[go: up one dir, main page]

CN104849311B - Two-fluid inerting water mists inhibit pipeline gas explosion experimental provision and experimental method - Google Patents

Two-fluid inerting water mists inhibit pipeline gas explosion experimental provision and experimental method Download PDF

Info

Publication number
CN104849311B
CN104849311B CN201510264637.6A CN201510264637A CN104849311B CN 104849311 B CN104849311 B CN 104849311B CN 201510264637 A CN201510264637 A CN 201510264637A CN 104849311 B CN104849311 B CN 104849311B
Authority
CN
China
Prior art keywords
fluid
gas
inner cavity
valve
inerting
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201510264637.6A
Other languages
Chinese (zh)
Other versions
CN104849311A (en
Inventor
裴蓓
余明高
陈立伟
杨勇
朱新娜
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Henan University of Technology
Original Assignee
Henan University of Technology
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Henan University of Technology filed Critical Henan University of Technology
Priority to CN201510264637.6A priority Critical patent/CN104849311B/en
Publication of CN104849311A publication Critical patent/CN104849311A/en
Application granted granted Critical
Publication of CN104849311B publication Critical patent/CN104849311B/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Investigating Or Analyzing Materials Using Thermal Means (AREA)
  • Measuring Volume Flow (AREA)

Abstract

本发明涉及一种双流体惰化细水雾抑制管道瓦斯爆炸实验装置及实验方法,可有效解决进行双流体惰化细水雾抑制管道瓦斯爆炸仿真实验分析的问题,技术方案是,包括透明的有机玻璃管、水箱、惰性气体瓶、空气瓶和甲烷气瓶,有机玻璃管上分别设置有与其内腔相连通的放气管、与其内腔相连通的进气管,感应端伸入有机玻璃管内腔的温度传感器、感应端伸入有机玻璃管内腔的压力传感器、喷射端伸入有机玻璃管内腔的双流体喷头以及点火端伸入有机玻璃管内腔的高压脉冲点火器,本发明实验装置结构新颖独特,简单合理,实验方法简单,实验过程稳定,直观,使用方法易操作控制,雾化量通过调节气瓶压力实现,抑爆效果好。

The invention relates to an experimental device and method for suppressing pipeline gas explosion by two-fluid inerting fine water mist, which can effectively solve the problem of the simulation experiment analysis of two-fluid inerting fine water mist suppressing pipeline gas explosion. The technical solution is to include transparent Plexiglass tube, water tank, inert gas bottle, air bottle and methane gas cylinder, the plexiglass tube is respectively provided with an air discharge tube connected with its inner cavity, and an air inlet tube connected with its inner cavity, and the sensing end extends into the inner cavity of the plexiglass tube The temperature sensor, the pressure sensor whose sensing end extends into the inner cavity of the plexiglass tube, the dual-fluid nozzle whose injection end extends into the inner cavity of the plexiglass tube, and the high-voltage pulse igniter whose ignition end extends into the inner cavity of the plexiglass tube, the experimental device of the present invention has a novel and unique structure , simple and reasonable, the experimental method is simple, the experimental process is stable and intuitive, the method of use is easy to operate and control, the atomization amount is realized by adjusting the pressure of the gas cylinder, and the explosion suppression effect is good.

Description

双流体惰化细水雾抑制管道瓦斯爆炸实验装置及实验方法Two-fluid inerting fine water mist suppression pipeline gas explosion experimental device and experimental method

技术领域technical field

本发明涉及火灾安全实验装置,特别是一种双流体惰化细水雾抑制管道瓦斯爆炸实验装置及实验方法。The invention relates to a fire safety experiment device, in particular to a two-fluid inerting fine water mist suppression pipeline gas explosion experiment device and an experiment method.

背景技术Background technique

瓦斯广泛存在于煤层气、矿井通风气及化工用气中,其在矿井巷道、输气管道及储气设备中常因泄露引发爆炸灾害,成为我国最受关注的安全问题之一。随着社会发展对抑爆技术出了更高要求,即在抑爆的同时,要求对环境友好、对工艺介质无污染,因此研究清洁、高效的抑爆技术势在必行。Gas widely exists in coalbed methane, mine ventilation gas and chemical gas, and it often causes explosion disasters due to leakage in mine roadways, gas transmission pipelines and gas storage equipment, which has become one of the most concerned safety issues in my country. With the development of society, there are higher requirements for explosion suppression technology, that is, it is required to be environmentally friendly and non-polluting to the process medium while suppressing explosions. Therefore, it is imperative to study clean and efficient explosion suppression technologies.

惰性气体与细水雾都是常见的经济、环保的灭火控爆材料。目前,相应的惰性气体、水雾抑爆装置在液化石油、天然气储罐及管道运输保护、煤矿井下瓦斯防爆抑爆等领域都有初步应用。然而,由于惰性气体抑爆、防灭火时需要较高的浓度,例如CO2灭火系统的设计浓度高达34%,采空区注N2抑制瓦斯爆炸时O2浓度指标要求小于12%,应用时往往需要大量高压气瓶组、复杂管道等。细水雾用于抑爆实践主要为单流体细水雾(纯水雾),其雾化依靠控制水压高低与喷嘴结构来实现,对于煤矿巷道、工业气体管道等长距离受限空间,需要高压动力源,抑爆效果受到水雾粒径、浓度、水雾区长度等因素的影响,这些因素限制了惰性气体与细水雾抑爆技术的应用。Inert gas and fine water mist are common economical and environmentally friendly materials for fire extinguishing and explosion control. At present, the corresponding inert gas and water mist explosion suppression devices have preliminary applications in the fields of liquefied petroleum, natural gas storage tanks and pipeline transportation protection, underground gas explosion prevention and suppression in coal mines, etc. However, due to the high concentration of inert gas for explosion suppression and fire prevention, for example, the design concentration of CO 2 fire extinguishing system is as high as 34%, and the O 2 concentration index requirement for injection of N 2 in the goaf to suppress gas explosion is less than 12%. A large number of high-pressure gas cylinder groups, complex pipelines, etc. are often required. The practice of fine water mist for explosion suppression is mainly single-fluid fine water mist (pure water mist), and its atomization is realized by controlling the level of water pressure and nozzle structure. High pressure power source, the effect of explosion suppression is affected by factors such as water mist particle size, concentration, length of water mist area, etc. These factors limit the application of inert gas and fine water mist explosion suppression technology.

