CN105047509A - Focusing device for large-beam-current electronic beam targeting X-ray source with micro beams - Google Patents
Focusing device for large-beam-current electronic beam targeting X-ray source with micro beams Download PDFInfo
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Abstract
本发明公开了大束流电子束打靶微束斑X射线源的聚焦装置,包括电子束通道管、聚光镜模块、过渡段模块、物镜模块、可动光阑模块、物镜光阑座和靶;聚光镜模块上端与电子枪连接,下端固连过渡段模块;过渡段模块下端固连物镜模块,物镜模块下端套接物镜光阑座,物镜光阑座内部安装可动光阑。可动光阑模块有2个,末端中心位置分别对称开有半V型孔;当光阑片左右移动,通过控制叠加区域,形成连续不同尺寸孔径的通光孔。电子束通过电子束通道管从上到下依次穿过聚光镜模块、过渡段模块、物镜模块和可动光阑模块,到达靶平面;通过轰击靶产生X射线;优点在于,高精度的可动光阑通光孔尺寸能够实现不同束斑直径的电子束的快速切换。
The invention discloses a focusing device for a large beam current electron beam targeting a micro-beam spot X-ray source, including an electron beam channel tube, a condenser lens module, a transition section module, an objective lens module, a movable diaphragm module, an objective lens diaphragm seat and a target; The upper end is connected with the electron gun, and the lower end is fixedly connected with the transition section module; the lower end of the transition section module is fixedly connected with the objective lens module, and the lower end of the objective lens module is sleeved with the objective lens diaphragm seat, and a movable diaphragm is installed inside the objective lens diaphragm seat. There are 2 movable diaphragm modules, and half V-shaped holes are symmetrically opened in the center of the ends; when the diaphragm moves left and right, through the control of the overlapping area, continuous apertures of different sizes are formed. The electron beam passes through the electron beam channel tube from top to bottom sequentially through the condenser module, the transition section module, the objective lens module and the movable diaphragm module, and reaches the target plane; X-rays are generated by bombarding the target; the advantage is that the high-precision movable light The aperture size of the aperture enables fast switching of electron beams with different beam spot diameters.
Description
技术领域technical field
本发明属于三维无损显微观测技术领域,具体涉及大束流电子束打靶微束斑X射线源的聚焦装置。The invention belongs to the technical field of three-dimensional non-destructive microscopic observation, and in particular relates to a focusing device for a large-beam electron beam targeting a micro-beam spot X-ray source.
背景技术Background technique
微束斑X射线源是产生高清晰度X射线透视显微图象的必备部件之一。通常有两种方案产生微束斑X射线源:一是普通X射线管与X射线光学元件相结合;但是,X射线光学元件在材料性能和稳定性方面要求很高,设计时需要考虑如何降低从各种X射线光学元件传输到样品上的有用X射线光子数的损失和其热负载问题;安装时要考虑有无应变、定位是否精确以及光学元件整体稳定性等问题;二是将高速运动的电子束汇聚成微焦点,使其轰击金属靶面,产生微小束斑的X射线,即“细聚焦X射线源”;由于造价较低,控制方便,目前广泛应用于X射线显微成像和X射线显微CT等领域。The micro-spot X-ray source is one of the necessary components for producing high-definition X-ray fluoroscopy microscopic images. There are usually two ways to generate micro-beam spot X-ray sources: one is the combination of ordinary X-ray tubes and X-ray optical components; however, X-ray optical components have high requirements in terms of material performance and stability, and how to reduce the The loss of useful X-ray photons transmitted from various X-ray optical components to the sample and its thermal load; when installing, consider whether there is strain, whether the positioning is accurate, and the overall stability of the optical components; the second is to move at high speed The electron beam converges into a micro-focus, which bombards the metal target surface to generate X-rays with tiny beam spots, that is, "fine-focus X-ray source"; due to its low cost and easy control, it is widely used in X-ray microscopic imaging and X-ray micro-CT and other fields.
“细聚焦X射线源”通常采用两级透镜聚焦系统,距离靶平面较近的磁透镜称为物镜,距离靶面较远的磁透镜为聚光镜。靶面处入射电子束的能量,束流和束斑经过与靶材作用后,决定了X射线束的强度和分布。因此,设计优化两级透镜聚焦系统在保证靶面电子束束流的同时又获得小束斑一直是“细聚焦X射线源”工作者的目标。"Fine focus X-ray source" usually adopts a two-stage lens focusing system. The magnetic lens closer to the target plane is called the objective lens, and the magnetic lens farther away from the target plane is called the condenser lens. The energy, beam current and beam spot of the incident electron beam at the target surface determine the intensity and distribution of the X-ray beam after they interact with the target. Therefore, designing and optimizing the two-stage lens focusing system to obtain a small beam spot while ensuring the electron beam current on the target surface has always been the goal of the "fine-focus X-ray source" workers.
