CN104928141A - Preparation method of lycium ruthenicum honey fruit wine - Google Patents
Preparation method of lycium ruthenicum honey fruit wine Download PDFInfo
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- CN104928141A CN104928141A CN201510420649.3A CN201510420649A CN104928141A CN 104928141 A CN104928141 A CN 104928141A CN 201510420649 A CN201510420649 A CN 201510420649A CN 104928141 A CN104928141 A CN 104928141A
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- 238000002360 preparation method Methods 0.000 title claims description 7
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Classifications
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- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12G—WINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
- C12G3/00—Preparation of other alcoholic beverages
- C12G3/04—Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs
- C12G3/06—Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs with flavouring ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/25—Araliaceae (Ginseng family), e.g. ivy, aralia, schefflera or tetrapanax
- A61K36/258—Panax (ginseng)
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
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- A—HUMAN NECESSITIES
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/72—Rhamnaceae (Buckthorn family), e.g. buckthorn, chewstick or umbrella-tree
- A61K36/725—Ziziphus, e.g. jujube
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- A—HUMAN NECESSITIES
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- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/73—Rosaceae (Rose family), e.g. strawberry, chokeberry, blackberry, pear or firethorn
- A61K36/734—Crataegus (hawthorn)
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/73—Rosaceae (Rose family), e.g. strawberry, chokeberry, blackberry, pear or firethorn
- A61K36/738—Rosa (rose)
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- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12G—WINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
- C12G3/00—Preparation of other alcoholic beverages
- C12G3/02—Preparation of other alcoholic beverages by fermentation
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Abstract
本发明公开了一种黑果枸杞蜂蜜果酒的制备方法,旨在提供一种具有滋养气血、减缓衰老、美容养颜之功效的果酒的制备方法。将党参蜂蜜和黄芪蜂蜜混匀,加活性炭吸附;将混合蜂蜜稀释,通过薄膜过滤器;滤液通过真空薄膜离心式蒸发器;将黑果枸杞榨汁加入果胶酶酶解;离心过滤;将所得的澄清液中加入混合蜂蜜搅拌均匀;将红枸杞和沙棘打浆混合;将黑果枸杞果渣果皮及沙棘与红枸杞混合浆液加入混合蜂蜜,加热灭菌,调节pH值;将混合液加入SO2及高糖酵母发酵;将酒液倒罐陈酿;将甘草、玫瑰、山楂、酸枣核、甜叶菊和西洋参加入发酵酒中震荡提取;将蜂蜜与黑果枸杞酶解液的混合液及浸提酒液混合调配,调整酸糖比,过滤灭菌,充氮包装,得到成品。The invention discloses a method for preparing fruit wine with black fruit wolfberry honey, and aims to provide a method for preparing fruit wine with the functions of nourishing qi and blood, slowing down aging, and beautifying and beautifying the skin. Mix Codonopsis honey and Astragalus honey, add activated carbon for adsorption; dilute the mixed honey, pass through a membrane filter; Add mixed honey to the clarified solution and stir evenly; beat red wolfberry and seabuckthorn; add black wolfberry pomace peel and seabuckthorn and red wolfberry mixed slurry into mixed honey, heat and sterilize, adjust pH value; add SO 2 to the mixture and high-sugar yeast fermentation; pour the wine into a tank for aging; add licorice, rose, hawthorn, jujube seed, stevia and American ginseng into the fermented wine and shake to extract; mix honey and black fruit wolfberry enzymatic hydrolysis solution and extract wine The liquid is mixed and prepared, the acid-sugar ratio is adjusted, filtered and sterilized, packed with nitrogen, and the finished product is obtained.
Description
技术领域technical field
本发明涉及饮料制造技术领域,特别是涉及一种黑果枸杞蜂蜜果酒的制备方法。The invention relates to the technical field of beverage production, in particular to a method for preparing black wolfberry honey wine.
背景技术Background technique
果酒是利用新鲜水果为原料,在保存水果原有营养成分的情况下,利用自然发酵或人工添加酵母菌来分解糖分而制造出的具有保健、营养型酒。果酒以其独特的风味及色泽,成为新的消费时尚。Fruit wine is a healthy and nutritious wine produced by using fresh fruits as raw materials, and using natural fermentation or artificially adding yeast to decompose sugar while preserving the original nutrients of the fruits. With its unique flavor and color, fruit wine has become a new consumption fashion.
果酒清亮透明、酸甜适口、醇厚纯净而无异味,具有原果实特有的芳香,与白酒、啤酒等其他酒类相比,果酒的营养价值更高,果酒里含有大量的多酚,可以起到抑制脂肪在人体中堆积的作用,它含有人体所需多种氨基酸和维生素B1、B2、维生素C及铁、钾、镁、锌等矿物元素,果酒中虽然含有酒精,但含量与白酒和葡萄酒比起来非常低,一般为5到10度,最高的也只有14度,适当饮用果酒对健康是有好处的。Fruit wine is clear and transparent, sweet and sour, mellow and pure without peculiar smell. It has the unique aroma of the original fruit. Compared with liquor, beer and other alcohols, fruit wine has higher nutritional value. Inhibit the accumulation of fat in the human body, it contains a variety of amino acids needed by the human body, vitamin B 1 , B 2 , vitamin C and mineral elements such as iron, potassium, magnesium, zinc, etc. Although fruit wine contains alcohol, its content is similar to that of white wine and Compared with wine, it is very low, generally 5 to 10 degrees, and the highest is only 14 degrees. Proper drinking of fruit wine is good for health.
