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CN105061646B - Polyacrylamide production line - Google Patents

Polyacrylamide production line Download PDF

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Publication number
CN105061646B
CN105061646B CN201510440232.3A CN201510440232A CN105061646B CN 105061646 B CN105061646 B CN 105061646B CN 201510440232 A CN201510440232 A CN 201510440232A CN 105061646 B CN105061646 B CN 105061646B
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filter
exsiccator
polyacrylamide
production line
pipe
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CN105061646A (en
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高军
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Essen (chinese) Co Ltd
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Essen (chinese) Co Ltd
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Abstract

The invention relates to a polyacrylamide production line. A reactor prefilter, an oil inlet lubrication polymerization reactor, an oil inlet lubrication smashing and pelleting device and a polyacrylamide colloid drying production line are connected in sequence, and the polyacrylamide colloid drying production line is respectively connected to a screening and grinding device and a pulse dust tail gas treatment device. The polyacrylamide production line is simple in structure, impurities in polyacrylamide production raw materials can be effectively filtered, the discharging time of a reactor is shortened, the amount of polymerization reactions is increased, colloid pelleting can be effectively lubricated, colloidal particles with the grain diameters of about 4 mm are obtained while the molecular weight of polyacrylamide is not reduced, required drying air quantity and energy consumption are reduced, the drying condition and standing time of materials are easily adjusted and controlled, the production capacity and product quality are improved, and the tail gas is effectively dedusted.

Description

A kind of polyacrylamide production line
Technical field
The present invention relates to polyacrylamide production technology, specifically a kind of polyacrylamide production line.
Background technology
Polyacrylamide production is, with acrylamide aqueous solution as raw material, in the presence of initiator, to carry out polyreaction, The polyacrylamide blob of viscose that generates after the completion of reaction is cleaved, pelletize, drying, crushing, final prepared polyacrylamide amine product.Third The raw materials such as acrylamide aqueous solution are polymerized in typically directly adding reactor, and in raw material, impurity directly influences polyacrylamide amine product Dissolubility.When polymerizable raw material reacts, traditional reactor is cylindrical, directly by the outlet discharge of its bottom, blob of viscose shape Polyacrylamide discharge is difficult, in follow-up dry run, as drying machine does not have the charging of steady and continuous, product is excessively done It is dry, crosslinking is caused, makes the dissolubility of product be deteriorated, reduce production efficiency and product quality.Polyacrylamide colloid is in pelletize Adhesion is easily formed in journey, thus causes over-drying in dry run, caused crosslinking, so as to the dissolubility of final products is poor, drop Low yield quality.The drying of polyacrylamide, should evaporate substantial amounts of moisture, and control material temperature can not be too high again, while Hot-spot to be also prevented, so the efficient and energy-conservation of drying machine just seems especially prominent.It is conventionally employed vibration fluidized bed dry Dry machine, is dried to polyacrylamide by dried medium, and dried medium is directly discharged, and thermal waste is unfavorable for energy-saving and emission-reduction.Poly- third After acrylamide colloidal solid is dried, Jing cyclone separator is separated, still containing micro- in the tail gas after the separation of polyacrylamide colloid granule Fine grained, is such as filtered using traditional sack cleaner, and dust-containing tail gas directly impact filter bag, the direct detention of filter bag into cleaner unit Dust, dust are fast by detention speed, and filter bag efficiency of dust collection reduces fast, causes frequently pulse backblowing deashing, cleaner unit filterer Make that the time is short, efficiency is low, and equipment frequent switching is fragile.
The content of the invention
For the above-mentioned deficiency of prior art, the invention provides a kind of simple structure, can effectively filter polyacrylamide Impurity in raw materials for production, shortens the reactor discharge time, increases the quantity of polyreaction, and energy effectively lubricating granulating from colloid, really Protecting Molecular Weight for Polyacrylamide does not reduce while obtaining particle diameter is being dried air quantity and energy consumption, material needed for 4mm or so micelles, reduction Drying condition, the time of staying be easy to adjust and control, improve production capacity and product quality, and effectively to tails dedusting Polyacrylamide production line.