在两级透镜细聚焦X射线源中,靶面处电子束的性能由于受到物镜指标、聚光镜指标和电子间库仑力效应的因素影响,导致电子束束流的切换过程非常复杂,不利于实现动态过程的实时观测;而且物镜和聚光镜之间相互影响,很难实现独立调整;同时在利用微焦斑X射线源进行CT成像检测时,在微焦斑X射线源与探测器间的位置固定的条件下,其视野范围大小与分辨率高低成反比,即视野大分辨率低;视野小分辨率高。在检测时,一般是先采用大视野低分辨率进行扫描样品,而后根据需要选择感兴趣的区域进行小视野高分辨率检测样品,通常利用多维工件台移动被测样品,使得X射线源与被测样品间的、被测样品与探测器间的距离发生变化来实现大小视野的切换;由于受到承载样品的工件台的运动响应速度限制,同时如果样品的质量比较大,难以实现快速切换,需要切换时间将会增多,影响了样品的检测效率,这对有时需要检测样品的瞬态过程是很不利的。In the two-stage lens fine-focus X-ray source, the performance of the electron beam at the target surface is affected by the factors of the objective lens index, the condenser lens index and the Coulomb force effect between the electrons, resulting in a very complicated switching process of the electron beam current, which is not conducive to the realization of dynamic Real-time observation of the process; and the interaction between the objective lens and the condenser, it is difficult to achieve independent adjustment; at the same time, when the micro-focus spot X-ray source is used for CT imaging detection, the position between the micro-focus spot X-ray source and the detector is fixed. Under certain conditions, the size of the field of view is inversely proportional to the resolution, that is, a large field of view has a low resolution; a small field of view has a high resolution. During detection, the sample is generally scanned with a large field of view and low resolution, and then the area of interest is selected to detect the sample with a small field of view and high resolution according to the needs. Usually, the multi-dimensional workpiece table is used to move the sample to make the X-ray source and the object The distance between the measured samples and between the measured sample and the detector changes to realize the switching of the large and small field of view; due to the limitation of the motion response speed of the workpiece table carrying the sample, and if the quality of the sample is relatively large, it is difficult to achieve fast switching. The switching time will increase, which affects the detection efficiency of the sample, which is very unfavorable for the transient process that sometimes needs to detect the sample.
发明内容Contents of the invention
本发明针对利用X射线源进行CT成像检测时,系统的检测视野与分辨率无法同时兼顾,同时受到承载样品的工件台运动的响应速度限制以及样品的质量的影响,需要的切换时间增多,不利于实现动态过程的实时观测。基于上述原因,本发明提出一种可快速切换视野与分辨率的的两级透镜聚焦系统装置,具体是指一种大束流电子束打靶微束斑X射线源的聚焦装置。The present invention aims at using X-ray source for CT imaging detection, the detection field of view and resolution of the system cannot be taken into account at the same time, and at the same time, it is limited by the response speed of the movement of the workpiece table carrying the sample and the quality of the sample, and the required switching time is increased. It is beneficial to realize the real-time observation of the dynamic process. Based on the above reasons, the present invention proposes a two-stage lens focusing system device that can quickly switch the field of view and resolution, specifically a focusing device for targeting a micro-spot X-ray source with a large beam current electron beam.
大束流电子束打靶微束斑X射线源的聚焦装置,包括电子束通道管、聚光镜模块、过渡段模块、物镜模块、可动光阑模块、物镜光阑座和靶。A focusing device for a large-current electron beam targeting a micro-spot X-ray source, including an electron beam channel tube, a condenser lens module, a transition section module, an objective lens module, a movable diaphragm module, an objective lens diaphragm seat and a target.
该聚焦装置整体为圆柱形结构,电子束通道管采用空心管,位于聚光镜模块和物镜模块的中心轴线上;包括上电子束通道管和下电子束通道管;上电子束通道管上端与电子枪连接,上电子束通道管下端穿过聚光镜模块;下电子束通道管上端与聚光镜模块相连接,下电子束通道管下端穿过物镜模块与物镜光阑座连接;上电子束通道管与下电子束通道管套接在一起。The focusing device has a cylindrical structure as a whole, and the electron beam channel tube is a hollow tube, which is located on the central axis of the condenser module and the objective lens module; it includes an upper electron beam channel tube and a lower electron beam channel tube; the upper end of the upper electron beam channel tube is connected to the electron gun , the lower end of the upper electron beam channel tube passes through the condenser module; the upper end of the lower electron beam channel tube is connected with the condenser lens module, and the lower end of the lower electron beam channel tube passes through the objective lens module and is connected with the objective diaphragm seat; the upper electron beam channel tube is connected with the lower electron beam channel tube The channel pipes are socketed together.
电子束通过电子束通道管从上到下依次穿过聚光镜模块、过渡段模块、物镜模块和可动光阑模块,到达靶平面;通过轰击靶产生X射线。The electron beam passes through the electron beam channel tube from top to bottom sequentially through the condenser lens module, the transition section module, the objective lens module and the movable diaphragm module, and reaches the target plane; X-rays are generated by bombarding the target.
