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CN104970996A - Nourishing and color protecting shampoo and preparation method thereof - Google Patents

Nourishing and color protecting shampoo and preparation method thereof Download PDF

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Publication number
CN104970996A
CN104970996A CN201510339501.7A CN201510339501A CN104970996A CN 104970996 A CN104970996 A CN 104970996A CN 201510339501 A CN201510339501 A CN 201510339501A CN 104970996 A CN104970996 A CN 104970996A
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Prior art keywords
vitamin
shampoo
mixture
nourishing
extracting solution
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CN201510339501.7A
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Chinese (zh)
Inventor
吴克
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Jiangsu Qilikang Skin Pharmaceutical Co Ltd
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Jiangsu Qilikang Skin Pharmaceutical Co Ltd
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Priority to CN201510339501.7A priority Critical patent/CN104970996A/en
Publication of CN104970996A publication Critical patent/CN104970996A/en
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Abstract

The invention relates to a nourishing and color protecting shampoo and a preparation method thereof. The shampoo comprises a dendrobium extract liquid, a Chinese Gall extract liquid, a ginseng extract liquid, an antiseptic, a lavender extract liquid, vitamin B, black sesame powder, ethanol, vitamin E, ethylene glycol distearate, chitosan, deionized water, milk, a humectant and garlic oil. The preparation method comprises the following steps: weighing raw materials, mixing the dendrobium extract liquid, the Chinese Gall extract liquid, the ginseng extract liquid, the lavender extract liquid, the black sesame powder, ethanol and chitosan, stirring, adding the antiseptic, vitamin B and the humectant, and stirring to obtain a first mixture; mixing ethylene glycol distearate, milk, vitamin E and garlic oil, carrying out ultrasonic vibration to obtain a second mixture, adding the second mixture to the first mixture in a dropwise manner, heating to 40-50DEG C, and carrying out heat insulation to obtain a semi-finished product; and carrying out high pressure distillation on the semi-finished product to obtain a finished product. The shampoo can protect hair and color the hair, so the shampoo is convenient, damages to human body are reduced, and the shampoo is suitable for industrial production.