蜂蜜酒有近3000年的文化底蕴,加之酒体具有营养健身、滋补强体、保健美容、延缓衰老的特征,越来越受到众多消费者的青睐。当今饮酒低度化、健康化的趋势与蜂蜜酒天然、绿色、健康的特点融为一体,为此种酒赢得众多消费人群释放了更大的空间。在老年人中饮酒者所占的比例较大。但是面对他们生理变化中器官功能减退和新陈代谢能力逐渐降低的客观现实,适量饮用低度酒,可和血行气、壮神御寒,颇有益处。每每细品小酢,不但使人神怡气舒,还能增加胃液分泌,促进食物的消化吸收,又可扩张小血管改善血液循环。Honey wine has nearly 3,000 years of cultural heritage, and the wine body has the characteristics of nutrition and fitness, nourishing and strengthening, health care and beauty, and delaying aging, so it is more and more favored by many consumers. Today's low-alcohol and healthy drinking trend is integrated with the natural, green and healthy characteristics of mead, which releases more space for this kind of wine to win many consumers. Among the elderly, the proportion of alcohol drinkers is relatively large. However, in the face of the objective reality of their organ dysfunction and metabolic capacity gradually decreasing during their physiological changes, moderate drinking of low-alcohol alcohol can harmonize blood and promote qi, strengthen the spirit and keep out the cold, which is quite beneficial. Every time you taste small vinegar, it not only makes you feel refreshed, but also increases the secretion of gastric juice, promotes the digestion and absorption of food, and expands small blood vessels to improve blood circulation.
目前市面上的发酵型果酒一般采用单一果汁发酵,补充糖分带皮发酵等方式进行相关生产。在发酵过程中,花青素等还原性成分易被氧化。在丧失还原性成分功能性的同时产生不良的气味与色泽,使产品品质收到极大影响。而且蜂蜜酒的种类单一,无法满足市场的多样化需求。At present, the fermented fruit wines on the market are generally produced by single fruit juice fermentation, supplemented with sugar and fermentation with skin. During the fermentation process, reducing components such as anthocyanins are easily oxidized. While losing the functionality of the reducing ingredients, it produces bad smell and color, which greatly affects the product quality. And the kind of mead is single, can't satisfy the diversified demand of market.
发明内容Contents of the invention
本发明的目的是针对现有技术中存在的技术缺陷,而提供一种具有滋养气血、减缓衰老、美容养颜之功效的黑果枸杞蜂蜜果酒的制备方法。The object of the present invention is to aim at the technical defects existing in the prior art, and provide a kind of preparation method of the black fruit wolfberry honey fruit wine with the effect of nourishing qi and blood, slowing down aging, beautifying and beautifying skin.
为实现本发明的目的所采用的技术方案是:The technical scheme adopted for realizing the purpose of the present invention is:
一种黑果枸杞蜂蜜果酒的制备方法,包括如下步骤:A preparation method of black fruit wolfberry honey wine, comprising the steps of:
(1)将党参蜂蜜和黄芪蜂蜜分别加热到40-50℃,在密封设备内趁热过滤,去除杂质及死蜂;(1) Heat Codonopsis honey and Astragalus honey to 40-50°C respectively, and filter while hot in a sealed device to remove impurities and dead bees;
(2)将步骤(1)得到的党参蜂蜜和黄芪蜂蜜按照重量比1:1-1:5混合均匀,并保持40-50℃;加入1-3%活性炭均匀混合,吸附0.5-3h,除去蜂蜜中的不良气味,再经过滤除去活性炭颗粒;(2) Mix Codonopsis honey and Astragalus honey obtained in step (1) evenly according to the weight ratio of 1:1-1:5, and keep at 40-50°C; add 1-3% activated carbon to mix evenly, adsorb for 0.5-3h, remove Bad smell in honey, and then filter to remove activated carbon particles;
(3)将步骤(2)得到的混合蜂蜜稀释20-30倍,通过0.45-0.65μm薄膜过滤器;所得滤液再通过真空薄膜离心式蒸发器,其中,真空薄膜离心式蒸发器的真空度为-0.095~-0.092MPa,转速为300r/min,温度为50-60℃,控制所得混合蜂蜜的含水量为15-18%;(3) the mixed honey that step (2) obtains is diluted 20-30 times, by 0.45-0.65 μ m film filter; -0.095~-0.092MPa, the rotating speed is 300r/min, the temperature is 50-60°C, and the water content of the obtained mixed honey is controlled to be 15-18%;