聚光镜模块上端与电子枪连接,聚光镜模块下端固连过渡段模块;The upper end of the condenser module is connected to the electron gun, and the lower end of the condenser module is fixedly connected to the transition section module;
聚光镜模块包括聚光镜上磁轭,聚光镜下磁轭,聚光镜极靴组件,聚光镜线圈组件和聚光镜密封环;The condenser module includes the condenser upper yoke, the condenser lower yoke, the condenser pole shoe assembly, the condenser coil assembly and the condenser sealing ring;
聚光镜上磁轭和聚光镜下磁轭均采用内部中空的圆柱体,对扣固定放置,并用聚光镜密封环密封隔离,聚光镜上下磁轭的中轴线与电子束通道管的中轴线相同。聚光镜极靴组件包括聚光镜上极靴和聚光镜下极靴,均采用内部中空的圆柱体,聚光镜上下极靴通过极靴隔磁环装配成一体,与电子束通道管的中轴线相同;聚光镜极靴组件的水平中心线与电子束通道管的中心轴线垂直,且交点位置为聚光镜位置。聚光镜线圈组件为圆环形,包括聚光镜线圈和聚光镜骨架,通过线圈架安装在聚光镜极靴组件外部与聚光镜上下磁轭中间的中空部分。The upper yoke of the condenser and the lower yoke of the condenser are both hollow cylinders inside, fixedly placed with buckles, and sealed and isolated with the condenser sealing ring. The central axis of the upper and lower yokes of the condenser is the same as the central axis of the electron beam passage tube. The condenser pole piece assembly includes the condenser upper pole piece and the condenser bottom pole piece, both of which are hollow cylinders inside. The condenser upper and lower pole pieces are assembled into one body through the pole piece spacer magnetic ring, which is the same as the central axis of the electron beam channel tube; the condenser pole piece The horizontal centerline of the assembly is perpendicular to the central axis of the electron beam passage tube, and the position of the intersection is the position of the condenser. The condenser coil assembly is circular, including the condenser coil and the condenser frame, and is installed on the hollow part between the outside of the condenser pole shoe assembly and the upper and lower magnetic yokes of the condenser through the coil frame.
过渡段模块采用内部中空的圆柱体,圆柱体的中轴线与电子束通道管的中轴线相同。The transition section module adopts a hollow cylinder inside, and the central axis of the cylinder is the same as the central axis of the electron beam passage tube.
过渡段模块下端固连物镜模块,物镜模块包括物镜上模块和物镜下模块,物镜线圈组件和物镜密封环;物镜上模块呈倒“山”字型,物镜下模块采用内部中空的圆锥体。The lower end of the transition section module is fixedly connected to the objective lens module, and the objective lens module includes an objective lens upper module and an objective lens lower module, an objective lens coil assembly and an objective lens sealing ring; the objective lens upper module is in the shape of an inverted "mountain", and the objective lens lower module adopts a hollow cone inside.
物镜上模块和物镜下模块对扣固定放置,中空内部放置物镜线圈组件;物镜上模块和物镜下模块的轴对称中心与电子束通道管的中心轴相同,同时在轴对称中心上开有通道,以便电子束通过。The upper module of the objective lens and the lower module of the objective lens are fixedly placed with buckles, and the objective lens coil assembly is placed inside the hollow; the axisymmetric center of the upper module of the objective lens and the lower module of the objective lens is the same as the central axis of the electron beam channel tube, and a channel is opened on the axisymmetric center. for the electron beam to pass through.
物镜线圈组件为圆环形,安放在物镜密封环上,物镜密封环通过螺钉与物镜上模块相连并固定,同时放置在物镜下模块上方;物镜上模块和物镜下模块在水平方向形成间隙,间隙的中心位置与轴线的相交点是物镜位置;The objective lens coil assembly is circular and placed on the objective lens sealing ring. The objective lens sealing ring is connected and fixed with the upper module of the objective lens through screws, and placed above the lower module of the objective lens at the same time; the upper module of the objective lens and the lower module of the objective lens form a gap in the horizontal direction. The intersection point of the central position of and the axis is the position of the objective lens;
物镜模块下端套接物镜光阑座,物镜光阑座内部安装可动光阑。The lower end of the objective lens module is sleeved with an objective lens diaphragm seat, and a movable diaphragm is installed inside the objective lens diaphragm seat.