The technical solution used in the present invention is:A kind of polyacrylamide production line, including reactor fore filter, oil-feed Lubricious polymeric reactor, oil inlet lubricating crush prilling granulator, polyacrylamide colloid drying production line, screening lapping device and arteries and veins Rush dust exhaust gas processing device, reactor fore filter, oil inlet lubricating polymer reactor, oil inlet lubricating crush prilling granulator and Polyacrylamide colloid drying production line is sequentially connected, and polyacrylamide colloid drying production line connects screening lapping device respectively With pulse dust exhaust gas processing device.
Further, the reactor fore filter includes feed pipe, the filter of more than and discharge pipe, The filter includes cylinder, upper end cover, crimping plate and filter bag, and upper end cover encapsulation cylinder is suitable for reading, and cylinder upper inside wall is provided with One circle boss, by upper end cover elastic compression joint on boss, in the middle part of crimping plate, hollow out connects its underpart to crimping many spring stacks of plate Jing The filter bag being articulated in cylinder;Feed pipe connects the filter cylinder boss upper portion side wall of more than respectively, one with On filter cylinder bottom be all connected with discharge pipe, discharge pipe connection oil inlet lubricating polymer reactor;The filter bag Precision is 10 microns;The upper end cover side is movably hinged on cylinder upper flanges face, opposite side Jing lock-screws or locking The tight connector drum upper flanges face of hook active lock.
Further, the oil inlet lubricating polymer reactor includes tank body, and tank body top is provided with charging aperture, and tank base sets There is connection oil inlet lubricating to crush the discharging opening of prilling granulator, in inverted cone-shaped, discharging opening is arranged at inverted cone to the tank body lower part The tank base of shape, the conical surface of the tank body of inverted cone-shaped are provided with air inlet and the fuel feed hole of more than one, fuel feed hole connection profit Oil tank;The air inlet of more than one and fuel feed hole are distributed in the taper seat cross-sectional circumferential of the tank body of inverted cone-shaped;It is described The miscella of light oil and oil emulsion is set in grease-box.
Further, the oil inlet lubricating crushes prilling granulator includes heavy pre-mill, conveying worm, comminutor, profit Oil tank, flow transducer and atomizer, the weighed conveying worm of pulverizer connect comminutor, are arranged in comminutor The atomizer of comminutor upper cavity, atomizer Jing flow controllers connection lubricating can, flow controller connection are weighed Pre-mill, sets the miscella of light oil and oil emulsion in lubricating can.
Further, the polyacrylamide colloid drying production line include the first blast pipe, the big blower fan of the first air intake, The little blower fan of one air intake, the first exsiccator, the second blast pipe, the big blower fan of the second air intake, the little blower fan of the second air intake, the second exsiccator and Backwind tube, the big blower fan of first air intake and the little blower fan of the first air intake are set in turn on the first blast pipe, and the first blast pipe enters Gas connects the first exsiccator;The big blower fan of second air intake and the little blower fan of the second air intake are arranged on the second blast pipe, and second enters Airduct air inlet connects the second exsiccator, and the second exsiccator Jing backwind tubes return-air connects the first blast pipe, and the discharging of the first exsiccator connects Cigarette receiving chimney, the second exsiccator return air connect the air inlet of the first exsiccator, the second exsiccator discharging connection screening grinding dress Put and pulse dust exhaust gas processing device.
Further, the pulse dust exhaust gas processing device includes tail gas discharging pipe, pulsed jet cloth filter, air-introduced machine And filter, tail gas discharging pipe is connected to the second exsiccator, and pulsed jet cloth filter, air-introduced machine and filter are set in turn in tail On gas delivery pipe, the tail gas discharging pipe connects pulsed jet cloth filter along pulsed jet cloth filter side wall tangent to periphery direction, The filter be accurate filter, the pulsed jet cloth filter be pulse flat bag dust remover, the pulsed jet cloth filter Pulse jet time be 10S.
Yet further, the screening lapping device includes one-level with upper screen cloth and roll grinding machine, and one-level is with upper screen cloth It is correspondingly connected to the second exsiccator, screen cloth top feeding connection roll grinding machine, screen cloth bottom and the external rewinding of roll grinding machine.
