[go: up one dir, main page]

CN104839222A - Cowpea seed treatment agent and treatment method thereof - Google Patents

Cowpea seed treatment agent and treatment method thereof Download PDF

Info

Publication number
CN104839222A
CN104839222A CN201510167298.XA CN201510167298A CN104839222A CN 104839222 A CN104839222 A CN 104839222A CN 201510167298 A CN201510167298 A CN 201510167298A CN 104839222 A CN104839222 A CN 104839222A
Authority
CN
China
Prior art keywords
cowpea
parts
cowpea seed
seed
polyvinyl alcohol
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201510167298.XA
Other languages
Chinese (zh)
Other versions
CN104839222B (en
Inventor
韦永梁
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Ningbo Yuanzhicube Energy Technology Co ltd
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Priority to CN201510167298.XA priority Critical patent/CN104839222B/en
Publication of CN104839222A publication Critical patent/CN104839222A/en
Application granted granted Critical
Publication of CN104839222B publication Critical patent/CN104839222B/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

本发明公开了一种豇豆种子处理剂及其处理方法,豇豆种子处理剂包括以下重量份数的组分:无光触媒0.1-5份、纳米银0.005-0.1份、抗菌肽0.1-3.5份、木醋液1-20份、表面活性剂0.01-0.3份和无菌水70-80份。通过对豇豆种子进行处理,可有效地杀灭附在豇豆种子上的真菌、细菌,通过在豇豆种子表面包覆含有杀菌剂、杀虫剂和保水剂等成分的聚乙烯醇薄膜,通过聚乙烯醇的降解和保水剂的作用,使杀菌剂、杀虫剂等有效成分缓慢地释放出来,可长效地保护豇豆种子免受细菌、真菌和害虫等的危害。The invention discloses a treatment agent for cowpea seeds and a treatment method thereof. The treatment agent for cowpea seeds comprises the following components in parts by weight: 0.1-5 parts of non-photocatalyst, 0.005-0.1 parts of nano-silver, 0.1-3.5 parts of antibacterial peptide, wood 1-20 parts of vinegar, 0.01-0.3 parts of surfactant and 70-80 parts of sterile water. By treating the cowpea seeds, the fungus and bacteria attached to the cowpea seeds can be effectively killed. By coating the surface of the cowpea seeds with a polyvinyl alcohol film containing fungicides, insecticides and water-retaining agents, etc., the polyethylene The degradation of alcohol and the function of water-retaining agent can slowly release active ingredients such as fungicides and insecticides, which can protect cowpea seeds from bacteria, fungi and pests for a long time.

Description

一种豇豆种子处理剂及其处理方法A kind of cowpea seed treatment agent and treatment method thereof

技术领域technical field

本发明涉及农作物栽培技术领域,尤其涉及一种豇豆种子处理剂及其处理方法。The invention relates to the technical field of crop cultivation, in particular to a cowpea seed treatment agent and a treatment method thereof.

背景技术Background technique

豇豆是我国重要的经济作物,是深受人们喜爱的家常菜之一,其具有理中益气、健胃补肾、调颜养身、和五脏、生精髓、止消渴、解毒等功效。豇豆种子含大量淀粉、脂肪油、蛋白质、烟酸、维生素B1和B2。干豆角含有大量的植物纤维,还有润肠通便的作用。Cowpea is an important economic crop in my country and one of the home-cooked dishes that are loved by people. It has the functions of nourishing Qi, invigorating the stomach, nourishing the kidney, regulating the appearance and body, harmonizing the five internal organs, nourishing the essence, quenching thirst, and detoxifying. Cowpea seeds contain a lot of starch, fatty oil, protein, niacin, vitamins B1 and B2. Dried beans contain a lot of plant fiber, and also have the effect of laxative.

种子处理是指种子播种前采用的物理、化学或生物处理措施的总称,目的是促使种子发芽快而整齐、幼苗生长健壮、预防病虫害和促使某些作物早熟。播种前对豇豆种子进行处理,可消灭附在种子上的真菌、细菌,防止播种时把病菌带入田间,对豇豆的增产及病虫害的防治有着重要的作用。Seed treatment refers to the general term for physical, chemical or biological treatment measures used before sowing seeds, with the purpose of promoting fast and neat germination of seeds, robust growth of seedlings, prevention of pests and diseases, and early maturity of certain crops. Treating cowpea seeds before sowing can eliminate fungi and bacteria attached to the seeds and prevent germs from being brought into the field during sowing, which plays an important role in increasing cowpea production and preventing pests and diseases.

现有的豇豆种子处理剂存在着处理效果差、持续时间短、对人体伤害和环境污染较大,以及种衣剂成膜性和粘接强度较差等问题。The existing cowpea seed treatment agent has the problems of poor treatment effect, short duration, great harm to human body and environmental pollution, poor film-forming property and bonding strength of the seed coating agent, and the like.

