CN104905999A - Gardenia perfume and preparation method thereof - Google Patents
Gardenia perfume and preparation method thereof Download PDFInfo
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- CN104905999A CN104905999A CN201510270344.9A CN201510270344A CN104905999A CN 104905999 A CN104905999 A CN 104905999A CN 201510270344 A CN201510270344 A CN 201510270344A CN 104905999 A CN104905999 A CN 104905999A
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- perfume
- gardenia
- flos gardeniae
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Abstract
The invention relates to perfume, in particular to a gardenia perfume and a preparation method thereof. The gardenia perfume is prepared by mixing, by volume, 10-20% of natural essential oil extracted and purified from gardenia through a supercritical fluid CO2 extraction method, 2-5% of an essential oil emulsifying agent and 75-88% of an ethanol solution with the concentration of 95%. The gardenia perfume is prepared by mixing the pure natural plant essential oil extracted and purified from gardenia through the physical method, thereby containing no synthetic material and maintaining fragrance and elegance of the gardenia. The fragrance is harmonious and natural and lasts long. The gardenia perfume has very high application value and wide market prospects.
Description
Technical field
The present invention relates to a kind of perfume, particularly relate to a kind of Flos Gardeniae perfume and preparation method thereof.
Background technology
Flos Gardeniae system Maguireothamnus speciosus SHANZHIZI flower, have another name called Fructus Gardeniae flower, tongue of sparrow flower, Osmanthus forrestii, beautiful Flos Nelumbinis etc., floral white, gives off a strong fragrance, and is one of famous eight large fragrant flowers of China.Bitter in the mouth, cold in nature, clearing away lung-heat to relieve cough, cooling blood for hemostasis, cure mainly cough due to lung-heat, epistaxis, expectorant.Its volatilization main body of oil be linalool, JSM-LAC (Z)-7-Decen-5-olide, farnesene,
β-myrcene, essence of Niobe, ocimene etc., can be used for multiple odor type cosmetics, fancy soap essence and highclass perfumes essence, has clearing away heat-fire, treatment calentura, eases off the pressure, the effect of moisturizing skin.
The method of existing extraction Flos Gardeniae volatile oil is by the lixiviate of fresh Flos Gardeniae petroleum ether room temperature, after filtration, concentrating under reduced pressure obtains extractum, then by under the low temperature of extractum-15 DEG C again ~-20 DEG C that obtains, use dehydrated alcohol process, removing lipids and waxiness, obtain quintessence oil liquid, yield is generally 0.05 ~ 0.06%, and the shortcoming of this method is that fragrance is poor, color is comparatively dark, yield is lower; In addition, supercritical fluid technology is widely used in the extraction of volatile oil component in recent years, its have activity substance content high, do not have the advantages such as pest is residual, environmental protection, this extracting method will have larger value.
Summary of the invention
The object of the invention is to deepen the processing of Flos Gardeniae, improve the economic benefit of product, provide a kind of Flos Gardeniae perfume and preparation method thereof, the standby Flos Gardeniae perfume of this legal system has effect of refreshment, salubrious environment.
To achieve these goals, present invention employs following technical scheme:
A kind of Flos Gardeniae perfume, this perfume adopts supercritical fluid CO by Flos Gardeniae
2the allotment of the natural essential oil of extraction Hydrolysis kinetics, quintessence oil emulsifying agent and alcoholic solution forms: it is percentages by volume, and natural essential oil is 10 ~ 20%, quintessence oil emulsifying agent 2 ~ 5%, and concentration is the alcoholic solution 75 ~ 88% of 95%.
The preparation method of its Flos Gardeniae perfume comprises the steps:
(1) preparation of Flos Gardeniae quintessence oil
Flos Gardeniae is put into extraction kettle, and arranging extracting pressure is 15 ~ 25MPa, extraction temperature 30 ~ 40 DEG C, separating still pressure 10 ~ 15MPa, temperature 20 ~ 30 DEG C, CO
2flow is 20 ~ 30kg/h; Through the extraction of 60 ~ 90min, release volatile oil from separating still drain hole, Flos Gardeniae quintessence oil can be obtained.
(2) perfume allotment
Under the condition of room temperature 20 ~ 25 DEG C, allocate in proportion, the perfume of allotment under the condition of 20 ~ 25 DEG C ripe 2 ~ 3 months, fill.
As preferably, above-mentioned steps (1) extracting pressure 20MPa, extraction temperature 35 DEG C, separating still pressure 15MPa, temperature 20 DEG C, CO
2flow 25kg/h, extraction time 90min are optimum.
