[go: up one dir, main page]

CN104721121A - Skin care type cosmetic - Google Patents

Skin care type cosmetic Download PDF

Info

Publication number
CN104721121A
CN104721121A CN201510146755.7A CN201510146755A CN104721121A CN 104721121 A CN104721121 A CN 104721121A CN 201510146755 A CN201510146755 A CN 201510146755A CN 104721121 A CN104721121 A CN 104721121A
Authority
CN
China
Prior art keywords
extract
cactus
papaya
skin care
supernatant
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201510146755.7A
Other languages
Chinese (zh)
Other versions
CN104721121B (en
Inventor
袁珂
王广华
杨中汉
牛英鹏
贾姗姗
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shanghai Aiying Health Technology Co ltd
Original Assignee
Jiyang College of Zhejiang A&F University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Jiyang College of Zhejiang A&F University filed Critical Jiyang College of Zhejiang A&F University
Priority to CN201510146755.7A priority Critical patent/CN104721121B/en
Publication of CN104721121A publication Critical patent/CN104721121A/en
Application granted granted Critical
Publication of CN104721121B publication Critical patent/CN104721121B/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Cosmetics (AREA)

Abstract

The invention relates to a skin care type cosmetic and belongs to the technical field of cosmetics. The skin care type cosmetic is prepared from a common floweringquince fruit extract, a common jasminorange leaf and twig and pomelo peel extract, cholla stem mucilage polysaccharides, okra pectin and royal jelly according to the weight ratio of (10-20): (20-40): (10-40): (10-30): (10-20). The skin care type cosmetic provided by the invention has reasonable mixture ratio of components and shows good synergy and excellent effects in the aspects of improving skin wrinkles, resisting oxidation, resisting radiation, clearing free radicals, weakening color spots and decomposing melanin.

Description

一种护肤类化妆品skin care cosmetics

技术领域 technical field

本发明属于化妆品技术领域,具体为一种护肤类化妆品。 The invention belongs to the technical field of cosmetics, in particular to a skin care cosmetic.

背景技术 Background technique

化妆品及护肤品对人类的美化和护肤起着重要的作用,美容已经成为21世纪十大热门行业之一。在经济快速发展的过程中,中国的化妆品市场从小到大,从弱到强,品牌是层出不穷,目前中国的化妆品市场已经成为全球最大的市场。伴随着国内消费者对化妆品等日化行业的认知与熟悉,越来越多的消费者对安全、健康、有效的护理方法更加关注,尤其是植物草本类护肤品的出现,进一步促进了化妆品行业的快速发展。我国拥有丰富的中草药资源,因此天然植物类的化妆品今后将会具有更大的发展潜力和市场空间。天然化妆品是从天然植物中提取出来的,能对人体的皮肤起到营养保护和养颜等作用,又不会对皮肤造成刺激性损伤的功能成分。因此从植物中提取天然成分的植物性化妆品是相对科学和环保的方法。 Cosmetics and skin care products play an important role in human beautification and skin care, and beauty has become one of the top ten hot industries in the 21st century. In the process of rapid economic development, China's cosmetics market has grown from small to large, from weak to strong, and brands have emerged in an endless stream. At present, China's cosmetics market has become the largest market in the world. Along with domestic consumers' awareness and familiarity with cosmetics and other daily chemical industries, more and more consumers pay more attention to safe, healthy and effective care methods, especially the emergence of herbal skin care products, which further promotes the cosmetics market. The rapid development of the industry. my country is rich in Chinese herbal medicine resources, so natural plant cosmetics will have greater development potential and market space in the future. Natural cosmetics are functional ingredients extracted from natural plants, which can provide nutrition, protection and beauty to the skin of the human body without causing irritating damage to the skin. Therefore, botanical cosmetics that extract natural ingredients from plants are a relatively scientific and environmentally friendly method.

发明内容 Contents of the invention

针对现有技术中存在的上述问题,本发明的目的在于设计提供一种护肤类化妆品的技术方案,其组分配比合理,在改善皮肤皱纹、抗氧化防辐射、清除自由基、淡化色斑、分解黑色素方面显示出良好的协同作用和优异的功效。 In view of the above-mentioned problems existing in the prior art, the object of the present invention is to design and provide a technical scheme of skin care cosmetics, which has a reasonable component ratio and can improve skin wrinkles, anti-oxidation and radiation protection, scavenge free radicals, dilute pigmentation, It shows good synergy and excellent efficacy in decomposing melanin.