Description

A kind of nourishing color fixative shampoo and preparation method thereof
Technical field
The present invention relates to daily necessities field, be specifically related to a kind of nourishing color fixative shampoo and preparation method thereof.
Background technology
Shampoo is article of everyday use conventional in people's daily life; along with growth in the living standard, life stress is large, and the health of most people is all in sub-health state; white hair becomes younger trend clearly; although existing shampoo kind is a lot, to nourish, submissive, anti-dandruff, the shampoo of good combination property is also smaller; the hoary-headed crowd of a kind of special improvement of research and development is needed to use; both can meet nourishing scalp, and the colouring of existing hair can be given again, effectively protect the image of people.
Summary of the invention
For the deficiencies in the prior art, the object of the present invention is to provide a kind of nourishing color fixative shampoo and preparation method thereof, this shampoo nourishes scalp, and effect of color protection is good, and the dark person in middle and old age friend more by poliosis likes.
For solving prior art problem, the technical scheme that the present invention takes is:
A kind of nourishing color fixative shampoo, comprise the following raw material counted by weight: dendrobium extract 2.4-3.6 part, five Monetariamoneta (L.)(Monetariaannulus (L.)) extracting solution 5.2-6.4 parts, Radix Ginseng extractive solution 0.1-0.6 part, antiseptic 0.02-0.08 part, lavandula angustifolia extracting solution 0.08-1.15 part, vitamin B 0.01-0.05 part, Semen Sesami Nigrum powder 0.05-0.09 part, ethanol 5-20 part, vitamin E 0.08-1.25 part, stearic acid diethylene glycol dilaurate 1.5-2.6 part, chitosan 2-5 part, deionized water 30-45 part, milk 1-5 part, wetting agent 0.1-0.3 part, Oleum Bulbus Allii 0.1-0.5 part.
As above-mentioned nourishing color fixative shampoo preferably, comprise the following raw material counted by weight: dendrobium extract 2.8-3.4 part, five Monetariamoneta (L.)(Monetariaannulus (L.)) extracting solution 5.8-6.0 parts, Radix Ginseng extractive solution 0.2-0.4 part, antiseptic 0.04-0.06 part, lavandula angustifolia extracting solution 1.0-1.12 part, vitamin B 0.02-0.04 part, Semen Sesami Nigrum powder 0.06-0.07 part, ethanol 12-18 part, vitamin E 1.0-1.2 part, stearic acid diethylene glycol dilaurate 1.8-2.4 part, chitosan 3-4 part, deionized water 38-42 part, milk 2-4 part, wetting agent 0.1-0.3 part, Oleum Bulbus Allii 0.2-0.4 part.
As above-mentioned nourishing color fixative shampoo preferably, the order number of described Semen Sesami Nigrum powder is 600-800 order.
The preparation method of above-mentioned nourishing color fixative shampoo, comprises the following steps:
Step 1, take raw material, by dendrobium extract, five Monetariamoneta (L.)(Monetariaannulus (L.)) extracting solution, Radix Ginseng extractive solution, lavandula angustifolia extracting solution, Semen Sesami Nigrum powder, ethanol and chitosan mixing, the speed of 150-200rpm stirs 2-5min, add antiseptic, vitamin B and wetting agent again, 500-800rpm stirs to obtain the first mixture;
Step 2, after stearic acid diethylene glycol dilaurate, milk, vitamin E and Oleum Bulbus Allii being mixed, vibration of ultrasonic wave 10-20min, obtains the second mixture, is instilled in the first mixture by the second mixture, is incubated 10-15min and obtains semi-finished product after being heated to 40-50 DEG C;
Step 3, obtains finished product by semi-finished product high pressure distillation 5-8min.
As above-mentioned preparation method preferably, step 2, the second mixture instillation speed is that 5-10 drips/s.
As above-mentioned preparation method preferably, step 3, the pressure of high pressure distillation is 800-850MPa.
beneficial effect
The present invention nourishes color fixative shampoo and nourishes effective, and life-time service contributes to painting on hair, reduces the number of times of dyeing hair, decreases the injury of chemicals to human body.In addition, the cooperation of Herba Dendrobii and Oleum Bulbus Allii, substantially increases nourishing and the effect of color protection of shampoo, adopts dropwise mixed material in preparation process, improve the utilization rate of raw material, reduce into product cost, is applicable to large-scale production.
Detailed description of the invention
Below in conjunction with specific embodiment, technical scheme of the present invention is further described, should be appreciated that specific embodiment described herein only in order to explain the present invention, do not form restriction of the present invention.
embodiment 1
A kind of nourishing color fixative shampoo, comprises the following raw material counted by weight: dendrobium extract 2.4 parts, five Monetariamoneta (L.)(Monetariaannulus (L.)) extracting solution 5.2 parts, Radix Ginseng extractive solution 0.1 part, antiseptic 0.02 part, lavandula angustifolia extracting solution 0.08 part, vitamin B 0.01 part, 600 darkish eye black sesame powders 0.05 part, ethanol 5 parts, vitamin E 0.08 part, stearic acid diethylene glycol dilaurate 1.5 parts, chitosan 2 parts, deionized water 30 parts, 1 part, milk, wetting agent 0.1 part, Oleum Bulbus Allii 0.1 part.
