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CN104877286A - High-strength complex fiber panel and preparation method thereof - Google Patents

High-strength complex fiber panel and preparation method thereof Download PDF

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Publication number
CN104877286A
CN104877286A CN201510310764.5A CN201510310764A CN104877286A CN 104877286 A CN104877286 A CN 104877286A CN 201510310764 A CN201510310764 A CN 201510310764A CN 104877286 A CN104877286 A CN 104877286A
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China
Prior art keywords
parts
strength composite
fibrous plate
composite fibrous
preparation
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CN201510310764.5A
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Chinese (zh)
Inventor
秦勇
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Suzhou De Xiang Decorative Engineering Co Ltd
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Suzhou De Xiang Decorative Engineering Co Ltd
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Priority to CN201510310764.5A priority Critical patent/CN104877286A/en
Publication of CN104877286A publication Critical patent/CN104877286A/en
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Abstract

The invention discloses a high-strength complex fiber panel and a preparation method thereof. The high-strength complex fiber panel comprises the following ingredients in parts by weight: 11-18 parts of formalized polyvinyl alcohol fiber, 7-15 parts of viscose, 3-7 parts of glass fiber, 6-11 parts of hexamethylol melamine resin, 4-10 parts of bisphenol F type epoxy resin, 3-7 parts of aluminium oxide, 6-10 parts of magnesium carbonate, 5-9 parts of basalt powder, and 15-25 parts of normal butanol. The preparation method of the high-strength complex fiber panel comprises the processes of smashing, stirring, pressing and the like. The prepared complex fiber panel has the characteristics of high breaking strength and compressive strength.