双流体惰化细水雾是指通过双流体喷嘴,将细水雾和惰性气体输送至爆炸性区域水的一种抑爆方法。前人研究表明,具有较小比表面积的细微雾滴抑爆作用越明显,而以惰性气体作为稀释气体,惰性气体良好的空间分散性会加快雾滴的分散性及弥散性,综合发挥惰性气体与细水雾抑爆优势,产生抑爆协同增效效应。而目前尚没有报道对于如何利用双流体惰化细水雾抑制管道瓦斯爆炸的实验装置及实验方法。Two-fluid inerting fine water mist refers to an explosion suppression method that delivers fine water mist and inert gas to water in explosive areas through a two-fluid nozzle. Previous studies have shown that fine droplets with a smaller specific surface area are more effective in suppressing explosions, and when inert gas is used as a dilution gas, the good spatial dispersion of the inert gas will speed up the dispersion and dispersibility of the droplets, and the comprehensive use of the inert gas Combined with the advantages of fine water mist explosion suppression, it produces a synergistic effect of explosion suppression. However, there is no report on the experimental device and experimental method for how to use the two-fluid inerting fine water mist to suppress the pipeline gas explosion.

发明内容Contents of the invention

针对上述情况,为克服现有技术之缺陷,本发明之目的就是提供一种双流体惰化细水雾抑制管道瓦斯爆炸实验装置及实验方法,可有效解决进行双流体惰化细水雾抑制管道瓦斯爆炸仿真实验分析的问题。In view of the above situation, in order to overcome the defects of the prior art, the purpose of the present invention is to provide a two-fluid inerting fine water mist suppression pipeline gas explosion experimental device and experimental method, which can effectively solve the problem of dual-fluid inerting fine water mist suppression pipeline Problems in gas explosion simulation experiment analysis.

本发明解决的技术方案是,The technical scheme that the present invention solves is,

一种双流体惰化细水雾抑制管道瓦斯爆炸实验装置,包括透明的有机玻璃管、水箱、惰性气体瓶、空气瓶和甲烷气瓶,有机玻璃管为一端开口的中空结构,其口部上设置有用于密封的PVC薄膜,有机玻璃管上分别设置有与其内腔相连通的放气管、与其内腔相连通的进气管,感应端伸入有机玻璃管内腔的温度传感器、感应端伸入有机玻璃管内腔的压力传感器、喷射端伸入有机玻璃管内腔的双流体喷头以及点火端伸入有机玻璃管内腔的高压脉冲点火器,惰性气体瓶的出气口经电磁阀与双流体喷头的进气口相连,水箱的出水口与双流体喷头的进液口相连,空气瓶的出气口经串联的第一止逆阀和第一质量流量控制器与进气管的进气口相连,甲烷气瓶经串联的第二止逆阀和第二质量流量控制器与进气管的进气口相连,高压脉冲点火器上设置有感应端正对高压脉冲点火器的点火电极上设置有能够感应其点火状态的光电传感器,光电传感器的信号输出端与摄像机的信号输入端相连,摄像机、电磁阀、温度传感器和压力传感器的信号输出端分别与数据采集仪的信号输入端相连,数据采集仪的信号输出端与计算机相连。A two-fluid inertized water mist suppression pipeline gas explosion experimental device, including a transparent plexiglass tube, a water tank, an inert gas bottle, an air bottle and a methane gas bottle, the plexiglass tube is a hollow structure with one end open, and its mouth is A PVC film for sealing is provided, and the plexiglass tube is respectively provided with an air discharge pipe connected to its inner cavity, an air intake pipe connected to its inner cavity, a temperature sensor whose sensing end extends into the inner cavity of the plexiglass tube, and a sensor end extending into the organic glass tube. The pressure sensor in the inner cavity of the glass tube, the dual-fluid nozzle whose injection end extends into the inner cavity of the plexiglass tube, and the high-voltage pulse igniter whose ignition end extends into the inner cavity of the plexiglass tube, the gas outlet of the inert gas bottle passes through the solenoid valve and the inlet of the dual-fluid nozzle The water outlet of the water tank is connected with the liquid inlet of the dual-fluid nozzle, the air outlet of the air bottle is connected with the air inlet of the air inlet pipe through the first check valve and the first mass flow controller connected in series, and the methane gas cylinder is connected through The second non-return valve and the second mass flow controller connected in series are connected to the air inlet of the intake pipe, and the high-voltage pulse igniter is provided with a sensing end facing the ignition electrode of the high-voltage pulse igniter. Sensor, the signal output end of the photoelectric sensor is connected with the signal input end of the camera, the signal output end of the camera, solenoid valve, temperature sensor and pressure sensor is respectively connected with the signal input end of the data acquisition instrument, and the signal output end of the data acquisition instrument is connected with the computer connected.

一种双流体惰化细水雾抑制管道瓦斯爆炸实验方法,包括以下步骤:An experimental method for suppressing pipeline gas explosion by two-fluid inerting fine water mist, comprising the following steps:

一、安装试验装置,试验装置包括透明的有机玻璃管、水箱、惰性气体瓶、空气瓶和甲烷气瓶,有机玻璃管为一端开口的中空结构,其口部上设置有用于密封的PVC薄膜,有机玻璃管上分别设置有与其内腔相连通的放气管、与其内腔相连通的进气管,感应端伸入有机玻璃管内腔的温度传感器、感应端伸入有机玻璃管内腔的压力传感器、喷射端伸入有机玻璃管内腔的双流体喷头以及点火端伸入有机玻璃管内腔的高压脉冲点火器,惰性气体瓶的出气口经电磁阀与双流体喷头的进气口相连,水箱的出水口与双流体喷头的进液口相连,空气瓶的出气口经串联的第一止逆阀和第一质量流量控制器与进气管的进气口相连,甲烷气瓶经串联的第二止逆阀和第二质量流量控制器与进气管的进气口相连,高压脉冲点火器上设置有感应端正对高压脉冲点火器的点火电极上设置有能够感应其点火状态的光电传感器,光电传感器的信号输出端与摄像机的信号输入端相连,摄像机、电磁阀、温度传感器和压力传感器的信号输出端分别与数据采集仪的信号输入端相连,数据采集仪的信号输出端与计算机相连;所述的放气管上设置有排气阀;所述的电磁阀与双流体喷头之间的管道上设置有流量计;1. Install the test device. The test device includes a transparent plexiglass tube, a water tank, an inert gas cylinder, an air cylinder and a methane gas cylinder. The plexiglass tube is a hollow structure with one end open, and a PVC film for sealing is arranged on its mouth. The plexiglass tube is respectively provided with an air discharge pipe connected to its inner cavity, an air intake pipe connected to its inner cavity, a temperature sensor whose sensing end extends into the inner cavity of the plexiglass tube, a pressure sensor whose sensing end extends into the inner cavity of the plexiglass tube, and a spray The two-fluid nozzle with the end extending into the inner cavity of the plexiglass tube and the high-voltage pulse igniter with the ignition end extending into the inner cavity of the plexiglass tube. The gas outlet of the inert gas bottle is connected with the inlet of the dual-fluid nozzle through a solenoid valve. The water outlet of the water tank is connected with the The liquid inlet of the dual-fluid spray head is connected, the gas outlet of the air cylinder is connected with the inlet of the intake pipe through the first check valve and the first mass flow controller connected in series, and the methane gas cylinder is connected through the second check valve and the first mass flow controller connected in series. The second mass flow controller is connected to the air inlet of the air intake pipe. The high-voltage pulse igniter is provided with a sensing end facing the ignition electrode of the high-voltage pulse igniter. A photoelectric sensor capable of sensing its ignition state is provided on the high-voltage pulse igniter. The signal output end of the photoelectric sensor It is connected with the signal input end of the camera, and the signal output ends of the camera, electromagnetic valve, temperature sensor and pressure sensor are respectively connected with the signal input end of the data acquisition instrument, and the signal output end of the data acquisition instrument is connected with the computer; An exhaust valve is provided; a flow meter is provided on the pipeline between the solenoid valve and the dual-fluid nozzle;

二、打开摄像机,压力传感器、温度传感器和光电传感器均接通电源,数据采集仪连接计算机并打开Labview 2009数据采集软件,在进行爆炸试验之前,调试好数据采集软件并试运行一次,检查软件是否正常运行,以保证得到的实验数据准确,调整摄像机相机位置,使其镜头正对有机玻璃管,调整相机镜头焦距,并进行一次抓拍,以保证拍摄的到的图片清晰,以便后期进行图片处理;2. Turn on the camera, connect the pressure sensor, temperature sensor and photoelectric sensor to the power supply, connect the data acquisition instrument to the computer and open the Labview 2009 data acquisition software. Before the explosion test, debug the data acquisition software and run it once to check whether the software Normal operation to ensure the accuracy of the experimental data obtained, adjust the position of the camera so that the lens is facing the plexiglass tube, adjust the focal length of the camera lens, and take a snapshot to ensure that the captured pictures are clear for later image processing;

三、打开排气阀、第一止回阀和第二止回阀,向有机玻璃管腔体通入机玻璃管腔体4倍体积的甲烷和空气的混合气体,从而排尽有机玻璃管腔体内原有的空气,关闭排气阀、第一止回阀和第二止回阀;3. Open the exhaust valve, the first check valve and the second check valve, and pass the mixed gas of methane and air 4 times the volume of the organic glass tube cavity into the organic glass tube cavity, thereby exhausting the organic glass tube cavity The original air in the body, close the exhaust valve, the first check valve and the second check valve;

四、进行双流体惰化细水雾抑制瓦斯爆炸测试,打开电磁阀控制双流体喷头开始喷雾,设定惰性气体压力与喷雾时间;4. Carry out the gas explosion suppression test of the two-fluid inert fine water mist, open the solenoid valve to control the two-fluid nozzle to start spraying, and set the inert gas pressure and spray time;

五、进行瓦斯爆炸实验测试,通过高压脉冲点火器电压点火,瞬间光电传感器捕捉点火电极发出的电火花并转换成电信号,触发摄像机工作,同时利用温度传感器、压力传感器监测火焰温度及爆炸压力变化;5. Carry out the gas explosion experiment test, ignite through the voltage of the high-voltage pulse igniter, and the instantaneous photoelectric sensor captures the electric spark emitted by the ignition electrode and converts it into an electrical signal to trigger the camera to work. At the same time, the temperature sensor and pressure sensor are used to monitor the flame temperature and explosion pressure changes ;

六、保存温度数据、压力数据和摄像机拍摄的爆炸火焰图片;通入4倍空气,排净管道腔体内气体,准备进行下一次试验;6. Save the temperature data, pressure data and the picture of the explosion flame taken by the camera; let in 4 times the air, drain the gas in the pipeline cavity, and prepare for the next test;

七、对高速摄像机拍摄的爆炸火焰图片进行处理,得到火焰前锋速度;7. Process the explosion flame picture taken by the high-speed camera to obtain the flame front speed;

八、对抑制剂惰化抑制效果进行评价分析。8. Evaluate and analyze the inerting inhibition effect of the inhibitor.

本发明实验装置结构新颖独特,简单合理,实验方法简单,实验过程稳定,直观,可直接利用煤矿、工业企业现有的惰性气体管道、水路管道,适用于可燃气体管道的防爆控火;双流体喷嘴结构简单,占据空间小,安装方便,使用方法易操作控制,雾化量通过调节气瓶压力实现,抑爆效果好,使用方便效果好,有是瓦斯爆炸实验装置上的创新。The experimental device of the present invention has novel and unique structure, simple and reasonable, simple experimental method, stable and intuitive experimental process, can directly use the existing inert gas pipelines and water pipelines of coal mines and industrial enterprises, and is suitable for explosion-proof and fire-controlling of combustible gas pipelines; two-fluid The nozzle has a simple structure, takes up little space, is easy to install, and is easy to operate and control when used. The amount of atomization is realized by adjusting the pressure of the gas cylinder. The effect of suppressing explosion is good, and it is easy to use.

附图说明Description of drawings

图1为本发明的结构示意图。Fig. 1 is a structural schematic diagram of the present invention.

具体实施方式Detailed ways

以下结合附图对本发明的具体实施方式作进一步详细说明。The specific implementation manners of the present invention will be described in further detail below in conjunction with the accompanying drawings.