The preparation method of above-mentioned nourishing color fixative shampoo, comprises the following steps:
Step 1, take raw material, by dendrobium extract, five Monetariamoneta (L.)(Monetariaannulus (L.)) extracting solution, Radix Ginseng extractive solution, lavandula angustifolia extracting solution, Semen Sesami Nigrum powder, ethanol and chitosan mixing, the speed of 150rpm stirs 2min, add antiseptic, vitamin B and wetting agent again, 500rpm stirs to obtain the first mixture;
Step 2, after stearic acid diethylene glycol dilaurate, milk, vitamin E and Oleum Bulbus Allii being mixed, vibration of ultrasonic wave 10min, obtains the second mixture, is instilled in the first mixture by the second mixture with the speed of 5/s, is incubated 10min and obtains semi-finished product after being heated to 40 DEG C;
Semi-finished product are obtained finished product at the high pressure distillation 5min of 800MPa by step 3.
embodiment 2
A kind of nourishing color fixative shampoo, comprise the following raw material counted by weight: dendrobium extract 2.8-3.4 part, five Monetariamoneta (L.)(Monetariaannulus (L.)) extracting solution 5.8-6.0 parts, Radix Ginseng extractive solution 0.2-0.4 part, antiseptic 0.04-0.06 part, lavandula angustifolia extracting solution 1.0-1.12 part, vitamin B 0.02-0.04 part, 800 darkish eye black sesame powder 0.06-0.07 parts, ethanol 12-18 part, vitamin E 1.0-1.2 part, stearic acid diethylene glycol dilaurate 1.8-2.4 part, chitosan 3-4 part, deionized water 38-42 part, milk 2-4 part, wetting agent 0.1-0.3 part, Oleum Bulbus Allii 0.2-0.4 part.
The preparation method of above-mentioned nourishing color fixative shampoo, comprises the following steps:
Step 1, take raw material, by dendrobium extract, five Monetariamoneta (L.)(Monetariaannulus (L.)) extracting solution, Radix Ginseng extractive solution, lavandula angustifolia extracting solution, Semen Sesami Nigrum powder, ethanol and chitosan mixing, the speed of 180rpm stirs 4min, add antiseptic, vitamin B and wetting agent again, 600rpm stirs to obtain the first mixture;
Step 2, after stearic acid diethylene glycol dilaurate, milk, vitamin E and Oleum Bulbus Allii being mixed, vibration of ultrasonic wave 15min, obtains the second mixture, is instilled in the first mixture by the second mixture with 8/s, is incubated 12min and obtains semi-finished product after being heated to 45 DEG C;
Step 3, obtains finished product by semi-finished product high pressure distillation 7min under 820MPa.
embodiment 3
A kind of nourishing color fixative shampoo, comprise the following raw material counted by weight: dendrobium extract 2.4-3.6 part, five Monetariamoneta (L.)(Monetariaannulus (L.)) extracting solution 5.2-6.4 parts, Radix Ginseng extractive solution 0.1-0.6 part, antiseptic 0.02-0.08 part, lavandula angustifolia extracting solution 0.08-1.15 part, vitamin B 0.01-0.05 part, 800 darkish eye black sesame powder 0.05-0.09 parts, ethanol 5-20 part, vitamin E 0.08-1.25 part, stearic acid diethylene glycol dilaurate 1.5-2.6 part, chitosan 2-5 part, deionized water 30-45 part, milk 1-5 part, wetting agent 0.1-0.3 part, Oleum Bulbus Allii 0.1-0.5 part.
The preparation method of above-mentioned nourishing color fixative shampoo, comprises the following steps:
Step 1, take raw material, by dendrobium extract, five Monetariamoneta (L.)(Monetariaannulus (L.)) extracting solution, Radix Ginseng extractive solution, lavandula angustifolia extracting solution, Semen Sesami Nigrum powder, ethanol and chitosan mixing, the speed of 200rpm stirs 5min, add antiseptic, vitamin B and wetting agent again, 800rpm stirs to obtain the first mixture;
Step 2, after stearic acid diethylene glycol dilaurate, milk, vitamin E and Oleum Bulbus Allii being mixed, vibration of ultrasonic wave 20min, obtains the second mixture, is instilled in the first mixture by the second mixture with the speed of 10/s, is incubated 15min and obtains semi-finished product after being heated to 50 DEG C;
Semi-finished product are distilled 8min and obtain finished product by step 3 under the high pressure of 850MPa.
comparative example 1
A kind of nourishing color fixative shampoo, comprise the following raw material counted by weight: five Monetariamoneta (L.)(Monetariaannulus (L.)) extracting solution 5.8-6.0 parts, Radix Ginseng extractive solution 0.2-0.4 part, antiseptic 0.04-0.06 part, lavandula angustifolia extracting solution 1.0-1.12 part, vitamin B 0.02-0.04 part, 800 darkish eye black sesame powder 0.06-0.07 parts, ethanol 12-18 part, vitamin E 1.0-1.2 part, stearic acid diethylene glycol dilaurate 1.8-2.4 part, chitosan 3-4 part, deionized water 38-42 part, milk 2-4 part, wetting agent 0.1-0.3 part, Oleum Bulbus Allii 0.2-0.4 part.
The preparation method of above-mentioned nourishing color fixative shampoo, comprises the following steps:
Step 1, takes raw material, and by five Monetariamoneta (L.)(Monetariaannulus (L.)) extracting solution, Radix Ginseng extractive solution, lavandula angustifolia extracting solution, Semen Sesami Nigrum powder, ethanol and chitosan mixing, the speed of 180rpm stirs 4min, then adds antiseptic, vitamin B and wetting agent, and 600rpm stirs to obtain the first mixture;
