CN104946334A - Multifunctional high-efficiency synthetic ammonia gas-making briquette dry powder adhesive and preparation method thereof - Google Patents
Multifunctional high-efficiency synthetic ammonia gas-making briquette dry powder adhesive and preparation method thereof Download PDFInfo
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- CN104946334A CN104946334A CN201510274042.9A CN201510274042A CN104946334A CN 104946334 A CN104946334 A CN 104946334A CN 201510274042 A CN201510274042 A CN 201510274042A CN 104946334 A CN104946334 A CN 104946334A
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- ammonia gas
- efficient synthesis
- synthesis ammonia
- multifunctional efficient
- molded coal
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- 238000002360 preparation method Methods 0.000 title claims abstract description 32
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 title claims abstract description 29
- 239000000843 powder Substances 0.000 title claims abstract description 19
- 239000000853 adhesive Substances 0.000 title abstract description 9
- 230000001070 adhesive effect Effects 0.000 title abstract description 9
- 239000004484 Briquette Substances 0.000 title abstract description 5
- 229910021529 ammonia Inorganic materials 0.000 title abstract 4
- 239000003245 coal Substances 0.000 claims abstract description 32
- 230000003197 catalytic effect Effects 0.000 claims abstract description 18
- 238000000034 method Methods 0.000 claims abstract description 15
- 229920002472 Starch Polymers 0.000 claims abstract description 11
- 239000005995 Aluminium silicate Substances 0.000 claims abstract description 8
- 235000012211 aluminium silicate Nutrition 0.000 claims abstract description 8
- 238000006243 chemical reaction Methods 0.000 claims abstract description 8
- ONCZQWJXONKSMM-UHFFFAOYSA-N dialuminum;disodium;oxygen(2-);silicon(4+);hydrate Chemical compound O.[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[Na+].[Na+].[Al+3].[Al+3].[Si+4].[Si+4].[Si+4].[Si+4] ONCZQWJXONKSMM-UHFFFAOYSA-N 0.000 claims abstract description 8
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims abstract description 8
- 229940080314 sodium bentonite Drugs 0.000 claims abstract description 8
- 229910000280 sodium bentonite Inorganic materials 0.000 claims abstract description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 8
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000000779 smoke Substances 0.000 claims abstract description 7
- 239000007787 solid Substances 0.000 claims abstract description 7
- 239000000203 mixture Substances 0.000 claims abstract description 4
- 238000003756 stirring Methods 0.000 claims abstract description 4
- 239000011230 binding agent Substances 0.000 claims description 34
- 230000015572 biosynthetic process Effects 0.000 claims description 21
- 238000003786 synthesis reaction Methods 0.000 claims description 21
- 239000003795 chemical substances by application Substances 0.000 claims description 15
- 230000004048 modification Effects 0.000 claims description 15
- 238000012986 modification Methods 0.000 claims description 15
- 241000196324 Embryophyta Species 0.000 claims description 12
- 239000004021 humic acid Substances 0.000 claims description 12
- 235000019890 Amylum Nutrition 0.000 claims description 9
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 9
- 239000007800 oxidant agent Substances 0.000 claims description 9
- 159000000000 sodium salts Chemical class 0.000 claims description 9
- 239000005864 Sulphur Substances 0.000 claims description 6
- FGIUAXJPYTZDNR-UHFFFAOYSA-N potassium nitrate Chemical compound [K+].[O-][N+]([O-])=O FGIUAXJPYTZDNR-UHFFFAOYSA-N 0.000 claims description 6
- 238000005516 engineering process Methods 0.000 claims description 4
- 240000003183 Manihot esculenta Species 0.000 claims description 3
- 235000016735 Manihot esculenta subsp esculenta Nutrition 0.000 claims description 3
- 241001560086 Pachyrhizus Species 0.000 claims description 3
- 240000008042 Zea mays Species 0.000 claims description 3
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 claims description 3
- 235000002017 Zea mays subsp mays Nutrition 0.000 claims description 3
- 239000002253 acid Substances 0.000 claims description 3
- 239000003513 alkali Substances 0.000 claims description 3
- 235000005822 corn Nutrition 0.000 claims description 3
- AXZAYXJCENRGIM-UHFFFAOYSA-J dipotassium;tetrabromoplatinum(2-) Chemical compound [K+].[K+].[Br-].[Br-].[Br-].[Br-].[Pt+2] AXZAYXJCENRGIM-UHFFFAOYSA-J 0.000 claims description 3
