attractant Liquid for Adult Monochamus monochamus was prepared. Absorb 20 grams of the attractant solution with absorbent cotton and seal it with a polyethylene film to prepare the attractant lure core for the adult chrysalis monochamus.

引诱剂诱芯的包装:(1)不包装,作为对照;(2)PA/纯铝/PE膜包装,将引诱剂诱芯用聚酰胺-纯铝-聚乙烯复合膜密封包装,其中聚酰胺厚度15微米,聚乙烯厚度55微米,纯铝厚度50微米;(3)PA/PE膜包装,将引诱剂诱芯用聚酰胺-聚乙烯共挤膜密封包装,其中聚酰胺厚度15微米,聚乙烯厚度55微米;(4)PA/EVOH/PA/PE膜包装,将引诱剂诱芯用聚酰胺-乙烯-乙烯醇共聚物-聚酰胺-聚乙烯共挤膜密封包装,其中聚酰胺厚度15微米,乙烯-乙烯醇共聚物厚度15微米,聚乙烯厚度55微米;(5)PE/PVDC/PE膜包装,将引诱剂诱芯用聚乙烯-聚偏二氯乙烯-聚乙烯共挤膜密封包装,其中聚偏二氯乙烯厚度15微米,聚乙烯厚度55微米;(6)PA/EVOH/PA/PE膜和PE/PVDC/PE膜二次封装,将引诱剂诱芯用聚酰胺-乙烯-乙烯醇共聚物-聚酰胺-聚乙烯共挤膜密封包装(聚酰胺厚度15微米,乙烯-乙烯醇共聚物厚度15微米,聚乙烯厚度55微米),然后再用聚乙烯-聚偏二氯乙烯-聚乙烯共挤膜密封包装(聚偏二氯乙烯厚度15微米,聚乙烯厚度55微米);(7)PE/PVDC/PA/EVOH/PA/PE膜包装,将引诱剂诱芯先用聚乙烯-聚偏二氯乙烯-聚酰胺-乙烯-乙烯醇共聚物-聚酰胺-聚乙烯共挤膜密封包装(聚乙烯厚度55微米,聚偏二氯乙烯厚度15微米,聚酰胺厚度15微米,乙烯-乙烯醇共聚物厚度15微米,聚乙烯厚度55微米)。将上述7类包装好的(含未包装对照)诱芯置于室内室温下贮存10个月(2013年7月26日到2014年5月25日)。 Packaging of attractant lures: (1) No packaging, as a control; (2) PA/pure aluminum/PE film packaging, the attractant lures are sealed with polyamide-pure aluminum-polyethylene composite film, of which polyamide The thickness is 15 microns, the thickness of polyethylene is 55 microns, and the thickness of pure aluminum is 50 microns; (3) PA/PE film packaging, the attractant core is sealed and packaged with polyamide-polyethylene co-extrusion film, in which the thickness of polyamide is 15 microns, and the thickness of polyamide is 15 microns. The thickness of ethylene is 55 microns; (4) PA/EVOH/PA/PE film packaging, the attractant core is sealed with polyamide-ethylene-vinyl alcohol copolymer-polyamide-polyethylene co-extrusion film, in which polyamide thickness is 15 Micron, the thickness of ethylene-vinyl alcohol copolymer is 15 microns, and the thickness of polyethylene is 55 microns; (5) PE/PVDC/PE film packaging, the attractant core is sealed with polyethylene-polyvinylidene chloride-polyethylene co-extrusion film Packaging, in which the thickness of polyvinylidene chloride is 15 microns, and the thickness of polyethylene is 55 microns; (6) PA/EVOH/PA/PE film and PE/PVDC/PE film secondary packaging, the attractant lure core with polyamide-ethylene -Vinyl alcohol copolymer-polyamide-polyethylene co-extrusion film sealing package (polyamide thickness 15 microns, ethylene-vinyl alcohol copolymer thickness 15 microns, polyethylene thickness 55 microns), and then polyethylene-polyethylene dichloride Ethylene-polyethylene co-extrusion film sealed packaging (polyvinylidene chloride thickness 15 microns, polyethylene thickness 55 microns); (7) PE/PVDC/PA/EVOH/PA/PE film packaging, the attractant lure core is used first Polyethylene-polyvinylidene chloride-polyamide-ethylene-vinyl alcohol copolymer-polyamide-polyethylene co-extrusion film sealed packaging (polyethylene thickness 55 microns, polyvinylidene chloride thickness 15 microns, polyamide thickness 15 microns , ethylene-vinyl alcohol copolymer thickness 15 microns, polyethylene thickness 55 microns). The above-mentioned 7 types of packaged lures (including unpackaged control) were stored at room temperature for 10 months (from July 26, 2013 to May 25, 2014).

野外测试工作在福建泰宁进行(2014年5月26日-2014年6月8日),所用诱捕器根据专利“一种松褐天牛诱捕器”(公开号:CN203313934U)制作,将上述包装和存储10个月后的诱芯拆封后安装在诱捕器上,另设1个临时制作的诱芯作为对照。野外诱虫测试设5空间重复,各处理随机排序,相邻诱捕器间隔80-100米,每周收集和统计各诱捕器捕获松褐天牛的数量,测试结果见表1。 The field test was carried out in Taining, Fujian Province (May 26, 2014-June 8, 2014). The trap used was made according to the patent "A Trapper for Monochamus alternatus" (public number: CN203313934U), and the above packaging And the lures stored for 10 months were unpacked and installed on the traps, and another temporarily made lure was used as a control. In the field trap test, 5 spatial repetitions were set, each treatment was randomly sorted, and the interval between adjacent traps was 80-100 meters. The number of monochamus captured by each trap was collected and counted every week. The test results are shown in Table 1.