可动光阑模块有2个,分别为对称的左光阑调节模块和右光阑调节模块,左光阑调节模块包括左光阑的驱动部件、左光阑杆和左光阑片;右光阑调节模块包括右光阑的驱动部件、右光阑杆和右光阑片;There are 2 movable aperture modules, which are symmetrical left aperture adjustment module and right aperture adjustment module respectively. The left aperture adjustment module includes the driving part of the left aperture, the left aperture rod and the left aperture plate; The diaphragm adjustment module includes the driving part of the right diaphragm, the right diaphragm rod and the right diaphragm plate;
左光阑的驱动部件和右光阑的驱动部件分别安装在物镜光阑座的两侧,左光阑杆和右光阑杆分别连接左光阑的驱动部件和右光阑的驱动部件,左光阑杆和右光阑杆分别连接左光阑片和右光阑片,左光阑片和右光阑片对称相对设置;The driving part of the left diaphragm and the driving part of the right diaphragm are respectively installed on both sides of the objective lens diaphragm seat, and the left diaphragm rod and the right diaphragm rod are respectively connected with the driving part of the left diaphragm and the driving part of the right diaphragm. The aperture rod and the right aperture rod are respectively connected to the left aperture plate and the right aperture plate, and the left aperture plate and the right aperture plate are arranged symmetrically relative to each other;
物镜光阑座整体呈圆环形结构,物镜光阑座与下电子束通道管的下端采用螺纹连接,位于物镜下模块的下方,物镜光阑座的中心轴线与电子束通道管的中心轴线相同,物镜光阑座的圆环中心内部放置左光阑片和右光阑片,物镜光阑座侧面分别对称开有两个通孔,作为左光阑杆和右光阑杆左右移动的通道,左光阑片和右光阑片的末端中心位置分别对称开有V型缺口,两端对称的左光阑片和右光阑片相互叠加,形成小孔;左光阑的驱动部件和右光阑的驱动部件控制左光阑杆和右光阑杆分别左右移动,进而带动左光阑片和右光阑片左右移动,通过控制左光阑片和右光阑片的叠加区域,形成连续不同尺寸孔径的通光孔。当左光阑片和右光阑片完全重叠时,通光孔最小为0,当左光阑片和右光阑片完全拼接在一起形成的孔为最大通光孔。The objective lens diaphragm seat is in the form of a ring structure as a whole. The objective lens diaphragm seat and the lower end of the lower electron beam passage tube are connected by threads, and are located below the lower module of the objective lens. The central axis of the objective lens diaphragm seat is the same as the central axis of the electron beam passage tube. , the left and right diaphragms are placed in the center of the ring of the objective lens diaphragm seat, and two through holes are symmetrically opened on the sides of the objective lens diaphragm seat, which are used as channels for the left and right diaphragm rods to move left and right. The ends of the left diaphragm and the right diaphragm are respectively symmetrically opened with V-shaped gaps, and the symmetrical left and right diaphragms are superimposed on each other to form a small hole; the driving part of the left diaphragm and the right diaphragm The drive part of the diaphragm controls the left and right diaphragm rods to move left and right respectively, and then drives the left diaphragm and the right diaphragm to move left and right. By controlling the superposition area of the left diaphragm and the right diaphragm, a continuous difference is formed. Clear aperture of the size aperture. When the left aperture plate and the right aperture plate overlap completely, the minimum aperture is 0, and the hole formed when the left aperture plate and the right aperture plate are completely spliced together is the maximum aperture.
靶工作时通过真空吸附在物镜光阑座的下方,表面上设有内凹,在内凹处镀上或溅射上一层重金属薄膜。When the target is working, it is vacuum-adsorbed under the aperture seat of the objective lens. There is a concave on the surface, and a layer of heavy metal film is plated or sputtered on the concave.
电子枪发射出的电子束经过聚光镜模块,在由聚光镜上下磁轭、聚光镜线圈组件和聚光镜上下极靴形成的磁场作用下,形成平行束;经过物镜模块时,通过调节可动光阑模块,选择可动光阑模块上合适的通光孔调节靶面电子束的入射角,改变靶平面处的束流大小和束斑尺寸;电子束经过物镜模块,物镜模块一方面通过工作距离和物镜线圈组件中电流的优化,获得高强度和亮度的X射线束,保证靶平面处大束流下微束斑;另一方面在聚光镜线圈电流不变时微调物镜线圈电流,找到靶平面处的电子清晰像,配合可移动光阑模块的通光孔变化快速完成束流的切换;电子束通过物镜光阑后轰击靶产生X射线。The electron beam emitted by the electron gun passes through the condenser module, and forms a parallel beam under the action of the magnetic field formed by the upper and lower yokes of the condenser, the coil assembly of the condenser and the upper and lower pole pieces of the condenser; The appropriate aperture on the moving diaphragm module adjusts the incident angle of the electron beam on the target surface, and changes the beam current size and beam spot size at the target plane; the electron beam passes through the objective lens module, and the objective lens module passes through the working distance and the current in the objective lens coil assembly The optimization of the X-ray beam with high intensity and brightness can ensure the large beam at the target plane to flow down the micro-beam spot; on the other hand, when the coil current of the condenser lens remains unchanged, the current of the objective lens coil can be fine-tuned to find a clear image of the electron at the target plane. The aperture of the aperture module changes quickly to complete the switching of the beam current; the electron beam bombards the target after passing through the aperture of the objective lens to generate X-rays.
本发明的优点在于:The advantages of the present invention are:
(1)一种大束流电子束打靶微束斑X射线源的聚焦系统装置,物镜模块和聚光镜模块可独立调整各自的线圈组件激励电流。(1) A focusing system device for targeting a micro-spot X-ray source with a large beam current electron beam. The objective lens module and the condenser lens module can independently adjust the excitation current of their respective coil components.
(2)一种大束流电子束打靶微束斑X射线源的聚焦系统装置,高精度的可动光阑通光孔尺寸能够实现不同束斑直径的电子束的快速切换。(2) A focusing system device for targeting a micro-spot X-ray source with a large beam current electron beam. The high-precision movable aperture aperture size can realize rapid switching of electron beams with different beam spot diameters.
