CN105011364A - Health-care cigarette filter tip using hawthorns and preparation method thereof - Google Patents
Health-care cigarette filter tip using hawthorns and preparation method thereof Download PDFInfo
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- CN105011364A CN105011364A CN201510349658.8A CN201510349658A CN105011364A CN 105011364 A CN105011364 A CN 105011364A CN 201510349658 A CN201510349658 A CN 201510349658A CN 105011364 A CN105011364 A CN 105011364A
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- filter core
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- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 23
- 241001092040 Crataegus Species 0.000 title claims abstract description 19
- 238000002360 preparation method Methods 0.000 title claims description 10
- 235000014493 Crataegus Nutrition 0.000 title abstract 4
- 239000000835 fiber Substances 0.000 claims abstract description 19
- 108010010803 Gelatin Proteins 0.000 claims abstract description 11
- 229920000159 gelatin Polymers 0.000 claims abstract description 11
- 239000008273 gelatin Substances 0.000 claims abstract description 11
- 235000019322 gelatine Nutrition 0.000 claims abstract description 11
- 235000011852 gelatine desserts Nutrition 0.000 claims abstract description 11
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 claims abstract description 8
- 229920000053 polysorbate 80 Polymers 0.000 claims abstract description 8
- 240000002853 Nelumbo nucifera Species 0.000 claims abstract description 7
- 235000006508 Nelumbo nucifera Nutrition 0.000 claims abstract description 7
- 235000006510 Nelumbo pentapetala Nutrition 0.000 claims abstract description 7
- 244000223014 Syzygium aromaticum Species 0.000 claims abstract description 7
- 235000016639 Syzygium aromaticum Nutrition 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 7
- PNEYBMLMFCGWSK-UHFFFAOYSA-N Alumina Chemical compound [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 18
- 235000009917 Crataegus X brevipes Nutrition 0.000 claims description 15
- 235000013204 Crataegus X haemacarpa Nutrition 0.000 claims description 15
- 235000009685 Crataegus X maligna Nutrition 0.000 claims description 15
- 235000009444 Crataegus X rubrocarnea Nutrition 0.000 claims description 15
- 235000009486 Crataegus bullatus Nutrition 0.000 claims description 15
- 235000017181 Crataegus chrysocarpa Nutrition 0.000 claims description 15
- 235000009682 Crataegus limnophila Nutrition 0.000 claims description 15
- 235000004423 Crataegus monogyna Nutrition 0.000 claims description 15
- 235000002313 Crataegus paludosa Nutrition 0.000 claims description 15
- 235000009840 Crataegus x incaedua Nutrition 0.000 claims description 15
- 239000002131 composite material Substances 0.000 claims description 15
- 239000006070 nanosuspension Substances 0.000 claims description 12
- 239000004372 Polyvinyl alcohol Substances 0.000 claims description 10
- 229920002451 polyvinyl alcohol Polymers 0.000 claims description 10
- 229940068984 polyvinyl alcohol Drugs 0.000 claims description 10
- 235000019422 polyvinyl alcohol Nutrition 0.000 claims description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 9
- 229920006221 acetate fiber Polymers 0.000 claims description 8
- 239000000843 powder Substances 0.000 claims description 7
- 240000000560 Citrus x paradisi Species 0.000 claims description 6
- 230000001112 coagulating effect Effects 0.000 claims description 6
- 239000012467 final product Substances 0.000 claims description 6
- 239000012530 fluid Substances 0.000 claims description 6
- 238000009987 spinning Methods 0.000 claims description 6
- 238000003756 stirring Methods 0.000 claims description 6
- 229940070527 tourmaline Drugs 0.000 claims description 6
- 229910052613 tourmaline Inorganic materials 0.000 claims description 6
- 239000011032 tourmaline Substances 0.000 claims description 6
- 238000001914 filtration Methods 0.000 claims description 5
- 238000002166 wet spinning Methods 0.000 claims description 4
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims description 3
- 238000004026 adhesive bonding Methods 0.000 claims description 3
- 238000001035 drying Methods 0.000 claims description 3
- 239000012535 impurity Substances 0.000 claims description 3
- 239000007788 liquid Substances 0.000 claims description 3
- 238000000034 method Methods 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 3
- 229920006395 saturated elastomer Polymers 0.000 claims description 3
- 238000007493 shaping process Methods 0.000 claims description 3
- 229910052938 sodium sulfate Inorganic materials 0.000 claims description 3
- 235000011152 sodium sulphate Nutrition 0.000 claims description 3
- 235000007106 Crataegus suborbiculata Nutrition 0.000 claims 1
- 241000073432 Crataegus suborbiculata Species 0.000 claims 1
- 235000013202 a hawthorn Nutrition 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 7
- 230000029087 digestion Effects 0.000 abstract description 2