表1显示:没有包装但存储了10个月的诱芯、PA/纯铝/PE包装并存储10个月的诱芯(包装全部开裂)均只诱到极少量的松褐天牛,而采用PA/PE共挤膜、PA/EVOH/PA/PE共挤膜、PA/EVOH/PA/PE共挤膜和PE/PVDC/PE共挤膜二次封装、PE/PVDC/PA/EVOH/PA/PE共挤膜包装的诱芯均诱捕到较多的松褐天牛,其中采用PA/EVOH/PA/PE和PE/PVDC/PE共挤膜二次封装、PE/PVDC/PA/EVOH/PA/PE共挤膜封装两种方法包装的诱芯诱捕松褐天牛的数量更多,与临时制作诱芯的诱捕数最接近。上述结果说明:PA/PE共挤膜、PA/EVOH/PA/PE共挤膜、PA/EVOH/PA/PE共挤膜和PE/PVDC/PE共挤膜二次封装、PE/PVDC/PA/EVOH/PA/PE共挤膜均可作为松褐天牛成虫引诱剂诱芯的包装材料,采用上述材料包装松褐天牛成虫引诱剂诱芯的存储有效期不少于10个月,其中以PA/EVOH/PA/PE共挤膜和PE/PVDC/PE共挤膜二次封装、PE/PVDC/PA/EVOH/PA/PE共挤膜包装两种方案最优。 Table 1 shows that: lures without packaging but stored for 10 months, lures packaged in PA/pure aluminum/PE and stored for 10 months (packages are all cracked) all only lured a very small amount of Alpinia monochamus, while using PA/PE co-extrusion film, PA/EVOH/PA/PE co-extrusion film, PA/EVOH/PA/PE co-extrusion film and PE/PVDC/PE co-extrusion film secondary packaging, PE/PVDC/PA/EVOH/PA /PE co-extrusion film packaging lure cores trap more pine nuts, which adopt PA/EVOH/PA/PE and PE/PVDC/PE co-extrusion film secondary packaging, PE/PVDC/PA/EVOH/ PA/PE co-extrusion film encapsulation two ways of packing the number of trapping Alchacha monochamus is more, which is the closest to the number of trapping the temporary lure. The above results show that: PA/PE co-extrusion film, PA/EVOH/PA/PE co-extrusion film, PA/EVOH/PA/PE co-extrusion film and PE/PVDC/PE co-extrusion film secondary packaging, PE/PVDC/PA /EVOH/PA/PE co-extruded film can be used as the packaging material for the attractant lure core of the adult monochamus alternatus, and the storage validity period of the attractant core for the adult monochamus alternatus packaged with the above materials is not less than 10 months. PA/EVOH/PA/PE co-extrusion film and secondary packaging of PE/PVDC/PE co-extrusion film, and PE/PVDC/PA/EVOH/PA/PE co-extrusion film packaging are the best.

表1不同材料包装下引诱剂诱芯的松褐天牛野外捕获量(头/每诱捕器)Table 1 The amount of wild monochamus caught in attractant lure cores packed with different materials (head/trap)

实施例2Example 2

一、松褐天牛成虫引诱剂诱芯的制备和包装(不同厚度PVDC膜)1. Preparation and packaging of attractant lures for adult pine beetles (PVDC films with different thicknesses)

诱芯制备:根据专利“一种松褐天牛成虫引诱剂(公开号:CN102986739A)”由本实验室制作松褐天牛成虫引诱剂诱液。将20克引诱剂诱液用脱脂棉吸附后用聚乙烯薄膜密封,即制得松褐天牛成虫引诱剂诱芯。 Lure core preparation: according to the patent "An Attractant for Adult Monochamus alternatus (Publication No.: CN102986739A)", the laboratory prepared the attractant solution for Adult Monochamus alternata. Absorb 20 grams of the attractant solution with absorbent cotton and seal it with a polyethylene film to prepare the attractant lure core for the adult chrysalis monochamus.

引诱剂诱芯的包装:(1)PA/EVOH/PA/PE和PE/PVDC/PE共挤膜二次封装,将引诱剂诱芯先用聚酰胺-乙烯-乙烯醇共聚物-聚酰胺-聚乙烯共挤膜密封包装(聚酰胺厚度15微米,乙烯-乙烯醇共聚物厚度15微米,聚乙烯厚度55微米),然后再用聚乙烯-聚偏二氯乙烯-聚乙烯共挤膜密封包装(聚乙烯厚度55微米),聚偏氯乙烯的厚度分别为5微米、10微米、15微米、20微米和25微米;(2)PE/PVDC/PA/EVOH/PA/PE共挤膜包装,将引诱剂诱芯用聚乙烯-聚偏二氯乙烯-聚酰胺-乙烯-乙烯醇共聚物-聚酰胺-聚乙烯共挤膜密封包装(聚乙烯厚度55微米,聚酰胺厚度15微米,乙烯-乙烯醇共聚物厚度15微米,聚乙烯厚度55微米),聚偏二氯乙烯的厚度分别为5微米、10微米、15微米、20微米和25微米。 Packaging of attractant lures: (1) PA/EVOH/PA/PE and PE/PVDC/PE co-extrusion film secondary packaging, the attractant lures are first coated with polyamide-ethylene-vinyl alcohol copolymer-polyamide- PE co-extrusion film sealing package (polyamide thickness 15 microns, ethylene-vinyl alcohol copolymer thickness 15 microns, polyethylene thickness 55 microns), and then polyethylene-polyvinylidene chloride-polyethylene co-extrusion film sealing packaging (The thickness of polyethylene is 55 microns), and the thickness of polyvinylidene chloride is 5 microns, 10 microns, 15 microns, 20 microns and 25 microns; (2) PE/PVDC/PA/EVOH/PA/PE co-extrusion film packaging, The attractant lure core is sealed and packaged with polyethylene-polyvinylidene chloride-polyamide-ethylene-vinyl alcohol copolymer-polyamide-polyethylene co-extruded film (thickness of polyethylene is 55 microns, thickness of polyamide is 15 microns, vinyl- The thickness of vinyl alcohol copolymer is 15 microns, the thickness of polyethylene is 55 microns), and the thickness of polyvinylidene chloride is 5 microns, 10 microns, 15 microns, 20 microns and 25 microns respectively.

