CN105036700A - Preparation process of multicolor hollow ceramic plate - Google Patents
Preparation process of multicolor hollow ceramic plate Download PDFInfo
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- CN105036700A CN105036700A CN201510426310.4A CN201510426310A CN105036700A CN 105036700 A CN105036700 A CN 105036700A CN 201510426310 A CN201510426310 A CN 201510426310A CN 105036700 A CN105036700 A CN 105036700A
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- hollow
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- 238000002360 preparation method Methods 0.000 title claims abstract description 35
- 239000000919 ceramic Substances 0.000 title claims abstract description 28
- 239000000203 mixture Substances 0.000 claims description 54
- 229910052708 sodium Inorganic materials 0.000 claims description 48
- 239000011734 sodium Substances 0.000 claims description 48
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 36
- 238000005516 engineering process Methods 0.000 claims description 31
- PNEYBMLMFCGWSK-UHFFFAOYSA-N Alumina Chemical compound [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 30
- 239000002994 raw material Substances 0.000 claims description 30
- 238000001035 drying Methods 0.000 claims description 28
- 238000001694 spray drying Methods 0.000 claims description 27
- 239000000758 substrate Substances 0.000 claims description 27
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 claims description 24
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 24
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 24
- 238000000227 grinding Methods 0.000 claims description 24
- 229910052611 pyroxene Inorganic materials 0.000 claims description 24
- 239000010703 silicon Substances 0.000 claims description 24
- 229910052710 silicon Inorganic materials 0.000 claims description 24
- 235000019832 sodium triphosphate Nutrition 0.000 claims description 24
- 239000000454 talc Substances 0.000 claims description 24
- 235000012222 talc Nutrition 0.000 claims description 24
- 229910052623 talc Inorganic materials 0.000 claims description 24
- 239000012745 toughening agent Substances 0.000 claims description 24
- 239000012752 auxiliary agent Substances 0.000 claims description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 18
- 239000005995 Aluminium silicate Substances 0.000 claims description 12
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 claims description 12
- 101710194948 Protein phosphatase PhpP Proteins 0.000 claims description 12
- 239000006004 Quartz sand Substances 0.000 claims description 12
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 claims description 12
- 235000012211 aluminium silicate Nutrition 0.000 claims description 12
- 230000002902 bimodal effect Effects 0.000 claims description 12
- 239000010433 feldspar Substances 0.000 claims description 12
- 239000005350 fused silica glass Substances 0.000 claims description 12
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 12
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims description 12
- 229910052744 lithium Inorganic materials 0.000 claims description 12
- 239000003595 mist Substances 0.000 claims description 12
- HWGNBUXHKFFFIH-UHFFFAOYSA-I pentasodium;[oxido(phosphonatooxy)phosphoryl] phosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O HWGNBUXHKFFFIH-UHFFFAOYSA-I 0.000 claims description 12
- 239000000843 powder Substances 0.000 claims description 12
- 239000011028 pyrite Substances 0.000 claims description 12
- NIFIFKQPDTWWGU-UHFFFAOYSA-N pyrite Chemical compound [Fe+2].[S-][S-] NIFIFKQPDTWWGU-UHFFFAOYSA-N 0.000 claims description 12
- 229910052683 pyrite Inorganic materials 0.000 claims description 12
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N titanium dioxide Inorganic materials O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 12
- UNXRWKVEANCORM-UHFFFAOYSA-I triphosphate(5-) Chemical compound [O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O UNXRWKVEANCORM-UHFFFAOYSA-I 0.000 claims description 12
- 229910052742 iron Inorganic materials 0.000 claims description 10
- 238000007493 shaping process Methods 0.000 claims description 10
- 230000032683 aging Effects 0.000 claims description 9
- 239000011363 dried mixture Substances 0.000 claims description 9
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 claims description 6
- 229910021502 aluminium hydroxide Inorganic materials 0.000 claims description 6
- 239000010977 jade Substances 0.000 claims description 6
- 238000003756 stirring Methods 0.000 claims description 6
- 229920002134 Carboxymethyl cellulose Polymers 0.000 claims description 3
- 239000001768 carboxy methyl cellulose Substances 0.000 claims description 3
- 235000010948 carboxy methyl cellulose Nutrition 0.000 claims description 3
- 239000008112 carboxymethyl-cellulose Substances 0.000 claims description 3
- 238000009826 distribution Methods 0.000 claims description 3