发明内容Contents of the invention

本发明公开了一种豇豆种子处理剂及其处理方法,通过对豇豆种子进行处理,可有效地杀灭附在豇豆种子上的真菌、细菌,通过在豇豆种子表面包覆含有杀菌剂、杀虫剂和保水剂等成分的聚乙烯醇薄膜,通过聚乙烯醇的降解,使杀菌剂、杀虫剂等有效成分缓慢地释放出来,可长效地保护豇豆种子免受细菌、真菌和害虫等的危害。The invention discloses a cowpea seed treatment agent and a treatment method thereof. By treating the cowpea seeds, fungi and bacteria attached to the cowpea seeds can be effectively killed. The polyvinyl alcohol film composed of additives and water-retaining agents, through the degradation of polyvinyl alcohol, slowly releases active ingredients such as fungicides and insecticides, which can protect cowpea seeds from bacteria, fungi and pests for a long time harm.

本发明提供的技术方案为:The technical scheme provided by the invention is:

一种豇豆种子处理剂,包括以下重量份数的组分:无光触媒0.1-5份、纳米银0.005-0.1份、抗菌肽0.1-3.5份、木醋液1-20份、表面活性剂0.01-0.3份和无菌水70-80份。A cowpea seed treatment agent, comprising the following components in parts by weight: 0.1-5 parts of non-photocatalyst, 0.005-0.1 parts of nano-silver, 0.1-3.5 parts of antibacterial peptide, 1-20 parts of wood vinegar, and 0.01-0.01 parts of surfactant 0.3 parts and 70-80 parts of sterile water.

优选的是,所述的豇豆种子处理剂中,所述表面活性剂为蔗糖酯、十六烷基三甲基氯化铵和十二烷基二甲基苄基氯化铵中的任意一种或几种。Preferably, in the described cowpea seed treatment agent, the surfactant is any one of sucrose ester, cetyl trimethyl ammonium chloride and dodecyl dimethyl benzyl ammonium chloride or several.

优选的是,所述的豇豆种子处理剂中,所述纳米银的粒径为20-50nm。Preferably, in the cowpea seed treatment agent, the particle size of the nano-silver is 20-50nm.

一种豇豆种子的处理方法,包括:A processing method of cowpea seeds, comprising:

步骤一、使用豇豆种子处理剂于30-40℃下浸泡豇豆种子1-6h,之后将所述豇豆种子晾干后除去表面水分待用;Step 1. Soak the cowpea seeds at 30-40° C. for 1-6 hours with a cowpea seed treatment agent, then dry the cowpea seeds and remove the surface moisture for later use;

步骤二、将重量份数为1-10份的聚乙烯醇加入到20-50份的水中,在室温下充分溶胀1.0-2.0h,之后升温到65-95℃搅拌2.0-4.0h至聚乙烯醇完全溶解,冷却至室温后,再向聚乙烯醇水溶液中加入保水剂1-10份、分散剂1-2份、50%多菌灵可湿性粉剂0.001-3.0份和多杀菌素0.001-3.0份,搅拌1.0-2.0h,得混合液,将重量份数为0.01-0.1份的成膜助剂与所述混合液混合均匀得到混有成膜助剂的聚乙烯醇水溶液,并冷却至30-35℃,备用;Step 2: Add 1-10 parts by weight of polyvinyl alcohol to 20-50 parts of water, fully swell at room temperature for 1.0-2.0 hours, then raise the temperature to 65-95°C and stir for 2.0-4.0 hours to form polyethylene After the alcohol is completely dissolved and cooled to room temperature, add 1-10 parts of water-retaining agent, 1-2 parts of dispersant, 0.001-3.0 parts of 50% carbendazim wettable powder and 0.001-3.0 parts of spinosad to the polyvinyl alcohol aqueous solution part, stirred for 1.0-2.0h to obtain a mixed solution, and the film-forming aid in parts by weight of 0.01-0.1 part was mixed with the mixed solution to obtain a polyvinyl alcohol aqueous solution mixed with a film-forming aid, and cooled to 30 -35℃, standby;

步骤三、首先向具有多个连续凹槽的不锈钢模具的凹槽内涂抹脱模剂,所述凹槽的规格大于所述豇豆种子的规格,之后将步骤一中处理后的豇豆种子放入所述凹槽中,每个凹槽对应放置一粒豇豆种子,再将步骤二中得到的所述混有成膜助剂的聚乙烯醇水溶液均匀地涂抹在所述豇豆种子表面,于室温下放置10-120min,使豇豆种子表面形成一层薄膜,最后从所述不锈钢模具上取出豇豆种子,得到表面包覆薄膜的豇豆种子;以及,Step 3, first smear release agent in the groove of the stainless steel mold that has a plurality of continuous grooves, the specification of described groove is greater than the specification of described cowpea seed, put the cowpea seed processed in step one into place afterwards In the grooves, each groove corresponds to place a cowpea seed, and then the polyvinyl alcohol aqueous solution mixed with film-forming aid obtained in step 2 is evenly applied to the surface of the cowpea seed, and placed at room temperature 10-120min, make the cowpea seed surface form a layer of thin film, finally take out cowpea seed from described stainless steel mold, obtain the cowpea seed of surface coating film; And,

步骤四、将步骤三得到的豇豆种子在2-4℃下黑暗处理5-7天,即可进行播种。Step 4: Treat the cowpea seeds obtained in Step 3 in the dark at 2-4° C. for 5-7 days before sowing.