将上述包装好的诱芯置于室内室温下贮存10个月(2014年7月20日到2015年5月19日),后测定其诱芯质量损失,并开展野外诱虫测试工作(结果见图2和表2)。 The above-mentioned packaged lures were stored at room temperature for 10 months (from July 20, 2014 to May 19, 2015), and then the mass loss of the lures was measured, and field trap tests were carried out (results see Figure 2 and Table 2).

二、不同厚度PVDC共挤膜包装下松褐天牛成虫引诱剂诱芯质量损失的测定2. Determination of the mass loss of the attractant lure core of Monochamus alternatus adults under different thickness PVDC co-extrusion film packaging

不同厚度聚偏二氯乙烯层共挤膜包装存储10个月后引诱剂诱芯的质量损失情况见图2。图2显示:无论是采用PA/EVOH/PA/PE、PE/PVDC/PE共挤膜二次包装,还是采用PE/PVDC/PA/EVOH/PA/PE共挤膜一次包装,当聚偏二氯乙烯层厚度大于15微米(含15微米)时引诱剂诱液的质量损失均明显较小。 Figure 2 shows the mass loss of the attractant lures after 10 months of storage in polyvinylidene chloride layer co-extruded film packages with different thicknesses. Figure 2 shows: Whether it is secondary packaging of PA/EVOH/PA/PE, PE/PVDC/PE co-extrusion film, or primary packaging of PE/PVDC/PA/EVOH/PA/PE co-extrusion film, when poly When the thickness of the vinyl chloride layer was greater than 15 microns (including 15 microns), the mass loss of the attractant liquid was significantly smaller.

三、不同厚度PVDC共挤膜包装下松褐天牛成虫引诱剂诱芯的野外诱虫测试3. Insect-attracting test of the attractant core of adult chrysalis monochamus under different thickness PVDC co-extruded film packaging

野外测试工作在福建泰宁(2015年5月20日-6月3日)进行,所用诱捕器根据专利“一种松褐天牛诱捕器”(公开号:CN203313934U)制作,将上述包装和存储10个月的诱芯拆封后安装在诱捕器上,另设1个临时制作的诱芯作为对照。野外诱虫试验设5空间重复,各处理随机排序,相邻诱捕器间隔80-100米,每周收集和统计各诱捕器捕获松褐天牛的数量,测试结果见表2。 The field test was carried out in Taining, Fujian Province (May 20-June 3, 2015). The trap used was made according to the patent "A Trapper for Monochamus alternatus" (public number: CN203313934U). The above-mentioned packaging and storage The 10-month-old lure was unpacked and installed on the trap, and another temporarily made lure was used as a control. In the field trapping experiment, 5 spatial repetitions were set up, each treatment was randomly sorted, and the interval between adjacent traps was 80-100 meters. The number of monochamus captured by each trap was collected and counted every week. The test results are shown in Table 2.

表2显示:无论是采用PA/EVOH/PA/PE、PE/PVDC/PE共挤膜二次包装,还是采用PE/PVDC/PA/EVOH/PA/PE共挤膜包装,存储10个月后的各种诱芯均捕获较多的松褐天牛,但当采用聚偏二氯乙烯层厚度大于15微米(含15微米)的共挤膜包装时,诱芯捕获的松褐天牛数量均明显更多。 Table 2 shows: no matter it is packaged with PA/EVOH/PA/PE, PE/PVDC/PE co-extruded film or PE/PVDC/PA/EVOH/PA/PE co-extruded film, after 10 months of storage All kinds of lures captured more monochamus, but when the polyvinylidene chloride layer thickness was greater than 15 microns (including 15 microns) co-extrusion film packaging, the number of monochamus captured by the lures was average Significantly more.

表2不同厚度PVDC共挤膜包装下诱芯的野外松褐天牛诱捕量(头/每诱捕器)Table 2 Trapping quantity of wild monochamus alternatus in lure cores packed with PVDC co-extruded film with different thicknesses (head/trap)

实施例3Example 3

一、松褐天牛成虫引诱剂诱芯的制备和包装(不同厚度PA膜)1. Preparation and packaging of lure cores for adult pine beetles (PA films with different thicknesses)

诱芯制备:根据专利“一种松褐天牛成虫引诱剂(公开号:CN102986739A)”由本实验室制作松褐天牛成虫引诱剂诱液。将20克引诱剂诱液用脱脂棉吸附后用聚乙烯薄膜密封,即制得松褐天牛成虫引诱剂诱芯。 Lure core preparation: according to the patent "An Attractant for Adult Monochamus alternatus (Publication No.: CN102986739A)", the laboratory prepared the attractant solution for Adult Monochamus alternata. Absorb 20 grams of the attractant solution with absorbent cotton and seal it with a polyethylene film to prepare the attractant lure core for the adult chrysalis monochamus.