- 229920000609 methyl cellulose Polymers 0.000 claims description 3
- 239000001923 methylcellulose Substances 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 3
- 230000035939 shock Effects 0.000 abstract description 5
- 230000000694 effects Effects 0.000 abstract description 3
- 238000004140 cleaning Methods 0.000 abstract description 2
- 230000007613 environmental effect Effects 0.000 abstract description 2
- 239000004615 ingredient Substances 0.000 abstract 3
- 238000012360 testing method Methods 0.000 description 28
- 208000037656 Respiratory Sounds Diseases 0.000 description 9
- 238000009413 insulation Methods 0.000 description 6
- 238000007710 freezing Methods 0.000 description 3
- 239000002932 luster Substances 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 238000010998 test method Methods 0.000 description 3
- -1 black earth Substances 0.000 description 2
- 239000003086 colorant Substances 0.000 description 2
- 238000000465 moulding Methods 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P40/00—Technologies relating to the processing of minerals
- Y02P40/60—Production of ceramic materials or ceramic elements, e.g. substitution of clay or shale by alternative raw materials, e.g. ashes
Landscapes
- Compositions Of Oxide Ceramics (AREA)
Abstract
A multicolor hollow ceramic plate is prepared from an ingredient 1, an ingredient 2 and an ingredient 3 in a weight ratio of 1:2:1. The invention provides a preparation process of a multicolor hollow ceramic plate, which has good performance, safety, fireproof, environmental protection, good self-cleaning performance, rich bright and mild color, no stain, good decorative effect, and thermal shock resistance and frost resistance superior to those of the prior art.
Description
Technical field
The present invention relates to the preparation technology of a kind of Multicolor hollow pottery plate.
Background technology
It is by being dried by original ore soil that current existing wet vacuum squeezes the preparation of mud moulding process Raw, and by moisture controlled at 5%-9%, broken by Raymond machine, material fineness is made to control below 60 orders, then put in storage, finally by formula batching, then finished product hollow ceramic plate can be obtained by mud extruder, drying tower, kiln.
As application number: shaping hollow ceramic plate of a kind of Multi-color wet described in 201210116644.8 and preparation method thereof, although the finished product pottery plate various colors that this technique provides, bright in luster, good decorating effect, its thermal shock resistance and anti-freezing property lower.
Summary of the invention
In order to overcome the problems referred to above, the invention provides the preparation technology of a kind of Multicolor hollow pottery plate.
For achieving the above object, technical scheme provided by the invention is:
A preparation technology for Multicolor hollow pottery plate, its by weight ratio be the batching one of 1:2:1, batching two, batching three be prepared from; Wherein:
Batching one is made up of the raw material of following per-cent: carclazyte 30-35%, pyrite tailing 20-30%, black earth 5-8%, quartz sand 10-15%, auxiliary agent 7%, silicon pyroxene 3%, idiosome toughener 3%, rotten sodium 0.3%, Fe
2o
30.4-0.6% and goth black 2.3%;
Batching two is made up of the raw material of following per-cent: talcum 28-32%, black earth 15-20%, kaolin 11-14%, rutile 20-28%, zirconium white 7-12%, rotten sodium 0.3%, fluidizer 0.4-0.6% and orange 4.3-5.8%;
Batching three is made up of the raw material of following per-cent: bimodal Alpha-alumina micro mist 20-29%, Reactive alumina 11-15%, fused quartz 21-28%, lithium feldspar 8-13%, silicon pyroxene 3%, talcum 3%, idiosome toughener 3%, rotten sodium 0.3%, dispergator 0.4% and iron oxide red 4.3-5.8%.
In described batching one, the raw material of auxiliary agent is made up of brown alundum powder 1-1.8, tripoly phosphate sodium STPP 2-4, jade powder 5.5-6.5, tripoly phosphate sodium STPP 1-2, aluminium hydroxide 12-15.
In described batching two, described fluidizer is methylcellulose gum or carboxymethyl cellulose.
The preparation technology of described batching one comprises the following steps:
1) by after brown alundum powder, tripoly phosphate sodium STPP, jade powder, tripoly phosphate sodium STPP, aluminium hydroxide mixing, grinding distribution is even, obtains auxiliary agent;
2) auxiliary agent step 1) obtained and carclazyte, pyrite tailing, black earth, quartz sand, silicon pyroxene, idiosome toughener, rotten sodium, Fe
2o
3and goth black co-grinding, cross 100-200 mesh sieve;
3) by step 2) mixture that the obtains water that adds same weight puts into stirrer together and is uniformly mixed 0.5-1 hour;
4) mixture after step 3) being stirred carries out drying by spray-drying tower, until biodiversity is 5-6%;
5) dried for step 4) mixture is put into ageing tower old 20 hours, namely obtain batching one.