附图说明Description of drawings
图1是本发明聚焦系统装置的整体结构图;Fig. 1 is the overall structural diagram of the focusing system device of the present invention;
图2是本发明聚光镜模块的结构示意图;Fig. 2 is the structural representation of condenser lens module of the present invention;
图2a是本发明聚光镜极靴的结构示意图;Fig. 2 a is the structural representation of condenser lens pole shoe of the present invention;
图3是本发明物镜模块的结构图;Fig. 3 is the structural diagram of objective lens module of the present invention;
图4是本发明可动光阑模块的结构示意图;Fig. 4 is a schematic structural diagram of the movable diaphragm module of the present invention;
图4a是本发明左光阑片的结构示意图;Fig. 4a is a schematic structural view of the left diaphragm of the present invention;
图4b是本发明右光阑片的结构示意图;Fig. 4b is a structural schematic diagram of the right diaphragm plate of the present invention;
图5是本发明物镜光阑座的结构图;Fig. 5 is the structural diagram of objective lens diaphragm seat of the present invention;
图6是本发明靶的结构图;Fig. 6 is a structural diagram of the target of the present invention;
图7是本发明平行模式工作的示意图;Fig. 7 is a schematic diagram of parallel mode operation of the present invention;
图8是本发明可动光阑切换束流的光路示意图;Fig. 8 is a schematic diagram of the optical path of the movable diaphragm switching beam of the present invention;
101-密封圈a;102-压紧螺母;103-聚光镜上磁轭;104-聚光镜极靴组件;1041-聚光镜上极靴;1042-聚光镜下极靴;1043-极靴隔磁环;1044-聚光镜位置;105-聚光镜密封环;106-聚光镜线圈组件;1061-聚光镜线圈;1062-聚光镜骨架;107-密封圈b;108-聚光镜下磁轭;201-物镜上模块;202-物镜线圈组件;203-物镜下模块;204-物镜密封环;205-密封圈c、206-密封圈d;207-物镜位置;301-过渡段;401-左光阑调节模块;402-右光阑调节模块;4011-左光阑的驱动部件;4012-左光阑杆;4013-左光阑密封圈;4014-左光阑片;4021-右光阑的驱动部件;4022-右光阑杆;4023-右光阑密封圈;4024-右光阑片;403-通光孔;502-下电子束通道管;501-上电子束通道管;601-物镜光阑座;602-密封圈e;603-密封圈f;604-靶;6041-重金属薄膜;101-Sealing ring a; 102-Compression nut; 103-Magnetic yoke on condenser; 104-Condenser pole shoe assembly; 1041-Condenser upper pole shoe; 1042-Condenser lower pole shoe; Condenser position; 105-condenser sealing ring; 106-condenser coil assembly; 1061-condenser coil; 1062-condenser frame; 107-sealing ring b; 108-condenser yoke; 203-objective lens lower module; 204-objective lens sealing ring; 205-sealing ring c, 206-sealing ring d; 207-objective lens position; 301-transition section; 401-left aperture adjustment module; 402-right aperture adjustment module; 4011-the driving part of the left diaphragm; 4012-the left diaphragm rod; 4013-the sealing ring of the left diaphragm; 4014-the left diaphragm; 4021-the driving part of the right diaphragm; 4022-the right diaphragm rod; 4023-right Diaphragm sealing ring; 4024-right diaphragm plate; 403-optical hole; 502-lower electron beam channel tube; 501-upper electron beam channel tube; 601-objective lens diaphragm seat; 602-sealing ring e; 603-seal Circle f; 604-target; 6041-heavy metal film;
具体实施方式Detailed ways
下面将结合附图和实施例对本发明作进一步的详细说明。The present invention will be further described in detail with reference to the accompanying drawings and embodiments.
大束流电子束打靶微束斑X射线源的聚焦装置,包括电子束通道管、聚光镜模块、过渡段模块、物镜模块、可动光阑模块、物镜光阑座和靶。A focusing device for a large-current electron beam targeting a micro-spot X-ray source, including an electron beam channel tube, a condenser lens module, a transition section module, an objective lens module, a movable diaphragm module, an objective lens diaphragm seat and a target.
聚焦装置整体为圆柱形结构,如图1所示,电子束通道管整体位于聚焦装置的中心轴线上,采用硬铝或铜材料制成的空心管,电子束通道管包括上电子束通道管501和下电子束通道管502;上电子束通道管501上端与电子枪连接,上电子束通道管501下端穿过聚光镜模块;下电子束通道管502上端与聚光镜模块相连接,下电子束通道管502下端穿过物镜模块与物镜光阑座601通过螺纹连接;上电子束通道管501与下电子束通道管502套接在一起。The focusing device has a cylindrical structure as a whole. As shown in Figure 1, the electron beam channel tube is located on the central axis of the focusing device as a whole, and is made of a hollow tube made of duralumin or copper. The electron beam channel tube includes an upper electron beam channel tube 501 and the lower electron beam channel tube 502; the upper end of the upper electron beam channel tube 501 is connected with the electron gun, and the lower end of the upper electron beam channel tube 501 passes through the condenser module; the upper end of the lower electron beam channel tube 502 is connected with the condenser module, and the lower electron beam channel tube 502 The lower end passes through the objective lens module and is threadedly connected with the objective lens aperture seat 601 ; the upper electron beam channel tube 501 and the lower electron beam channel tube 502 are socketed together.