引诱剂诱芯的包装:(1)PA/EVOH/PA/PE和PE/PVDC/PE共挤膜二次封装,将引诱剂诱芯先用聚酰胺-乙烯-乙烯醇共聚物-聚酰胺-聚乙烯共挤膜密封包装(乙烯-乙烯醇共聚物厚度15微米,聚乙烯厚度55微米),然后再用聚乙烯-聚偏二氯乙烯-聚乙烯共挤膜密封包装(聚乙烯厚度55微米,聚偏二氯乙烯的厚度15微米),聚酰胺厚度分别为15微米、20微米、25微米和30微米;(2)PE/PVDC/PA/EVOH/PA/PE共挤膜包装,将引诱剂诱芯用聚乙烯-聚偏二氯乙烯-聚酰胺-乙烯-乙烯醇共聚物-聚酰胺-聚乙烯共挤膜密封包装(聚乙烯厚度55微米,聚偏二氯乙烯厚度15微米,乙烯-乙烯醇共聚物厚度15微米,聚乙烯厚度55微米),聚酰胺厚度分别为15微米、20微米、25微米和30微米。 Packaging of attractant lures: (1) PA/EVOH/PA/PE and PE/PVDC/PE co-extrusion film secondary packaging, the attractant lures are first coated with polyamide-ethylene-vinyl alcohol copolymer-polyamide- PE co-extrusion film sealing packaging (ethylene-vinyl alcohol copolymer thickness 15 microns, polyethylene thickness 55 microns), and then polyethylene-polyvinylidene chloride-polyethylene co-extrusion film sealing packaging (polyethylene thickness 55 microns , the thickness of polyvinylidene chloride is 15 microns), the thickness of polyamide is 15 microns, 20 microns, 25 microns and 30 microns respectively; (2) PE/PVDC/PA/EVOH/PA/PE co-extrusion film packaging, will attract The agent lure is sealed with polyethylene-polyvinylidene chloride-polyamide-ethylene-vinyl alcohol copolymer-polyamide-polyethylene co-extruded film (thickness of polyethylene is 55 microns, thickness of polyvinylidene chloride is 15 microns, vinyl - Vinyl alcohol copolymer thickness 15 microns, polyethylene thickness 55 microns), polyamide thickness 15 microns, 20 microns, 25 microns and 30 microns respectively.

将上述包装好的诱芯置于室内室温下贮存10个月(2014年7月25日到2015年5月24日),后测定其诱芯质量损失,并开展野外诱虫测试工作(结果见图3和表3)。 The above-mentioned packaged lures were stored at room temperature for 10 months (from July 25, 2014 to May 24, 2015), and then the quality loss of the lures was measured, and field trap tests were carried out (results see Figure 3 and Table 3).

二、不同厚度PA共挤膜包装下松褐天牛成虫引诱剂诱芯质量损失的测定2. Determination of the mass loss of the attractant core of Monochamus alternatus adults under different thicknesses of PA co-extrusion film packaging

不同厚度聚酰胺层共挤膜包装存储10个月后引诱剂诱芯的质量损失情况见图3。图3显示:无论是采用PA/EVOH/PA/PE、PE/PVDC/PE共挤膜二次包装,还是采用PE/PVDC/PA/EVOH/PA/PE共挤膜一次包装,随着聚酰胺厚度的增加,诱芯的质量损失逐渐变小,但各种聚酰胺层厚度(15~30微米)包装下诱芯的质量损失均较小。 Figure 3 shows the mass loss of the attractant lures after storage for 10 months in polyamide layer co-extruded film packages with different thicknesses. Figure 3 shows: Whether it is secondary packaging of PA/EVOH/PA/PE, PE/PVDC/PE co-extrusion film, or primary packaging of PE/PVDC/PA/EVOH/PA/PE co-extrusion film, with the polyamide As the thickness increases, the mass loss of the lure becomes smaller gradually, but the mass loss of the lure under various polyamide layer thicknesses (15-30 microns) is small.

三、不同厚度PA共挤膜包装下松褐天牛成虫引诱剂诱芯的野外诱虫测试3. Insect trap test of the attractant core of adult chrysalis monochamus under different thickness PA co-extrusion film packaging

野外测试工作在福建泰宁(2015年5月25日-6月8日)进行,所用诱捕器根据专利“一种松褐天牛诱捕器”(公开号:CN203313934U)制作,将上述包装和存储10个月的诱芯拆封后安装在诱捕器上,另设1个临时制作的诱芯作为对照。野外诱虫试验设5空间重复,各处理随机排序,相邻诱捕器间隔80~100米,每周收集和统计各诱捕器捕获松褐天牛的数量,测试结果见表3。 The field test was carried out in Taining, Fujian Province (May 25-June 8, 2015). The trap used was made according to the patent "A Trapper for Monochamus alternatus" (public number: CN203313934U). The above-mentioned packaging and storage The 10-month-old lure was unpacked and installed on the trap, and another temporarily made lure was used as a control. In the wild insect trap experiment, 5 spatial repetitions were set up, each treatment was randomly sorted, and the interval between adjacent traps was 80-100 meters. The number of monochamus captured by each trap was collected and counted every week. The test results are shown in Table 3.

表3显示:无论是采用PA/EVOH/PA/PE、PE/PVDC/PE共挤膜二次包装,还是采用PE/PVDC/PA/EVOH/PA/PE共挤膜包装,存储10个月后的各种诱芯均捕获较多的松褐天牛,说明聚酰胺层厚度为15~30微米均可满足引诱剂诱芯的包装要求。 Table 3 shows that whether it is packaged with PA/EVOH/PA/PE, PE/PVDC/PE co-extrusion film, or PE/PVDC/PA/EVOH/PA/PE co-extrusion film, after 10 months of storage All kinds of lures captured more pine beetles, indicating that the polyamide layer thickness of 15-30 microns can meet the packaging requirements of attractant lures.

表3不同厚度A共挤膜包装下诱芯的野外松褐天牛诱捕量(头/每诱捕器)Table 3 Trapping quantity of wild monochamus under different thickness A co-extrusion film packaging (head/per trap)

实施例4Example 4

诱芯制备:根据专利“一种松褐天牛成虫引诱剂(公开号:CN102986739A)”由本实验室制作松褐天牛成虫引诱剂诱液。将20克引诱剂诱液用脱脂棉吸附后用聚乙烯薄膜密封,即制得松褐天牛成虫引诱剂诱芯。 Lure core preparation: according to the patent "An Attractant for Adult Monochamus alternatus (Publication No.: CN102986739A)", the laboratory prepared the attractant solution for Adult Monochamus alternata. Absorb 20 grams of the attractant solution with absorbent cotton and seal it with a polyethylene film to prepare the attractant lure core for the adult chrysalis monochamus.