The preparation technology of described batching two comprises the following steps:
1) get talcum, black earth, kaolin, rutile, zirconium white, rotten sodium, fluidizer and orange co-grinding, cross 100-200 mesh sieve;
2) water mixture that step 1) obtains being added same weight is put into stirrer together and is uniformly mixed 0.5-1 hour;
3) by step 2) stir after mixture carry out drying by spray-drying tower, until biodiversity is 9-12%;
4) dried for step 3) mixture is put into ageing tower old 25 hours, namely obtain batching two.
The preparation technology of described batching three comprises the following steps:
1) get bimodal Alpha-alumina micro mist, Reactive alumina, fused quartz, lithium feldspar, silicon pyroxene, talcum, idiosome toughener, rotten sodium, dispergator and iron oxide red co-grinding, cross 100-200 mesh sieve;
2) water mixture that step 1) obtains being added same weight is put into stirrer together and is uniformly mixed 0.5-1 hour;
3) by step 2) stir after mixture carry out drying by spray-drying tower, until biodiversity is 4-5%;
4) dried for step 3) mixture is put into ageing tower old 21 hours, namely obtain batching three.
The preparation technology of described hollow ceramic plate comprises the following steps:
1) be the batching one of 1:2:1 by weight ratio, batching two, batching three add mix and blend in stirrer, and add the water mixed grinding 9 hours of same weight;
2) mixture after step 1) being ground carries out drying by spray-drying tower, until biodiversity is 25%;
3) by step 2) to squeeze mud by de-airing extruder shaping for dried mixture, obtains pottery board member base substrate;
4) pottery board member base substrate step 3) obtained carries out drying by spray-drying tower, until biodiversity is less than 3%;
5) dried for step 4) pottery board member base substrate being put into temperature is that the kiln of 1429 DEG C is calcined, and after completing, insulation 14 hours, namely obtains finished product hollow ceramic plate.
the usefulness of technique scheme is:
The invention provides the preparation technology of a kind of Multicolor hollow pottery plate, by the hollow ceramic plate obtained by preparation method of the present invention, functional, fire safety, environmental protection, self-cleaning is good, and various colors is bright in luster, color and luster is gentle, without color spot, decorative effect is good, and the hollow ceramic plate that thermal shock resistance and frost resistance provide higher than prior art.
Embodiment
embodiment 1
A preparation technology for Multicolor hollow pottery plate, its by weight ratio be the batching one of 1:2:1, batching two, batching three be prepared from; Wherein:
Batching one is made up of the raw material of following per-cent: carclazyte 34%, pyrite tailing 26%, black earth 6%, quartz sand 12%, auxiliary agent 7%, silicon pyroxene 3%, idiosome toughener 3%, rotten sodium 0.3%, Fe
2o
30.5% and goth black 2.3%;
Batching two is made up of the raw material of following per-cent: talcum 31%, black earth 20%, kaolin 12%, rutile 20%, zirconium white 8%, rotten sodium 0.3%, fluidizer 0.4% and orange 4.9%;
Batching three is made up of the raw material of following per-cent: bimodal Alpha-alumina micro mist 28%, Reactive alumina 14%, fused quartz 28%, lithium feldspar 10%, silicon pyroxene 3%, talcum 3%, idiosome toughener 3%, rotten sodium 0.3%, dispergator 0.4% and iron oxide red 5.1%.
In described batching one, the raw material of auxiliary agent is made up of brown alundum powder 1-1.8, tripoly phosphate sodium STPP 2-4, jade powder 5.5-6.5, tripoly phosphate sodium STPP 1-2, aluminium hydroxide 12-15.
In described batching two, described fluidizer is methylcellulose gum or carboxymethyl cellulose.
The preparation technology of described batching one comprises the following steps:
1) by after brown alundum powder, tripoly phosphate sodium STPP, jade powder, tripoly phosphate sodium STPP, aluminium hydroxide mixing, grinding distribution is even, obtains auxiliary agent;
2) auxiliary agent step 1) obtained and carclazyte, pyrite tailing, black earth, quartz sand, silicon pyroxene, idiosome toughener, rotten sodium, Fe
2o
3and goth black co-grinding, cross 100-200 mesh sieve;
3) by step 2) mixture that the obtains water that adds same weight puts into stirrer together and is uniformly mixed 0.5-1 hour;
4) mixture after step 3) being stirred carries out drying by spray-drying tower, until biodiversity is 5-6%;
5) dried for step 4) mixture is put into ageing tower old 20 hours, namely obtain batching one.