电子束通过上电子束通道管501和下电子束通道管502从上到下依次穿过聚光镜模块,物镜模块和物镜光阑座601,到达靶604平面;通过轰击靶604上的重金属薄膜6041产生X射线。The electron beam passes through the upper electron beam channel tube 501 and the lower electron beam channel tube 502 from top to bottom sequentially through the condenser module, the objective lens module and the objective lens diaphragm seat 601, and reaches the plane of the target 604; it is generated by bombarding the heavy metal film 6041 on the target 604 X-rays.
聚光镜模块如图2所示:包括聚光镜上磁轭103,聚光镜下磁轭108,聚光镜极靴组件104,聚光镜密封环105和聚光镜线圈组件106;The condenser module is shown in Figure 2: it includes a condenser upper yoke 103, a condenser lower yoke 108, a condenser pole shoe assembly 104, a condenser seal ring 105 and a condenser coil assembly 106;
聚光镜极靴组件104如图2a所示,包括聚光镜上极靴1041和聚光镜下极靴1042,均采用内部中空的圆柱体,两者安装时保证有一定的间距S2,且与极靴隔磁环1043装配成一体;聚光镜极靴组件104的水平中心线与上电子束通道管501的中心轴线垂直,且交点位置为聚光镜位置1044;聚光镜上极靴1041的圆柱体直径为D11,聚光镜下极靴1042的圆柱体直径为D21。The condenser pole shoe assembly 104 is shown in Figure 2a, including the condenser upper pole shoe 1041 and the condenser lower pole shoe 1042, both of which are hollow cylinders inside, and a certain distance S2 is guaranteed when the two are installed, and the pole shoe is separated from the pole shoe by a magnetic ring 1043 is assembled into one; the horizontal centerline of the condenser pole shoe assembly 104 is perpendicular to the central axis of the upper electron beam passage tube 501, and the intersection position is the condenser position 1044; the cylinder diameter of the upper pole shoe 1041 of the condenser is D11, and the lower pole shoe of the condenser The cylinder diameter of 1042 is D21.
聚光镜上磁轭103和聚光镜下磁轭108均采用内部中空的圆柱体,对扣放置,并用聚光镜密封环105密封隔离,聚光镜密封环105和聚光镜上磁轭103、聚光镜下磁轭108接触处设有密封圈b107;电子枪与聚光镜上磁轭103之间通过压紧螺母102固定,用密封圈a101密封。The upper yoke 103 of the condenser and the lower yoke 108 of the condenser all adopt internal hollow cylinders, which are buckled and placed, and are sealed and isolated with the condenser seal ring 105. There is a sealing ring b107; the electron gun and the yoke 103 on the condenser are fixed by a compression nut 102 and sealed with a sealing ring a101.
在聚光镜极靴组件104外部与聚光镜上下磁轭中间的中空部分之间安装聚光镜线圈组件106,聚光镜线圈组件106包括聚光镜线圈1061和聚光镜骨架1062;聚光镜线圈组件106为圆环形,固定在聚光镜骨架1062上。The condenser coil assembly 106 is installed between the hollow part in the middle of the condenser pole shoe assembly 104 and the upper and lower magnetic yokes of the condenser, the condenser coil assembly 106 comprises a condenser coil 1061 and a condenser skeleton 1062; the condenser coil assembly 106 is a ring, fixed on the condenser skeleton 1062 on.
聚光镜下磁轭108下端连接过渡段模块和下电子束通道管502,过渡段模块下端固连物镜模块。聚光镜模块通过过渡段模块连接物镜模块,聚光镜模块,过渡段模块和物镜模块之间的固连均通过螺钉实现连接;The lower end of the yoke 108 under the condenser is connected to the transition section module and the lower electron beam passage tube 502, and the lower end of the transition section module is fixedly connected to the objective lens module. The condenser module is connected to the objective lens module through the transition section module, and the solid connections between the condenser lens module, the transition section module and the objective lens module are all connected by screws;
过渡段模块包括过渡段301,过渡段301采用内部中空的圆柱体,圆柱体的中轴线与电子束通道管的中轴线相同;The transition section module includes a transition section 301, the transition section 301 adopts a hollow cylinder, and the central axis of the cylinder is the same as the central axis of the electron beam passage tube;
物镜模块如图3所示:包括物镜上模块201和物镜下模块203,物镜线圈组件202,和物镜密封环204;物镜上模块201呈倒“山”字型,由物镜上磁轭和物镜上极靴由一块纯铁材料或球墨铸铁加工而成;物镜下模块203采用内部中空的圆锥体,由物镜下磁轭和物镜下极靴由一块纯铁材料或球墨铸铁加工而成;物镜上模块201和物镜下模块203对扣放置,中空内部放置物镜线圈组件202;物镜上模块201和物镜下模块203的轴对称中心与电子束通道管的中心轴相同,同时在轴对称中心上开有通道,以便电子束通过;物镜上模块201和物镜下模块203在水平方向形成间隙,间隙的中心位置与轴线的相交点是物镜位置207;物镜的上下模块构和间隙成了物镜模块的磁路;物镜上模块201和物镜下模块203分别安有密封圈c205和密封圈d206。The objective lens module is shown in Figure 3: it includes an objective lens upper module 201 and an objective lens lower module 203, an objective lens coil assembly 202, and an objective lens sealing ring 204; The pole shoe is processed from a piece of pure iron or ductile iron; the lower module 203 of the objective lens is a hollow cone, and the lower yoke of the objective lens and the lower pole piece of the objective lens are processed from a piece of pure iron material or ductile iron; the upper module of the objective lens 201 and the objective lens lower module 203 are buckled, and the objective lens coil assembly 202 is placed inside the hollow; the axisymmetric center of the objective lens upper module 201 and the objective lens lower module 203 is the same as the central axis of the electron beam passage tube, and a channel is opened on the axisymmetric center , so that the electron beam passes through; the upper module 201 of the objective lens and the lower module 203 of the objective lens form a gap in the horizontal direction, and the intersecting point between the center position of the gap and the axis is the objective lens position 207; the upper and lower modules of the objective lens form the magnetic circuit of the objective lens module with the gap; The upper module 201 of the objective lens and the lower module 203 of the objective lens are equipped with a sealing ring c205 and a sealing ring d206 respectively.