将引诱剂诱芯用聚酰胺-乙烯-乙烯醇共聚物-聚酰胺-聚乙烯共挤膜密封包装(聚酰胺厚度15微米,乙烯-乙烯醇共聚物厚度15微米,聚乙烯厚度55微米),然后再用聚乙烯-聚偏二氯乙烯-聚乙烯共挤膜密封包装(聚乙烯厚度55,聚偏氯乙烯厚度7微米),存储10个月,得诱芯A。 The attractant core is sealed and packaged with polyamide-ethylene-vinyl alcohol copolymer-polyamide-polyethylene co-extrusion film (polyamide thickness 15 microns, ethylene-vinyl alcohol copolymer thickness 15 microns, polyethylene thickness 55 microns), Then use polyethylene-polyvinylidene chloride-polyethylene co-extrusion film to seal and pack (polyethylene thickness 55, polyvinylidene chloride thickness 7 microns), store for 10 months, and get lure A.

将引诱剂诱芯用聚酰胺-乙烯-乙烯醇共聚物-聚酰胺-聚乙烯共挤膜密封包装(聚酰胺厚度15微米,乙烯-乙烯醇共聚物厚度15微米,聚乙烯厚度55微米),然后再用聚乙烯-聚偏二氯乙烯-聚乙烯共挤膜密封包装(聚乙烯厚度55,聚偏氯乙烯厚度12微米),存储10个月,得诱芯B。 The attractant core is sealed and packaged with polyamide-ethylene-vinyl alcohol copolymer-polyamide-polyethylene co-extrusion film (polyamide thickness 15 microns, ethylene-vinyl alcohol copolymer thickness 15 microns, polyethylene thickness 55 microns), Then use polyethylene-polyvinylidene chloride-polyethylene co-extrusion film to seal and pack (polyethylene thickness 55, polyvinylidene chloride thickness 12 microns), store for 10 months, and get lure B.

将引诱剂诱芯用聚酰胺-乙烯-乙烯醇共聚物-聚酰胺-聚乙烯共挤膜密封包装(聚酰胺厚度15微米,乙烯-乙烯醇共聚物厚度15微米,聚乙烯厚度55微米),然后再用聚乙烯-聚偏二氯乙烯-聚乙烯共挤膜密封包装(聚乙烯厚度55,聚偏氯乙烯厚度17微米),存储10个月,得诱芯C。 The attractant core is sealed and packaged with polyamide-ethylene-vinyl alcohol copolymer-polyamide-polyethylene co-extrusion film (polyamide thickness 15 microns, ethylene-vinyl alcohol copolymer thickness 15 microns, polyethylene thickness 55 microns), Then use polyethylene-polyvinylidene chloride-polyethylene co-extrusion film to seal and pack (polyethylene thickness 55, polyvinylidene chloride thickness 17 microns), store for 10 months, and get lure C.

将引诱剂诱芯用聚酰胺-乙烯-乙烯醇共聚物-聚酰胺-聚乙烯共挤膜密封包装(聚酰胺厚度15微米,乙烯-乙烯醇共聚物厚度15微米,聚乙烯厚度55微米),然后再用聚乙烯-聚偏二氯乙烯-聚乙烯共挤膜密封包装(聚乙烯厚度55,聚偏氯乙烯厚度22微米),存储10个月,得诱芯D。 The attractant core is sealed and packaged with polyamide-ethylene-vinyl alcohol copolymer-polyamide-polyethylene co-extrusion film (polyamide thickness 15 microns, ethylene-vinyl alcohol copolymer thickness 15 microns, polyethylene thickness 55 microns), Then use polyethylene-polyvinylidene chloride-polyethylene co-extrusion film to seal and pack (polyethylene thickness 55, polyvinylidene chloride thickness 22 microns), store for 10 months, and get lure D.

将引诱剂诱芯用聚乙烯-聚偏二氯乙烯-聚酰胺-乙烯-乙烯醇共聚物-聚酰胺-聚乙烯共挤膜密封包装(聚乙烯厚度55微米,聚酰胺厚度15微米,乙烯-乙烯醇共聚物厚度15微米,聚乙烯厚度55微米,聚偏二氯乙烯厚度7微米),存储10个月,得诱芯E。 The attractant lure core is sealed and packaged with polyethylene-polyvinylidene chloride-polyamide-ethylene-vinyl alcohol copolymer-polyamide-polyethylene co-extruded film (thickness of polyethylene is 55 microns, thickness of polyamide is 15 microns, vinyl- The thickness of vinyl alcohol copolymer is 15 microns, the thickness of polyethylene is 55 microns, and the thickness of polyvinylidene chloride is 7 microns), and it is stored for 10 months to obtain lure E.

将引诱剂诱芯用聚乙烯-聚偏二氯乙烯-聚酰胺-乙烯-乙烯醇共聚物-聚酰胺-聚乙烯共挤膜密封包装(聚乙烯厚度55微米,聚酰胺厚度15微米,乙烯-乙烯醇共聚物厚度15微米,聚乙烯厚度55微米,聚偏二氯乙烯厚度12微米),存储10个月,得诱芯F。 The attractant lure core is sealed and packaged with polyethylene-polyvinylidene chloride-polyamide-ethylene-vinyl alcohol copolymer-polyamide-polyethylene co-extruded film (thickness of polyethylene is 55 microns, thickness of polyamide is 15 microns, vinyl- The thickness of vinyl alcohol copolymer is 15 microns, the thickness of polyethylene is 55 microns, and the thickness of polyvinylidene chloride is 12 microns), and it is stored for 10 months to obtain lure F.