The preparation technology of described batching two comprises the following steps:
1) get talcum, black earth, kaolin, rutile, zirconium white, rotten sodium, fluidizer and orange co-grinding, cross 100-200 mesh sieve;
2) water mixture that step 1) obtains being added same weight is put into stirrer together and is uniformly mixed 0.5-1 hour;
3) by step 2) stir after mixture carry out drying by spray-drying tower, until biodiversity is 9-12%;
4) dried for step 3) mixture is put into ageing tower old 25 hours, namely obtain batching two.
The preparation technology of described batching three comprises the following steps:
1) get bimodal Alpha-alumina micro mist, Reactive alumina, fused quartz, lithium feldspar, silicon pyroxene, talcum, idiosome toughener, rotten sodium, dispergator and iron oxide red co-grinding, cross 100-200 mesh sieve;
2) water mixture that step 1) obtains being added same weight is put into stirrer together and is uniformly mixed 0.5-1 hour;
3) by step 2) stir after mixture carry out drying by spray-drying tower, until biodiversity is 4-5%;
4) dried for step 3) mixture is put into ageing tower old 21 hours, namely obtain batching three.
The preparation technology of described hollow ceramic plate comprises the following steps:
1) be the batching one of 1:2:1 by weight ratio, batching two, batching three add mix and blend in stirrer, and add the water mixed grinding 9 hours of same weight;
2) mixture after step 1) being ground carries out drying by spray-drying tower, until biodiversity is 25%;
3) by step 2) to squeeze mud by de-airing extruder shaping for dried mixture, obtains pottery board member base substrate;
4) pottery board member base substrate step 3) obtained carries out drying by spray-drying tower, until biodiversity is less than 3%;
5) dried for step 4) pottery board member base substrate being put into temperature is that the kiln of 1429 DEG C is calcined, and after completing, insulation 14 hours, namely obtains finished product hollow ceramic plate.
embodiment 2
The preparation technology of a kind of Multicolor hollow pottery plate as described in Example 1, wherein:
Batching one is made up of the raw material of following per-cent: carclazyte 32%, pyrite tailing 28%, black earth 5%, quartz sand 14%, auxiliary agent 7%, silicon pyroxene 3%, idiosome toughener 3%, rotten sodium 0.3%, Fe
2o
30.6% and goth black 2.3%;
Batching two is made up of the raw material of following per-cent: talcum 29%, black earth 18%, kaolin 13%, rutile 22%, zirconium white 10%, rotten sodium 0.3%, fluidizer 0.5% and orange 5.3%;
Batching three is made up of the raw material of following per-cent: bimodal Alpha-alumina micro mist 25%, Reactive alumina 12%, fused quartz 26%, lithium feldspar 9%, silicon pyroxene 3%, talcum 3%, idiosome toughener 3%, rotten sodium 0.3%, dispergator 0.4% and iron oxide red 5.6%.
The preparation technology of described hollow ceramic plate comprises the following steps:
1) be the batching one of 1:2:1 by weight ratio, batching two, batching three add mix and blend in stirrer, and add the water mixed grinding 7 hours of same weight;
2) mixture after step 1) being ground carries out drying by spray-drying tower, until biodiversity is 27%;
3) by step 2) to squeeze mud by de-airing extruder shaping for dried mixture, obtains pottery board member base substrate;
4) pottery board member base substrate step 3) obtained carries out drying by spray-drying tower, until biodiversity is less than 3%;
5) dried for step 4) pottery board member base substrate being put into temperature is that the kiln of 1430 DEG C is calcined, and after completing, insulation 13 hours, namely obtains finished product hollow ceramic plate.
embodiment 3
The preparation technology of a kind of Multicolor hollow pottery plate as described in Example 1, wherein:
Batching one is made up of the raw material of following per-cent: carclazyte 30%, pyrite tailing 30%, black earth 5%, quartz sand 15%, auxiliary agent 7%, silicon pyroxene 3%, idiosome toughener 3%, rotten sodium 0.3%, Fe
2o
30.4% and goth black 2.3%;
Batching two is made up of the raw material of following per-cent: talcum 32%, black earth 15%, kaolin 14%, rutile 20%, zirconium white 12%, rotten sodium 0.3%, fluidizer 0.4% and orange 5.8%;
Batching three is made up of the raw material of following per-cent: bimodal Alpha-alumina micro mist 20%, Reactive alumina 15%, fused quartz 21%, lithium feldspar 13%, silicon pyroxene 3%, talcum 3%, idiosome toughener 3%, rotten sodium 0.3%, dispergator 0.4% and iron oxide red 4.3%.