Step 2, after stearic acid diethylene glycol dilaurate, milk, vitamin E and Oleum Bulbus Allii being mixed, vibration of ultrasonic wave 15min, obtains the second mixture, is instilled in the first mixture by the second mixture with 8/s, is incubated 12min and obtains semi-finished product after being heated to 45 DEG C;
Step 3, obtains finished product by semi-finished product high pressure distillation 7min under 820MPa.
comparative example 2
A kind of nourishing color fixative shampoo, comprise the following raw material counted by weight: dendrobium extract 2.8-3.4 part, five Monetariamoneta (L.)(Monetariaannulus (L.)) extracting solution 5.8-6.0 parts, Radix Ginseng extractive solution 0.2-0.4 part, antiseptic 0.04-0.06 part, lavandula angustifolia extracting solution 1.0-1.12 part, vitamin B 0.02-0.04 part, 800 darkish eye black sesame powder 0.06-0.07 parts, ethanol 12-18 part, vitamin E 1.0-1.2 part, stearic acid diethylene glycol dilaurate 1.8-2.4 part, chitosan 3-4 part, deionized water 38-42 part, milk 2-4 part, wetting agent 0.1-0.3 part.
The preparation method of above-mentioned nourishing color fixative shampoo, comprises the following steps:
Step 1, take raw material, by dendrobium extract, five Monetariamoneta (L.)(Monetariaannulus (L.)) extracting solution, Radix Ginseng extractive solution, lavandula angustifolia extracting solution, Semen Sesami Nigrum powder, ethanol and chitosan mixing, the speed of 180rpm stirs 4min, add antiseptic, vitamin B and wetting agent again, 600rpm stirs to obtain the first mixture;
Step 2, after stearic acid diethylene glycol dilaurate, milk, vitamin E mixing, vibration of ultrasonic wave 15min, obtains the second mixture, is instilled in the first mixture by the second mixture with 8/s, is incubated 12min and obtains semi-finished product after being heated to 45 DEG C;
Step 3, obtains finished product by semi-finished product high pressure distillation 7min under 820MPa.
comparative example 3
A kind of nourishing color fixative shampoo, comprise the following raw material counted by weight: dendrobium extract 2.8-3.4 part, five Monetariamoneta (L.)(Monetariaannulus (L.)) extracting solution 5.8-6.0 parts, Radix Ginseng extractive solution 0.2-0.4 part, antiseptic 0.04-0.06 part, lavandula angustifolia extracting solution 1.0-1.12 part, vitamin B 0.02-0.04 part, 800 darkish eye black sesame powder 0.06-0.07 parts, ethanol 12-18 part, vitamin E 1.0-1.2 part, stearic acid diethylene glycol dilaurate 1.8-2.4 part, chitosan 3-4 part, deionized water 38-42 part, milk 2-4 part, wetting agent 0.1-0.3 part, Oleum Bulbus Allii 0.2-0.4 part.
The preparation method of above-mentioned nourishing color fixative shampoo, comprises the following steps:
Step 1, take raw material, by dendrobium extract, five Monetariamoneta (L.)(Monetariaannulus (L.)) extracting solution, Radix Ginseng extractive solution, lavandula angustifolia extracting solution, Semen Sesami Nigrum powder, ethanol and chitosan mixing, the speed of 180rpm stirs 4min, add antiseptic, vitamin B and wetting agent again, 600rpm stirs to obtain the first mixture;
Step 2, after stearic acid diethylene glycol dilaurate, milk, vitamin E and Oleum Bulbus Allii being mixed, vibration of ultrasonic wave 15min, obtains the second mixture, is poured in the first mixture by the second mixture, is incubated 12min and obtains semi-finished product after being heated to 45 DEG C;
Step 3, obtains finished product by semi-finished product high pressure distillation 7min under 820MPa.
performance test
The nourishing color fixative shampoo prepared by embodiment of the present invention 1-3 and comparative example 1-3 carries out Performance Detection, wherein, effect of color protection selects 60 white hair people as experimental subject, be divided into six groups, often group shampoo not of the same race is washed hair once, continue after six months, record result, the data obtained is as shown in the table:
From experimental data, the present invention nourishes color fixative shampoo color fixative and nourishes successful, and experimental subject continued use after six months, and alopecia phenomenon obviously reduces, and effect of color protection is good, effectively improved the image of user.In addition, the collaborative promotion of dendrobium extract and Oleum Bulbus Allii, improves the color fixative of shampoo of the present invention and nourishes effect, effectively improve raw material availability, reduce the cost of shampoo, being applicable to industrialization.
The foregoing is only the specific embodiment of the present invention; but protection scope of the present invention is not limited thereto; any those of ordinary skill in the art are in the technical scope disclosed by the present invention; the change can expected without creative work or replacement, all should be encompassed within protection scope of the present invention.Therefore, the protection domain that protection scope of the present invention should limit with claims is as the criterion.