优选的是,所述的豇豆种子的处理方法中,所述步骤一中的豇豆种子处理剂由以下重量份数的组分组成:无光触媒2.5份、纳米银0.05份、抗菌肽1.8份、木醋液10.5份、表面活性剂0.15份和无菌水75份。Preferably, in the treatment method of described cowpea seeds, the cowpea seed treatment agent in the said step 1 is made up of the following components by weight: 2.5 parts of non-photocatalysts, 0.05 parts of nano-silver, 1.8 parts of antimicrobial peptides, wood 10.5 parts of vinegar, 0.15 parts of surfactant and 75 parts of sterile water.

优选的是,所述的豇豆种子的处理方法中,所述步骤一中的豇豆种子与豇豆种子处理剂的质量比为0.5。Preferably, in the treatment method of described cowpea seeds, the mass ratio of cowpea seeds and cowpea seed treatment agent in the described step 1 is 0.5.

优选的是,所述的豇豆种子的处理方法中,所述保水剂为聚丙烯酰胺、聚丙烯酸铵和聚丙烯酸钾中的任意一种或几种。Preferably, in the method for treating cowpea seeds, the water retaining agent is any one or more of polyacrylamide, ammonium polyacrylate and potassium polyacrylate.

优选的是,所述的豇豆种子的处理方法中,所述脱模剂为二甲基硅油。Preferably, in the treatment method of described cowpea seeds, the release agent is simethicone.

优选的是,所述的豇豆种子的处理方法中,所述成膜助剂为醇酯十二。Preferably, in the method for treating cowpea seeds, the film-forming aid is alcohol ester twelve.

本发明公开了一种豇豆种子处理剂及其处理方法。在种子处理剂中添加有无光触媒,无光触媒主要成分是超纳米微分子磷酸二氧化钛化合物,在有光、无光状态均有极强的杀菌、防霉等功能。在种子处理剂中添加有纳米银,极少的纳米银可产生强大的杀菌作用,可在数分钟内杀死650多种细菌,广谱杀菌且无任何的耐药性,无任何毒性反应,是最新一代的天然抗菌剂。在种子处理剂中添加有抗菌肽,抗菌肽具有抗菌活性高、不易产生抗性突变、热稳定性好等优点,对部分真菌、原虫、病毒等均具有强力的杀伤作用。在种子处理剂中添加有木醋液,木醋液因含有许多酚类物质,具有杀菌、消毒、防虫等功效。用豇豆种子处理剂浸泡豇豆种子,可有效地杀灭附在豇豆种子上的真菌、细菌及害虫,且无耐药性。保水剂是一种吸水能力特别强的功能性高分子材料,无毒无害,反复释水、吸水,还能吸收肥料、农药、并缓慢释放,增加肥效、药效,通过在豇豆种子表面包覆含有杀菌剂、杀虫剂和保水剂等成分的聚乙烯醇薄膜,聚乙烯醇薄膜具有成膜性好,干燥快,粘接性强,不影响种子发芽等优点,通过聚乙烯醇的降解和保水剂的作用,使杀菌剂、杀虫剂等有效成分缓慢地释放出来,可长效地保护豇豆种子免受细菌、真菌和害虫等的危害。The invention discloses a cowpea seed treatment agent and a treatment method thereof. A non-photocatalyst is added to the seed treatment agent. The main component of the non-photocatalyst is an ultra-nanometer micromolecular titanium dioxide phosphate compound, which has extremely strong sterilization and anti-mildew functions in both the light and non-light states. Nano-silver is added to the seed treatment agent. A very small amount of nano-silver can produce a strong bactericidal effect, which can kill more than 650 kinds of bacteria within a few minutes. It is broad-spectrum bactericidal without any drug resistance and no toxic reaction. Is the latest generation of natural antibacterial agents. Antimicrobial peptides are added to the seed treatment agent. Antimicrobial peptides have the advantages of high antibacterial activity, less resistance to mutations, and good thermal stability. They have strong killing effects on some fungi, protozoa, and viruses. The wood vinegar is added to the seed treatment agent, and the wood vinegar has the functions of sterilization, disinfection and insect repelling because it contains many phenolic substances. Soaking the cowpea seeds with the cowpea seed treatment agent can effectively kill fungi, bacteria and pests attached to the cowpea seeds without drug resistance. The water-retaining agent is a functional polymer material with particularly strong water absorption capacity. It is non-toxic and harmless. It can release and absorb water repeatedly, and can also absorb fertilizers and pesticides and release them slowly, increasing the fertilizer and drug effects. Covered with polyvinyl alcohol film containing fungicides, insecticides and water-retaining agents. The polyvinyl alcohol film has the advantages of good film formation, fast drying, strong adhesion, and does not affect seed germination. Through the degradation of polyvinyl alcohol With the function of water-retaining agent, the active ingredients such as fungicides and insecticides are slowly released, which can protect cowpea seeds from bacteria, fungi and pests for a long time.