所述的一种护肤类化妆品,其特征在于由木瓜提取物、九里香和柚子皮提取物、仙人掌粘液多糖、黄秋葵果胶、蜂王浆按照重量比10-20 : 20-40 : 10-40 : 10-30 : 10-20的比例制成; The skin care cosmetic is characterized in that it consists of papaya extract, mulberry and pomelo peel extracts, cactus mucus polysaccharide, okra pectin, and royal jelly in a weight ratio of 10-20 : 20-40 : 10-40 : 10 -30 : Made with a ratio of 10-20;

所述的木瓜提取物采用以下方法制备:将木瓜切片后低温烘干,将干燥后的木瓜片置破碎提取器的容器中,按照木瓜重量1kg则含水乙醇5-8升的比例加入60%-80%含水乙醇进行破碎提取1-2次,每次提取时间为1-3分钟,将提取液抽滤,弃去滤渣,合并得到的提取液在70℃以下采用真空薄膜浓缩装置进行闪蒸浓缩至原体积的1/6-1/10,继续将浓缩液进行真空干燥成干粉,用研钵研细后得到木瓜提取物干粉; The papaya extract is prepared by the following method: slice the papaya and dry it at low temperature, place the dried papaya slices in a container of a crushing extractor, add 60%- 80% water-containing ethanol is crushed and extracted 1-2 times, each extraction time is 1-3 minutes, the extract is filtered with suction, the filter residue is discarded, and the combined extract is flashed and concentrated below 70°C using a vacuum thin film concentration device To 1/6-1/10 of the original volume, continue to vacuum-dry the concentrated solution into a dry powder, and grind it with a mortar to obtain a dry powder of papaya extract;

所述的九里香和柚子皮提取物采用以下方法制备:取干燥的九里香叶和干燥的柚子果皮,按照重量比1:1-2混合,然后置破碎提取器的容器中,按照原料重量1kg则含水乙醇6-8升的比例加入70%-100%乙醇进行破碎提取2-3次,每次提取时间为1-4分钟,将提取液抽滤,弃去滤渣,合并得到的提取液在60℃以下采用真空薄膜浓缩装置进行闪蒸浓缩至原体积的1/7-1/9,继续将浓缩液进行真空干燥成干粉,用研钵研细后得九里香和柚子皮提取物干粉; The described extract of mulberry and pomelo peel is prepared by the following method: take dried mulberry leaves and dried pomelo peel, mix them according to the weight ratio of 1:1-2, and then put them in the container of the crushing extractor, and mix them according to the weight of raw materials 1kg Then add 70%-100% ethanol to the ratio of 6-8 liters of aqueous ethanol to carry out crushing and extraction 2-3 times, each extraction time is 1-4 minutes, the extract is filtered with suction, the filter residue is discarded, and the combined extract is obtained in Below 60°C, use a vacuum thin film concentration device to flash concentrate to 1/7-1/9 of the original volume, continue to vacuum-dry the concentrated solution into a dry powder, and use a mortar to grind it finely to obtain a dry powder of Murata and pomelo peel extract;

所述的仙人掌粘液多糖采用以下方法制备:取新鲜的仙人掌洗净,除刺去皮,切成小块,称重,置破碎提取器的容器中,加入仙人掌鲜重4-8倍量的蒸馏水,进行高速搅拌破碎1-3分钟,将破碎后的仙人掌粘浆转移出,进行高速离心分离,取上清液,将上清液进行减压浓缩至原体积的1/3-1/6,加入无水乙醇,边加边搅拌,1-4℃下静止醇析,高速离心分离,弃去上清液,沉淀物低温干燥后,得到仙人掌粘液多糖; The described cactus mucus polysaccharide is prepared by the following method: take fresh cactus, wash, remove thorns and peel, cut into small pieces, weigh them, put them in a container of a broken extractor, and add distilled water of 4-8 times the fresh weight of the cactus , perform high-speed stirring and crushing for 1-3 minutes, transfer the crushed cactus slime, perform high-speed centrifugation, take the supernatant, and concentrate the supernatant under reduced pressure to 1/3-1/6 of the original volume, Add absolute ethanol, stir while adding, static alcohol analysis at 1-4°C, high-speed centrifugation, discard the supernatant, and dry the precipitate at low temperature to obtain cactus mucus polysaccharide;