由图1给出,本发明一种双流体惰化细水雾抑制管道瓦斯爆炸实验装置,包括透明的有机玻璃管、水箱、惰性气体瓶、空气瓶和甲烷气瓶,有机玻璃管10为一端开口的中空结构,其口部上设置有用于密封的PVC薄膜20,有机玻璃管上分别设置有与其内腔相连通的放气管5、与其内腔相连通的进气管17,感应端伸入有机玻璃管内腔的温度传感器7、感应端伸入有机玻璃管内腔的压力传感器8、喷射端伸入有机玻璃管内腔的双流体喷头6以及点火端伸入有机玻璃管内腔的高压脉冲点火器12,惰性气体瓶4的出气口经电磁阀3与双流体喷头6的进气口相连,水箱1的出水口与双流体喷头6的进液口相连,空气瓶14的出气口经串联的第一止逆阀13a和第一质量流量控制器11a与进气管17的进气口相连,甲烷气瓶15经串联的第二止逆阀13b和第二质量流量控制器11b与进气管17的进气口相连,高压脉冲点火器12上设置有感应端正对高压脉冲点火器的点火电极上设置有能够感应其点火状态的光电传感器9,光电传感器9的信号输出端与摄像机16的信号输入端相连,摄像机16、电磁阀3、温度传感器7和压力传感器8的信号输出端分别与数据采集仪18的信号输入端相连,数据采集仪18的信号输出端与计算机19相连。Provided by Fig. 1, a kind of two-fluid inerting fine water mist suppression pipeline gas explosion experimental device of the present invention comprises transparent plexiglass tube, water tank, inert gas bottle, air bottle and methane gas bottle, and plexiglass tube 10 is one end The hollow structure of the opening is provided with a PVC film 20 for sealing on its mouth, and the plexiglass tube is respectively provided with an air release pipe 5 communicating with its inner cavity and an air intake pipe 17 communicating with its inner cavity, and the sensing end extends into the organic A temperature sensor 7 in the inner cavity of the glass tube, a pressure sensor 8 whose sensing end extends into the inner cavity of the plexiglass tube, a dual-fluid nozzle 6 whose injection end extends into the inner cavity of the plexiglass tube, and a high-voltage pulse igniter 12 whose ignition end extends into the inner cavity of the plexiglass tube, The gas outlet of the inert gas bottle 4 is connected to the air inlet of the dual-fluid nozzle 6 through the solenoid valve 3, the water outlet of the water tank 1 is connected to the liquid inlet of the dual-fluid nozzle 6, and the gas outlet of the air bottle 14 is connected through the first stop in series. The reverse valve 13a and the first mass flow controller 11a are connected to the air inlet of the air inlet pipe 17, and the methane cylinder 15 is connected to the air inlet of the air inlet pipe 17 through the second check valve 13b in series and the second mass flow controller 11b. connected, the high-voltage pulse igniter 12 is provided with a sensing end facing the ignition electrode of the high-voltage pulse igniter, and a photoelectric sensor 9 capable of sensing its ignition state is provided, and the signal output terminal of the photoelectric sensor 9 is connected with the signal input terminal of the camera 16, and the camera 16. The signal output ends of the electromagnetic valve 3, the temperature sensor 7 and the pressure sensor 8 are respectively connected to the signal input ends of the data acquisition instrument 18, and the signal output ends of the data acquisition instrument 18 are connected to the computer 19.

所述的放气管上设置有排气阀5a;The air discharge pipe is provided with an exhaust valve 5a;

所述的电磁阀3与双流体喷头6之间的管道上设置有流量计2;A flow meter 2 is arranged on the pipeline between the solenoid valve 3 and the dual-fluid nozzle 6;

所述的有机玻璃管为120mm×120mm×840mm的横向有机透明玻璃管,有效容积为12.096L,一侧封闭,管体上设置有底座,可开展垂直或水平不同状态的惰化抑爆实验,为保证实验人员安全,另一端由PVC薄膜密封,爆炸时破裂达到泄压的作用;The plexiglass tube is a horizontal organic transparent glass tube of 120mm×120mm×840mm, with an effective volume of 12.096L, one side is closed, and a base is provided on the tube body, which can carry out inerting explosion suppression experiments in different vertical or horizontal states. In order to ensure the safety of the experimenters, the other end is sealed by a PVC film, which can be ruptured to relieve pressure when it explodes;

所述的摄像机16为拍摄速度2000帧/s以上的高速摄像机以捕捉甲烷爆炸过程中的火焰形状及火焰锋面位置;The camera 16 is a high-speed camera with a shooting speed of more than 2000 frames/s to capture the flame shape and the flame front position in the methane explosion process;

所述的双流体喷头6为市售产品(现有技术),如日本池内公司生产的BIM系列虹吸式微雾喷嘴,其雾滴粒径范围20-40纳米;Described two-fluid nozzle 6 is a commercially available product (prior art), such as the BIM series siphon type micro-mist nozzle produced by Ikechi Company in Japan, whose droplet size range is 20-40 nanometers;

所述的数据采集仪18为市售产品(现有技术),如MC公司生产的型号为USB-1608FSPlus型的数据采集卡,能够采集温度传感器采集、压力传感器在甲烷爆炸过程中的温度和压力信号、电磁阀开通和关闭的时间信号以及摄像机采集的图像信号,并通过数据采集卡将数据传输到计算机;Described data acquisition instrument 18 is commercially available product (prior art), and the model that produces as MC company is the data acquisition card of USB-1608FSPlus type, can gather the temperature and the pressure of temperature sensor collection, pressure sensor in the methane explosion process signal, the time signal of solenoid valve opening and closing, and the image signal collected by the camera, and transmit the data to the computer through the data acquisition card;

所述的高压脉动点火器12为市售产品(现有技术),如西安顺泰热工机电设备有限公司生产的HEI19系列高热能点火器;点火电压为6KV。The high-voltage pulsating igniter 12 is a commercially available product (prior art), such as the HEI19 series high-heat energy igniter produced by Xi'an Shuntai Thermal Mechanical and Electrical Equipment Co., Ltd.; the ignition voltage is 6KV.