Using above technical scheme, it is an advantage of the invention that:
1st, from feed pipe respectively to feeding in the cylinder of more than one filter, raw material was by sending in place of crimping plate hollow out Filter bag, the impurity filtered in bag filtration removal plurality of raw materials of 10 micron accuracies of Jing, to guarantee follow-up polyacrylamide amine product Dissolubility, improve product quality;Can open around side with reference to upper end cover, opposite side is locked by lock-screw or locking bail, is passed through Upper end cover presses spring stack, holds out against sub- fishplate bar on the boss of cylinder medial wall by spring stack, and filter bag stable connection can be by beating Upper end cover trip spring post is opened to crimping the compression of plate, filter bag is removed in order to replacing in time, is thereby further ensured that filtration Quality.
2nd, the tank base of inverted cone-shaped is drawn in discharge efficiency and is effectively improved by discharging opening discharge;In the tank of inverted cone-shaped The conical surface of body is provided with the air inlet of more than and fuel feed hole, to tank body into send lubrication by fuel feed hole by grease-box Oil, lubricates blob of viscose material in which, can further improve the tank body discharge efficiency of inverted cone-shaped, and polyacrylamide blob of viscose can be made convenient It is quickly sent to subsequently cut into little blob of viscose and continuous conveying is to drying machine, it is ensured that product good dissolubility, while shortens reaction The discharge time of device, the quantity for doing polyreaction is increased, so as to improve production capacity and product quality;Lubricating oil is using light Matter oil and oil emulsion mixing, low-residual, environmental friendliness, beneficial to separating from finished product.
3rd, in polyacrylamide colloid pelletize, by atomizer atomization lubricating oil, polyacrylamide blob of viscose can be made Fast and easy cuts pelletize, and fast and effectively cutting way guarantees that molecular weight is non-degradable, it is ensured that Molecular Weight for Polyacrylamide does not drop Low and obtained granule is uniform, loose while little micelle of the particle diameter in 4mm or so can be obtained, with good mobility, easily It is dried in follow-up.Lubricating oil is mixed by light oil and oil emulsion, connects pre-mill of weighing using flow controller, by spiral transferring Machine control is sent to be automatically added to, effective control consumption of lubricating oil and lubricant effect, environmental friendliness, beneficial to separating from finished product.
4th, air is heated in the little blower fan ignition of first and second air intake, and hot-air sends into first and second exsiccator, to exsiccator Interior polyacrylamide particle is dried, and the dried hot-air in the second exsiccator is by the first air intake of backwind tube loopback Pipe, reclaims the heat of hot-air in the second exsiccator, for improving the intake air temperature of the first blast pipe, reduces neat gas burner Energy consumption, at the same by the vapor in the hot-air reclaimed in the second exsiccator can also combustion-supporting first neat gas burner, improve combustion Efficiency is burnt, neat gas burner energy consumption is further reduced, plays energy-saving and emission-reduction effect.
5th, bag dust collector has special gas channel, and air current flow is unobstructed, is easy to improve aerofluxuss and regurgitates efficiency;
After dust-containing tail gas passages through which vital energy circulates rushes sack cleaner dust removal by filtration, Jing accurate filters are filtered compared with fine dust again, enter one Step improves the filterability of dust;Tail gas discharging pipe connects bag pulse dedusting along pulsed jet cloth filter side wall tangent to periphery direction Device, when dust-containing tail gas enter pulsed jet cloth filter by tail gas discharging pipe, not directly just to filter bag, tail gas is tangential in cleaner unit Into and rotate around inwall, the rapid subsidence of larger particles dust can be improved, it is to avoid big dust particle directly blows to filter bag, causes The efficiency of dust collection of filter bag quickly reduce and reverse gas cleaning frequent switching, can ensure that effective dedusting time and the efficiency of cleaner unit Take into account, improve exhaust emissions speed and dust removing effects, while equipment is without frequent switching, increase the service life.
6th, screen cloth is sieved to dried colloidal solid, and larger particles connect roll by its top feeding after being sized Grinder is ground into required size again, outside the relatively fine particle after the relatively fine particle of screen cloth bottom screening and the crushing of roll grinding machine Material is received, the quality of final product can be effectively guaranteed.