所述的黄秋葵果胶采用以下方法制备:取洗净晾干的黄秋葵嫩果,以横段面切片后低温烘干,将烘干后的黄秋葵果实置于提取容器中,按照原料重量为1kg则蒸馏水的用量为6-10升的比例加入蒸馏水煎煮提取2-3次,每次30-90分钟,进行高速离心分离,取上清液;得到的上清液在60-70℃条件下采用真空薄膜浓缩装置进行闪蒸浓缩至原体积的1/6-1/10,然后向浓缩液中加入92-95%的乙醇,使得含醇量达到80%,1-4℃以下静止醇析,出现大量的沉淀,高速离心分离,弃去上清液,收集沉淀物,40℃-50℃烘干,得到黄秋葵果胶。 The described okra pectin is prepared by the following method: take the tender okra fruit that has been washed and dried, slice it in cross-section and then dry it at low temperature, place the dried okra fruit in an extraction container, and take the okra fruit according to the weight of the raw material as 1kg. The amount of distilled water is 6-10 liters, add distilled water to decoct and extract 2-3 times, each time for 30-90 minutes, carry out high-speed centrifugation, and take the supernatant; the obtained supernatant is used at 60-70°C The vacuum thin film concentrating device performs flash evaporation and concentration to 1/6-1/10 of the original volume, and then adds 92-95% ethanol to the concentrated solution to make the alcohol content reach 80%, and static alcohol analysis below 1-4°C, When a large amount of precipitation occurs, it is centrifuged at a high speed, the supernatant is discarded, the precipitate is collected, and dried at 40° C. to 50° C. to obtain okra pectin.

所述的一种护肤类化妆品,其特征在于木瓜提取物、九里香和柚子皮提取物、仙人掌粘液多糖、黄秋葵果胶、蜂王浆的重量比为12-18 : 25-35 : 15-35 : 15-25 : 12-18。 The skin care cosmetic is characterized in that the weight ratio of papaya extract, mulberry and pomelo peel extract, cactus mucus polysaccharide, okra pectin, and royal jelly is 12-18 : 25-35 : 15-35 : 15 -25 : 12-18.

所述的一种护肤类化妆品,其特征在于木瓜提取物、九里香和柚子皮提取物、仙人掌粘液多糖、黄秋葵果胶、蜂王浆的重量比为14-16 : 28-32 : 18-30 : 18-22 : 15-16。 The skin care cosmetic is characterized in that the weight ratio of papaya extract, mulberry and pomelo peel extracts, cactus mucus polysaccharide, okra pectin, and royal jelly is 14-16 : 28-32 : 18-30 : 18 -22 : 15-16.

所述的一种护肤类化妆品,其特征在于所述木瓜提取物的制备方法中:按照木瓜重量1kg则含水乙醇6-7升的比例加入65%-75%含水乙醇进行破碎提取1次,每次提取时间为2分钟,闪蒸浓缩至原体积的1/7-1/9。 The skin care cosmetic is characterized in that in the preparation method of the papaya extract: according to the weight of papaya 1kg, the ratio of 6-7 liters of hydrous ethanol is added to 65%-75% hydrous ethanol for crushing and extraction once, every The extraction time is 2 minutes, and the flash concentration is 1/7-1/9 of the original volume.

所述的一种护肤类化妆品,其特征在于所述九里香和柚子皮提取物提取物的制备方法中:九里香叶和干燥的柚子果皮的重量比1:1.5混合,按照原料重量1kg则含水乙醇7升的比例加入80%-90%乙醇进行破碎提取,每次提取时间为2-3分钟,提取液闪蒸浓缩至原体积的1/8。 The described skin care cosmetic is characterized in that in the preparation method of the extract of mulberry and pomelo peel extract: the weight ratio of mulberry leaves and dried pomelo peel is mixed at 1:1.5, and the water content is 1kg according to the weight of raw materials. The ratio of 7 liters of ethanol is added with 80%-90% ethanol for crushing and extraction, and the extraction time is 2-3 minutes each time, and the extract is flash concentrated to 1/8 of the original volume.

所述的一种护肤类化妆品,其特征在于所述仙人掌粘液多糖的制备方法中:加入仙人掌鲜重5-7倍量的蒸馏水,进行高速搅拌破碎2分钟,将上清液进行减压浓缩至原体积的1/4-1/5。 The skin care cosmetic is characterized in that in the preparation method of the cactus mucus polysaccharide: add distilled water in an amount 5-7 times the fresh weight of the cactus, perform high-speed stirring and crushing for 2 minutes, and concentrate the supernatant under reduced pressure to 1/4-1/5 of the original volume.