将引诱剂诱芯用聚乙烯-聚偏二氯乙烯-聚酰胺-乙烯-乙烯醇共聚物-聚酰胺-聚乙烯共挤膜密封包装(聚乙烯厚度55微米,聚酰胺厚度15微米,乙烯-乙烯醇共聚物厚度15微米,聚乙烯厚度55微米,聚偏二氯乙烯厚度17微米),存储10个月,得诱芯G。 The attractant lure core is sealed and packaged with polyethylene-polyvinylidene chloride-polyamide-ethylene-vinyl alcohol copolymer-polyamide-polyethylene co-extruded film (thickness of polyethylene is 55 microns, thickness of polyamide is 15 microns, vinyl- Vinyl alcohol copolymer with a thickness of 15 microns, polyethylene with a thickness of 55 microns, and polyvinylidene chloride with a thickness of 17 microns), stored for 10 months, and lure G was obtained.

将引诱剂诱芯用聚乙烯-聚偏二氯乙烯-聚酰胺-乙烯-乙烯醇共聚物-聚酰胺-聚乙烯共挤膜密封包装(聚乙烯厚度55微米,聚酰胺厚度15微米,乙烯-乙烯醇共聚物厚度15微米,聚乙烯厚度55微米,聚偏二氯乙烯厚度22微米),存储10个月,得诱芯H。 The attractant lure core is sealed and packaged with polyethylene-polyvinylidene chloride-polyamide-ethylene-vinyl alcohol copolymer-polyamide-polyethylene co-extruded film (thickness of polyethylene is 55 microns, thickness of polyamide is 15 microns, vinyl- The thickness of vinyl alcohol copolymer is 15 microns, the thickness of polyethylene is 55 microns, and the thickness of polyvinylidene chloride is 22 microns), and it is stored for 10 months to obtain lure H.

将引诱剂诱芯用聚酰胺-乙烯-乙烯醇共聚物-聚酰胺-聚乙烯共挤膜密封包装(聚酰胺厚度18微米,乙烯-乙烯醇共聚物厚度15微米,聚乙烯厚度55微米),然后再用聚乙烯-聚偏二氯乙烯-聚乙烯共挤膜密封包装(聚乙烯厚度55,聚偏氯乙烯厚度7微米),存储10个月,得诱芯I。 The attractant core is sealed and packaged with polyamide-ethylene-vinyl alcohol copolymer-polyamide-polyethylene co-extrusion film (polyamide thickness 18 microns, ethylene-vinyl alcohol copolymer thickness 15 microns, polyethylene thickness 55 microns), Then use polyethylene-polyvinylidene chloride-polyethylene co-extrusion film to seal and pack (polyethylene thickness 55, polyvinylidene chloride thickness 7 microns), store for 10 months, and get lure I.

将引诱剂诱芯用聚酰胺-乙烯-乙烯醇共聚物-聚酰胺-聚乙烯共挤膜密封包装(聚酰胺厚度24微米,乙烯-乙烯醇共聚物厚度15微米,聚乙烯厚度55微米),然后再用聚乙烯-聚偏二氯乙烯-聚乙烯共挤膜密封包装(聚乙烯厚度55,聚偏氯乙烯厚度12微米),存储10个月,得诱芯J。 The attractant core is sealed and packaged with polyamide-ethylene-vinyl alcohol copolymer-polyamide-polyethylene co-extrusion film (polyamide thickness 24 microns, ethylene-vinyl alcohol copolymer thickness 15 microns, polyethylene thickness 55 microns), Then use polyethylene-polyvinylidene chloride-polyethylene co-extrusion film to seal and pack (polyethylene thickness 55, polyvinylidene chloride thickness 12 microns), store for 10 months, and get lure J.

将引诱剂诱芯用聚酰胺-乙烯-乙烯醇共聚物-聚酰胺-聚乙烯共挤膜密封包装(聚酰胺厚度28微米,乙烯-乙烯醇共聚物厚度15微米,聚乙烯厚度55微米),然后再用聚乙烯-聚偏二氯乙烯-聚乙烯共挤膜密封包装(聚乙烯厚度55,聚偏氯乙烯厚度17微米),存储10个月,得诱芯K。 The attractant core is sealed and packaged with polyamide-ethylene-vinyl alcohol copolymer-polyamide-polyethylene co-extruded film (polyamide thickness 28 microns, ethylene-vinyl alcohol copolymer thickness 15 microns, polyethylene thickness 55 microns), Then use polyethylene-polyvinylidene chloride-polyethylene co-extrusion film to seal and pack (polyethylene thickness 55, polyvinylidene chloride thickness 17 microns), store for 10 months, and get lure K.

将引诱剂诱芯用聚乙烯-聚偏二氯乙烯-聚酰胺-乙烯-乙烯醇共聚物-聚酰胺-聚乙烯共挤膜密封包装(聚酰胺厚度18微米,聚乙烯厚度55微米,乙烯-乙烯醇共聚物厚度15微米,聚乙烯厚度55微米,聚偏二氯乙烯厚度7微米),存储10个月,得诱芯L。 The attractant lure core is sealed and packaged with polyethylene-polyvinylidene chloride-polyamide-ethylene-vinyl alcohol copolymer-polyamide-polyethylene co-extruded film (polyamide thickness 18 microns, polyethylene thickness 55 microns, ethylene- The thickness of vinyl alcohol copolymer is 15 microns, the thickness of polyethylene is 55 microns, and the thickness of polyvinylidene chloride is 7 microns), and it is stored for 10 months to obtain lure L.