Flos Gardeniae perfume of the present invention is allocated formed by the extraction of Flos Gardeniae employing physical method, refining Pure natural plant essential oil, not containing any synthetic, maintain the fragrance that Flos Gardeniae has simple and elegant, fragrance harmony and natural, fragrance is held time length, has very high using value and wide market prospect.
Further illustrate the present invention below in conjunction with detailed description of the invention, but the scope of protection of present invention is not limited to following embodiments.
detailed description of the invention:
Embodiment 1: the preparation of Flos Gardeniae quintessence oil
Flos Gardeniae is put into extraction kettle, and arranging extracting pressure is 20MPa, extraction temperature 35 DEG C, separating still pressure 15MPa, temperature 20 DEG C, CO
2flow is 25kg/h; Through the extraction of 90min, release volatile oil from separating still drain hole, Flos Gardeniae quintessence oil can be obtained.
Embodiment 2: perfume is allocated
Under the condition of room temperature 20 ~ 25 DEG C, click volume ratio allotment:
| Flos Gardeniae quintessence oil | Quintessence oil emulsifying agent | Alcoholic solution | |
| Example 1 | 10 | 2 | 88 |
| Example 2 | 15 | 4 | 81 |
| Example 3 | 20 | 5 | 75 |
Deployed perfume under the condition of 20 ~ 25 DEG C ripe 2 ~ 3 months, fill.
Flos Gardeniae quintessence oil prepared by the present invention is again through the allotment of alcoholic solution and the ageing of a period of time after freezing, and product is stablized, through the gas Chromatographic Determination of different times, figure is consistent, simultaneously quintessence oil was through 2 ~ 3 months naturally volatilized, and fragrance is constant, illustrates that this technique is stablized through freezing, formulated product.
Claims (2)
1. a Flos Gardeniae perfume, is characterized in that: this perfume adopts supercritical fluid CO by Flos Gardeniae
2the allotment of the natural essential oil of extraction Hydrolysis kinetics, quintessence oil emulsifying agent and alcoholic solution forms: it is percentages by volume, and natural essential oil is 10 ~ 20%, quintessence oil emulsifying agent 2 ~ 5%, and concentration is the alcoholic solution 75 ~ 88% of 95%.
2. kind to prepare the preparation method of Flos Gardeniae perfume according to claim 1, it is characterized in that the method comprises the following steps:
(1) preparation of Flos Gardeniae quintessence oil
Flos Gardeniae is put into extraction kettle, and arranging extracting pressure is 15 ~ 25MPa, extraction temperature 30 ~ 40 DEG C, separating still pressure 10 ~ 15MPa, temperature 20 ~ 30 DEG C, CO
2flow is 20 ~ 30kg/h; Through the extraction of 60 ~ 90min, release volatile oil from separating still drain hole, the allotment of Flos Gardeniae quintessence oil (2) perfume can be obtained
Under the condition of room temperature 20 ~ 25 DEG C, allocate in proportion, the perfume of allotment under the condition of 20 ~ 25 DEG C ripe 2 ~ 3 months, fill.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510270344.9A CN104905999A (en) | 2015-05-26 | 2015-05-26 | Gardenia perfume and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510270344.9A CN104905999A (en) | 2015-05-26 | 2015-05-26 | Gardenia perfume and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104905999A true CN104905999A (en) | 2015-09-16 |
Family
ID=54075734
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510270344.9A Pending CN104905999A (en) | 2015-05-26 | 2015-05-26 | Gardenia perfume and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104905999A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106265320A (en) * | 2016-09-05 | 2017-01-04 | 马鞍山纽盟知识产权管理服务有限公司 | A kind of simple and elegant delicate fragrance type perfume |
| CN106727000A (en) * | 2016-12-30 | 2017-05-31 | 六安市裕安区天缘中药材种植专业合作社 | Gardenia essential oil face pack |
| EP4035653A1 (en) | 2021-01-29 | 2022-08-03 | Chanel Parfums Beauté | Oily extract from gardenia jasminoides flowers and cosmetic compositions comprising same |
-
2015
- 2015-05-26 CN CN201510270344.9A patent/CN104905999A/en active Pending
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106265320A (en) * | 2016-09-05 | 2017-01-04 | 马鞍山纽盟知识产权管理服务有限公司 | A kind of simple and elegant delicate fragrance type perfume |
| CN106727000A (en) * | 2016-12-30 | 2017-05-31 | 六安市裕安区天缘中药材种植专业合作社 | Gardenia essential oil face pack |
| EP4035653A1 (en) | 2021-01-29 | 2022-08-03 | Chanel Parfums Beauté | Oily extract from gardenia jasminoides flowers and cosmetic compositions comprising same |
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| C06 | Publication | ||
| PB01 | Publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20150916 |
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| WD01 | Invention patent application deemed withdrawn after publication |