(4)将新鲜的黑果枸杞榨汁,之后加入果胶酶酶解,其中,所述果胶酶的添加量为1%,酶解温度为40℃,酶解时间为1-2h;所得酶解液于4℃、转速为1500r/min的条件下离心过滤,离心后的过滤液于4℃下通过0.45-0.65μm薄膜过滤器,澄清液4℃下密封避光备用,果皮果渣备用;(4) Squeeze fresh black wolfberry juice, and then add pectinase for enzymolysis, wherein the added amount of pectinase is 1%, the enzymolysis temperature is 40°C, and the enzymolysis time is 1-2h; the obtained Centrifuge and filter the enzymolysis solution at 4°C and 1500r/min, the filtrate after centrifugation passes through a 0.45-0.65μm membrane filter at 4°C, seal the clarified liquid at 4°C and keep it away from light for later use, and the peel and pomace for later use ;
(5)将步骤(4)所得的澄清液中加入步骤(3)所得的含水量为15-17%的混合蜂蜜搅拌均匀得到混合液,澄清液与混合蜂蜜的重量比为1:1-1:5,控制混合液的含水量为20-23%,4℃下密封避光保存;(5) Add the mixed honey with a water content of 15-17% obtained in step (3) to the clarified liquid obtained in step (4) and stir evenly to obtain a mixed liquid. The weight ratio of the clarified liquid to the mixed honey is 1:1-1 :5, the water content of the control mixture is 20-23%, and it is sealed and protected from light at 4°C;
(6)将新鲜红枸杞和沙棘打浆,按照重量比为1:1-5:1的比例混合,4℃下密封储存;(6) Fresh red wolfberry and seabuckthorn are beaten, mixed according to the ratio of 1:1-5:1 by weight, and sealed and stored at 4°C;
(7)将步骤(4)中产生的黑果枸杞果渣果皮及步骤(6)中的沙棘与红枸杞混合浆液加入步骤(3)中的混合蜂蜜,加水混合,加热至85℃,30min灭菌,柠檬酸调节pH值为3.5-4.0;其中,黑果枸杞果渣果皮:沙棘与红枸杞混合浆液:混合蜂蜜为1:1:4,通过加水控制所得混合液的含糖量为20-25%;(7) Add the black wolfberry pomace peel produced in step (4) and the mixed slurry of seabuckthorn and red wolfberry in step (6) to the mixed honey in step (3), add water to mix, heat to 85°C, and extinguish for 30 minutes bacterium, citric acid to adjust the pH value to 3.5-4.0; wherein, black fruit pomace fruit peel: seabuckthorn and red wolfberry mixed slurry: mixed honey is 1:1:4, and the sugar content of the mixed solution obtained by adding water is controlled to be 20- 25%;
(8)将步骤(7)所得混合液加入到发酵罐中,加入SO2及高糖酵母,SO2的加入量为0.3g/L,高糖酵母的接种量为5-9%,发酵温度为25-28℃,时间为5-8d;(8) Step (7) gained mixed solution is joined in fermenter, adds SO2 and high sugar yeast, SO Add-on is 0.3g/L, and the inoculum size of high sugar yeast is 5-9%, and fermentation temperature is 25 -28℃, the time is 5-8d;
(9)将步骤(8)得到的酒液倒罐陈酿90d,发酵结束,静置沉淀,取上清液经过0.35-0.45μm的薄膜过滤器过滤,换至储酒罐中储存,储存温度为8-13℃,湿度为80-90%;(9) pour the wine liquid obtained in step (8) into a tank and age for 90 days. After the fermentation is over, let it stand for precipitation, take the supernatant and filter it through a 0.35-0.45 μm membrane filter, and then store it in a wine storage tank. The storage temperature is 8-13℃, humidity 80-90%;
(10)将适量甘草、玫瑰、山楂、酸枣核、甜叶菊和西洋参干燥后,分别粉碎筛分;其中甘草、红枸杞、玫瑰、山楂、酸枣核和西洋参为80-150目,甜叶菊40-60目,储存备用;(10) After drying appropriate amount of licorice, rose, hawthorn, jujube seed, stevia and American ginseng, crush and sieve them respectively; among them, licorice, red wolfberry, rose, hawthorn, wild jujube seed and American ginseng are 80-150 mesh, and stevia is 40- 60 mesh, stored for future use;
(11)将步骤(10)的组分按比例加入到步骤(9)所得到的发酵酒中震荡提取24h,料液比为1:10,温度为35℃,提取液离心15min,取上清液经过0.35-0.45μm薄膜过滤器过滤,滤液为浸提酒液密封避光保存;(11) Add the components of step (10) in proportion to the fermented wine obtained in step (9) and extract by shaking for 24 hours, the ratio of solid to liquid is 1:10, the temperature is 35°C, the extract is centrifuged for 15 minutes, and the supernatant is taken The liquid is filtered through a 0.35-0.45 μm membrane filter, and the filtrate is the extraction wine liquid, sealed and protected from light;
(12)将步骤(5)中蜂蜜与黑果枸杞酶解液的混合液及步骤(11)所得的浸提酒液混合调配,加入0.01-1.5%的茶多酚,加入柠檬酸和白砂糖调整酸糖比,使用0.35-0.45μm的薄膜过滤器进行膜过滤,滤液灭菌,充氮包装,得到黑果枸杞蜂蜜果酒成品。(12) Mix the mixture of honey and wolfberry enzymatic hydrolysis solution in step (5) and the extraction liquor obtained in step (11), add 0.01-1.5% tea polyphenols, add citric acid and white sugar Adjust the acid-sugar ratio, use a 0.35-0.45 μm membrane filter for membrane filtration, sterilize the filtrate, pack with nitrogen filling, and obtain the finished product of black wolfberry honey wine.