将引诱剂诱芯用聚乙烯-聚偏二氯乙烯-聚酰胺-乙烯-乙烯醇共聚物-聚酰胺-聚乙烯共挤膜密封包装(聚酰胺厚度24微米,聚乙烯厚度55微米,乙烯-乙烯醇共聚物厚度15微米,聚乙烯厚度55微米,聚偏二氯乙烯厚度12微米),存储10个月,得诱芯M。 The attractant lure core is sealed and packaged with polyethylene-polyvinylidene chloride-polyamide-ethylene-vinyl alcohol copolymer-polyamide-polyethylene co-extruded film (polyamide thickness 24 microns, polyethylene thickness 55 microns, ethylene- The thickness of vinyl alcohol copolymer is 15 microns, the thickness of polyethylene is 55 microns, and the thickness of polyvinylidene chloride is 12 microns), and it is stored for 10 months to obtain lure M.

将引诱剂诱芯用聚乙烯-聚偏二氯乙烯-聚酰胺-乙烯-乙烯醇共聚物-聚酰胺-聚乙烯共挤膜密封包装(聚酰胺厚度28微米,聚乙烯厚度55微米,乙烯-乙烯醇共聚物厚度15微米,聚乙烯厚度55微米,聚偏二氯乙烯厚度17微米),存储10个月,得诱芯N。 The attractant core is sealed and packaged with polyethylene-polyvinylidene chloride-polyamide-ethylene-vinyl alcohol copolymer-polyamide-polyethylene co-extruded film (polyamide thickness 28 microns, polyethylene thickness 55 microns, ethylene- The thickness of vinyl alcohol copolymer is 15 microns, the thickness of polyethylene is 55 microns, and the thickness of polyvinylidene chloride is 17 microns), and it is stored for 10 months, and the lure N is obtained.

利用诱芯A、诱芯B、诱芯C、诱芯D、诱芯E、诱芯F、诱芯G、诱芯H、诱芯I、诱芯J、诱芯K、诱芯L、诱芯M、诱芯N分别进行野外测试,得到的结果和表2、表3类似,说明按照权利要求1所述的方法包装的松褐天牛引诱剂诱芯的存储有效期长,是较好的包装方法。 Using Lure A, Lure B, Lure C, Lure D, Lure E, Lure F, Lure G, Lure H, Lure I, Lure J, Lure K, Lure L, Lure Core M, lure N carry out field test respectively, and the result that obtains is similar to table 2, table 3, illustrates that according to the storage effective period of the monochamus alternatus attractant lure core that the method for claim 1 packs is long, is better method of packing.

所述及材料的来源见表4。 See Table 4 for descriptions and sources of materials.

表4材料来源Table 4 Sources of materials

以上所述仅为本发明的较佳实施例,凡依本发明申请专利范围所做的均等变化与修饰,皆应属本发明的涵盖范围。 The above descriptions are only preferred embodiments of the present invention, and all equivalent changes and modifications made according to the scope of the patent application of the present invention shall fall within the scope of the present invention.

Claims (7)

1.一种松褐天牛成虫引诱剂诱芯的包装方法,其特征在于:采用PA/PE共挤膜、PA/EVOH/PA/PE共挤膜、PE/PVDC/PE共挤膜、PE/PVDC/PA/EVOH/PA/PE共挤膜中的一种或两种密封包装松褐天牛成虫引诱剂诱芯。 1. A packaging method for the attractant lure core of Monochamus alternatus adults, characterized in that: PA/PE co-extrusion film, PA/EVOH/PA/PE co-extrusion film, PE/PVDC/PE co-extrusion film, PE co-extrusion film, PE co-extrusion film are adopted /PVDC/PA/EVOH/PA/PE co-extruded film of one or two kinds of sealed package of adult monochamus alternatus attractant lure core. 2.根据权利要求1所述的松褐天牛成虫引诱剂诱芯的包装方法,其特征在于:将引诱剂诱芯先用PA/EVOH/PA/PE共挤膜密封包装,然后再用PE/PVDC/PE共挤膜进行二次密封包装。 2. the packaging method of the attractant lure core of Monochamus alternatus adult according to claim 1, is characterized in that: the attractant lure core is sealed and packaged with PA/EVOH/PA/PE co-extrusion film earlier, and then with PE /PVDC/PE co-extrusion film for secondary sealing packaging. 3.根据权利要求1所述的松褐天牛成虫引诱剂诱芯的包装方法,其特征在于:将引诱剂诱芯用PE/PVDC/PA/EVOH/PA/PE共挤膜密封包装。 3 . The packaging method of the attractant lure core of Monochamus alternatus adults according to claim 1 , characterized in that: the attractant lure core is sealed and packaged with PE/PVDC/PA/EVOH/PA/PE co-extrusion film. 4.根据权利要求1或2所述的松褐天牛成虫引诱剂诱芯的包装方法,其特征在于:所述的PE/PVDC/PE共挤膜中PVDC层的厚度为5~25微米。 4. The packaging method of the attractant lure core of Monochamus alternatus adults according to claim 1 or 2, characterized in that: the thickness of the PVDC layer in the PE/PVDC/PE co-extrusion film is 5-25 microns. 5.根据权利要求1或3所述的松褐天牛成虫引诱剂诱芯的包装方法,其特征在于:所述的PE/PVDC/PA/EVOH/PA/PE共挤膜中PVDC层的厚度为5~25微米,PA层的厚度为15~30微米。 5. the packaging method of the attractant lure core of Monochamus alternatus adults according to claim 1 or 3, is characterized in that: the thickness of the PVDC layer in the PE/PVDC/PA/EVOH/PA/PE co-extrusion film 5-25 microns, and the thickness of the PA layer is 15-30 microns. 6.根据权利要求4所述的松褐天牛成虫引诱剂诱芯的包装方法,其特征在于:所述的PE/PVDC/PE共挤膜中PVDC层的厚度为15~25微米。 6 . The packaging method of the attractant lure core of Monochamus alternatus adults according to claim 4 , characterized in that: the thickness of the PVDC layer in the PE/PVDC/PE co-extrusion film is 15-25 microns. 7.根据权利要求5所述的松褐天牛成虫引诱剂诱芯的包装方法,其特征在于:所述的PE/PVDC/PA/EVOH/PA/PE共挤膜中PVDC层的厚度为15~25微米,PA层的厚度为15~30微米。 7. the packaging method of the attractant lure core of Monochamus alternatus adults according to claim 5, is characterized in that: the thickness of the PVDC layer in the described PE/PVDC/PA/EVOH/PA/PE co-extrusion film is 15 ~25 microns, the thickness of the PA layer is 15-30 microns.
CN201510487775.0A 2015-08-11 2015-08-11 Packaging method for adult monochamus alternatus attractant lure core Pending CN105109830A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201510487775.0A CN105109830A (en) 2015-08-11 2015-08-11 Packaging method for adult monochamus alternatus attractant lure core