- 239000011790 ferrous sulphate Substances 0.000 claims description 3
- 235000003891 ferrous sulphate Nutrition 0.000 claims description 3
- BAUYGSIQEAFULO-UHFFFAOYSA-L iron(2+) sulfate (anhydrous) Chemical compound [Fe+2].[O-]S([O-])(=O)=O BAUYGSIQEAFULO-UHFFFAOYSA-L 0.000 claims description 3
- 229910000359 iron(II) sulfate Inorganic materials 0.000 claims description 3
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Substances [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 claims description 3
- 235000015320 potassium carbonate Nutrition 0.000 claims description 3
- VKJKEPKFPUWCAS-UHFFFAOYSA-M potassium chlorate Chemical compound [K+].[O-]Cl(=O)=O VKJKEPKFPUWCAS-UHFFFAOYSA-M 0.000 claims description 3
- 235000010333 potassium nitrate Nutrition 0.000 claims description 3
- 239000004323 potassium nitrate Substances 0.000 claims description 3
- 229910001487 potassium perchlorate Inorganic materials 0.000 claims description 3
- 239000012286 potassium permanganate Substances 0.000 claims description 3
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 3
- KKCBUQHMOMHUOY-UHFFFAOYSA-N sodium oxide Chemical compound [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 claims description 3
- 229910001948 sodium oxide Inorganic materials 0.000 claims description 3
- 239000007921 spray Substances 0.000 claims description 3
- 238000001694 spray drying Methods 0.000 claims description 3
- 238000004519 manufacturing process Methods 0.000 abstract description 11
- 230000000694 effects Effects 0.000 abstract description 4
- 239000003607 modifier Substances 0.000 abstract 3
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 abstract 2
- 239000011734 sodium Substances 0.000 abstract 2
- 229910052708 sodium Inorganic materials 0.000 abstract 2
- 235000019698 starch Nutrition 0.000 abstract 2
- 239000008107 starch Substances 0.000 abstract 2
- 238000009835 boiling Methods 0.000 abstract 1
- 238000001035 drying Methods 0.000 abstract 1
- 238000002156 mixing Methods 0.000 abstract 1
- 238000005453 pelletization Methods 0.000 abstract 1
- 238000005507 spraying Methods 0.000 abstract 1
- 239000011593 sulfur Substances 0.000 abstract 1
- 229910052717 sulfur Inorganic materials 0.000 abstract 1
- 239000003292 glue Substances 0.000 description 4
- 239000000126 substance Substances 0.000 description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 239000004927 clay Substances 0.000 description 2
- 239000003337 fertilizer Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000006004 Quartz sand Substances 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 239000004568 cement Substances 0.000 description 1
- 238000003776 cleavage reaction Methods 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 238000005034 decoration Methods 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 239000011152 fibreglass Substances 0.000 description 1
- 239000003063 flame retardant Substances 0.000 description 1
- 239000011464 hollow brick Substances 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 239000012774 insulation material Substances 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 230000007017 scission Effects 0.000 description 1
- 238000009991 scouring Methods 0.000 description 1
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- Catalysts (AREA)
- Solid Fuels And Fuel-Associated Substances (AREA)
Abstract
The invention discloses a multifunctional high-efficiency synthetic ammonia gas-making briquette dry powder adhesive and a preparation method thereof. The multifunctional high-efficiency synthetic ammonia gas-making briquette dry powder adhesive is compounded from an adhesive with reaction activity for CO2, a catalytic modifier and a solid sulfur smoke suppressor. The multifunctional high-efficiency synthetic ammonia gas-making briquette dry powder adhesive comprises the following components in percentage by mass: 30% of plant starch, 30% of sodium humate, 15% of sodium bentonite, 15% of kaolin and 10% of catalytic modifier. The method comprises the following steps: mixing multiple coals, and crushing; adding the dry powder adhesive which accounts for 5 wt% of the coal blend, wherein the dry powder adhesive comprises the following components in percentage by mass: 30% of plant starch, 30% of sodium humate, 15% of sodium bentonite, 15% of kaolin and 10% of catalytic modifier; stirring, and spraying water; and finally, pelletizing, drying and making gas. The method does not need adhesive boiling, thereby simplifying the production technique and further lowering the production cost.