一种双流体惰化细水雾抑制管道瓦斯爆炸实验方法,包括以下步骤:An experimental method for suppressing pipeline gas explosion by two-fluid inerting fine water mist, comprising the following steps:

一、安装试验装置,试验装置包括透明的有机玻璃管10、水箱1、惰性气体瓶4、空气瓶4和甲烷气瓶5,有机玻璃管10为一端开口的中空结构,其口部上设置有用于密封的PVC薄膜20,有机玻璃管上分别设置有与其内腔相连通的放气管5、与其内腔相连通的进气管17,感应端伸入有机玻璃管内腔的温度传感器7、感应端伸入有机玻璃管内腔的压力传感器8、喷射端伸入有机玻璃管内腔的双流体喷头6以及点火端伸入有机玻璃管内腔的高压脉冲点火器12,惰性气体瓶4的出气口经电磁阀3与双流体喷头6的进气口相连,水箱1的出水口与双流体喷头6的进液口相连,空气瓶14的出气口经串联的第一止逆阀13a和第一质量流量控制器11a与进气管17的进气口相连,甲烷气瓶15经串联的第二止逆阀13b和第二质量流量控制器11b与进气管17的进气口相连,高压脉冲点火器12上设置有感应端正对高压脉冲点火器的点火电极上设置有能够感应其点火状态的光电传感器9,光电传感器9的信号输出端与摄像机16的信号输入端相连,摄像机16、电磁阀3、温度传感器7和压力传感器8的信号输出端分别与数据采集仪18的信号输入端相连,数据采集仪18的信号输出端与计算机19相连;所述的放气管上设置有排气阀5a;所述的电磁阀3与双流体喷头6之间的管道上设置有流量计2;One, install test device, test device comprises transparent plexiglass tube 10, water tank 1, inert gas bottle 4, air bottle 4 and methane gas bottle 5, plexiglass tube 10 is the hollow structure of one end opening, and useful On the sealed PVC film 20, the plexiglass tube is respectively provided with an air release pipe 5 communicating with its inner chamber, an air intake pipe 17 communicating with its inner cavity, a temperature sensor 7 whose sensing end extends into the lumen of the organic glass tube, and a sensing end extending into the inner cavity of the organic glass tube. A pressure sensor 8 inserted into the lumen of the plexiglass tube, a dual-fluid nozzle 6 extending into the lumen of the plexiglass tube at the injection end, and a high-voltage pulse igniter 12 with the ignition end extending into the lumen of the plexiglass tube, and the gas outlet of the inert gas bottle 4 passes through the solenoid valve 3 It is connected with the air inlet of the dual-fluid nozzle 6, the water outlet of the water tank 1 is connected with the liquid inlet of the dual-fluid nozzle 6, and the gas outlet of the air bottle 14 is connected through the first check valve 13a and the first mass flow controller 11a connected in series. It is connected with the air inlet of the air inlet pipe 17, and the methane cylinder 15 is connected with the air inlet of the air inlet pipe 17 through the second non-return valve 13b and the second mass flow controller 11b connected in series, and the high pressure pulse igniter 12 is provided with an induction A photoelectric sensor 9 capable of sensing its ignition state is arranged on the ignition electrode facing the high-voltage pulse igniter. The signal output end of the photoelectric sensor 9 is connected with the signal input end of the camera 16. The camera 16, the solenoid valve 3, the temperature sensor 7 and the pressure The signal output end of sensor 8 links to each other with the signal input end of data acquisition instrument 18 respectively, and the signal output end of data acquisition instrument 18 links to each other with computer 19; Described deflation pipe is provided with exhaust valve 5a; Described electromagnetic valve 3 A flow meter 2 is arranged on the pipeline between the two-fluid nozzle 6;

二、打开摄像机,压力传感器、温度传感器和光电传感器均接通电源,数据采集仪连接计算机并打开Labview 2009数据采集软件,在进行爆炸试验之前,调试好数据采集软件并试运行一次,检查软件是否正常运行,以保证得到的实验数据准确,调整摄像机相机位置,使其镜头正对有机玻璃管,调整相机镜头焦距,并进行一次抓拍,以保证拍摄的到的图片清晰,以便后期进行图片处理;2. Turn on the camera, connect the pressure sensor, temperature sensor and photoelectric sensor to the power supply, connect the data acquisition instrument to the computer and open the Labview 2009 data acquisition software. Before the explosion test, debug the data acquisition software and run it once to check whether the software Normal operation to ensure the accuracy of the experimental data obtained, adjust the position of the camera so that the lens is facing the plexiglass tube, adjust the focal length of the camera lens, and take a snapshot to ensure that the captured pictures are clear for later image processing;

三、打开排气阀、第一止回阀和第二止回阀,向有机玻璃管腔体通入机玻璃管腔体4倍体积的甲烷和空气的混合气体,其中甲烷的体积浓度保持为9.5%;从而排尽有机玻璃管腔体内原有的空气,关闭排气阀、第一止回阀和第二止回阀;实际操作中可设定好质量流量控制器的参数后;根据其流量和时间来把控充入的气体体积量;Three, open the exhaust valve, the first check valve and the second check valve, pass into the mixed gas of methane and air of 4 times the volume of the organic glass tube cavity to the organic glass tube cavity, wherein the volumetric concentration of methane remains as 9.5%; so that the original air in the plexiglass tube cavity is exhausted, and the exhaust valve, the first check valve and the second check valve are closed; after the parameters of the mass flow controller can be set in actual operation; according to its Flow and time to control the volume of gas charged;

四、进行双流体惰化细水雾抑制瓦斯爆炸测试,打开电磁阀控制双流体喷头开始喷雾,设定惰性气体压力与喷雾时间;4. Carry out the gas explosion suppression test of the two-fluid inert fine water mist, open the solenoid valve to control the two-fluid nozzle to start spraying, and set the inert gas pressure and spray time;

五、进行瓦斯爆炸实验测试,通过高压脉冲点火器电压点火,瞬间光电传感器捕捉点火电极发出的电火花并转换成电信号,触发摄像机工作,同时利用温度传感器、压力传感器监测火焰温度及爆炸压力变化;5. Carry out the gas explosion experiment test, ignite through the voltage of the high-voltage pulse igniter, and the instantaneous photoelectric sensor captures the electric spark emitted by the ignition electrode and converts it into an electrical signal to trigger the camera to work. At the same time, the temperature sensor and pressure sensor are used to monitor the flame temperature and explosion pressure changes ;