与现有技术相比,本发明的有益效果是:Compared with prior art, the beneficial effect of the present invention is:
1、本发明的果酒采用多种天然植物为原料制备而成,配方中,黑果枸杞含有丰富的原花青素、花青素,这些物质都具有抗氧化、清除自由基等功效,对于抗衰老、美容养颜有良好的效果。红枸杞具有滋补肝肾、益精明目、抗衰老、调节免疫力等功效。玫瑰中含有300多种化学成份,如芳香的醇、醛、脂肪酸、酚和含香精的油和脂,常食玫瑰制品中以柔肝醒胃,舒气活血,美容养颜,令人神爽。山楂,消食健胃,行气散瘀,化浊降脂。酸枣核能够宁心安神、养肝、敛汗。甜叶菊可以减肥养颜、养阴生津、帮助消化,促进胰腺、脾胃功能和清热解毒。古语云:“西洋参性凉而补,凡欲用人参而不受人参之温者皆可用之”。故补而不燥是西洋参的特别之处。甘草,中医认为甘草有益气补中、调和诸药的功效,是中药中的“国老”,是最常用的中药药材之一,大部分中药药方都搭配了甘草,特别是由于其甜味能盖过其他药材的苦辛味。黄芪蜂蜜和党参蜂蜜其除有蜂蜜之特性外,更益于补中、益气生津,对胃肠滞纳难受、脾胃虚弱、气血两亏有辅助疗效。以上药食同源组分之间相互配伍,能够起到美容养颜,滋养气血之功效。1. The fruit wine of the present invention is prepared from a variety of natural plants. In the formula, Lycium barbarum is rich in proanthocyanidins and anthocyanins. These substances have the effects of anti-oxidation and scavenging free radicals. Beauty has a good effect. Red wolfberry has the functions of nourishing liver and kidney, improving eyesight, anti-aging, and regulating immunity. Roses contain more than 300 kinds of chemical components, such as aromatic alcohols, aldehydes, fatty acids, phenols, and essential oils and fats. Rose products are often eaten to soften the liver and refresh the stomach, soothe qi and activate blood circulation, beautify the skin, and make people feel refreshed. Hawthorn, digestion and invigorating the stomach, promoting qi and dispelling blood stasis, reducing turbidity and reducing fat. Jujube seed can calm the mind, nourish the liver, and suppress sweat. Stevia can lose weight and beautify, nourish yin and promote body fluid, help digestion, promote pancreas, spleen and stomach functions, and clear away heat and detoxify. An old saying goes: "American ginseng is cool in nature and nourishing. Anyone who wants to use ginseng without the warmth of ginseng can use it." Therefore, nourishing but not drying is the special feature of American ginseng. Licorice, traditional Chinese medicine believes that licorice is good for Qi, nourishing the middle, and harmonizing the effects of various medicines. Overwhelms the bitterness of other herbs. Astragalus honey and Codonopsis honey not only have the properties of honey, but also benefit the vital energy and promote fluid production, and have auxiliary effects on gastrointestinal stagnation, weak spleen and stomach, and deficiency of both Qi and blood. The compatibility between the above medicinal and food homologous components can play the role of beautifying and nourishing the skin and nourishing qi and blood.
2.本发明的黑果枸杞蜂蜜果酒的制备方法,针对不同的有效成分采取不同的加工工艺和条件,使有效成分完全被得到利用;整个加工过程中采用膜过滤灭菌技术,保留热敏性、功能性成分;在灌装时又采用真空充氮密封包装,隔绝氧气使芳香气味不至于随时间而散失,并且对于其中原花青素、花青素等还原性强的有效成分得到最佳的保护。2. The preparation method of black fruit wolfberry honey wine of the present invention adopts different processing techniques and conditions for different active ingredients, so that the active ingredients can be fully utilized; membrane filtration sterilization technology is adopted in the whole processing process to retain heat sensitivity and function Non-toxic ingredients; when filling, vacuum nitrogen-filled sealed packaging is used to isolate oxygen so that the aroma will not be lost over time, and the active ingredients with strong reducibility such as proanthocyanidins and anthocyanins are best protected.
具体实施方式Detailed ways
以下结合具体实施例对本发明作进一步详细说明。The present invention will be described in further detail below in conjunction with specific examples.
实施例1Example 1
(1)党参蜂蜜15kg、黄芪蜂蜜15kg分别加热至45℃,在密封设备内趁热采用孔径为100目的尼龙网过滤,滤去杂质、死蜂等物质。(1) 15kg of Codonopsis honey and 15kg of Astragalus honey were heated to 45°C respectively, and filtered while hot in a sealed device with a nylon mesh with a pore size of 100 mesh to remove impurities, dead bees and other substances.
(2)将步骤(1)中的党参蜂蜜和黄芪蜂蜜混合均匀,并保持45℃。加入3%的活性炭均匀混合,吸附2h,除去蜂蜜中的不良气味,经过滤除去活性炭颗粒。(2) Mix Codonopsis honey and Astragalus honey in step (1) evenly, and keep at 45°C. Add 3% activated carbon and mix evenly, absorb for 2h, remove bad smell in honey, remove activated carbon particles by filtration.
(3)将步骤(2)得到的混合蜂蜜稀释30倍,通过0.45μm的薄膜过滤器。所得滤液再通过真空薄膜离心式蒸发器,真空度为-0.095MPa,转速为300r/min,温度为50℃,控制所得混合蜂蜜的含水量15%。(3) Dilute the mixed honey obtained in step (2) 30 times, and pass through a 0.45 μm membrane filter. The obtained filtrate passes through a vacuum film centrifugal evaporator again, the vacuum degree is -0.095MPa, the rotating speed is 300r/min, the temperature is 50°C, and the water content of the obtained mixed honey is controlled to 15%.