Claims (6)

1. one kind is nourished color fixative shampoo, it is characterized in that, comprise the following raw material counted by weight: dendrobium extract 2.4-3.6 part, five Monetariamoneta (L.)(Monetariaannulus (L.)) extracting solution 5.2-6.4 parts, Radix Ginseng extractive solution 0.1-0.6 part, antiseptic 0.02-0.08 part, lavandula angustifolia extracting solution 0.08-1.15 part, vitamin B 0.01-0.05 part, Semen Sesami Nigrum powder 0.05-0.09 part, ethanol 5-20 part, vitamin E 0.08-1.25 part, stearic acid diethylene glycol dilaurate 1.5-2.6 part, chitosan 2-5 part, deionized water 30-45 part, milk 1-5 part, wetting agent 0.1-0.3 part, Oleum Bulbus Allii 0.1-0.5 part.
2. nourishing color fixative shampoo according to claim 1, it is characterized in that, comprise the following raw material counted by weight: dendrobium extract 2.8-3.4 part, five Monetariamoneta (L.)(Monetariaannulus (L.)) extracting solution 5.8-6.0 parts, Radix Ginseng extractive solution 0.2-0.4 part, antiseptic 0.04-0.06 part, lavandula angustifolia extracting solution 1.0-1.12 part, vitamin B 0.02-0.04 part, Semen Sesami Nigrum powder 0.06-0.07 part, ethanol 12-18 part, vitamin E 1.0-1.2 part, stearic acid diethylene glycol dilaurate 1.8-2.4 part, chitosan 3-4 part, deionized water 38-42 part, milk 2-4 part, wetting agent 0.1-0.3 part, Oleum Bulbus Allii 0.2-0.4 part.
3. nourishing color fixative shampoo according to claim 1, is characterized in that: the order number of described Semen Sesami Nigrum powder is 600-800 order.
4. the preparation method of nourishing color fixative shampoo according to claim 1, is characterized in that, comprise the following steps:
Step 1, take raw material, by dendrobium extract, five Monetariamoneta (L.)(Monetariaannulus (L.)) extracting solution, Radix Ginseng extractive solution, lavandula angustifolia extracting solution, Semen Sesami Nigrum powder, ethanol and chitosan mixing, the speed of 150-200rpm stirs 2-5min, add antiseptic, vitamin B and wetting agent again, 500-800rpm stirs to obtain the first mixture;
Step 2, after stearic acid diethylene glycol dilaurate, milk, vitamin E and Oleum Bulbus Allii being mixed, vibration of ultrasonic wave 10-20min, obtains the second mixture, is instilled in the first mixture by the second mixture, is incubated 10-15min and obtains semi-finished product after being heated to 40-50 DEG C;
Step 3, obtains finished product by semi-finished product high pressure distillation 5-8min.
5. the preparation method of nourishing color fixative shampoo according to claim 4, is characterized in that: step 2, and the second mixture instillation speed is that 5-10 drips/s.
6. the preparation method of nourishing color fixative shampoo according to claim 4, is characterized in that: step 3, and the pressure of high pressure distillation is 800-850MPa.
CN201510339501.7A 2015-06-18 2015-06-18 Nourishing and color protecting shampoo and preparation method thereof Pending CN104970996A (en)

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CN105748346A (en) * 2016-02-29 2016-07-13 安徽理工大学 Scurf-removing alopecia-preventing hair shampoo
CN108379184A (en) * 2018-03-26 2018-08-10 天马(安徽)国药科技股份有限公司 A kind of stem of noble dendrobium peptide tender-white repairing liquid

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105748346A (en) * 2016-02-29 2016-07-13 安徽理工大学 Scurf-removing alopecia-preventing hair shampoo
CN108379184A (en) * 2018-03-26 2018-08-10 天马(安徽)国药科技股份有限公司 A kind of stem of noble dendrobium peptide tender-white repairing liquid

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