六、引爆成功后,保存温度数据、压力数据和高速摄像机拍摄的爆炸火焰图片;通入4倍空气,排净管道腔体内气体,准备进行下一次试验;6. After the detonation is successful, save the temperature data, pressure data and the picture of the explosion flame taken by the high-speed camera; enter 4 times the air, drain the gas in the pipeline cavity, and prepare for the next test;

七、对高速摄像机拍摄的爆炸火焰图片进行处理,得到火焰前锋速度,具体计算公式为:7. Process the explosion flame picture taken by the high-speed camera to obtain the flame front speed. The specific calculation formula is:

其中:in:

L管道总长度,单位,mm;LThe total length of the pipeline, unit, mm;

zf,all火焰传播方向图片像素值,pixel;z f, all flame propagation direction image pixel value, pixel;

i时刻火焰前锋处的像素值,pixel; The pixel value at the flame front at time i, pixel;

ti火焰前锋到达i处的时间,ms。t i The time when the flame front arrives at point i, ms.

八、对抑制剂惰化抑制效果进行评价分析,具体评价爆炸超压峰值、最大火焰速度等重要的爆炸危险性评价参数。8. Evaluate and analyze the inerting suppression effect of the inhibitor, and specifically evaluate the important explosion risk evaluation parameters such as the peak value of explosion overpressure and the maximum flame velocity.

例如爆炸超压峰值与最大火焰速度是评价爆炸危险性的两个重要参数。For example, the peak value of explosion overpressure and the maximum flame velocity are two important parameters to evaluate the risk of explosion.

为了比较双流体惰化细水雾的抑爆效果,将所有实验结果均与体积浓度9.5%的纯甲烷预混气的爆炸参数进行比较,其中有机玻璃管最大爆炸超压为292.3407mbar。其中,双流体喷头压力为0.2Mpa,0.3Mpa,0.4Mpa时,惰性气体消耗量分别为0.45L/s,0.6L/s,0.77L/s,最大喷雾速率分别为0.67mL/s,0.64mL/s,0.53mL/s。根据通入时间,可以得到惰性气体占有机玻璃管体积百分比数,具体结果如下表1-5所示。In order to compare the explosion suppression effect of two-fluid inert water mist, all experimental results were compared with the explosion parameters of pure methane premixed gas with a volume concentration of 9.5%, and the maximum explosion overpressure of the plexiglass tube was 292.3407mbar. Among them, when the pressure of the two-fluid nozzle is 0.2Mpa, 0.3Mpa, and 0.4Mpa, the inert gas consumption is 0.45L/s, 0.6L/s, 0.77L/s, and the maximum spray rate is 0.67mL/s, 0.64mL /s, 0.53mL/s. According to the feeding time, the volume percentage of the organic glass tube occupied by the inert gas can be obtained, and the specific results are shown in Table 1-5 below.

表1双流体喷嘴通入惰性气体占管道体积分数Table 1 The volume fraction of inert gas injected into the pipeline by the dual-fluid nozzle

表2单独CO2对甲烷爆炸最大超压的影响Table 2 Effect of CO2 alone on the maximum overpressure of methane explosion

表3单独超细水雾喷雾时间对甲烷爆炸最大超压的影响(其中超细水雾喷雾速率为0.42mL/min)Table 3 Effect of individual ultrafine water mist spray time on the maximum overpressure of methane explosion (wherein the ultrafine water mist spray rate is 0.42mL/min)

表4含CO2的双流体惰化细水雾对甲烷爆炸最大超压的影响Table 4 Effect of CO2-containing two -fluid inert water mist on maximum overpressure of methane explosion

表5含CO2的双流体惰化细水雾对甲烷爆炸最大火焰传播速度的影响Table 5 Effect of two -fluid inertized water mist containing CO2 on the maximum flame propagation velocity of methane explosion

通过上述试验结果可以看出,含N2、CO2等惰气的双流体细水雾抑爆效果明显,随着喷雾时间的延长,爆炸火焰的速度峰值逐渐下降,当喷雾时间大于3s时,经多次点火无法引爆。与纯惰性气体、细水雾抑爆相比,双流体惰化细水雾发挥了惰性气体与细水雾的抑爆优势,大幅降低了惰气浓度和细水雾的用量,对于工业管道等受限空间的抑爆具有一定现实价值。From the above test results, it can be seen that the two-fluid fine water mist containing N2, CO2 and other inert gases has obvious explosion suppression effect. With the extension of the spray time, the peak velocity of the explosion flame gradually decreases. The secondary ignition failed to detonate. Compared with pure inert gas and fine water mist for explosion suppression, the two-fluid inerted fine water mist takes advantage of the explosion suppression advantages of inert gas and fine water mist, and greatly reduces the concentration of inert gas and the amount of fine water mist. It is suitable for industrial pipelines, etc. Explosion suppression in confined spaces has certain practical value.

由上述情况可以清楚的看出,与现有技术相比,本发明具有以下优点:Can clearly find out by above-mentioned situation, compared with prior art, the present invention has the following advantages:

(1)实现了点火、压力、温度、火焰监测的同步控制;(1) The synchronous control of ignition, pressure, temperature and flame monitoring is realized;

(2)无需对实验腔体抽真空,预混气体的比例配气快速、方法简单,工作效率提高2倍以上;(2) No need to evacuate the experimental chamber, the proportion of premixed gas is quickly distributed, the method is simple, and the work efficiency is increased by more than 2 times;

(3)双流体细水雾喷头采用气动虹吸式,为普通商业购买双流体细水雾喷头,易购得,无需水泵设施;(3) The dual-fluid fine water mist nozzle adopts the pneumatic siphon type, and the dual-fluid fine water mist nozzle is purchased for ordinary businesses, which is easy to buy and does not require water pump facilities;

(4)喷雾可通过远程控制电磁阀压力喷放,并通过控制气瓶压力调节雾滴粒径,可靠性高,用水量少;(4) The spray can be sprayed by remotely controlling the pressure of the solenoid valve, and the particle size of the droplets can be adjusted by controlling the pressure of the gas cylinder, with high reliability and less water consumption;

(5)有机玻璃管上设置有底座,可开展垂直或水平不同状态的惰化抑爆实验。(5) There is a base on the plexiglass tube, which can carry out inerting explosion suppression experiments in different vertical or horizontal states.