(4)将新鲜的黑果枸杞经过挑选,称取15kg,清洗,榨汁,加入果胶酶进行酶解,果胶酶的添加量为1%,酶解温度为40℃,酶解时间为1.5h,之后,于4℃、转速为1500r/min的条件下离心过滤,此温度下再通过0.45μm的薄膜过滤器,澄清液低温(4℃)密封避光备用,果皮果渣低温(4℃)储存备用。(4) Fresh black wolfberry is selected, weighed 15kg, cleaned, squeezed the juice, added pectinase to carry out enzymolysis, the addition of pectinase is 1%, the enzymolysis temperature is 40 ℃, and the enzymolysis time is After 1.5h, centrifuge and filter at 4°C and a rotating speed of 1500r/min, then pass through a 0.45μm membrane filter at this temperature, seal the clarified liquid at low temperature (4°C) and keep it away from light for later use. ℃) for storage.
(5)取步骤(4)所得的澄清液7.5kg加入步骤(3)所得的混合蜂蜜10kg搅拌均匀,控制所得混合液的含水量为20%,低温密封避光保存(4℃)。(5) Get 7.5kg of clarified liquid of step (4) gained and add the mixed honey 10kg of step (3) gained and stir evenly, control the water content of gained mixed liquid to be 20%, low-temperature sealed dark preservation (4 ℃).
(6)挑选干净、完好的红枸杞、沙棘,称取3.5kg红枸杞,1.5kg沙棘果,分别将其打浆、混合,低温密封储存(4℃)。(6) Select clean and intact red wolfberry and seabuckthorn, weigh 3.5kg red wolfberry and 1.5kg seabuckthorn fruit, beat and mix them respectively, and store them in a sealed seal at low temperature (4°C).
(7)将步骤(4)所得的黑果枸杞果渣果皮、步骤(6)所得的沙棘与红枸杞混合浆液加入步骤(3)所得的混合蜂蜜20kg,加水混合,加热至85℃,30min灭菌,柠檬酸调节pH值为3.7。其中,按照重量比,黑果枸杞果渣果皮:沙棘与红枸杞混合浆液:混合蜂蜜为1:1:4,通过加水量控制混合液中含糖量为25%。(7) Add 20 kg of mixed honey obtained in step (3) to the black fruit pomace peel of wolfberry obtained in step (4), the mixed slurry of seabuckthorn and red wolfberry obtained in step (6), add water to mix, heat to 85 ° C, and extinguish for 30 minutes Bacteria, adjusted to pH 3.7 with citric acid. Wherein, according to the weight ratio, the ratio of black wolfberry pomace peel: seabuckthorn and red wolfberry mixed slurry: mixed honey is 1:1:4, and the sugar content in the mixed solution is controlled to be 25% by adding water.
(8)将步骤(7)所得的混合液加入发酵罐中,加入SO2和高糖酵母发酵,其中,SO2的加入量为0.3g/L,高糖酵母接种量7%,发酵温度26℃,时间6d。(8) Add the mixed solution of step (7) gained in the fermenter, add SO 2 and high sugar yeast fermentation, wherein, the addition of SO 2 is 0.3g/L, the high sugar yeast inoculum is 7%, and the fermentation temperature is 26 ℃, time 6d.
(9)将步骤(8)中酒液倒灌陈酿90d。发酵结束,静置沉淀,取上清液经过0.45μm薄膜过滤器过滤,换至储酒罐中储存,储存温度为8℃,湿度80%。(9) pouring the liquor in the step (8) back and aging for 90 days. After the fermentation is over, let it stand for precipitation, take the supernatant and filter it through a 0.45 μm membrane filter, and then store it in a wine storage tank at a temperature of 8°C and a humidity of 80%.
(10)将甘草、玫瑰、山楂、酸枣核、甜叶菊和西洋参常规干燥后,按步骤(9)中发酵液总量,按重量比例称取甘草0.5%、玫瑰1%、山楂2%、酸枣核0.3%、甜叶菊0.5%、西洋参0.7%分别粉碎筛分。其中甘草、红枸杞、玫瑰、山楂、酸枣核、西洋参为80-150目,甜叶菊40-60目。(10) After routinely drying licorice, rose, hawthorn, jujube seed, stevia and American ginseng, weigh 0.5% of licorice, 1% of rose, 2% of hawthorn, wild jujube according to the total amount of fermentation broth in step (9) by weight Kernel 0.3%, stevia 0.5%, and American ginseng 0.7% were crushed and sieved respectively. Among them, licorice, red wolfberry, rose, hawthorn, jujube seed, and American ginseng are 80-150 mesh, and stevia is 40-60 mesh.
(11)将步骤(10)中的各个组分加入到步骤(9)所得到的发酵酒中震荡浸提24h,料液比1:10,温度35℃,提取液离心15min,取上清液经过0.45μm薄膜过滤过滤,滤液为浸提酒液密封避光保存。(11) Add each component in step (10) to the fermented wine obtained in step (9) and shake and extract for 24 hours, the ratio of solid to liquid is 1:10, the temperature is 35°C, the extract is centrifuged for 15 minutes, and the supernatant is taken After filtering through a 0.45 μm membrane, the filtrate is the extraction wine liquid, sealed and protected from light.