Description
Technical field
The invention belongs to chemical material technical field, particularly relate to a kind of multifunctional efficient synthesis ammonia gas preparation molded coal starchy binder and preparation method thereof.
Background technology
Starchy binder is formed by rubber powder, scouring quartz sand and cement.Be single-component batching during site operation, water added and can use.Batching and constructing operation simple, and workability is good, and obviously, water-fast, weathering, durable and surperficial leakless, be applicable to the decoration of various finishing material to energy-saving effect, is also the preferably selection of hollow brick external wall made of hollow building blocks heat-preserving building.What this product adopted is heat preserving mode outside buildings, fire-retardant self-extinguishing type EPS plate is utilized to be heat-insulation material, exterior wall surface is attached to high-performance adhesive, outward coated with after the fiberglass gridding cloth with alkaline resistance properties, with a kind of heat insulation system dispersibling binding agent cover, the external wall elastic coating of high weathering is finishing systems.It has lightweight, energy-saving effect obviously, ornamental strong, the buildings of good, the facing of weathering excellent performance, water resistance and the resistance to cleavage feature such as moulding Feng Shi outward.
The lime-carbonated moulded coal of the current each small and medium chemical fertilizer widespread use of China, clay moulded coal, clear water rod type coal etc., need to boil glue, complex manufacturing, production cost is higher.
Summary of the invention
The object of the present invention is to provide a kind of multifunctional efficient synthesis ammonia gas preparation molded coal starchy binder and preparation method thereof, be intended to solve needing that existing domestic production coal starchy binder exists and boil glue, complex manufacturing, the problem that production cost is higher.
The present invention is achieved in that a kind of multifunctional efficient synthesis ammonia gas preparation molded coal starchy binder, and this multifunctional efficient synthesis ammonia gas preparation molded coal starchy binder adopts CO
2the binding agent of reactive behavior, catalytic modification agent, solid sulphur smoke suppressor three major types be composited; Comprise according to mass percent: 30% plant amylum, 30% Sodium salts humic acids, 15% sodium bentonite, 15% kaolin, 10% catalytic modification agent.
Further, described 30% plant amylum makes 200 object fine powders by cassava, pachyrhizus, corn through complicated technology, then through soda acid pasting technique technique, makes the instant mixed plant powder with very strong cohesive property.
Further, described 30% humic acids is by the former powder of humic acidss more than content >=50, and through alkali reaction, pH value is at 10-11, and temperature of reaction, at 95 DEG C, is reacted 1 hour, then through obtaining Sodium salts humic acids fine powder from core spray-drying tower at a high speed.
Further, described catalytic modification agent is made up of ignition dope and mixed type strong oxidizer, according to mass percent is:
Catalytic modification agent=40% ignition dope+60% mixed type strong oxidizer.
Further, described ignition dope is made up of sodium oxide, and described mixed type strong oxidizer is made up of 25% potassium permanganate+25% saltpetre+25% Potcrate+25% potassium perchlorate according to mass percent.
Further, described solid sulphur smoke suppressor is made up of 40% salt of wormwood+40% sodium carbonate+20% ferrous sulfate according to mass percent.
Another object of the present invention is to the preparation method providing a kind of multifunctional efficient synthesis ammonia gas preparation molded coal starchy binder, the preparation method of this multifunctional efficient synthesis ammonia gas preparation molded coal starchy binder comprises the following steps:
Step one, mixes multiple coal, does break process;
Step 2, add the starchy binder accounting for Mixture Density Networks quality 5%, starchy binder comprises according to mass percent: then 30% plant amylum, 30% Sodium salts humic acids, 15% sodium bentonite, 15% kaolin, 10% catalytic modification agent stir and spray water;
Step 3, finally carries out, pressure ball, oven dry and gas making.
Method of the present invention does not need to boil glue, and production technique simplifies, and reduce further production cost.
Accompanying drawing explanation
Fig. 1 is preparation method's schema of the multifunctional efficient synthesis ammonia gas preparation molded coal starchy binder that the embodiment of the present invention provides.