物镜线圈组件202为圆环形,由物镜线圈骨架和物镜线圈组成的;物镜线圈组件202安放在物镜密封环204上,物镜密封环204通过螺钉与物镜上模块201相连并固定,同时放置在物镜下模块203上方;The objective lens coil assembly 202 is circular and is made up of the objective lens coil skeleton and the objective lens coil; the objective lens coil assembly 202 is placed on the objective lens sealing ring 204, and the objective lens sealing ring 204 is connected and fixed with the upper module 201 of the objective lens by screws, and is placed on the objective lens at the same time. Above the lower module 203;
可动光阑模块有2个,如图4所示,分别为对称的左光阑调节模块401和右光阑调节模块402,左光阑调节模块401包括左光阑的驱动部件4011、左光阑杆4012、左光阑密封圈4013和左光阑片4014;右光阑调节模块402包括右光阑的驱动部件4021、右光阑杆4022、右光阑密封圈4023和右光阑片4024;There are two movable aperture modules, as shown in Figure 4, which are symmetrical left aperture adjustment module 401 and right aperture adjustment module 402 respectively, the left aperture adjustment module 401 includes the driving part 4011 of the left aperture, the left aperture Diaphragm rod 4012, left diaphragm sealing ring 4013 and left diaphragm plate 4014; right diaphragm adjustment module 402 includes right diaphragm driving part 4021, right diaphragm rod 4022, right diaphragm sealing ring 4023 and right diaphragm plate 4024 ;
左光阑的驱动部件4011和右光阑的驱动部件4021分别安装在物镜光阑座601内部的两个凸台上,左光阑杆4012和右光阑杆4022分别连接左光阑的驱动部件4011和右光阑的驱动部件4021,左光阑杆4012和右光阑杆4022上分别设有左光阑密封圈4013和右光阑密封圈4023;左光阑杆4012和右光阑杆4022分别连接左光阑片4014和右光阑片4024,左光阑片4014和右光阑片4024对称相对设置。The driving part 4011 of the left diaphragm and the driving part 4021 of the right diaphragm are installed on the two bosses inside the objective lens diaphragm seat 601 respectively, and the left diaphragm rod 4012 and the right diaphragm rod 4022 are respectively connected with the driving part of the left diaphragm 4011 and the driving part 4021 of the right diaphragm, the left diaphragm rod 4012 and the right diaphragm rod 4022 are respectively provided with a left diaphragm sealing ring 4013 and a right diaphragm sealing ring 4023; the left diaphragm rod 4012 and the right diaphragm rod 4022 The left aperture plate 4014 and the right aperture plate 4024 are respectively connected, and the left aperture plate 4014 and the right aperture plate 4024 are symmetrically arranged opposite to each other.
如图4a和图4b所示,左光阑片4014和右光阑片4024的末端中心位置分别对称开有半V型孔,两端对称的左光阑片4014和右光阑片4024上下相互叠加,左光阑的驱动部件4011控制左光阑杆4012左右运动,右光阑的驱动部件4021控制右光阑杆4022左右移动,进而带动左光阑片4014和右光阑片4024左右移动,控制两端对称左光阑片4014和右光阑片4024的叠加区域,形成连续不同尺寸孔径的通光孔403,当左光阑片4014和右光阑片4024完全重叠时,通光孔403最小为0,当左光阑片4014和右光阑片4024完全拼接在一起形成的孔为最大通光孔403。As shown in Figure 4a and Figure 4b, the central positions of the ends of the left diaphragm 4014 and the right diaphragm 4024 are respectively symmetrically opened with a half-V-shaped hole, and the symmetrical left diaphragm 4014 and the right diaphragm 4024 mutually up and down. Superposition, the driving part 4011 of the left aperture controls the left and right diaphragm rod 4012 to move left and right, the driving part 4021 of the right diaphragm controls the right diaphragm rod 4022 to move left and right, and then drives the left diaphragm plate 4014 and the right diaphragm plate 4024 to move left and right, Control the overlapping area of the symmetrical left diaphragm 4014 and the right diaphragm 4024 to form continuous apertures 403 of different sizes. When the left diaphragm 4014 and the right diaphragm 4024 completely overlap, the aperture 403 The minimum value is 0, and the hole formed when the left aperture plate 4014 and the right aperture plate 4024 are completely spliced together is the maximum light aperture 403 .