- 210000002784 stomach Anatomy 0.000 abstract description 2
- 235000001759 Citrus maxima Nutrition 0.000 abstract 1
- 244000276331 Citrus maxima Species 0.000 abstract 1
- 238000010521 absorption reaction Methods 0.000 abstract 1
- 229920002301 cellulose acetate Polymers 0.000 abstract 1
- 239000002105 nanoparticle Substances 0.000 abstract 1
- 239000000244 polyoxyethylene sorbitan monooleate Substances 0.000 abstract 1
- 229920000136 polysorbate Polymers 0.000 abstract 1
- 229950008882 polysorbate Drugs 0.000 abstract 1
- 229940068968 polysorbate 80 Drugs 0.000 abstract 1
- 239000000725 suspension Substances 0.000 abstract 1
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 6
- 239000003546 flue gas Substances 0.000 description 6
- 239000000463 material Substances 0.000 description 4
- 239000000779 smoke Substances 0.000 description 3
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 2
- 238000001179 sorption measurement Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 description 1
- 206010013786 Dry skin Diseases 0.000 description 1
- 229940126678 chinese medicines Drugs 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 230000036449 good health Effects 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- HTMIBDQKFHUPSX-UHFFFAOYSA-N methdilazine Chemical group C1N(C)CCC1CN1C2=CC=CC=C2SC2=CC=CC=C21 HTMIBDQKFHUPSX-UHFFFAOYSA-N 0.000 description 1
- 229960002715 nicotine Drugs 0.000 description 1
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 description 1
- 150000004005 nitrosamines Chemical class 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 230000000391 smoking effect Effects 0.000 description 1
- 230000009967 tasteless effect Effects 0.000 description 1
- 235000021419 vinegar Nutrition 0.000 description 1
- 239000000052 vinegar Substances 0.000 description 1
Landscapes
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The invention discloses a health-care cigarette filter tip using hawthorns. The health-care cigarette filter tip is characterized by being prepared via following raw materials comprising, by weight, 40 to 60 parts of cellulose acetate fibers, 2 to 4 parts of hawthorns, 2 to 4 parts of shaddock peels, 1 to 2 parts of clove, 1 to 2 parts of lotus leaves, 1 to 2 parts of gelatin, 5 to 10 parts of polysorbate, 0.3 to 0.5 parts of polysorbate-80, and 1 to 2 parts of inorganic nanoparticle suspensions. The health-care cigarette filter tip using hawthorns is high in filter efficiency and good in harm-reducing effect and health-care effect without affecting odor absorption and has functions of purifying breath, clearing stomach and helping digestion.
Description
Technical field
The present invention relates to cigarette filter tip rod field, be specifically related to a kind of hawthorn filter-tip for health-care cigarette and preparation method thereof.
Background technology
Cigarette filter tip rod is the important component part of cigarette, and flue gas is filtered in its effect, reduces the harmful components in flue gas, reduces the harm that smoking produces human body.Filter rod is generally made up of forming paper, tow and overlapping glue, and the strand material generally used both at home and abroad at present has acetate silk and tacryl tow.Acetate silk have nontoxic, tasteless, be easy to processing, the advantage that strainability is good is strand material the most frequently used at present, and its shortcoming is the harmful substance such as CO, BaP can not adsorbed in flue gas, harm reduction limited use.The cigarette filter made with homogenous material is subject to self-characteristic and limits, be difficult to the harmful components in fully effective filtering cigarette smoke, therefore the composite cigarette filter of development and application multiple material making, while reaching abundant reducing tar and reducing harm effect, keep cigarette odor-absorbing, become the Main way of research and development at present.
Summary of the invention
The object of this invention is to provide a kind of hawthorn filter-tip for health-care cigarette, filter efficiency is high, and harm reduction is effective.
The present invention is achieved by the following technical solutions:
A kind of hawthorn filter-tip for health-care cigarette, it is obtained by the raw material of following weight parts:
Acetate fiber 40-60, hawthorn 2-4, pomelo peel 2-4, cloves 1-2, lotus leaf 1-2, gelatin 1-2, polyvinyl alcohol 5-10, Tween-80 0.3-0.5, inorganic nano suspension 1-2;
Described inorganic nano suspension is obtained by the raw material of following weight parts: nano-tourmaline powder 5-10, nano aluminium oxide 3-5, softex kw 0.05-0.1, water 60-80; Softex kw is added to the water 800-1000r/min to stir 3-5min by the preparation method of described inorganic nano suspension, then adds nano-tourmaline powder and nano aluminium oxide ultrasonic disperse 10-15min, to obtain final product.