(12)将步骤(5)中混合蜂蜜与黑果枸杞酶解液的混合液及步骤(11)得到的浸提酒液按1:7混合调配,加入茶多酚0.85%,加入柠檬酸和白砂糖调整酸糖比,使用0.45μm薄膜过滤膜过滤,滤液灭菌处理后,充氮包装,得到黑果枸杞蜂蜜果酒成品。(12) Mix the honey in step (5) with the enzymatic hydrolyzate of Lycium barbarum and the liquor extracted in step (11) at a ratio of 1:7, add 0.85% tea polyphenols, add citric acid and White granulated sugar is used to adjust the acid-sugar ratio, filtered through a 0.45 μm membrane filter, and the filtrate is sterilized and packed with nitrogen to obtain the finished product of black wolfberry honey wine.
实施例2Example 2
(1)党参蜂蜜10kg和黄芪蜂蜜10kg分别加热至45℃,在密封设备内趁热使用孔径为100目的尼龙网过滤,滤去杂质、死蜂等物质。(1) 10 kg of Codonopsis honey and 10 kg of Astragalus honey are heated to 45°C respectively, and filtered while hot in a sealed device using a nylon mesh with a pore size of 100 mesh to remove impurities, dead bees and other substances.
(2)将步骤(1)所得蜂蜜混合均匀,并保持45℃。加入2%活性炭均匀混合,吸附2h,除去蜂蜜中的不良气味,经过滤除去活性炭颗粒。(2) Mix the honey obtained in step (1) evenly and keep it at 45°C. Add 2% activated carbon and mix evenly, adsorb for 2 hours, remove the bad smell in honey, and remove activated carbon particles by filtration.
(3)将步骤(2)所得混合蜂蜜稀释25倍,通过0.45μm薄膜过滤器。滤液再通过真空薄膜离心式蒸发器,真空度-0.094MPa,转速300r/min,温度50℃,控制混合蜂蜜含水量16%。(3) Dilute the mixed honey obtained in step (2) by 25 times, and pass it through a 0.45 μm membrane filter. The filtrate is then passed through a vacuum thin film centrifugal evaporator with a vacuum degree of -0.094 MPa, a rotating speed of 300 r/min, and a temperature of 50° C. to control the water content of the mixed honey to 16%.
(4)将新鲜的黑果枸杞经过挑选,称取12kg,清洗,榨汁,采用果胶酶进行酶解处理,果胶酶的添加量为1%,酶解温度40℃,酶解时间1.5h。于4℃、转速1500r/min离心过滤,此温度下通过0.45μm薄膜过滤器,澄清液低温(4℃)密封避光备用,果皮果渣低温(4℃)储存备用。(4) After selecting fresh black wolfberry, weigh 12kg, wash, squeeze the juice, and use pectinase to carry out enzymolysis treatment. h. Centrifuge at 4°C with a rotation speed of 1500r/min. At this temperature, pass through a 0.45 μm membrane filter. The clarified liquid is sealed at low temperature (4°C) and protected from light for later use. The peel and pomace are stored at low temperature (4°C) for later use.
(5)将步骤(4)所得的澄清液8kg加入步骤(3)所得的混合蜂蜜10kg搅拌均匀,控制含水量20%,低温密封避光保存(4℃)。(5) Add 8 kg of clarified liquid obtained in step (4) to 10 kg of mixed honey obtained in step (3) and stir evenly, control the water content to 20%, and store in a sealed and dark place at low temperature (4° C.).
(6)挑选干净、新鲜完好红枸杞、沙棘,称取2kg红枸杞,1kg沙棘果,分别将其打浆、混合,低温密封储存(4℃)。(6) Select clean, fresh and intact red wolfberry and seabuckthorn, weigh 2kg of red wolfberry and 1kg of seabuckthorn fruit, beat and mix them respectively, and store them sealed at low temperature (4°C).
(7)将步骤(4)所得黑果枸杞果渣果皮、步骤(6)中沙棘与红枸杞混合浆液加入步骤(3)所得混合蜂蜜10kg,加水混合,加热至85℃,30min灭菌,柠檬酸调节pH值为3.7。其中,按重量比黑果枸杞果渣果皮:沙棘与红枸杞混合浆液:混合蜂蜜=1:1:4,通过加水量控制混合液中含糖量22%。(7) Add 10 kg of mixed honey obtained in step (3) to the black fruit pomace peel of wolfberry obtained in step (4), and the mixed slurry of seabuckthorn and red wolfberry in step (6), add water to mix, heat to 85°C, sterilize for 30 minutes, lemon The acid adjusts the pH to 3.7. Wherein, the ratio by weight of black wolfberry pomace peel: seabuckthorn and red wolfberry mixed slurry: mixed honey is 1:1:4, and the sugar content in the mixed solution is controlled to 22% by adding water.
(8)将步骤(7)所得混合液加入到发酵罐中,加入SO2和高糖酵母进行发酵。其中,SO2的加入量为0.3g/L,高糖酵母接种量6%,发酵温度26℃,时间5d。(8) Add the mixed solution obtained in step (7) into a fermenter, add SO 2 and high sugar yeast to ferment. Among them, the addition amount of SO 2 is 0.3g/L, the inoculum amount of high sugar yeast is 6%, the fermentation temperature is 26°C, and the time is 5d.