The preparation technology of described hollow ceramic plate comprises the following steps:
1) be the batching one of 1:2:1 by weight ratio, batching two, batching three add mix and blend in stirrer, and add the water mixed grinding 10 hours of same weight;
2) mixture after step 1) being ground carries out drying by spray-drying tower, until biodiversity is 30%;
3) by step 2) to squeeze mud by de-airing extruder shaping for dried mixture, obtains pottery board member base substrate;
4) pottery board member base substrate step 3) obtained carries out drying by spray-drying tower, until biodiversity is less than 3%;
5) dried for step 4) pottery board member base substrate being put into temperature is that the kiln of 1435 DEG C is calcined, and after completing, insulation 13 hours, namely obtains finished product hollow ceramic plate.
embodiment 4
The preparation technology of a kind of Multicolor hollow pottery plate as described in Example 1, wherein:
Batching one is made up of the raw material of following per-cent: carclazyte 35%, pyrite tailing 20%, black earth 8%, quartz sand 10%, auxiliary agent 7%, silicon pyroxene 3%, idiosome toughener 3%, rotten sodium 0.3%, Fe
2o
30.6% and goth black 2.3%;
Batching two is made up of the raw material of following per-cent: talcum 28%, black earth 20%, kaolin 11%, rutile 28%, zirconium white 7%, rotten sodium 0.3%, fluidizer 0.6% and orange 4.3%;
Batching three is made up of the raw material of following per-cent: bimodal Alpha-alumina micro mist 29%, Reactive alumina 11%, fused quartz 28%, lithium feldspar 8%, silicon pyroxene 3%, talcum 3%, idiosome toughener 3%, rotten sodium 0.3%, dispergator 0.4% and iron oxide red 5.8%.
The preparation technology of described hollow ceramic plate comprises the following steps:
1) be the batching one of 1:2:1 by weight ratio, batching two, batching three add mix and blend in stirrer, and add the water mixed grinding 7 hours of same weight;
2) mixture after step 1) being ground carries out drying by spray-drying tower, until biodiversity is 20%;
3) by step 2) to squeeze mud by de-airing extruder shaping for dried mixture, obtains pottery board member base substrate;
4) pottery board member base substrate step 3) obtained carries out drying by spray-drying tower, until biodiversity is less than 3%;
5) dried for step 4) pottery board member base substrate being put into temperature is that the kiln of 1425 DEG C is calcined, and after completing, insulation 15 hours, namely obtains finished product hollow ceramic plate.
test method:
Operative norm of the present invention: standard GB/T/T27972-2011, test the finished product hollow ceramic plate obtained by above-mentioned four embodiments of the present invention respectively, result is as shown in table 1, and performance meets relevant regulations.
Table 1
Can be found out by table 1, through the finished product hollow ceramic plate obtained by above-mentioned four embodiments of the present invention, be about to by weight ratio be the batching one of 1:2:1, batching two, batching three be prepared from, batching one is made up of the raw material of following per-cent: carclazyte 30-35%, pyrite tailing 20-30%, black earth 5-8%, quartz sand 10-15%, auxiliary agent 7%, silicon pyroxene 3%, idiosome toughener 3%, rotten sodium 0.3%, Fe
2o
30.4-0.6% and goth black 2.3%; Batching two is made up of the raw material of following per-cent: talcum 28-32%, black earth 15-20%, kaolin 11-14%, rutile 20-28%, zirconium white 7-12%, rotten sodium 0.3%, fluidizer 0.4-0.6% and orange 4.3-5.8%; Batching three is made up of the raw material of following per-cent: bimodal Alpha-alumina micro mist 20-29%, Reactive alumina 11-15%, fused quartz 21-28%, lithium feldspar 8-13%, silicon pyroxene 3%, talcum 3%, idiosome toughener 3%, rotten sodium 0.3%, dispergator 0.4% and iron oxide red 4.3-5.8%; Be the batching one of 1:2:1 by weight ratio, batching two, batching three add mix and blend in stirrer, and add the water mixed grinding 7-10 hour of same weight; Mixture after grinding is carried out drying by spray-drying tower, until biodiversity is 20-30%; Dried mixture is squeezed mud by de-airing extruder shaping, obtain pottery board member base substrate; The pottery board member base substrate obtained is carried out drying by spray-drying tower, until biodiversity is less than 3%; It is that the kiln of 1425-1435 DEG C is calcined that dried pottery board member base substrate puts into temperature, is incubated the finished product hollow ceramic plate obtained for 13-15 hour after completing, and its performance meets concerned countries standard regulation.