Description

A kind of high-strength composite fibrous plate and preparation method thereof
Technical field
The invention belongs to dalle field, relate to a kind of fibrous plate and preparation method thereof, especially relate to a kind of high-strength composite fibrous plate and preparation method thereof.
Background technology
Fiberboard is that the waste materials such as dry to bark, wood shavings, branch, fruit are become wood pulp through fragmentation immersion, milling, vegetable fibre is interweaved again, then through Wet-pressing molding, drying treatment forms.Fiberboard can be divided into the kinds such as hardboard (HB), softboard (LDF, SB, IB), medium density fibre board (MDF) (MDF), high density fiberboard (HDF).The feature of softboard is that density is little, physical and mechanical property not as good as hardboard, mainly in construction work in insulation, insulation and sound-absorbing, sound insulation etc.The breadth of medium density fibre board (MDF) and high density fiberboard is large, even structure, intensity are high, dimensional stabilizing distortion is little, be easy to machining, edges of boards are firm, surfacing, be convenient to direct sticker and covering with paint.Slim, coventional type and thicker sheet material can be had.The folding strength of fibrous plate and ultimate compression strength have comparatively crucial function for the normal use of fibrous plate, therefore need to guarantee that fibrous plate has good folding strength and ultimate compression strength.
Summary of the invention
The technical problem solved: the intensity of the current fibrous plate for finishing material is lower, the intensity of finishing material can be affected time in for finishing material, for the problems referred to above, need the intensity of finishing material fibrous plate as folding strength and ultimate compression strength and hardness are improved, improve its physical strength, the safety performance of finishing material could be improved further.
Technical scheme: the invention discloses a kind of high-strength composite fibrous plate and preparation method thereof, described high-strength composite fibrous plate comprises the composition of following weight parts:
Polyvinyl formal fibre 11-18 part,
Viscose fiber 7-15 part,
Glass fibre 3-7 part,
Hexamethylol melamine resin 6-11 part,
Bisphenol f type epoxy resin 4-10 part,
Aluminum oxide 3-7 part,
Magnesiumcarbonate 6-10 part,
Basalt powder 5-9 part,
Propyl carbinol 15-25 part.
Further, described a kind of high-strength composite fibrous plate, comprises the composition of following weight parts:
Polyvinyl formal fibre 13-16 part,
Viscose fiber 9-13 part,
Glass fibre 4-6 part,
Hexamethylol melamine resin 7-10 part,
Bisphenol f type epoxy resin 5-8 part,
Aluminum oxide 4-6 part,
Magnesiumcarbonate 7-9 part,
Basalt powder 6-8 part,
Propyl carbinol 17-23 part.
Further, described a kind of high-strength composite fibrous plate, comprises the composition of following weight parts:
Polyvinyl formal fibre 15 parts,
Viscose fiber 11 parts,
5 parts, glass fibre,
Hexamethylol melamine resin 8 parts,
Bisphenol f type epoxy resin 6 parts,
5 parts, aluminum oxide,
8 parts, magnesiumcarbonate,
Basalt powder 7 parts,
Propyl carbinol 20 parts.
The preparation method of described a kind of high-strength composite fibrous plate, preparation method is made up of following steps:
Step 1: open pulverizer, respectively to adding aluminum oxide, magnesiumcarbonate and basalt powder in pulverizer, separately pulverizes, and is crushed to above-mentioned one-tenth and is divided into powder, and powder order number is 100 order-300 orders;
Step 2: the pot temperature of stirred pot is set as 70-90 DEG C, after tank temperature-stable to be mixed, in stirred pot, add polyvinyl formal fibre 11-18 part, viscose fiber 7-15 part, glass fibre 3-7 part, hexamethylol melamine resin 6-11 part, bisphenol f type epoxy resin 4-10 part, be stirred to evenly to material in stirred pot;
Step 3: add aluminum oxide 3-7 part, magnesiumcarbonate 6-10 part, basalt powder 5-9 part, propyl carbinol 15-25 part again in stirred pot, after adding mentioned component, then carries out stirring and becomes slurry;
Step 4: be poured into by slurry in compacting tool set, pours into after in compacting tool set, and rising die temperature is 60-70 DEG C, after temperature-stable, be forced into 50-70MPa, the press time is 2-5h, stop pressurizeing and being cooled to room temperature, cooling, prepares high-strength composite fibrous plate.
Further, the preparation method of described a kind of high-strength composite fibrous plate, in step 1, powder order number is 200 order-300 orders.
Further, the preparation method of described a kind of high-strength composite fibrous plate, raising die temperature in step 4 is 65 DEG C.
Further, the preparation method of described a kind of high-strength composite fibrous plate, in step 4 after temperature-stable, is forced into 60MPa.
Further, the preparation method of described a kind of high-strength composite fibrous plate, in step 4, the press time is 4h.
beneficial effect:filamentary material has more purposes in dalle, conventional filamentary material is used for changing less to the character of dalle in dalle, preparation method of the present invention is by improveing the material of dalle, effectively raise the intensity of dalle, folding strength and the ultimate compression strength of conjugated fibre sheet material are all greatly improved.Improve the physical strength of dalle preferably.
Embodiment
Embodiment 1
Step 1: open pulverizer, respectively to adding aluminum oxide, magnesiumcarbonate and basalt powder in pulverizer, separately pulverizes, and is crushed to above-mentioned one-tenth and is divided into powder, and powder order number is 300 orders; Step 2: the pot temperature of stirred pot is set as 90 DEG C, after tank temperature-stable to be mixed, in stirred pot, add polyvinyl formal fibre 18 parts, viscose fiber 7 parts, 7 parts, glass fibre, hexamethylol melamine resin 6 parts, bisphenol f type epoxy resin 10 parts, be stirred to evenly to material in stirred pot; Step 3: add 7 parts, aluminum oxide, 6 parts, magnesiumcarbonate, basalt powder 9 parts, propyl carbinol 15 parts again in stirred pot, after adding mentioned component, then carries out stirring and becomes slurry; Step 4: be poured into by slurry in compacting tool set, pours into after in compacting tool set, and raising die temperature is 70 DEG C, after temperature-stable, and be forced into 70MPa, the press time is 2h, and stop pressurizeing and being cooled to room temperature, cooling, prepares high-strength composite fibrous plate.