A preparation method for hawthorn filter-tip for health-care cigarette, comprises the following steps:
(1) by solid-liquid weight ratio 1:20-1:30, hawthorn, pomelo peel, cloves and lotus leaf are added to the water, first decoct 1-2h, more ultrasonic process 5-10min, obtain treatment fluid after filtration;
(2) gelatin is taken by weight and polyvinyl alcohol prepares the gelatin solution of 10-12% and the poly-vinyl alcohol solution of 12-14% respectively, mix after removing impurity, add inorganic nano suspension and Tween-80 and stir 15-30min in 400-600r/min, obtaining co-blended spinning stoste; By described co-blended spinning stoste spinning-drawing machine by wet spinning obtained composite fibre in 35-40 DEG C of coagulating bath, described coagulating bath is saturated aqueous sodium sulfate;
(3) by soak at room temperature 6-8h in the treatment fluid in (1) of the composite fibre in (2), after taking out, 50-60 DEG C of drying is complete, mixes boundling after acetate fiber, obtains filter core fibre bundle;
(4) by the filter core fibre bundle gluing in (3), shaping, cut off, make filter core; Filter core wraps up forming paper, to obtain final product.
Advantage of the present invention is:
Using gelatin and polyvinyl alcohol as matrix, carry out composite with inorganic nanometer powder, composite fibre is obtained by wet spinning, and Tween-80 is introduced in preparation process, strengthen composite fibre to the adsorption effect of nonpolarity element, composite fibre is made to have concurrently polarity, the high filtering ability of nonpolar harmful components, simultaneously because acetate fiber is different from composite fiber surface pore size, by obtained composite fibre and the blended obtained filter core of acetate fiber, both the granule foreign removing various diameter in flue gas had been conducive to, turn improve the adsorption capacity of filter tip to character harmful components various in flue gas, make the filter tip filter efficiency that obtains high, harm reduction is effective, and do not affect suction taste, meanwhile, in the extract that the Chinese medicines such as hawthorn are composite, carry out immersion treatment by composite fibre, effectively can reduce the harmful substance contents in flue gas, reduce the harm to human body, purify implication in addition, effect that clearing stomach helps digestion, good health care effect.
Detailed description of the invention
Non-limiting examples of the present invention is as follows:
A kind of hawthorn filter-tip for health-care cigarette, is prepared from by the component raw material of following weight (kg):
Acetate fiber 50, hawthorn 3, pomelo peel 3, cloves 1.5, lotus leaf 1.5, gelatin 1.5, polyvinyl alcohol 8, Tween-80 0.4, inorganic nano suspension 1.5;
Described inorganic nano suspension is obtained by the raw material of following weight parts: nano-tourmaline powder 8, nano aluminium oxide 4, softex kw 0.08, water 70; Softex kw is added to the water 1000r/min to stir 3min by the preparation method of described inorganic nano suspension, then adds nano-tourmaline powder and nano aluminium oxide ultrasonic disperse 10min, to obtain final product.
The preparation method of hawthorn filter-tip for health-care cigarette comprises the following steps:
(1) by solid-liquid weight ratio 1:20, hawthorn, pomelo peel, cloves and lotus leaf are added to the water, first decoct 1h, more ultrasonic process 5min, obtain treatment fluid after filtration;
(2) take gelatin by weight and polyvinyl alcohol prepares the gelatin solution of 12% and the poly-vinyl alcohol solution of 114% respectively, mix after removing impurity, add inorganic nano suspension and Tween-80 and stir 15min in 400r/min, obtaining co-blended spinning stoste; By described co-blended spinning stoste spinning-drawing machine by wet spinning obtained composite fibre in 40 DEG C of coagulating baths, described coagulating bath is saturated aqueous sodium sulfate;
(3) by soak at room temperature 8h in the treatment fluid in (1) of the composite fibre in (2), it is complete to take out rear 60 DEG C of dryings, mixes boundling after acetate fiber, obtains filter core fibre bundle;
(4) by the filter core fibre bundle gluing in (3), shaping, cut off, make filter core; Filter core wraps up forming paper, to obtain final product.
Test above-mentioned obtained cigarette filter, smoker's taste test shows that it is less on smoke impact, close with common filter tip; Compared with the fine filter tip of common vinegar, often prop up nicotine content in cigarette smoke and decline 59.1%, content of nitrosamines declines 44.9%, and tar content declines 16.5%.