Description of the drawings:
Fig. 1 is schematic structural view of the invention;
Fig. 2 is reactor fore filter structural representation of the present invention;
Fig. 3 is oil inlet lubricating polymer reactor structural representation of the present invention;
Fig. 4 is that oil inlet lubricating of the present invention crushes prilling granulator structural representation;
Fig. 5 is polyacrylamide colloid drying production line structural representation of the present invention;
Fig. 6 is pulse dust removal exhaust gas processing device structural representation of the present invention.
In figure:Reactor fore filter 1, feed pipe 1-1, discharge pipe 1-2, filter 1-3, cylinder 1-4, upper end Lid 1-5, hanger 1-6, lock-screw 1-7, spring stack 1-8, boss 1-9, crimp plate 1-10, and filter bag 1-11, oil inlet lubricating gather Reactor 2 is closed, tank body 2-1, charging aperture 2-2, discharging opening 2-3, air inlet 2-4, fuel feed hole 2-5, grease-box 2-6 enter glossy The broken prilling granulator 3 of smoothers, weigh pre-mill 3-1, conveying worm 3-2, comminutor 3-3, grease-box 3-4, flow transducer 3-5, atomizer 3-6, polyacrylamide colloid drying production line 4, the first blast pipe 4-1, the first air intake blower fan 4-2, first Neat gas burner 4-3, the first exsiccator 4-4, the second blast pipe 4-5, the second air intake blower fan 4-6, the second neat gas burner 4-7, the second exsiccator 4-8, backwind tube 4-9, auger 4-10 sieve lapping device 5, screen cloth 51, roll grinding machine 52, pulse powder Dirt exhaust gas processing device 6, tail gas discharging pipe 6-1, pulsed jet cloth filter 6-2, air-introduced machine 6-3, accurate filter 6-4.
Specific embodiment
Below in conjunction with accompanying drawing, the invention will be further described.
Shown in Fig. 1-6:A kind of polyacrylamide production line, including reactor fore filter 1, oil inlet lubricating polyreaction Device 2, oil inlet lubricating crushes prilling granulator 3, polyacrylamide colloid drying production line 4, screening lapping device 5 and pulse dust tail Flash Gas Compression Skid System 6, reactor fore filter 1, oil inlet lubricating polymer reactor 2, oil inlet lubricating crush prilling granulator 3 and poly- third Acrylamide colloid drying production line 4 is sequentially connected, and polyacrylamide colloid drying production line 4 connects screening lapping device 5 respectively With pulse dust exhaust gas processing device 6.Screening lapping device 5 includes one-level with upper screen cloth 5-1 and roll grinding machine 5-2, one-level With upper screen cloth 5-1 correspondence connection polyacrylamide colloids drying production line 4, screen cloth top feeding connection roll grinding machine, screen cloth Bottom and the external rewinding of roll grinding machine.
Reactor fore filter 1 includes feed pipe 1-1, the filter 1-3 and discharge pipe 1-2 of more than one, mistake Filter 1-3 includes cylinder 1-4, upper end cover 1-5, crimping plate 1-10 and filter bag 1-11, and upper end cover 1-5 is provided with hanger 1-6, on End cap 1-5 sides are movably hinged on cylinder 1-4 upper flanges face, the tight connector drum of opposite side Jing lock-screw 1-7 active locks 1-4 upper flanges face, cylinder 1-4 upper inside walls are provided with a circle boss 1-9, and plate many spring stack 1-8 of 1-10 Jing are by upper end for crimping On boss 1-9, in the middle part of crimping plate 1-10, hollow out connects the filter bag that its underpart is articulated in cylinder 1-4 to lid 1-5 elastic compression joints 1-11;Feed pipe 1-1 connects the filter cylinder boss upper portion side wall of more than, the filter cylinder of more than respectively Bottom is all connected with discharge pipe 1-2;The precision of filter bag is 10 microns.
Oil inlet lubricating polymer reactor 2 includes tank body 2-1 and grease-box 2-6, and tank body 2-1 tops are provided with connection discharge nozzle In inverted cone-shaped, discharging opening 2-3 is arranged at the tank body 2-1 bottoms of inverted cone-shaped for the charging aperture 2-2 of road 1-2, tank body 2-1 bottom, The conical surface of the tank body 2-1 of inverted cone-shaped is provided with the air inlet 2-4 and fuel feed hole 2-5 of more than, fuel feed hole 2-5 connection lubrications Fuel tank 2-6.The air inlet of more than one and fuel feed hole are distributed in the taper seat cross-sectional circumferential of the tank body of inverted cone-shaped.