The folding strength of the high-strength composite fibrous plate of embodiment 1 is 15.7MPa, and ultimate compression strength is 25.6MPa.
Embodiment 2
Step 1: open pulverizer, respectively to adding aluminum oxide, magnesiumcarbonate and basalt powder in pulverizer, separately pulverizes, and is crushed to above-mentioned one-tenth and is divided into powder, and powder order number is 100 orders; Step 2: the pot temperature of stirred pot is set as 70 DEG C, after tank temperature-stable to be mixed, in stirred pot, add polyvinyl formal fibre 11 parts, viscose fiber 15 parts, 3 parts, glass fibre, hexamethylol melamine resin 11 parts, bisphenol f type epoxy resin 4 parts, be stirred to evenly to material in stirred pot; Step 3: add 3 parts, aluminum oxide, 10 parts, magnesiumcarbonate, basalt powder 5 parts, propyl carbinol 25 parts again in stirred pot, after adding mentioned component, then carries out stirring and becomes slurry; Step 4: be poured into by slurry in compacting tool set, pours into after in compacting tool set, and raising die temperature is 60 DEG C, after temperature-stable, and be forced into 50MPa, the press time is 5h, and stop pressurizeing and being cooled to room temperature, cooling, prepares high-strength composite fibrous plate.
The folding strength of the high-strength composite fibrous plate of embodiment 2 is 14.9MPa, and ultimate compression strength is 24.3MPa.
Embodiment 3
Step 1: open pulverizer, respectively to adding aluminum oxide, magnesiumcarbonate and basalt powder in pulverizer, separately pulverizes, and is crushed to above-mentioned one-tenth and is divided into powder, and powder order number is 300 orders; Step 2: the pot temperature of stirred pot is set as 90 DEG C, after tank temperature-stable to be mixed, in stirred pot, add polyvinyl formal fibre 16 parts, viscose fiber 9 parts, 4 parts, glass fibre, hexamethylol melamine resin 10 parts, bisphenol f type epoxy resin 5 parts, be stirred to evenly to material in stirred pot; Step 3: add 4 parts, aluminum oxide, 9 parts, magnesiumcarbonate, basalt powder 6 parts, propyl carbinol 17 parts again in stirred pot, after adding mentioned component, then carries out stirring and becomes slurry; Step 4: be poured into by slurry in compacting tool set, pours into after in compacting tool set, and raising die temperature is 70 DEG C, after temperature-stable, and be forced into 70MPa, the press time is 2h, and stop pressurizeing and being cooled to room temperature, cooling, prepares high-strength composite fibrous plate.
The folding strength of the high-strength composite fibrous plate of embodiment 3 is 17.4MPa, and ultimate compression strength is 26.5MPa.
Embodiment 4
Step 1: open pulverizer, respectively to adding aluminum oxide, magnesiumcarbonate and basalt powder in pulverizer, separately pulverizes, and is crushed to above-mentioned one-tenth and is divided into powder, and powder order number is 200 orders; Step 2: the pot temperature of stirred pot is set as 70 DEG C, after tank temperature-stable to be mixed, in stirred pot, add polyvinyl formal fibre 13 parts, viscose fiber 13 parts, 6 parts, glass fibre, hexamethylol melamine resin 7 parts, bisphenol f type epoxy resin 8 parts, be stirred to evenly to material in stirred pot; Step 3: add 6 parts, aluminum oxide, 7 parts, magnesiumcarbonate, basalt powder 8 parts, propyl carbinol 23 parts again in stirred pot, after adding mentioned component, then carries out stirring and becomes slurry; Step 4: be poured into by slurry in compacting tool set, pours into after in compacting tool set, and raising die temperature is 60 DEG C, after temperature-stable, and be forced into 50MPa, the press time is 5h, and stop pressurizeing and being cooled to room temperature, cooling, prepares high-strength composite fibrous plate.
The folding strength of the high-strength composite fibrous plate of embodiment 4 is 18.1MPa, and ultimate compression strength is 27.3MPa.
Embodiment 5
Step 1: open pulverizer, respectively to adding aluminum oxide, magnesiumcarbonate and basalt powder in pulverizer, separately pulverizes, and is crushed to above-mentioned one-tenth and is divided into powder, and powder order number is 300 orders; Step 2: the pot temperature of stirred pot is set as 90 DEG C, after tank temperature-stable to be mixed, in stirred pot, add polyvinyl formal fibre 15 parts, viscose fiber 11 parts, 5 parts, glass fibre, hexamethylol melamine resin 8 parts, bisphenol f type epoxy resin 6 parts, be stirred to evenly to material in stirred pot; Step 3: add 5 parts, aluminum oxide, 8 parts, magnesiumcarbonate, basalt powder 7 parts, propyl carbinol 20 parts again in stirred pot, after adding mentioned component, then carries out stirring and becomes slurry; Step 4: be poured into by slurry in compacting tool set, pours into after in compacting tool set, and raising die temperature is 65 DEG C, after temperature-stable, and be forced into 60MPa, the press time is 4h, and stop pressurizeing and being cooled to room temperature, cooling, prepares high-strength composite fibrous plate.
The folding strength of the high-strength composite fibrous plate of embodiment 5 is 20.7MPa, and ultimate compression strength is 33.6MPa.
Comparative example 1
Step 1: open pulverizer, respectively to adding aluminum oxide, magnesiumcarbonate and basalt powder in pulverizer, separately pulverizes, and is crushed to above-mentioned one-tenth and is divided into powder, and powder order number is 300 orders; Step 2: the pot temperature of stirred pot is set as 90 DEG C, after tank temperature-stable to be mixed, adds viscose fiber 7 parts, 7 parts, glass fibre, bisphenol f type epoxy resin 10 parts, is stirred to evenly to material in stirred pot in stirred pot; Step 3: add 7 parts, aluminum oxide, 6 parts, magnesiumcarbonate, basalt powder 9 parts, propyl carbinol 15 parts again in stirred pot, after adding mentioned component, then carries out stirring and becomes slurry; Step 4: be poured into by slurry in compacting tool set, pours into after in compacting tool set, and raising die temperature is 70 DEG C, after temperature-stable, and be forced into 70MPa, the press time is 2h, and stop pressurizeing and being cooled to room temperature, cooling, prepares high-strength composite fibrous plate.
The folding strength of the high-strength composite fibrous plate of comparative example 1 is 11.6MPa, and ultimate compression strength is 19.5MPa.