test one:pottery plate thermal shock resistance is measured.
test materials:multicolor hollow pottery plate obtained by the present invention's four embodiments, application number are the hollow ceramic plate of 201210116644.8 and common pottery plate.
test method:according to standard GB/T/T27972-2011, undertaken by GB/T3810.9 regulation.
national standard:there is not crackle through 10 knock tests or burst.
test-results:
1, the Multicolor hollow pottery plate obtained by the embodiment of the present invention one:
In test, there is slight crackle the 22nd time, burst for the 25th time in flawless or burst phenomenon in product of the present invention 17 times above test.
2, the Multicolor hollow pottery plate obtained by the embodiment of the present invention two:
In test, there is slight crackle the 19th time, burst for the 22nd time in flawless or burst phenomenon in product of the present invention 17 times above test.
3, the Multicolor hollow pottery plate obtained by the embodiment of the present invention three:
In test, there is slight crackle the 17th time, burst for the 20th time in flawless or burst phenomenon in product of the present invention 15 times above test.
4, the Multicolor hollow pottery plate obtained by the embodiment of the present invention four:
In test, there is slight crackle the 18th time, burst for the 20th time in flawless or burst phenomenon in product of the present invention 17 times above test.
5, application number is the hollow ceramic plate of 201210116644.8:
In test, there is slight crackle the 14th time, burst for the 15th time in flawless or burst phenomenon in this product 12 times above test.
6, common pottery plate:
In test, flawless or burst phenomenon in this product 11 times above test, bursts for the 13rd time.
conclusion (of pressure testing):
Can find out by testing a test-results, through the finished product Multicolor hollow pottery plate obtained by above-mentioned four embodiments of the present invention, be about to by weight ratio be the batching one of 1:2:1, batching two, batching three be prepared from, batching one is made up of the raw material of following per-cent: carclazyte 30-35%, pyrite tailing 20-30%, black earth 5-8%, quartz sand 10-15%, auxiliary agent 7%, silicon pyroxene 3%, idiosome toughener 3%, rotten sodium 0.3%, Fe
2o
30.4-0.6% and goth black 2.3%; Batching two is made up of the raw material of following per-cent: talcum 28-32%, black earth 15-20%, kaolin 11-14%, rutile 20-28%, zirconium white 7-12%, rotten sodium 0.3%, fluidizer 0.4-0.6% and orange 4.3-5.8%; Batching three is made up of the raw material of following per-cent: bimodal Alpha-alumina micro mist 20-29%, Reactive alumina 11-15%, fused quartz 21-28%, lithium feldspar 8-13%, silicon pyroxene 3%, talcum 3%, idiosome toughener 3%, rotten sodium 0.3%, dispergator 0.4% and iron oxide red 4.3-5.8%; Be the batching one of 1:2:1 by weight ratio, batching two, batching three add mix and blend in stirrer, and add the water mixed grinding 7-10 hour of same weight; Mixture after grinding is carried out drying by spray-drying tower, until biodiversity is 20-30%; Dried mixture is squeezed mud by de-airing extruder shaping, obtain pottery board member base substrate; The pottery board member base substrate obtained is carried out drying by spray-drying tower, until biodiversity is less than 3%; It is that the kiln of 1425-1435 DEG C is calcined that dried pottery board member base substrate puts into temperature, the finished product hollow ceramic plate obtained for 13-15 hour is incubated after completing, thermal shock resistance exceedes the pottery plate that prior art provides, farther higher than common pottery plate, wherein best through the finished product pottery plate performance that the technical scheme described in embodiment one is obtained.
test two:finished product pottery plate anti-freezing property is measured.
test materials:multicolor hollow pottery plate obtained by the embodiment of the present invention one, application number are the hollow ceramic plate of 201210116644.8 and common pottery plate.
test method:according to standard GB/T/T27972-2011, undertaken by GB/T3810.12 regulation.
test-results:
1, the Multicolor hollow pottery plate obtained by the embodiment of the present invention one:
In test, there is slight crackle the 180th time, burst for the 190th time in flawless or burst phenomenon in product of the present invention 150 times above test.