(9)将步骤(8)中酒液倒灌陈酿90d。发酵结束,静置沉淀,取上清液经过0.45μm薄膜过滤器过滤,换至储酒罐中储存,储存温度为8℃,湿度80%。(9) pouring the liquor in the step (8) back and aging for 90 days. After the fermentation is over, let it stand for precipitation, take the supernatant and filter it through a 0.45 μm membrane filter, and then store it in a wine storage tank at a temperature of 8°C and a humidity of 80%.
(10)将甘草、玫瑰、山楂、酸枣核、甜叶菊和西洋参常规干燥后,按步骤(9)中发酵液总量,按重量比例称取甘草0.7%、玫瑰2%、山楂4%、酸枣核0.6%、甜叶菊0.8%、西洋参1.9%分别粉碎筛分。其中甘草、红枸杞、玫瑰、山楂、酸枣核、西洋参为80-150目,甜叶菊40-60目。(10) After routine drying of licorice, rose, hawthorn, wild jujube seed, stevia and American ginseng, weigh 0.7% of licorice, 2% of rose, 4% of hawthorn, wild jujube according to the total amount of fermentation broth in step (9) by weight Kernel 0.6%, stevia 0.8%, and American ginseng 1.9% were crushed and sieved respectively. Among them, licorice, red wolfberry, rose, hawthorn, jujube seed, and American ginseng are 80-150 mesh, and stevia is 40-60 mesh.
(11)将步骤(10)中的各个组分加入到步骤(9)所得到的发酵酒中震荡浸提24h,料液比1:10,温度35℃,提取液离心15min,取上清液经过0.45μm薄膜过滤器过滤,滤液为浸提酒液密封避光保存。(11) Add each component in step (10) to the fermented wine obtained in step (9) and shake and extract for 24 hours, the ratio of solid to liquid is 1:10, the temperature is 35°C, the extract is centrifuged for 15 minutes, and the supernatant is taken After filtering through a 0.45μm membrane filter, the filtrate is the extraction wine liquid, sealed and protected from light.
(12)将步骤(5)中混合蜂蜜与黑果枸杞酶解液的混合液及步骤(11)所得浸提酒液混合按1:10调配,加入茶多酚1.2%,加入适量柠檬酸和白砂糖调整酸糖比,经过0.45μm薄膜过滤器进行膜过滤,滤液灭菌,充氮包装,得到黑果枸杞蜂蜜果酒成品。(12) Mix the mixture of honey and wolfberry enzymolysis solution in step (5) and the leaching wine obtained in step (11) at a ratio of 1:10, add 1.2% tea polyphenols, add appropriate amount of citric acid and Adjust the acid-sugar ratio with white granulated sugar, filter through a 0.45 μm membrane filter, sterilize the filtrate, pack with nitrogen, and obtain the finished product of black fruit wolfberry honey wine.
实施例3Example 3
(1)党参蜂蜜15kg和黄芪蜂蜜30kg分别加热到45℃,在密封设备内趁热使用孔径为100目的尼龙网过滤,滤去杂质、死蜂等物质。(1) 15 kg of Codonopsis honey and 30 kg of Astragalus honey are heated to 45°C respectively, and filtered while hot in a sealed device using a nylon mesh with a pore size of 100 mesh to remove impurities, dead bees and other substances.
(2)将步骤(1)中的蜂蜜混合均匀,并保持45℃。加入3%活性炭均匀混合,吸附2h,除去蜂蜜中的不良气味,经过滤除去活性炭颗粒。(2) Mix the honey in step (1) evenly and keep it at 45°C. Add 3% activated carbon and mix evenly, adsorb for 2 hours, remove bad smell in honey, and remove activated carbon particles by filtration.
(3)将步骤(2)所得的混合蜂蜜稀释30倍,通过0.45μm薄膜过滤器。滤液再通过真空薄膜离心式蒸发器,真空度-0.095MPa,转速300r/min,温度50℃,控制混合蜂蜜的含水量17%。(3) Dilute the mixed honey obtained in step (2) by 30 times, and pass through a 0.45 μm membrane filter. The filtrate is then passed through a vacuum thin film centrifugal evaporator with a vacuum degree of -0.095 MPa, a rotating speed of 300 r/min, and a temperature of 50° C. to control the water content of the mixed honey to 17%.
(4)将新鲜的黑果枸杞经过挑选,称取25kg,清洗,榨汁,采用果胶酶进行酶解处理,果胶酶的添加量为1%,酶解温度40℃,酶解时间1.5h,于4℃、转速1500r/min的条件下离心过滤,此温度下通过0.45μm薄膜过滤器,澄清液低温(4℃)密封避光备用,果皮果渣低温(4℃)储存备用。(4) After selecting fresh black wolfberry, weigh 25kg, wash, squeeze the juice, and use pectinase to carry out enzymolysis treatment. h, centrifuge at 4°C and 1500r/min, pass through a 0.45μm membrane filter at this temperature, seal the clarified liquid at low temperature (4°C) and keep it away from light for later use, and store the peel and pomace at low temperature (4°C) for later use.