所述的一种护肤类化妆品,其特征在于所述黄秋葵果胶的制备方法中:按照原料重量为1kg则蒸馏水的用量为7-9升的比例加入蒸馏水煎煮提取,每次50-60分钟,上清液闪蒸浓缩至原体积的1/7-1/9,42℃-45℃烘干,得到黄秋葵果胶。 The skin care cosmetic is characterized in that in the preparation method of the okra pectin: according to the weight of the raw material being 1 kg, the amount of distilled water is 7-9 liters, adding distilled water and decocting for extraction, each time for 50-60 minutes , the supernatant is concentrated by flash evaporation to 1/7-1/9 of the original volume, and dried at 42°C-45°C to obtain okra pectin.

木瓜为蔷薇科植物贴梗海棠的干燥近成熟果实。夏、秋二季果实绿黄时采收,置沸水中烫至外皮灰白色,对半纵剖,晒干。木瓜性温、味酸,入肝、脾经; 具有健脾消食、抗疫杀虫、通乳抗癌、清热祛风的功效;主治胃痛,消化不良,肺热干咳,乳汁不通,湿疹,寄生虫病,抗痉挛、手脚痉挛疼痛等病症。木瓜中含有大量水分、碳水化合物、蛋白质、脂肪、多种维生素及多种人体必需的氨基酸,可有效补充人体的养分,增强机体的抗病能力。 Papaya is the dry and near-ripe fruit of the Rosaceae plant Begonia stalk. Harvest when the fruit is green and yellow in summer and autumn, scald in boiling water until the outer skin is off-white, cut in half longitudinally, and dry in the sun. Papaya is warm in nature, sour in taste, and enters the liver and spleen meridians; it has the effects of invigorating the spleen and eliminating food, anti-epidemic and killing insects, promoting milk and anti-cancer, clearing away heat and expelling wind; Insect disease, anti-spasm, spasm and pain in hands and feet and other diseases. Papaya contains a lot of water, carbohydrates, protein, fat, multivitamins and a variety of essential amino acids, which can effectively supplement the body's nutrients and enhance the body's disease resistance.

九里香为芸香科九里香属常绿灌木植物,又称九秋香、九树香、千里香、万里香、过山香,有时可长成小乔木样,株姿优美,枝叶秀丽,花香浓郁。根、茎、叶所含化学成分与千里香类同,产自福建、广东、海南、广西等南部。常见于离海岸不远的平地、缓坡、小丘的灌木丛中。九里香叶含多种香豆精类化合物,如九里香甲素、九里香乙素、九里香丙素,长叶九里香醛,另含黄酮类、氨基酸,另含挥发油,为芳香类植物,具有散瘀止痛;解毒消肿的作用,主治风湿骨痛,胃痛,牙痛,破伤风,跌扑肿痛;疮痈;蛇虫咬伤。用于胃痛,风湿痹痛;外治牙痛,跌扑肿痛,虫蛇咬伤。 Jiulixiang is an evergreen shrub of Rutaceae, also known as Jiuqiuxiang, Jiushuxiang, Qianlixiang, Wanlixiang, and Guoshanxiang. Sometimes it can grow into a small tree, with beautiful plant posture, beautiful branches and leaves, and strong floral fragrance. The chemical components contained in the roots, stems, and leaves are similar to those of Thyme, and they are produced in southern Fujian, Guangdong, Hainan, and Guangxi. Commonly found in bushes on flat land, gentle slopes, and hills not far from the coast. Jiulixiang leaves contain a variety of coumarin compounds, such as Jiulixiang A, Jiulixiang B, Jiulixiang C, Longye Jiulixiang aldehyde, flavonoids, amino acids, and volatile oil. It is an aromatic plant. Have dissipating blood stasis to relieve pain; The effect of detoxification and detumescence, mainly cures rheumatic bone pain, stomachache, toothache, tetanus, swelling and pain from tumbling, sore and carbuncle; Snake and insect bites. For stomachache, rheumatic arthralgia; external treatment of toothache, tumbling and swelling, insect bites.

柚子又名文旦,外皮很厚,大多在10-11月采摘。柚子多生长于南方,以福建、厦门所产柚子最为著名。其果实鲜食甘酸可口,沁人心脾,令人赞不绝口,柚子皮具有很高的药用价值和食用价值。且可入药,柚子皮性温,味苦、辛,柚子皮中含有黄酮类、挥发油等成分,具有散寒理气,燥湿化痰,润肠通便、降低血液粘稠度、预防脑中风、散寒燥湿等方面的作用。 Grapefruit, also known as Wendan, has a thick skin and is mostly picked in October-November. Most grapefruits grow in the south, and the grapefruits produced in Fujian and Xiamen are the most famous. Its fresh fruit is sweet and sour, delicious, refreshing, and it is full of praise. Grapefruit peel has high medicinal value and edible value. And it can be used as medicine. Grapefruit peel is warm, bitter and pungent. Grapefruit peel contains flavonoids, volatile oil and other ingredients. The effect of expelling cold and drying dampness, etc.