申请人要指出的是,本申请上述指出的仅仅是一种实施例,并不是用于限制本申请的保护范围,凡是用等同或等同替代手段所做出与本申请技术方案本质上相同的技术方案均属于本申请的保护范围。The applicant should point out that the above mentioned in the application is only an embodiment, and is not intended to limit the scope of protection of the application. Any technology that is essentially the same as the technical solution of the application is made by equivalent or equivalent replacement means The schemes all belong to the protection scope of the present application.

Claims (4)

1. a kind of two-fluid inerting water mists inhibit pipeline gas explosion experimental provision, including transparent organic glass pipe, water tank, Inert gas bottle, air bottle and methane gas cylinder, which is characterized in that lucite tube(10)For the hollow structure of one end open, The PVC film for sealing is provided on oral area(20), the deflation being connected with its inner cavity is respectively arranged on lucite tube Pipe(5), the air inlet pipe that is connected with its inner cavity(17), induction end stretch into the temperature sensor of organic glass tube cavity(7), induction The pressure sensor of organic glass tube cavity is stretched at end(8), ejection end stretch into the two-fluid nozzle of organic glass tube cavity(6)With And firing tip stretches into the high-voltage pulses device of organic glass tube cavity(12), inert gas bottle(4)Gas outlet through solenoid valve (3)With two-fluid nozzle(6)Air inlet be connected, water tank(1)Water outlet and two-fluid nozzle(6)Inlet be connected, it is empty Gas cylinder(14)The first check (non-return) valve for being concatenated of gas outlet(13a)With the first mass flow controller(11a)With air inlet pipe(17) Air inlet be connected, methane gas cylinder(15)The second check (non-return) valve being concatenated(13b)With the second mass flow controller(11b)With into Tracheae(17)Air inlet be connected, photoelectric sensor(9)Induction end face high-voltage pulses device(12)Ignitor, light Electric transducer(9)High-voltage pulses device can be incuded(12)Fired state, photoelectric sensor(9)Signal output end with take the photograph Camera(16)Signal input part be connected, video camera(16), solenoid valve(3), temperature sensor(7)And pressure sensor(8)'s Signal output end respectively with data collecting instrument(18)Signal input part be connected, data collecting instrument(18)Signal output end and meter Calculation machine(19)It is connected;The two-fluid nozzle(6)20-40 μm of mist droplet particle size range.
2. two-fluid inerting water mists according to claim 1 inhibit pipeline gas explosion experimental provision, which is characterized in that It is provided with air bleeding valve on the bleeder pipe(5a).
3. two-fluid inerting water mists according to claim 1 inhibit pipeline gas explosion experimental provision, which is characterized in that The solenoid valve(3)With two-fluid nozzle(6)Between pipeline on be provided with flowmeter(2).
4. a kind of two-fluid inerting water mists using experimental provision described in claim 1 inhibit pipeline gas explosion experiment side Method, which is characterized in that include the following steps:
One, experimental provision is installed, experimental provision includes transparent organic glass pipe(10), water tank(1), inert gas bottle(4), it is empty Gas cylinder(14 )With methane gas cylinder(15), lucite tube(10)For the hollow structure of one end open, it is provided with and is used on oral area The PVC film of sealing(20), the bleeder pipe being connected with its inner cavity is respectively arranged on lucite tube(5), with its inner cavity phase The air inlet pipe of connection(17), induction end stretch into the temperature sensor of organic glass tube cavity(7), induction end stretch into lucite tube The pressure sensor of inner cavity(8), ejection end stretch into the two-fluid nozzle of organic glass tube cavity(6)And firing tip stretch into it is organic The high-voltage pulses device of glass tube cavity(12), inert gas bottle(4)Gas outlet through solenoid valve(3)With two-fluid nozzle (6)Air inlet be connected, water tank(1)Water outlet and two-fluid nozzle(6)Inlet be connected, air bottle(14)Gas outlet The first check (non-return) valve being concatenated(13a)With the first mass flow controller(11a)With air inlet pipe(17)Air inlet be connected, methane Gas cylinder(15)The second check (non-return) valve being concatenated(13b)With the second mass flow controller(11b)With air inlet pipe(17)Air inlet It is connected, photoelectric sensor(9)Induction end face high-voltage pulses device(12)Ignitor, photoelectric sensor(9)It can Incude high-voltage pulses device(12)Fired state, photoelectric sensor(9)Signal output end and video camera(16)Signal Input terminal is connected, video camera(16), solenoid valve(3), temperature sensor(7)And pressure sensor(8)Signal output end difference With data collecting instrument(18)Signal input part be connected, data collecting instrument(18)Signal output end and computer(19)It is connected; It is provided with air bleeding valve on the bleeder pipe(5a);The solenoid valve(3)With two-fluid nozzle(6)Between pipeline on be arranged There is flowmeter(2);The two-fluid nozzle(6)20-40 μm of mist droplet particle size range;
Two, video camera is opened, pressure sensor, temperature sensor and photoelectric sensor are turned on power supply, data collecting instrument connection Computer simultaneously opens 2009 data acquisition softwares of Labview and has debugged data acquisition software simultaneously before carrying out explosive test Trial operation is primary, checks software whether normal operation, to ensure that obtained experimental data is accurate, adjusts video camera camera position, Make its camera lens face lucite tube, adjust camera lens focal length, and once captured, the picture arrived to ensure shooting is clear It is clear, so that the later stage carries out picture processing;
Three, air bleeding valve, the first check (non-return) valve and the second check (non-return) valve are opened, 4 times of machine glass tube chamber is passed through to organic glass tube chamber The methane of volume and the mixed gas of air close air bleeding valve, first to drain original air in organic glass tube chamber Check (non-return) valve and the second check (non-return) valve;
Four, two-fluid inerting water mists are carried out and inhibit gas explosion test, solenoid valve control two-fluid nozzle is opened and starts to spray, Set inert gas pressure and spray time;
Five, gas explosion experiment test is carried out, is lighted a fire by high-voltage pulses device voltage, moment photoelectric sensor captures igniting Electric spark that electrode is sent out simultaneously is converted into electric signal, triggers camera operation, while supervising using temperature sensor, pressure sensor Survey flame temperature and blast pressure variation;
Six, the explosive flame picture that storage temperature data, pressure data and video camera are shot;4 times of air are passed through, duct chamber is emptied Internal gas is ready for testing next time;
Seven, the explosive flame picture of high-speed camera shooting is handled, obtains flame front velocity;
Eight, evaluation analysis is carried out to inhibitor inerting inhibition.
CN201510264637.6A 2015-05-21 2015-05-21 Two-fluid inerting water mists inhibit pipeline gas explosion experimental provision and experimental method Expired - Fee Related CN104849311B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201510264637.6A CN104849311B (en) 2015-05-21 2015-05-21 Two-fluid inerting water mists inhibit pipeline gas explosion experimental provision and experimental method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201510264637.6A CN104849311B (en) 2015-05-21 2015-05-21 Two-fluid inerting water mists inhibit pipeline gas explosion experimental provision and experimental method