Embodiment
In order to make object of the present invention, technical scheme and advantage clearly understand, below in conjunction with embodiment, the present invention is further elaborated.Should be appreciated that specific embodiment described herein only in order to explain the present invention, be not intended to limit the present invention.
Below in conjunction with drawings and the specific embodiments, application principle of the present invention is further described.
The present invention is multifunctional efficient synthesis ammonia gas preparation molded coal starchy binder, it is the additive by three kinds of effects, through having the briquette binder of the features such as novel, multi-functional, efficient composite, substitute the lime-carbonated moulded coal of the current each small and medium chemical fertilizer widespread use of China, clay moulded coal, clear water rod type coal etc., art does not need to boil glue, production technique simplifies, and production cost declines further.
A kind of multifunctional efficient synthesis ammonia gas preparation molded coal starchy binder of the embodiment of the present invention, this multifunctional efficient synthesis ammonia gas preparation molded coal starchy binder adopts CO
2the binding agent of reactive behavior, catalytic modification agent, solid sulphur smoke suppressor three major types be composited; Comprise according to mass percent: 30% plant amylum, 30% Sodium salts humic acids, 15% sodium bentonite, 15% kaolin, 10% catalytic modification agent.
Further, described 30% plant amylum makes 200 object fine powders by cassava, pachyrhizus, corn through complicated technology, then through soda acid pasting technique technique, makes the instant mixed plant powder with very strong cohesive property.
Described 30% humic acids is by the former powder of humic acidss more than content >=50, and through alkali reaction, pH value is at 10-11, and temperature of reaction, at 95 DEG C, is reacted 1 hour, then through obtaining Sodium salts humic acids fine powder from core spray-drying tower at a high speed.
Further, described catalytic modification agent is made up of ignition dope and mixed type strong oxidizer, according to mass percent is:
Catalytic modification agent=40% ignition dope+60% mixed type strong oxidizer.
Further, described ignition dope is made up of sodium oxide, and described mixed type strong oxidizer is made up of 25% potassium permanganate+25% saltpetre+25% Potcrate+25% potassium perchlorate according to mass percent.
Further, described solid sulphur smoke suppressor is made up of 40% salt of wormwood+40% sodium carbonate+20% ferrous sulfate according to mass percent.
As shown in Figure 1, the preparation method of the multifunctional efficient synthesis ammonia gas preparation molded coal starchy binder of the embodiment of the present invention comprises the following steps:
S101: multiple coal is mixed, does break process;
S102: add the starchy binder accounting for Mixture Density Networks quality 5%, starchy binder comprises according to mass percent: then 30% plant amylum, 30% Sodium salts humic acids, 15% sodium bentonite, 15% kaolin, 10% catalytic modification agent stir and spray water;
S103: finally carry out, pressure ball, oven dry and gas making.
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, all any amendments done within the spirit and principles in the present invention, equivalent replacement and improvement etc., all should be included within protection scope of the present invention.
Claims (7)
1. a multifunctional efficient synthesis ammonia gas preparation molded coal starchy binder, is characterized in that, this multifunctional efficient synthesis ammonia gas preparation molded coal starchy binder adopts CO
2the binding agent of reactive behavior, catalytic modification agent, solid sulphur smoke suppressor three major types be composited; Comprise according to mass percent: 30% plant amylum, 30% Sodium salts humic acids, 15% sodium bentonite, 15% kaolin, 10% catalytic modification agent.
2. multifunctional efficient synthesis ammonia gas preparation molded coal starchy binder as claimed in claim 1, it is characterized in that, described 30% plant amylum makes 200 object fine powders by cassava, pachyrhizus, corn through complicated technology, then through soda acid pasting technique technique, makes close-burning instant mixed plant powder.
3. multifunctional efficient synthesis ammonia gas preparation molded coal starchy binder as claimed in claim 1, it is characterized in that, described 30% humic acids is by the former powder of humic acidss more than content >=50, through alkali reaction, pH value is at 10-11, temperature of reaction 95, DEG C reaction 1 hour, then through at a high speed obtaining Sodium salts humic acids fine powder from core spray-drying tower.
4. multifunctional efficient synthesis ammonia gas preparation molded coal starchy binder as claimed in claim 1, it is characterized in that, described catalytic modification agent is made up of ignition dope and mixed type strong oxidizer, according to mass percent is:
Catalytic modification agent=40% ignition dope+60% mixed type strong oxidizer.