具体实施方式Detailed ways

下面结合具体实施例对本发明做进一步的详细说明,以令本领域技术人员参照说明书文字能够据以实施。The present invention will be further described in detail below in conjunction with specific embodiments, so that those skilled in the art can implement it with reference to the description.

实施例1:Example 1:

一种豇豆种子处理剂,包括以下重量份数的组分:无光触媒0.1份、纳米银0.005份、抗菌肽0.1份、木醋液1份、蔗糖酯0.01份和无菌水70份。A cowpea seed treatment agent comprises the following components in parts by weight: 0.1 part of photocatalyst, 0.005 part of nano silver, 0.1 part of antibacterial peptide, 1 part of wood vinegar, 0.01 part of sucrose ester and 70 parts of sterile water.

所述的豇豆种子处理剂中,所述纳米银的粒径为20nm。In the cowpea seed treatment agent, the particle diameter of the nano-silver is 20nm.

一种豇豆种子的处理方法,包括:A processing method of cowpea seeds, comprising:

步骤一、使用豇豆种子处理剂于30℃下浸泡豇豆种子1h,之后将所述豇豆种子晾干后除去表面水分待用;Step 1, soak the cowpea seeds at 30° C. for 1 hour using the cowpea seed treatment agent, then dry the cowpea seeds and remove the surface moisture for later use;

步骤二、将重量份数为1.0份的聚乙烯醇加入到20份的水中,在室温下充分溶胀1.0h,之后升温到65℃搅拌2.0h至聚乙烯醇完全溶解,冷却至室温后,再向聚乙烯醇水溶液中加入聚丙烯酰胺1份、分散剂1份、50%多菌灵可湿性粉剂0.001份和多杀菌素0.001份,搅拌1.0h,得混合液,将重量份数为0.01份的醇酯十二与所述混合液混合均匀得到混有醇酯十二的聚乙烯醇水溶液,并冷却至30℃,备用;Step 2: Add 1.0 parts by weight of polyvinyl alcohol to 20 parts of water, fully swell at room temperature for 1.0 hours, then raise the temperature to 65°C and stir for 2.0 hours until the polyvinyl alcohol is completely dissolved, cool to room temperature, and then Add 1 part of polyacrylamide, 1 part of dispersant, 0.001 part of 50% carbendazim wettable powder and 0.001 part of spinosad to the aqueous solution of polyvinyl alcohol, stir for 1.0 h to obtain a mixed solution, and the parts by weight are 0.01 parts The alcohol ester twelve is mixed with the mixed solution to obtain a polyvinyl alcohol aqueous solution mixed with alcohol ester twelve, and cooled to 30°C for subsequent use;

步骤三、首先向具有多个连续凹槽的不锈钢模具的凹槽内涂抹二甲基硅油,所述凹槽的规格大于所述豇豆种子的规格,之后将步骤一中处理后的豇豆种子放入所述凹槽中,每个凹槽对应放置一粒豇豆种子,再将步骤二中得到的所述混有醇酯十二的聚乙烯醇水溶液均匀地涂抹在所述豇豆种子表面,于室温下放置10min,使豇豆种子表面形成一层薄膜,最后从所述不锈钢模具上取出豇豆种子,得到表面包覆薄膜的豇豆种子;以及,Step 3, first smear simethicone oil in the groove of the stainless steel mold that has a plurality of continuous grooves, the specification of described groove is greater than the specification of described cowpea seed, put the cowpea seed processed in step one afterwards In the groove, place a cowpea seed correspondingly in each groove, then apply the polyvinyl alcohol aqueous solution mixed with alcohol ester twelve obtained in step 2 to the surface of the cowpea seed evenly, and Place for 10min to form a thin film on the surface of the cowpea seeds, and finally take out the cowpea seeds from the stainless steel mold to obtain the cowpea seeds whose surface is coated with a film; and,

步骤四、将步骤三得到的豇豆种子在2℃下黑暗处理5天,即可进行播种。Step 4: Treat the cowpea seeds obtained in Step 3 in the dark at 2° C. for 5 days before sowing.

所述的豇豆种子的处理方法中,所述步骤一中的豇豆种子与豇豆种子处理剂的质量比为0.5。In the treatment method of described cowpea seeds, the mass ratio of the cowpea seeds in the described step 1 and the treatment agent for cowpea seeds is 0.5.

实施例2:Example 2:

一种豇豆种子处理剂,包括以下重量份数的组分:无光触媒5份、纳米银0.1份、抗菌肽3.5份、木醋液20份、十六烷基三甲基氯化铵0.3份和无菌水80份。A cowpea seed treatment agent, comprising the following components in parts by weight: 5 parts of non-photocatalyst, 0.1 part of nano-silver, 3.5 parts of antibacterial peptide, 20 parts of wood vinegar, 0.3 part of cetyltrimethylammonium chloride and 80 parts of sterile water.