(5)将步骤(4)所得澄清液12kg加入步骤(3)所得的混合蜂蜜15kg搅拌均匀,控制含水量23%,低温密封避光保存(4℃)。(5) Add 12 kg of clarified liquid gained in step (4) into 15 kg of mixed honey gained in step (3) and stir evenly, control the water content to 23%, and store in a sealed and dark place at low temperature (4° C.).
(6)挑选干净、完好红枸杞、沙棘,称取7.5kg红枸杞,2.5kg沙棘果,分别将其打浆、混合,低温密封储存(4℃)。(6) Select clean and intact red wolfberry and seabuckthorn, weigh 7.5kg of red wolfberry and 2.5kg of seabuckthorn fruit, beat and mix them respectively, and store them sealed at low temperature (4°C).
(7)将步骤(4)中黑果枸杞果渣果皮、步骤(6)所得沙棘与红枸杞混合浆液加入步骤(3)所得混合蜂蜜30kg,加水混合,加热至85℃,30min灭菌,柠檬酸调节pH值为3.7。其中,黑果枸杞果渣果皮:沙棘与红枸杞混合浆液:混合蜂蜜=1:1:4,通过加水量控制混合液中含糖量25%。(7) Add 30 kg of mixed honey obtained in step (3) to the black fruit pomace peel of wolfberry fruit in step (4), and the mixed slurry of seabuckthorn and red wolfberry obtained in step (6), add water to mix, heat to 85°C, sterilize for 30 minutes, lemon The acid adjusts the pH to 3.7. Wherein, black wolfberry pomace peel: seabuckthorn and red wolfberry mixed slurry: mixed honey = 1:1:4, and the sugar content in the mixed solution is controlled to 25% by adding water.
(8)将步骤(7)所得混合液加入发酵罐中,加入SO2和高糖酵母发酵,其中,SO2的加入量为0.3g/L,高糖酵母接种量9%,发酵温度26℃,时间8d。(8) Add the mixed solution obtained in step (7) into the fermenter, add SO 2 and high sugar yeast for fermentation, wherein the addition of SO 2 is 0.3g/L, the inoculation amount of high sugar yeast is 9%, and the fermentation temperature is 26°C , time 8d.
(9)将步骤(8)中酒液倒灌陈酿(90d)。发酵结束,静置沉淀,取上清液使用0.45μm薄膜过滤器过滤,换至储酒罐中,储酒温度为8℃,湿度80%。(9) pouring the liquor in the step (8) back for aging (90d). After the fermentation is over, let it sit for precipitation, take the supernatant and filter it with a 0.45 μm membrane filter, and then transfer it to a wine storage tank. The wine storage temperature is 8°C and the humidity is 80%.
(10)将甘草、玫瑰、山楂、酸枣核、甜叶菊和西洋参常规干燥后,按步骤(9)中发酵液总量,按重量比例称取甘草1%、玫瑰2.4%、山楂2.4%、酸枣核1.2%、甜叶菊1%、西洋参2%分别粉碎筛分。其中甘草、红枸杞、玫瑰、山楂、酸枣核、西洋参为80-150目,甜叶菊40-60目。(10) After routinely drying licorice, rose, hawthorn, wild jujube seed, stevia and American ginseng, weigh 1% of licorice, 2.4% of rose, 2.4% of hawthorn, wild jujube according to the total amount of fermentation broth in step (9) by weight Kernel 1.2%, stevia 1%, and American ginseng 2% were crushed and sieved respectively. Among them, licorice, red wolfberry, rose, hawthorn, jujube seed, and American ginseng are 80-150 mesh, and stevia is 40-60 mesh.
(11)将步骤(10)所得各个组分加入到步骤(9)所得到的发酵酒中震荡浸提24h,料液比1:10,温度35℃,提取液离心15min,取上清液经过0.45μm薄膜过滤器过滤,滤液为浸提酒液密封避光保存。(11) Add each component obtained in step (10) to the fermented wine obtained in step (9) and shake and extract for 24 hours, the ratio of solid to liquid is 1:10, the temperature is 35°C, the extract is centrifuged for 15 minutes, and the supernatant is taken through Filter with a 0.45 μm membrane filter, and the filtrate is the extraction wine liquid, sealed and protected from light.
(12)将步骤(5)中混合蜂蜜与黑果枸杞酶解液的混合液及步骤(11)所得的浸提酒液按1:15混合调配,加入茶多酚1.3%,加入适量柠檬酸和白砂糖调整酸糖比,使用0.45μm薄膜过滤器进行膜过滤,滤液灭菌,充氮包装,得到黑果枸杞蜂蜜果酒成品。(12) Mix the mixture of honey and wolfberry enzymolysis solution in step (5) and the liquor extracted from step (11) at a ratio of 1:15, add 1.3% tea polyphenols, and add an appropriate amount of citric acid Adjust the acid-sugar ratio with white granulated sugar, perform membrane filtration with a 0.45 μm membrane filter, sterilize the filtrate, pack with nitrogen filling, and obtain the finished product of black fruit wolfberry honey wine.
以上所述仅是本发明的优选实施方式,应当指出的是,对于本技术领域的普通技术人员来说,在不脱离本发明原理的前提下,还可以做出若干改进和润饰,这些改进和润饰也应视为本发明的保护范围。The above is only a preferred embodiment of the present invention, it should be pointed out that, for those of ordinary skill in the art, without departing from the principle of the present invention, some improvements and modifications can also be made, these improvements and Retouching should also be regarded as the protection scope of the present invention.
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