5. multifunctional efficient synthesis ammonia gas preparation molded coal starchy binder as claimed in claim 4, it is characterized in that, described ignition dope is made up of sodium oxide, and described mixed type strong oxidizer is made up of 25% potassium permanganate+25% saltpetre+25% Potcrate+25% potassium perchlorate according to mass percent.
6. multifunctional efficient synthesis ammonia gas preparation molded coal starchy binder as claimed in claim 1, is characterized in that, described solid sulphur smoke suppressor is made up of 40% salt of wormwood+40% sodium carbonate+20% ferrous sulfate according to mass percent.
7. a preparation method for multifunctional efficient synthesis ammonia gas preparation molded coal starchy binder, is characterized in that, the preparation method of this multifunctional efficient synthesis ammonia gas preparation molded coal starchy binder comprises the following steps:
Step one, mixes multiple coal, does break process;
Step 2, add the starchy binder accounting for Mixture Density Networks quality 5%, starchy binder comprises according to mass percent: then 30% plant amylum, 30% Sodium salts humic acids, 15% sodium bentonite, 15% kaolin, 10% catalytic modification agent stir and spray water;
Step 3, finally carries out, pressure ball, oven dry and gas making.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510274042.9A CN104946334A (en) | 2015-05-26 | 2015-05-26 | Multifunctional high-efficiency synthetic ammonia gas-making briquette dry powder adhesive and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510274042.9A CN104946334A (en) | 2015-05-26 | 2015-05-26 | Multifunctional high-efficiency synthetic ammonia gas-making briquette dry powder adhesive and preparation method thereof |
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| Publication Number | Publication Date |
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| CN104946334A true CN104946334A (en) | 2015-09-30 |
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| CN201510274042.9A Withdrawn CN104946334A (en) | 2015-05-26 | 2015-05-26 | Multifunctional high-efficiency synthetic ammonia gas-making briquette dry powder adhesive and preparation method thereof |
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| Country | Link |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115197761A (en) * | 2022-06-28 | 2022-10-18 | 福建坤净生环保科技有限公司 | Sludge granulation heat-increasing combustion multi-functional drying-free powder binder |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1043521A (en) * | 1988-12-22 | 1990-07-04 | 中国科学院山西煤炭化学研究所 | The preparation method of moulded coal |
| CN1102201A (en) * | 1993-11-01 | 1995-05-03 | 煤炭科学研究总院合肥研究所 | Method for making gas-forming briquette coal by using powdered coal |
| CN101798538A (en) * | 2010-03-08 | 2010-08-11 | 柳州化工股份有限公司 | Coupling compound moulded coal binder and preparation method thereof |
| CN101077986B (en) * | 2006-05-25 | 2010-11-03 | 林鼎华 | Multifunctional and highly effective synthesis ammonia gas preparation molded coal cementing agent |
| KR101464917B1 (en) * | 2014-05-13 | 2014-11-26 | 한국에너지기술연구원 | Hydrophobic coal-biomass granule type mixed fuel, apparatus and manufacturing method thereof |
-
2015
- 2015-05-26 CN CN201510274042.9A patent/CN104946334A/en not_active Withdrawn
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1043521A (en) * | 1988-12-22 | 1990-07-04 | 中国科学院山西煤炭化学研究所 | The preparation method of moulded coal |
| CN1102201A (en) * | 1993-11-01 | 1995-05-03 | 煤炭科学研究总院合肥研究所 | Method for making gas-forming briquette coal by using powdered coal |
| CN101077986B (en) * | 2006-05-25 | 2010-11-03 | 林鼎华 | Multifunctional and highly effective synthesis ammonia gas preparation molded coal cementing agent |
| CN101798538A (en) * | 2010-03-08 | 2010-08-11 | 柳州化工股份有限公司 | Coupling compound moulded coal binder and preparation method thereof |
| KR101464917B1 (en) * | 2014-05-13 | 2014-11-26 | 한국에너지기술연구원 | Hydrophobic coal-biomass granule type mixed fuel, apparatus and manufacturing method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115197761A (en) * | 2022-06-28 | 2022-10-18 | 福建坤净生环保科技有限公司 | Sludge granulation heat-increasing combustion multi-functional drying-free powder binder |
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Application publication date: 20150930 |
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