Oil inlet lubricating crushes prilling granulator 3 includes heavy pre-mill 3-1, conveying worm 3-2, comminutor 3-3, lubricating oil Case 3-4, flow transducer 3-5 and atomizer 3-6.Pulverizer 1 is correspondingly arranged in weighed helical feed below discharging opening 2-3 Machine 3-2 connects comminutor 3-3, and the atomizer 3-6 of comminutor upper cavity, atomizer 3-6 are arranged in comminutor 3-3 Jing flow controllers 3-5 connects lubricating can 3-4, and flow controller 3-5 connects the pre-mill 3-1 that weighs.Set light in lubricating can The miscella of matter oil and oil emulsion.
Polyacrylamide colloid drying production line 4 includes the big blower fan 4-2 of the first blast pipe 4-1, the first air intake, the first air intake Little blower fan 4-3, the first exsiccator 4-4, the second blast pipe 4-5, the big blower fan 4-6 of the second air intake, the little blower fan 4-7 of the second air intake, Two exsiccator 4-8 and backwind tube 4-9, the first air intake blower fan 4-2 and the first neat gas burner 4-3 are set in turn in the first air intake On pipe 4-1, the first blast pipe 4-1 air inlets connect the first exsiccator 4-4;Second air intake blower fan 4-6 and the second neat gas burner 4-7 is arranged on the second blast pipe 4-5, and the second blast pipe 4-5 air inlets connect the second exsiccator 4-8, and the second exsiccator 4-8 Jing are returned Airduct 4-9 return-airs connect the first blast pipe 4-1, the first exsiccator 4-4 charging connection comminutor 3-3, the first exsiccator 4-4 dischargings Connect the second exsiccator 4-8.
Pulse dust removal exhaust gas processing device 6 include tail gas discharging pipe 6-1, pulsed jet cloth filter 6-2, air-introduced machine 6-3 and Accurate filter 6-4, pulsed jet cloth filter 6-2, air-introduced machine 6-3 and accurate filter 6-4 are set in turn in tail gas discharging pipe On 6-1, tail gas discharging pipe connects pulsed jet cloth filter along pulsed jet cloth filter side wall tangent to periphery direction.Pulse bag is removed Dirt device is pulse flat bag dust remover, and the pulse jet time of pulsed jet cloth filter is 10S.Second exsiccator 4-8 discharging connections To one-level is with upper screen cloth 5-1 tops and connects the tail gas discharging pipe 6-1 of pulse dust exhaust gas processing device 6.

Claims (1)

1. a kind of polyacrylamide production line, it is characterised in that:Including reactor fore filter, oil inlet lubricating polyreaction Device, oil inlet lubricating are crushed at prilling granulator, polyacrylamide colloid drying production line, screening lapping device and pulse dust tail gas Reason device, reactor fore filter, oil inlet lubricating polymer reactor, oil inlet lubricating crush prilling granulator and polyacrylamide gel Body drying production line is sequentially connected, and polyacrylamide colloid drying production line connects screening lapping device and pulse dust tail respectively Flash Gas Compression Skid System;The reactor fore filter includes feed pipe, the filter of more than and discharge pipe, the mistake Filter includes cylinder, upper end cover, crimping plate and filter bag, and upper end cover encapsulation cylinder is suitable for reading, and it is convex that cylinder upper inside wall is provided with a circle Platform, by upper end cover elastic compression joint on boss, in the middle part of crimping plate, hollow out connects its underpart and is articulated in crimping many spring stacks of plate Jing Filter bag in cylinder;Feed pipe connects the filter cylinder boss upper portion side wall of more than, the mistake of more than respectively Filter cylinder body bottom is all connected with discharge pipe, discharge pipe connection oil inlet lubricating polymer reactor;The precision of the filter bag is 10 microns;The upper end cover side is movably hinged on cylinder upper flanges face, and opposite side Jing lock-screws or locking bail are movable Locking connector drum upper flanges face;The oil inlet lubricating polymer reactor includes tank body, and tank body top is provided with charging aperture, tank body Bottom is provided with the discharging opening that connection oil inlet lubricating crushes prilling granulator, and in inverted cone-shaped, discharging opening is arranged at the tank body lower part The