Claims (2)
1. a hawthorn filter-tip for health-care cigarette, is characterized in that, the filter core of described cigarette filter is obtained by the raw material of following weight parts:
Acetate fiber 40-60, hawthorn 2-4, pomelo peel 2-4, cloves 1-2, lotus leaf 1-2, gelatin 1-2, polyvinyl alcohol 5-10, Tween-80 0.3-0.5, inorganic nano suspension 1-2;
Described inorganic nano suspension is obtained by the raw material of following weight parts: nano-tourmaline powder 5-10, nano aluminium oxide 3-5, softex kw 0.05-0.1, water 60-80; Softex kw is added to the water 800-1000r/min to stir 3-5min by the preparation method of described inorganic nano suspension, then adds nano-tourmaline powder and nano aluminium oxide ultrasonic disperse 10-15min, to obtain final product.
2. the preparation method of a kind of hawthorn filter-tip for health-care cigarette according to claim 1, is characterized in that, comprise the following steps:
(1) by solid-liquid weight ratio 1:20-1:30, hawthorn, pomelo peel, cloves and lotus leaf are added to the water, first decoct 1-2h, more ultrasonic process 5-10min, obtain treatment fluid after filtration;
(2) gelatin is taken by weight and polyvinyl alcohol prepares the gelatin solution of 10-12% and the poly-vinyl alcohol solution of 12-14% respectively, mix after removing impurity, add inorganic nano suspension and Tween-80 and stir 15-30min in 400-600r/min, obtaining co-blended spinning stoste; By described co-blended spinning stoste spinning-drawing machine by wet spinning obtained composite fibre in 35-40 DEG C of coagulating bath, described coagulating bath is saturated aqueous sodium sulfate;
(3) by soak at room temperature 6-8h in the treatment fluid in (1) of the composite fibre in (2), after taking out, 50-60 DEG C of drying is complete, mixes boundling after acetate fiber, obtains filter core fibre bundle;
(4) by the filter core fibre bundle gluing in (3), shaping, cut off, make filter core; Filter core wraps up forming paper, to obtain final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510349658.8A CN105011364A (en) | 2015-06-23 | 2015-06-23 | Health-care cigarette filter tip using hawthorns and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510349658.8A CN105011364A (en) | 2015-06-23 | 2015-06-23 | Health-care cigarette filter tip using hawthorns and preparation method thereof |
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| Publication Number | Publication Date |
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| CN105011364A true CN105011364A (en) | 2015-11-04 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201510349658.8A Pending CN105011364A (en) | 2015-06-23 | 2015-06-23 | Health-care cigarette filter tip using hawthorns and preparation method thereof |
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| Country | Link |
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| CN (1) | CN105011364A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106175018A (en) * | 2016-07-08 | 2016-12-07 | 华南理工大学 | A kind of degradable disponsable hair care towel and preparation method thereof |
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|---|---|---|---|---|
| US20030003140A1 (en) * | 2001-02-28 | 2003-01-02 | Efrat Biopolymers Ltd. | Absorbable solid compositions for topical treatment of oral mucosal disorders |
| CN101637307A (en) * | 2009-06-16 | 2010-02-03 | 成进学 | Cigarette fiber filter tip powerfully filtering off toxic matters and releasing microelement anions |
| CN103082399A (en) * | 2012-10-09 | 2013-05-08 | 方力 | Snuff and preparation method thereof |
| CN104437401A (en) * | 2014-11-13 | 2015-03-25 | 蚌埠德美过滤技术有限公司 | Activated carbon material having electrostatic adsorption and anion releasing effect and preparation method thereof |
| CN104432504A (en) * | 2013-09-24 | 2015-03-25 | 北京中卫神农慢性病医学研究院有限公司 | Treatment type filter tip |
-
2015
- 2015-06-23 CN CN201510349658.8A patent/CN105011364A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20030003140A1 (en) * | 2001-02-28 | 2003-01-02 | Efrat Biopolymers Ltd. | Absorbable solid compositions for topical treatment of oral mucosal disorders |
| CN101637307A (en) * | 2009-06-16 | 2010-02-03 | 成进学 | Cigarette fiber filter tip powerfully filtering off toxic matters and releasing microelement anions |
| CN103082399A (en) * | 2012-10-09 | 2013-05-08 | 方力 | Snuff and preparation method thereof |
| CN104432504A (en) * | 2013-09-24 | 2015-03-25 | 北京中卫神农慢性病医学研究院有限公司 | Treatment type filter tip |
| CN104437401A (en) * | 2014-11-13 | 2015-03-25 | 蚌埠德美过滤技术有限公司 | Activated carbon material having electrostatic adsorption and anion releasing effect and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106175018A (en) * | 2016-07-08 | 2016-12-07 | 华南理工大学 | A kind of degradable disponsable hair care towel and preparation method thereof |
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| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20151104 |
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| RJ01 | Rejection of invention patent application after publication |