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201510487775.0A CN105109830A (en) 2015-08-11 2015-08-11 Packaging method for adult monochamus alternatus attractant lure core

Publications (1)

Publication Number Publication Date
CN105109830A true CN105109830A (en) 2015-12-02

Family

ID=54658015

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201510487775.0A Pending CN105109830A (en) 2015-08-11 2015-08-11 Packaging method for adult monochamus alternatus attractant lure core

Country Status (1)

Country Link
CN (1) CN105109830A (en)

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0889780B1 (en) * 1996-03-29 2004-07-14 Cryovac, Inc. Compositions and methods for selectively cross-linking films and improved film articles resulting therefrom
KR101023046B1 (en) * 2010-02-11 2011-03-24 대상 주식회사 Packaging method to suppress browning of fermented food during distribution
CN103753914A (en) * 2014-01-08 2014-04-30 合肥杰事杰新材料股份有限公司 Five-layer co-extrusion packaging material having high moisture barrier and barrier properties and preparation method thereof
CN203611513U (en) * 2013-09-27 2014-05-28 江阴升辉包装材料有限公司 High-barrier PVC (polyvinyl chloride) composite sheet
CN104371597A (en) * 2014-12-02 2015-02-25 河源市普立隆新材料科技有限公司 Preparation method of polypropylene type bonding resin for multi-layer coextrusion barrier packaging
CN104369508A (en) * 2014-12-11 2015-02-25 嘉合实业(苏州)有限公司 Degradable PP-EVOH high-barrier composite thin film
CN104670697A (en) * 2013-11-28 2015-06-03 天津海晶塑料制品有限公司 Safety packaging material of EPS (Expandable polystyrene)

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0889780B1 (en) * 1996-03-29 2004-07-14 Cryovac, Inc. Compositions and methods for selectively cross-linking films and improved film articles resulting therefrom
KR101023046B1 (en) * 2010-02-11 2011-03-24 대상 주식회사 Packaging method to suppress browning of fermented food during distribution
CN203611513U (en) * 2013-09-27 2014-05-28 江阴升辉包装材料有限公司 High-barrier PVC (polyvinyl chloride) composite sheet
CN104670697A (en) * 2013-11-28 2015-06-03 天津海晶塑料制品有限公司 Safety packaging material of EPS (Expandable polystyrene)
CN103753914A (en) * 2014-01-08 2014-04-30 合肥杰事杰新材料股份有限公司 Five-layer co-extrusion packaging material having high moisture barrier and barrier properties and preparation method thereof
CN104371597A (en) * 2014-12-02 2015-02-25 河源市普立隆新材料科技有限公司 Preparation method of polypropylene type bonding resin for multi-layer coextrusion barrier packaging
CN104369508A (en) * 2014-12-11 2015-02-25 嘉合实业(苏州)有限公司 Degradable PP-EVOH high-barrier composite thin film

Similar Documents

Publication Publication Date Title
JP7279135B2 (en) Antimicrobial gas-releasing agents, and systems and methods for their use
TWI523607B (en) Agricultural fumigation technology using a multilayer film containing a polyvinyl chloride (PVDC) vapor barrier
CN104097849B (en) Fresh-keeping packaging material capable of slowly releasing chlorine dioxide disinfectant and preparation method of fresh-keeping packaging material
JPH0249702A (en) Slow-acting pheromone agent
BRPI0816076B1 (en) Multilayer Active Oxygen Barrier Film and Packaging
US20190335746A1 (en) Antimicrobial gas releasing agents and systems and methods for using the same
JP2016505402A (en) Agricultural product storage polymer film, container made therefrom, and agricultural product storage related method
US11252971B2 (en) Antimicrobial packaging films
CN107379703A (en) A kind of control release type active packing film and preparation method thereof
CN100425138C (en) Luring agent for luring and collecting Dendroctonus valens
CN105109830A (en) Packaging method for adult monochamus alternatus attractant lure core
KR20150025564A (en) Process for preparing sustained-release lure for combating pests
CN105052860B (en) A kind of Monochamus alternatus Adults attractant lure and preparation method thereof
CN102599156A (en) Sex attractant and trapping core for Dendrolimus tabulaeformis and preparation method of trapping core
CA2588346C (en) Device for dispensing bark beetle pheromone in a controlled manner
JP3068235B2 (en) Packaging film, food freshness retaining material and freshness retaining method
US20240002119A1 (en) Packaging system with controlled release of active agent
CN206394126U (en) A kind of low absorption composite sheet for product packaging
US20210284410A1 (en) Super-hydrophobic thermoplastic films for packaging
TW202200359A (en) Laminated film materials and processes for manufacturing thereof and uses thereof
CN100438759C (en) Uses of verbenone repellants
CN201541531U (en) A kind of vacuum aluminized agricultural mulch film
CN102017945A (en) Holcocerus vicarious walker sex attractant
US20070157506A1 (en) Pest barrier
PT1652430E (en) Sustained pheromone releaser

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication
RJ01 Rejection of invention patent application after publication

Application publication date: 20151202