2, application number is the hollow ceramic plate of 201210116644.8:
In test, there is slight crackle the 150th time, burst for the 160th time in flawless or burst phenomenon in this product 130 times above test.
3, common pottery plate:
In test, there is slight crackle the 130th time, burst for the 140th time in flawless or burst phenomenon in this product 110 times above test.
conclusion (of pressure testing):
Can find out by testing two test-results, through the finished product Multicolor hollow pottery plate obtained by above-mentioned four embodiments of the present invention, be about to by weight ratio be the batching one of 1:2:1, batching two, batching three be prepared from, batching one is made up of the raw material of following per-cent: carclazyte 34%, pyrite tailing 26%, black earth 6%, quartz sand 12%, auxiliary agent 7%, silicon pyroxene 3%, idiosome toughener 3%, rotten sodium 0.3%, Fe
2o
30.5% and goth black 2.3%; Batching two is made up of the raw material of following per-cent: talcum 31%, black earth 20%, kaolin 12%, rutile 20%, zirconium white 8%, rotten sodium 0.3%, fluidizer 0.4% and orange 4.9%; Batching three is made up of the raw material of following per-cent: bimodal Alpha-alumina micro mist 28%, Reactive alumina 14%, fused quartz 28%, lithium feldspar 10%, silicon pyroxene 3%, talcum 3%, idiosome toughener 3%, rotten sodium 0.3%, dispergator 0.4% and iron oxide red 5.1%; Be the batching one of 1:2:1 by weight ratio, batching two, batching three add mix and blend in stirrer, and add the water mixed grinding 9 hours of same weight; Mixture after grinding is carried out drying by spray-drying tower, until biodiversity is 25%; Dried mixture is squeezed mud by de-airing extruder shaping, obtain pottery board member base substrate; The pottery board member base substrate obtained is carried out drying by spray-drying tower, until biodiversity is less than 3%; It is that the kiln of 1429 DEG C is calcined that dried pottery board member base substrate puts into temperature, and after completing, insulation obtained finished product hollow ceramic plate after 14 hours, and anti-freezing property exceedes the pottery plate that prior art provides, farther higher than common pottery plate.
Claims (6)
1. a preparation technology for Multicolor hollow pottery plate, is characterized in that: its by weight ratio be the batching one of 1:2:1, batching two, batching three be prepared from; Wherein: batching one is made up of the raw material of following per-cent: carclazyte 30-35%, pyrite tailing 20-30%, black earth 5-8%, quartz sand 10-15%, auxiliary agent 7%, silicon pyroxene 3%, idiosome toughener 3%, rotten sodium 0.3%, Fe
2o
30.4-0.6% and goth black 2.3%; Batching two is made up of the raw material of following per-cent: talcum 28-32%, black earth 15-20%, kaolin 11-14%, rutile 20-28%, zirconium white 7-12%, rotten sodium 0.3%, fluidizer 0.4-0.6% and orange 4.3-5.8%; Batching three is made up of the raw material of following per-cent: bimodal Alpha-alumina micro mist 20-29%, Reactive alumina 11-15%, fused quartz 21-28%, lithium feldspar 8-13%, silicon pyroxene 3%, talcum 3%, idiosome toughener 3%, rotten sodium 0.3%, dispergator 0.4% and iron oxide red 4.3-5.8%; The preparation technology of described hollow ceramic plate comprises the following steps:
1) be the batching one of 1:2:1 by weight ratio, batching two, batching three add mix and blend in stirrer, and add the water mixed grinding 7-10 hour of same weight;
2) mixture after step 1) being ground carries out drying by spray-drying tower, until biodiversity is 20-30%;
3) by step 2) to squeeze mud by de-airing extruder shaping for dried mixture, obtains pottery board member base substrate;
4) pottery board member base substrate step 3) obtained carries out drying by spray-drying tower, until biodiversity is less than 3%;
5) dried for step 4) pottery board member base substrate being put into temperature is that the kiln of 1425-1435 DEG C is calcined, and is incubated 13-15 hour, namely obtains finished product hollow ceramic plate after completing.
2. the preparation technology of a kind of Multicolor hollow pottery plate as claimed in claim 1, it is characterized in that: in described batching one, the raw material of auxiliary agent is made up of brown alundum powder 1-1.8, tripoly phosphate sodium STPP 2-4, jade powder 5.5-6.5, tripoly phosphate sodium STPP 1-2, aluminium hydroxide 12-15.