tank base of inverted cone-shaped, the conical surface of the tank body of inverted cone-shaped are provided with air inlet and the fuel feed hole of more than one, fuel feed hole Connection grease-box;The air inlet of more than one and fuel feed hole are distributed in the taper seat cross-sectional circumferential of the tank body of inverted cone-shaped On;The miscella of light oil and oil emulsion is set in the grease-box;The oil inlet lubricating crushing prilling granulator includes heavy pre- Grinding machine, conveying worm, comminutor, grease-box, flow transducer and atomizer, the weighed conveying worm of pulverizer connect Comminutor is connect, the atomizer of comminutor upper cavity, atomizer Jing flow controllers connection profit in comminutor, is arranged at Lubricating oil tank, flow controller connect pre-mill of weighing, and the miscella of light oil and oil emulsion is set in lubricating can;The polypropylene Amide colloid drying production line include the first blast pipe, the first air intake blower fan, the first neat gas burner, the first exsiccator, Two blast pipes, the second air intake blower fan, the second neat gas burner, the second exsiccator and backwind tube, first air intake blower fan and First neat gas burner is set in turn on the first blast pipe, and the first blast pipe air inlet connects the first exsiccator;Described second Air intake blower fan and the second neat gas burner are arranged on the second blast pipe, and the second blast pipe air inlet connects the second exsiccator, the Two exsiccator Jing backwind tubes return-airs connect the first blast pipe, the first exsiccator discharging connection chimney, the second exsiccator return air Connect the air inlet of the first exsiccator, the second exsiccator discharging connection screening lapping device and pulse dust exhaust gas processing device; The pulse dust exhaust gas processing device includes tail gas discharging pipe, pulsed jet cloth filter, air-introduced machine and filter, exhaust emissions Pipe is connected to the second exsiccator, and pulsed jet cloth filter, air-introduced machine and filter are set in turn on tail gas discharging pipe, the tail Gas delivery pipe connects pulsed jet cloth filter along pulsed jet cloth filter side wall tangent to periphery direction, and the filter is accurate mistake Filter, the pulsed jet cloth filter are pulse flat bag dust remover, and the pulse jet time of the pulsed jet cloth filter is 10S;The screening lapping device includes one-level with upper screen cloth and roll grinding machine, and it is dry that one-level is correspondingly connected to second with upper screen cloth Dry device, screen cloth top feeding connection roll grinding machine, screen cloth bottom and the external rewinding of roll grinding machine.
CN201510440232.3A 2015-05-06 2015-07-24 Polyacrylamide production line Active CN105061646B (en)

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CN201510225720.2A CN104861099A (en) 2015-05-06 2015-05-06 Polyacrylamide production line
CN2015102257202 2015-05-06
CN201510440232.3A CN105061646B (en) 2015-05-06 2015-07-24 Polyacrylamide production line

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CN107081121B (en) * 2017-06-09 2018-07-27 山东诺为制药流体系统有限公司 A kind of multi-functional continuous flow reaction system
CN108286873B (en) * 2018-01-22 2019-11-26 万达集团股份有限公司 A kind of New Polyacrylamide drying process
CN109265604A (en) * 2018-09-25 2019-01-25 中广核达胜加速器技术有限公司 A kind of preparation method of high molecular weight cation polyacrylamide
CN112535891B (en) * 2020-06-10 2025-04-15 成都思达能环保设备有限公司 Device and method for achieving reaction and filtration concentration
CN111804420B (en) * 2020-07-23 2021-12-10 安徽巨成精细化工有限公司 Grinder, proppant hybrid system based on polyacrylamide powder
CN113181852B (en) * 2021-05-25 2023-03-24 湖北理工学院 Method and equipment for preparing micronized medicine by using microreactor

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CN201071347Y (en) * 2007-05-31 2008-06-11 刘鹏 Device for producing water-swelling polymer polyacrylamide
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CN202355978U (en) * 2011-11-24 2012-08-01 肖文龙 Cyclone-type management device for recovering organic gas generated by spraying paint
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