所述的豇豆种子处理剂中,所述纳米银的粒径为50nm。In the cowpea seed treatment agent, the particle diameter of the nano-silver is 50nm.

一种豇豆种子的处理方法,包括:A processing method of cowpea seeds, comprising:

步骤一、使用豇豆种子处理剂于40℃下浸泡豇豆种子6h,之后将所述豇豆种子晾干后除去表面水分待用;Step 1, soak the cowpea seeds at 40° C. for 6 hours using the cowpea seed treatment agent, then dry the cowpea seeds and remove the surface moisture for later use;

步骤二、将重量份数为10份的聚乙烯醇加入到50份的水中,在室温下充分溶胀2.0h,之后升温到95℃搅拌4.0h至聚乙烯醇完全溶解,冷却至室温后,再向聚乙烯醇水溶液中加入聚丙烯酸铵10份、分散剂2份、50%多菌灵可湿性粉剂3.0份和多杀菌素3.0份,搅拌2.0h,得混合液,将重量份数为0.1份的醇酯十二与所述混合液混合均匀得到混有醇酯十二的聚乙烯醇水溶液,并冷却至35℃,备用;Step 2: Add 10 parts by weight of polyvinyl alcohol to 50 parts of water, fully swell at room temperature for 2.0 hours, then raise the temperature to 95°C and stir for 4.0 hours until the polyvinyl alcohol is completely dissolved, cool to room temperature, and then Add 10 parts of ammonium polyacrylate, 2 parts of dispersant, 3.0 parts of 50% carbendazim wettable powder and 3.0 parts of spinosad to the polyvinyl alcohol aqueous solution, stir for 2.0 hours to obtain a mixed solution, and the parts by weight are 0.1 parts The alcohol ester twelve is mixed with the mixed solution to obtain a polyvinyl alcohol aqueous solution mixed with alcohol ester twelve, and cooled to 35 ° C for subsequent use;

步骤三、首先向具有多个连续凹槽的不锈钢模具的凹槽内涂抹二甲基硅油,所述凹槽的规格大于所述豇豆种子的规格,之后将步骤一中处理后的豇豆种子放入所述凹槽中,每个凹槽对应放置一粒豇豆种子,再将步骤二中得到的所述混有醇酯十二的聚乙烯醇水溶液均匀地涂抹在所述豇豆种子表面,于室温下放置120min,使豇豆种子表面形成一层薄膜,最后从所述不锈钢模具上取出豇豆种子,得到表面包覆薄膜的豇豆种子;以及,Step 3, first smear simethicone oil in the groove of the stainless steel mold that has a plurality of continuous grooves, the specification of described groove is greater than the specification of described cowpea seed, put the cowpea seed processed in step one afterwards In the groove, place a cowpea seed correspondingly in each groove, then apply the polyvinyl alcohol aqueous solution mixed with alcohol ester twelve obtained in step 2 to the surface of the cowpea seed evenly, and Place it for 120min to form a film on the surface of the cowpea seeds, and finally take out the cowpea seeds from the stainless steel mold to obtain the cowpea seeds with a film-coated surface; and,

步骤四、将步骤三得到的豇豆种子在4℃下黑暗处理7天,即可进行播种。Step 4: Treat the cowpea seeds obtained in Step 3 in the dark at 4° C. for 7 days before sowing.

所述的豇豆种子的处理方法中,所述步骤一中的豇豆种子与豇豆种子处理剂的质量比为0.5。In the treatment method of described cowpea seeds, the mass ratio of the cowpea seeds in the described step 1 and the treatment agent for cowpea seeds is 0.5.

实施例3:Example 3:

一种豇豆种子处理剂,包括以下重量份数的组分:无光触媒2.5份、纳米银0.05份、抗菌肽1.8份、木醋液10份、十二烷基二甲基苄基氯化铵0.15份和无菌水75份。A cowpea seed treatment agent, comprising the following components in parts by weight: 2.5 parts of non-photocatalyst, 0.05 part of nano-silver, 1.8 parts of antibacterial peptide, 10 parts of wood vinegar, 0.15 parts of dodecyl dimethyl benzyl ammonium chloride parts and 75 parts of sterile water.

所述的豇豆种子处理剂中,所述纳米银的粒径为35nm。In the cowpea seed treatment agent, the particle diameter of the nano-silver is 35nm.