Publications (2)

Publication Number Publication Date
CN104849311A CN104849311A (en) 2015-08-19
CN104849311B true CN104849311B (en) 2018-10-23

Family

ID=53849115

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201510264637.6A Expired - Fee Related CN104849311B (en) 2015-05-21 2015-05-21 Two-fluid inerting water mists inhibit pipeline gas explosion experimental provision and experimental method

Country Status (1)

Country Link
CN (1) CN104849311B (en)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105136856A (en) * 2015-10-13 2015-12-09 国家安全生产监督管理总局化学品登记中心 Dust burning explosion tester with temperature-controllable ignition device
CN105536173A (en) * 2016-01-15 2016-05-04 中国人民解放军后勤工程学院 Method for restraining oil gas explosion in restricted space through gas-liquid two-phase explosion restraining agent
CN107796852A (en) * 2017-10-20 2018-03-13 安徽理工大学 One kind combination chamber structure suppresses gas explosion in underground coal mines test method
CN109991277B (en) * 2019-04-28 2021-07-27 河南理工大学 A turbulent premixed gas pipeline explosion test device and method
CN112169242B (en) * 2020-11-30 2022-04-26 河南理工大学 Composite gas-liquid two-phase fire extinguishing agent for inhibiting flame enhancement at initial stage of water mist fire extinguishing
CN114441732A (en) * 2021-08-10 2022-05-06 中国矿业大学 Testing device and testing method for gas explosion caused by rock piezoelectric effect
CN113552170A (en) * 2021-08-12 2021-10-26 北京石油化工学院 Device and method for inhibiting combustible gas explosion by using magnetic field
CN113834853B (en) * 2021-08-27 2024-01-12 北京石油化工学院 Device and method for testing explosion characteristics of fuel gas in oil-water-gas coexistence limited space
CN115315145B (en) * 2022-08-05 2025-01-10 武汉船用机械有限责任公司 An explosion-proof pressure relief electric control box
CN116559261B (en) * 2023-01-28 2024-12-03 大连理工大学 Inerting protection device and method for preventing leakage hydrogen explosion

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SE346619B (en) * 1970-12-02 1972-07-10 Ind Ab
CN204613136U (en) * 2015-05-21 2015-09-02 河南理工大学 A kind of two-fluid inerting water mists suppresses pipeline gas explosion experimental provision

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
"细水雾抑制管道瓦斯爆炸的实验研究";余明高 等;《煤炭学报》;20110331;第36卷(第3期);第417页左栏最后一段至第418页左栏第3段及图1 *
"超细水雾增强与抑制瓦斯爆炸的实验研究";张鹏鹏;《中国优秀硕士学位论文全文数据库 工程科技Ⅰ辑》;20130815(第8期);正文第16页第1段至第23页最后一段及图2.1 *

Also Published As

Publication number Publication date
CN104849311A (en) 2015-08-19

Similar Documents

Publication Publication Date Title
CN104849311B (en) Two-fluid inerting water mists inhibit pipeline gas explosion experimental provision and experimental method
Pei et al. Experimental study on suppression effect of inert gas two fluid water mist system on methane explosion
CN103775122A (en) Simulation experiment device of gas extraction and coal spontaneous combustion of spontaneous combustion-prone and high gas concentration coal seam goaf
CN113567496B (en) Experimental device and method for visualizing gas-dust composite explosion characteristics in airtight containers and their protection research
CN208399416U (en) It is a kind of to utilize the datonation-inhibition experimental provision of low-carbon mixed gas hydrate
CN209727824U (en) Gas-liquid two-phase medium suppression gas/coal dust composite system explosion experimental device
CN106769742B (en) A dust suppression agent, dust-proof agent dust removal effect test device and test method
CN201211404Y (en) Gas dust explosion suppression device
CN108362855A (en) A kind of quick-fried experimental provision of dust prevention and control
CN107103829A (en) It is a kind of simulate enclosure water mists go out spraying fire experimental provision
CN102930770A (en) Shock tube type combustible gas explosion experiment device
CN104390804A (en) Performance test system and test method for explosion suppression and explosion resistance mining device
CN113325034B (en) A test system and test method for coal mine gas and dust explosion
CN104436478A (en) Gas-solid two-phase jet type active fire resistance and explosion suppression method
CN206930608U (en) A kind of combined type suppresses flammable gas explosion experimental provision
CN204613136U (en) A kind of two-fluid inerting water mists suppresses pipeline gas explosion experimental provision
CN104482412A (en) Gas flame capturing and extinguishing device
CN204269392U (en) Mining datonation-inhibition device of blast prevention Performance Test System
CN105148433A (en) Sandblast fire-extinguishing device
CN105424699B (en) A kind of gas explosion impulse force detection means and detection method
CN103114869B (en) Device for suppressing gas explosion and application method for device
CN205015161U (en) Simulation direct injection natural gas engine's constant volume combustion system
CN109991277A (en) A kind of turbulent flow premixed gas pipe explosion experiment test device and method
CN204422518U (en) A kind of experimental provision of simulating original place subsequent explosion
CN203394564U (en) Electromagnetic type anti-explosion opening device

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
EXSB Decision made by sipo to initiate substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20181023

CF01 Termination of patent right due to non-payment of annual fee