Claims (8)

1. a high-strength composite fibrous plate, is characterized in that, described high-strength composite fibrous plate comprises the composition of following weight parts:
Polyvinyl formal fibre 11-18 part,
Viscose fiber 7-15 part,
Glass fibre 3-7 part,
Hexamethylol melamine resin 6-11 part,
Bisphenol f type epoxy resin 4-10 part,
Aluminum oxide 3-7 part,
Magnesiumcarbonate 6-10 part,
Basalt powder 5-9 part,
Propyl carbinol 15-25 part.
2. a kind of high-strength composite fibrous plate according to claim 1, is characterized in that, described high-strength composite fibrous plate comprises the composition of following weight parts:
Polyvinyl formal fibre 13-16 part,
Viscose fiber 9-13 part,
Glass fibre 4-6 part,
Hexamethylol melamine resin 7-10 part,
Bisphenol f type epoxy resin 5-8 part,
Aluminum oxide 4-6 part,
Magnesiumcarbonate 7-9 part,
Basalt powder 6-8 part,
Propyl carbinol 17-23 part.
3. a kind of high-strength composite fibrous plate according to claim 1, is characterized in that, described high-strength composite fibrous plate comprises the composition of following weight parts:
Polyvinyl formal fibre 15 parts,
Viscose fiber 11 parts,
5 parts, glass fibre,
Hexamethylol melamine resin 8 parts,
Bisphenol f type epoxy resin 6 parts,
5 parts, aluminum oxide,
8 parts, magnesiumcarbonate,
Basalt powder 7 parts,
Propyl carbinol 20 parts.
4. the preparation method of a kind of high-strength composite fibrous plate according to claim 1, it is characterized in that, preparation method is made up of following steps:
Step 1: open pulverizer, respectively to adding aluminum oxide, magnesiumcarbonate and basalt powder in pulverizer, separately pulverizes, and is crushed to above-mentioned one-tenth and is divided into powder, and powder order number is 100 order-300 orders;
Step 2: the pot temperature of stirred pot is set as 70-90 DEG C, after tank temperature-stable to be mixed, in stirred pot, add polyvinyl formal fibre 11-18 part, viscose fiber 7-15 part, glass fibre 3-7 part, hexamethylol melamine resin 6-11 part, bisphenol f type epoxy resin 4-10 part, be stirred to evenly to material in stirred pot;
Step 3: add aluminum oxide 3-7 part, magnesiumcarbonate 6-10 part, basalt powder 5-9 part, propyl carbinol 15-25 part again in stirred pot, after adding mentioned component, then carries out stirring and becomes slurry;
Step 4: be poured into by slurry in compacting tool set, pours into after in compacting tool set, and rising die temperature is 60-70 DEG C, after temperature-stable, be forced into 50-70MPa, the press time is 2-5h, stop pressurizeing and being cooled to room temperature, cooling, prepares high-strength composite fibrous plate.
5. the preparation method of a kind of high-strength composite fibrous plate according to claim 4, is characterized in that, in step 1, powder order number is 200 order-300 orders.
6. the preparation method of a kind of high-strength composite fibrous plate according to claim 4, is characterized in that, raising die temperature in step 4 is 65 DEG C.
7. the preparation method of a kind of high-strength composite fibrous plate according to claim 4, is characterized in that, in step 4 after temperature-stable, be forced into 60MPa.
8. the preparation method of a kind of high-strength composite fibrous plate according to claim 4, is characterized in that, in step 4, the press time is 4h.
CN201510310764.5A 2015-06-09 2015-06-09 High-strength complex fiber panel and preparation method thereof Pending CN104877286A (en)

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Publications (1)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105602204A (en) * 2016-02-17 2016-05-25 江苏瑞赛恩建材实业有限公司 Acoustic board for decorative building materials
CN109372391A (en) * 2018-10-11 2019-02-22 江山维尔美门业有限公司 A kind of anti-shrinkage fastening wire timber

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CN104058775A (en) * 2014-07-04 2014-09-24 陈欢娟 Refractory ceramic fiber board

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CN104058775A (en) * 2014-07-04 2014-09-24 陈欢娟 Refractory ceramic fiber board

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105602204A (en) * 2016-02-17 2016-05-25 江苏瑞赛恩建材实业有限公司 Acoustic board for decorative building materials
CN109372391A (en) * 2018-10-11 2019-02-22 江山维尔美门业有限公司 A kind of anti-shrinkage fastening wire timber

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Application publication date: 20150902