一种豇豆种子的处理方法,包括:A processing method of cowpea seeds, comprising:

步骤一、使用豇豆种子处理剂于35℃下浸泡豇豆种子3.5h,之后将所述豇豆种子晾干后除去表面水分待用;Step 1, soak the cowpea seeds at 35° C. for 3.5 hours using the cowpea seed treatment agent, then dry the cowpea seeds and remove the surface moisture for later use;

步骤二、将重量份数为5.5份的聚乙烯醇加入到35份的水中,在室温下充分溶胀1.5h,之后升温到80℃搅拌3.0h至聚乙烯醇完全溶解,冷却至室温后,再向聚乙烯醇水溶液中加入聚丙烯酸钾5份、分散剂1.5份、50%多菌灵可湿性粉剂1.5份和多杀菌素1.5份,搅拌1.5h,得混合液,将重量份数为0.05份的醇酯十二与所述混合液混合均匀得到混有醇酯十二的聚乙烯醇水溶液,并冷却至32℃,备用;Step 2: Add 5.5 parts by weight of polyvinyl alcohol to 35 parts of water, fully swell at room temperature for 1.5 hours, then raise the temperature to 80°C and stir for 3.0 hours until the polyvinyl alcohol is completely dissolved, cool to room temperature, and then Add 5 parts of potassium polyacrylate, 1.5 parts of dispersant, 1.5 parts of 50% carbendazim wettable powder and 1.5 parts of spinosad to the aqueous solution of polyvinyl alcohol, stir for 1.5 hours to obtain a mixed solution, and the parts by weight are 0.05 parts The alcohol ester twelve is mixed with the mixed solution evenly to obtain an aqueous solution of polyvinyl alcohol mixed with alcohol ester twelve, and cooled to 32°C for subsequent use;

步骤三、首先向具有多个连续凹槽的不锈钢模具的凹槽内涂抹二甲基硅油,所述凹槽的规格大于所述豇豆种子的规格,之后将步骤一中处理后的豇豆种子放入所述凹槽中,每个凹槽对应放置一粒豇豆种子,再将步骤二中得到的所述混有醇酯十二的聚乙烯醇水溶液均匀地涂抹在所述豇豆种子表面,于室温下放置65min,使豇豆种子表面形成一层薄膜,最后从所述不锈钢模具上取出豇豆种子,得到表面包覆薄膜的豇豆种子;以及,Step 3, first smear simethicone oil in the groove of the stainless steel mold that has a plurality of continuous grooves, the specification of described groove is greater than the specification of described cowpea seed, put the cowpea seed processed in step one afterwards In the groove, place a cowpea seed correspondingly in each groove, then apply the polyvinyl alcohol aqueous solution mixed with alcohol ester twelve obtained in step 2 to the surface of the cowpea seed evenly, and Place for 65min to form a thin film on the surface of the cowpea seeds, and finally take out the cowpea seeds from the stainless steel mold to obtain the cowpea seeds with a film-coated surface; and,

步骤四、将步骤三得到的豇豆种子在3℃下黑暗处理6天,即可进行播种。Step 4: Treat the cowpea seeds obtained in Step 3 in the dark at 3° C. for 6 days before sowing.

所述的豇豆种子的处理方法中,所述步骤一中的豇豆种子与豇豆种子处理剂的质量比为0.5。In the treatment method of described cowpea seeds, the mass ratio of the cowpea seeds in the described step 1 and the treatment agent for cowpea seeds is 0.5.

尽管本发明的实施方案已公开如上,但其并不仅仅限于说明书和实施方式中所列运用,它完全可以被适用于各种适合本发明的领域,对于熟悉本领域的人员而言,可容易地实现另外的修改,因此在不背离权利要求及等同范围所限定的一般概念下,本发明并不限于特定的细节和这里示出与描述的实施例。Although the embodiment of the present invention has been disclosed as above, it is not limited to the use listed in the specification and implementation, it can be applied to various fields suitable for the present invention, and it can be easily understood by those skilled in the art Therefore, the invention is not limited to the specific details and embodiments shown and described herein without departing from the general concept defined by the claims and their equivalents.

Claims (9)