物镜光阑座601如图5所示,整体呈圆环形结构,物镜光阑座601与下电子束通道管502的下端通过螺纹连接,位于在物镜下模块203的下方,物镜光阑601的中心轴线与电子束通道管的中心轴线相同,物镜光阑座601设有密封圈e602。Objective lens diaphragm seat 601 is shown in Figure 5, and the whole is circular ring structure, and the lower end of objective lens diaphragm seat 601 and lower electron beam channel tube 502 is connected by screw thread, is positioned at the below of module 203 under objective lens, and objective lens diaphragm 601 The central axis is the same as the central axis of the electron beam passage tube, and the objective lens aperture seat 601 is provided with a sealing ring e602.
物镜光阑座601的圆环中心放置左光阑片4014和右光阑片4024,直径大于等于左光阑片4014和右光阑片4024完全拼接后的尺寸,物镜光阑座601的两个侧面均分别对称开有一个通孔,作为左光阑杆4012和右光阑杆4022左右移动的通道,左光阑杆4012和右光阑杆4022伸入通孔,左右移动,可动光阑模块的移动方向垂直于电子束通道管的中心轴的轴线;通过控制可动光阑模块的运动形成不同直径的通光孔403。The ring center of the objective lens diaphragm seat 601 places the left diaphragm plate 4014 and the right diaphragm plate 4024, the diameter is greater than or equal to the size after the left diaphragm plate 4014 and the right diaphragm plate 4024 are completely spliced. A through hole is respectively symmetrically opened on the sides, as a passage for the left and right diaphragm rods 4012 and 4022 to move left and right. The moving direction of the module is perpendicular to the axis of the central axis of the electron beam passage tube; the light through holes 403 with different diameters are formed by controlling the movement of the movable diaphragm module.
靶604的结构如图6所示,设有密封圈f603,工作时通过真空吸附在物镜光阑座601的下方,靶604的材料为轻量元素,如铝;表面上设有内凹,在内凹处镀上或溅射上一层重金属薄膜6041,如钨。The structure of the target 604 is shown in Figure 6. It is provided with a sealing ring f603, and is sucked under the objective lens aperture seat 601 by vacuum during operation. The material of the target 604 is a light element, such as aluminum; A layer of heavy metal film 6041, such as tungsten, is plated or sputtered on the inner recess.
电子束从依次经过聚光镜模块产生的磁场、物镜模块产生的磁场,最后到达靶平面,为了避免电子在整个聚焦装置中随处乱飞,采用上电子束通道管501和下电子束通道管502、可动光阑模块和物镜光阑座601将电子限制在聚光镜模块和物镜模块的傍轴区域。The electron beam passes through the magnetic field generated by the condenser lens module and the magnetic field generated by the objective lens module in sequence, and finally reaches the target plane. The moving diaphragm module and objective lens diaphragm seat 601 confines the electrons to the paraxial region of the condenser lens module and the objective lens module.
大束流电子束打靶微束斑X射线源的聚焦系统装置中,如图7所示,通过设置聚光镜模块和物镜模块的位置、结构参数和线圈组件的激励实现两级聚焦系统的平行工作模式、从而在靶面处保证大束流的同时实现微束斑。In the focusing system device of the large-beam electron beam targeting the micro-beam spot X-ray source, as shown in Figure 7, the parallel working mode of the two-stage focusing system is realized by setting the position of the condenser module and the objective lens module, the structural parameters and the excitation of the coil assembly. In this way, a small beam spot can be realized while ensuring a large beam current at the target surface.
一种大束流电子束打靶微束斑X射线源的聚焦装置,可动光阑模块切换束流的光路如图8所示,具体方法如下:A focusing device for a large-beam current electron beam targeting a micro-beam spot X-ray source, the optical path of the movable diaphragm module switching the beam current is shown in Figure 8, and the specific method is as follows:
首先,通过设置聚焦系统装置的初始条件和优化靶平面处电子束的性能指标获得物镜模块的结构参数和电气参数;Firstly, the structural parameters and electrical parameters of the objective lens module are obtained by setting the initial conditions of the focusing system device and optimizing the performance index of the electron beam at the target plane;
然后,设置聚光镜模块的结构参数和电气参数,实现聚光镜模块和物镜模块之间电子束的运动与光轴平行,具体是通过设置聚光镜模块和物镜模块的位置、结构参数和线圈组件的激励获得平行模式下的两级透镜聚焦系统,获得大束流微束斑X射线源;Then, set the structural parameters and electrical parameters of the condenser module to realize that the movement of the electron beam between the condenser module and the objective lens module is parallel to the optical axis. The two-stage lens focusing system in the mode can obtain the X-ray source with large beam current and micro-beam spot;
最后,通过可动光阑的自动切换和物镜线圈电流的微调,实现大束流微束斑X射线源靶面处不同束斑大小的电子束快速切换,用于样品的实时观测。Finally, through the automatic switching of the movable diaphragm and the fine-tuning of the objective coil current, the rapid switching of electron beams with different beam spot sizes at the target surface of the large-beam micro-beam spot X-ray source is realized, which is used for real-time observation of samples.
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