3. the preparation technology of a kind of Multicolor hollow pottery plate as claimed in claim 1, is characterized in that: the preparation technology of described batching one comprises the following steps:
1) by after brown alundum powder 1-1.8, tripoly phosphate sodium STPP 2-4, jade powder 5.5-6.5, tripoly phosphate sodium STPP 1-2, aluminium hydroxide 12-15 mixing, grinding distribution is even, obtains auxiliary agent;
2) auxiliary agent step 1) obtained by 7% per-cent and carclazyte 34%, pyrite tailing 26%, black earth 6%, quartz sand 12%, silicon pyroxene 3%, idiosome toughener 3%, rotten sodium 0.3%, Fe
2o
30.5% and goth black 2.3% co-grinding, cross 100-200 mesh sieve;
3) by step 2) mixture that the obtains water that adds same weight puts into stirrer together and is uniformly mixed 0.5-1 hour;
4) mixture after step 3) being stirred carries out drying by spray-drying tower, until biodiversity is 5-6%;
5) dried for step 4) mixture is put into ageing tower old 20 hours, namely obtain batching one.
4. the preparation technology of a kind of Multicolor hollow pottery plate as claimed in claim 1, is characterized in that: the preparation technology of described batching two comprises the following steps:
1) get talcum 31%, black earth 20%, kaolin 12%, rutile 20%, zirconium white 8%, rotten sodium 0.3%, fluidizer 0.4% and orange 4.9% co-grinding, cross 100-200 mesh sieve;
2) water mixture that step 1) obtains being added same weight is put into stirrer together and is uniformly mixed 0.5-1 hour;
3) by step 2) stir after mixture carry out drying by spray-drying tower, until biodiversity is 9-12%;
4) dried for step 3) mixture is put into ageing tower old 25 hours, namely obtain batching two.
5. the preparation technology of a kind of Multicolor hollow pottery plate as claimed in claim 1, is characterized in that: the preparation technology of described batching three comprises the following steps:
1) get bimodal Alpha-alumina micro mist 28%, Reactive alumina 14%, fused quartz 28%, lithium feldspar 10%, silicon pyroxene 3%, talcum 3%, idiosome toughener 3%, rotten sodium 0.3%, dispergator 0.4% and iron oxide red 5.1% co-grinding, cross 100-200 mesh sieve;
2) water mixture that step 1) obtains being added same weight is put into stirrer together and is uniformly mixed 0.5-1 hour;
3) by step 2) stir after mixture carry out drying by spray-drying tower, until biodiversity is 4-5%;
4) dried for step 3) mixture is put into ageing tower old 21 hours, namely obtain batching three.
6. the preparation technology of a kind of Multicolor hollow pottery plate as claimed in claim 1, it is characterized in that: in described batching two, described fluidizer is methylcellulose gum or carboxymethyl cellulose.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110317041A (en) * | 2019-07-10 | 2019-10-11 | 福建省乐普陶板制造有限公司 | Useless pottery waste recovery reheating ceramic plate of one kind and preparation method thereof |
| CN110498668A (en) * | 2019-07-06 | 2019-11-26 | 福建省乐普陶板制造有限公司 | A kind of colorful glaze ceramic plate and preparation method thereof |
| CN110510989A (en) * | 2019-07-06 | 2019-11-29 | 福建省乐普陶板制造有限公司 | A kind of crystalline glaze ceramic plate and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102659388A (en) * | 2012-04-19 | 2012-09-12 | 福建华泰集团有限公司 | Multi-color wet molding hollow ceramic plate and manufacturing method thereof |
| CN103159458A (en) * | 2013-04-17 | 2013-06-19 | 成都理工大学 | Method for preparing color ceramic plate by utilizing pyrite tailing as main raw material |
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102659388A (en) * | 2012-04-19 | 2012-09-12 | 福建华泰集团有限公司 | Multi-color wet molding hollow ceramic plate and manufacturing method thereof |
| CN103159458A (en) * | 2013-04-17 | 2013-06-19 | 成都理工大学 | Method for preparing color ceramic plate by utilizing pyrite tailing as main raw material |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110498668A (en) * | 2019-07-06 | 2019-11-26 | 福建省乐普陶板制造有限公司 | A kind of colorful glaze ceramic plate and preparation method thereof |
| CN110510989A (en) * | 2019-07-06 | 2019-11-29 | 福建省乐普陶板制造有限公司 | A kind of crystalline glaze ceramic plate and preparation method thereof |
| CN110317041A (en) * | 2019-07-10 | 2019-10-11 | 福建省乐普陶板制造有限公司 | Useless pottery waste recovery reheating ceramic plate of one kind and preparation method thereof |
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