1. a cowpea seed inorganic agent, it is characterized in that, comprise the component of following parts by weight: without photocatalyst 0.1-5 part, Nano Silver 0.005-0.1 part, antibacterial peptide 0.1-3.5 part, pyroligneous liquor 1-20 part, surfactant 0.01-0.3 part and sterile water 70-80 part.
2. cowpea seed inorganic agent as claimed in claim 1, is characterized in that, described surfactant is any one or a few in sucrose ester, hexadecyltrimethylammonium chloride and dodecyl benzyl dimethyl ammonium chloride.
3. cowpea seed inorganic agent as claimed in claim 1, it is characterized in that, the particle diameter of described Nano Silver is 20-50nm.
4. a processing method for cowpea seed, is characterized in that, comprising:
Step one, use cowpea seed inorganic agent soak cowpea seed 1-6h at 30-40 DEG C, afterwards described cowpea seed are dried rear removing surface moisture stand-by;
Step 2, be that the polyvinyl alcohol of 1-10 part joins in the water of 20-50 part by parts by weight, at room temperature abundant swelling 1.0-2.0h, be warmed up to 65-95 DEG C of stirring 2.0-4.0h afterwards to dissolve completely to polyvinyl alcohol, after being cooled to room temperature, water-loss reducer 1-10 part is added again in polyvinyl alcohol water solution, dispersant 1-2 part, 50% carbendazol wettable powder 0.001-3.0 part and pleocidin 0.001-3.0 part, stir 1.0-2.0h, obtain mixed liquor, be that the coalescents of 0.01-0.1 part mixes with described mixed liquor the polyvinyl alcohol water solution obtaining being mixed with coalescents by parts by weight, and be cooled to 30-35 DEG C, for subsequent use,
Step 3, first to have multiple continuous groove stainless steel mould groove in smearing release agent, the specification of described groove is greater than the specification of described cowpea seed, afterwards the cowpea seed after process in step one is put into described groove, each groove correspondence places a cowpea seed, again the polyvinyl alcohol water solution being mixed with coalescents described in obtaining in step 2 is spread upon described cowpea seed surface equably, 10-120min is put in ambient temperatare, cowpea seed surface is made to form thin film, finally take out cowpea seed from described stainless steel mould, obtain the cowpea seed of Surface coating film, and,
Step 4, the cowpea seed dark processing 5-7 days at 2-4 DEG C step 3 obtained, can sow.
5. the processing method of cowpea seed as claimed in claim 4, it is characterized in that, the cowpea seed inorganic agent in described step one is made up of the component of following parts by weight: without photocatalyst 2.5 parts, Nano Silver 0.05 part, antibacterial peptide 1.8 parts, 10.5 parts, pyroligneous liquor, 0.15 part, surfactant and sterile water 75 parts.
6. the processing method of cowpea seed as claimed in claim 4, it is characterized in that, the mass ratio of the cowpea seed in described step one and cowpea seed inorganic agent is 0.5.
7. the processing method of cowpea seed as claimed in claim 4, is characterized in that, described water-loss reducer is any one or a few in polyacrylamide, ammonium polyacrylate and polyacrylic acid potassium.
8. the processing method of cowpea seed as claimed in claim 4, it is characterized in that, described releasing agent is dimethicone.
9. the processing method of cowpea seed as claimed in claim 4, it is characterized in that, described coalescents is alcohol ester 12.
CN201510167298.XA 2015-04-10 2015-04-10 A kind of cowpea seed inorganic agent and its processing method Expired - Fee Related CN104839222B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201510167298.XA CN104839222B (en) 2015-04-10 2015-04-10 A kind of cowpea seed inorganic agent and its processing method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201510167298.XA CN104839222B (en) 2015-04-10 2015-04-10 A kind of cowpea seed inorganic agent and its processing method

Publications (2)

Publication Number Publication Date
CN104839222A true CN104839222A (en) 2015-08-19
CN104839222B CN104839222B (en) 2018-03-09

Family

ID=53839527

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201510167298.XA Expired - Fee Related CN104839222B (en) 2015-04-10 2015-04-10 A kind of cowpea seed inorganic agent and its processing method

Country Status (1)

Country Link
CN (1) CN104839222B (en)

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105145558A (en) * 2015-09-02 2015-12-16 常州市长宇实用气体有限公司 Preparation method of self-degraded coated chlordane pesticide
CN108218594A (en) * 2018-04-16 2018-06-29 王智德 A kind of synergy volume increase anti-cure the disease antidote fertilizer freeze injury plant source traditional Chinese medicine fertilizer and preparation method
CN108260600A (en) * 2016-12-30 2018-07-10 党永富 Crop seed coat agent side effect prevention and control auxiliary agent and its application
CN108902187A (en) * 2018-06-29 2018-11-30 来安县杭姑娘生态农业有限公司 A kind of organic vegetable seed treatment
CN110809940A (en) * 2019-10-17 2020-02-21 常德市农林科学研究院 Method for prolonging storage time of cowpea seeds
CN110999923A (en) * 2019-12-09 2020-04-14 北京绿昇原生物科技有限公司 Targeted defense seed coating biological agent and preparation method thereof
CN111727688A (en) * 2020-07-16 2020-10-02 榆林市农业科学研究院 High-temperature sterilization method for mung bean seeds
CN111978178A (en) * 2020-07-24 2020-11-24 润泰化学(泰兴)有限公司 Preparation method of auxiliary film forming agent, film forming composition and preparation method of film forming composition
CN117397698A (en) * 2023-12-15 2024-01-16 中国农业大学 Wood vinegar antibacterial agent containing nano silver particles and preparation method and application thereof

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101049109A (en) * 2006-04-05 2007-10-10 东北农业大学 Nuisance free coating agent for seeds and preparation method
CN103478168A (en) * 2013-07-02 2014-01-01 江苏希旺农业科技有限公司 Disinfectants for matrix of organic vegetable
CN103664316A (en) * 2012-09-13 2014-03-26 何诚慧 Seed coating and preparation method thereof
CN104255816A (en) * 2014-09-03 2015-01-07 青岛锦绣水源商贸有限公司 Non-polluted antibacterial peptide biopesticide

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101049109A (en) * 2006-04-05 2007-10-10 东北农业大学 Nuisance free coating agent for seeds and preparation method
CN103664316A (en) * 2012-09-13 2014-03-26 何诚慧 Seed coating and preparation method thereof
CN103478168A (en) * 2013-07-02 2014-01-01 江苏希旺农业科技有限公司 Disinfectants for matrix of organic vegetable
CN104255816A (en) * 2014-09-03 2015-01-07 青岛锦绣水源商贸有限公司 Non-polluted antibacterial peptide biopesticide

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
应芳卿等: "豇豆制种技术", 《现代农业科技》 *
徐汉虹: "《农药剂型与加工配制》", 31 December 1997, 广东科技出版社 *

Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105145558A (en) * 2015-09-02 2015-12-16 常州市长宇实用气体有限公司 Preparation method of self-degraded coated chlordane pesticide
CN108260600A (en) * 2016-12-30 2018-07-10 党永富 Crop seed coat agent side effect prevention and control auxiliary agent and its application
CN108260600B (en) * 2016-12-30 2020-08-11 党永富 Crop seed coating agent side effect prevention and control auxiliary agent and application thereof
CN108218594A (en) * 2018-04-16 2018-06-29 王智德 A kind of synergy volume increase anti-cure the disease antidote fertilizer freeze injury plant source traditional Chinese medicine fertilizer and preparation method
CN108902187A (en) * 2018-06-29 2018-11-30 来安县杭姑娘生态农业有限公司 A kind of organic vegetable seed treatment
CN110809940A (en) * 2019-10-17 2020-02-21 常德市农林科学研究院 Method for prolonging storage time of cowpea seeds
CN110999923A (en) * 2019-12-09 2020-04-14 北京绿昇原生物科技有限公司 Targeted defense seed coating biological agent and preparation method thereof
CN111727688A (en) * 2020-07-16 2020-10-02 榆林市农业科学研究院 High-temperature sterilization method for mung bean seeds
CN111978178A (en) * 2020-07-24 2020-11-24 润泰化学(泰兴)有限公司 Preparation method of auxiliary film forming agent, film forming composition and preparation method of film forming composition
CN117397698A (en) * 2023-12-15 2024-01-16 中国农业大学 Wood vinegar antibacterial agent containing nano silver particles and preparation method and application thereof

Also Published As

Publication number Publication date
CN104839222B (en) 2018-03-09

Similar Documents

Publication Publication Date Title
CN104839222B (en) A kind of cowpea seed inorganic agent and its processing method
CN104336105B (en) Traditional Chinese medicine type crop seed-dressing agent and using method and application thereof
CN101455213B (en) Konjac seed-coating agent and preparation method thereof and coating method
CN106554781A (en) A kind of long-acting slow-release soil disinfection conditioner
CN100479661C (en) Environment-protective crop alimentary bacteriocide and application thereof
CN111296466B (en) A kind of coating dry preparation for preventing and controlling fruit tree seedling-borne diseases and insect pests and its preparation method and application
CN117247303A (en) Pesticide fertilizer composition with weeding effect and preparation method thereof
CN104273123A (en) Seedling-stage insect-prevention seed soaking solution for organically producing corns and gramineae grains and preparation method
US7368121B2 (en) Process for controlling moss and liverwort
CN105475356B (en) A kind of composition pesticide containing Propineb and prochloraz-manganese chloride complex
CN105248468A (en) Bactericide for preventing and controlling Red Fuji apple ring spot
CN105053023A (en) Seed treating agent by using microorganisms
CN102108033B (en) Chitin iodine aqua
CN106508927A (en) Ternary compound suspended seed coating agent
CN105165897A (en) High-temperature and high-humidity-resistant seed coating agent for efficiently preventing and treating rape plasmodiophora brassicae and preparation method therefor
CN104996469A (en) Composition for seed processing
CN104472507B (en) A kind of Bactericide composition preventing and treating soil-borne disease
CN105830577A (en) High-germination capacity disease-resistant corn seed treatment method
CN108522529B (en) Preparation method and application of allyl isothiocyanate sustained-release granules taking zeolite as carrier
CN109699665B (en) Seed coating agent containing captan and application thereof
CN102659471A (en) Mycelium drought-resistant seed coating and preparation method thereof
RU2292131C1 (en) Method for presowing seed treatment
CN1311749C (en) Method for preparing strong anti-biosis, multi-functional agricultural chemical prepn. used for ocean living things
CN101810191B (en) Soil disinfectant for preventing and controlling root rot of radix pseudo-ginseng and using method
JPWO2019004252A1 (en) Control method of potato cyst nematodes

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
EXSB Decision made by sipo to initiate substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant
TR01 Transfer of patent right

Effective date of registration: 20240218

Address after: 315012 room 1025, Liyuan North Road, Haishu District, Ningbo, Zhejiang, China, 755

Patentee after: Ningbo yuanzhicube Energy Technology Co.,Ltd.

Country or region after: China

Address before: No. 22, Branch 3, Beida Road, Pingxiang City, Guangxi Zhuang Autonomous Region, 532699

Patentee before: Wei Yongliang

Country or region before: China

TR01 Transfer of patent right
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20180309

CF01 Termination of patent right due to non-payment of annual fee