仙人掌含丰富的蛋白质、维生素、胡萝卜素、l0多种矿物质和l8种氨基酸,人体所必须的氨基酸几乎都在其中,还含有机酸类、糖类、黄酮类、生物碱类、甾醇类、萜类等具有较强药理作用的化学成分。仙人掌具有极强的清除自由基抗衰老能力。仙人掌多糖具有明显的降血糖,增强免疫功能。自我保护和抗辐射等功能和作用。仙人掌含有三萜皂甙,能直接调节人体分泌机能和调节脂肪酶的活性,促进多余脂肪迅速分解降至正常,并能有效的阻止脂肪在肠道吸收,抑制脂肪在肝内合成,对抗胆固醇、血管内壁的沉积,循序渐进的减轻体重,不但不损伤元气、反而补充营养、增加人体精力。仙人掌中的粘液多糖包括粘液质、果胶、阿拉伯半乳聚糖等杂聚多糖、纤维素、及淀粉等,仙人掌中的粘液多糖具有清热、解毒、保湿、防晒之功效。 Cactus is rich in protein, vitamins, carotene, more than 10 kinds of minerals and 18 kinds of amino acids, almost all of which are necessary for the human body, and also contains organic acids, sugars, flavonoids, alkaloids, sterols, Terpenoids and other chemical components with strong pharmacological effects. Cactus has a strong anti-aging ability to scavenge free radicals. Cactus polysaccharides can significantly lower blood sugar and enhance immune function. Functions and functions such as self-protection and anti-radiation. Cactus contains triterpene saponins, which can directly regulate the secretion function of the human body and the activity of lipase, promote the rapid decomposition of excess fat to normal, and can effectively prevent the absorption of fat in the intestine, inhibit the synthesis of fat in the liver, and fight against cholesterol, blood vessels The deposition on the inner wall can reduce weight step by step, not only does not damage the vitality, but instead supplements nutrition and increases the energy of the human body. The mucus polysaccharides in cactus include mucus, pectin, heteropolysaccharides such as arabinogalactan, cellulose, and starch, etc. The mucus polysaccharides in cactus have the functions of clearing away heat, detoxifying, moisturizing and sun protection.

黄秋葵为一年生草本植物,在我国南北方各地均有黄秋葵的种植。黄秋葵中富含蛋白质、脂肪、维生素、矿物质、膳食纤维、黄酮、果胶、多糖等功效成分,特别是黄秋葵的嫩果中富含的粘液状物质,是由多聚半乳糖、半乳聚糖和阿拉伯聚糖与果胶的混合物,其中果胶是一种可溶性纤维,它能促进体内有机物质的排泄,减少毒素的积累,降低血糖和胆固醇的含量。黏滑汁液能帮助消化,防止便秘。具有癌抗癌、补肾壮阳、增强免疫力、助消化等作用,同时黄秋葵中的水溶性纤维果胶对皮肤具有很好的保健作用,黄秋葵果胶还具有独特的美容养颜、增加皮肤弹性和延缓衰老、祛除皮肤褐斑及美白作用。 Okra is an annual herbaceous plant, which is planted all over the north and south of my country. Okra is rich in protein, fat, vitamins, minerals, dietary fiber, flavonoids, pectin, polysaccharides and other functional ingredients, especially the mucus-like substance rich in the tender fruit of okra, which is composed of polygalactose, galactose A mixture of sugar and arabinan and pectin, which is a soluble fiber that can promote the excretion of organic substances in the body, reduce the accumulation of toxins, and lower blood sugar and cholesterol levels. The slimy juice helps digestion and prevents constipation. It has the functions of anti-cancer, tonifying kidney and strengthening yang, enhancing immunity, and helping digestion. At the same time, the water-soluble fiber pectin in okra has a good health care effect on the skin. Aging, remove skin brown spots and whitening effect.

上述一种护肤类化妆品,具有以下有益效果: The above-mentioned skin care cosmetic has the following beneficial effects:

1.本发明为纯天然植物来源的植物提取物配方,绿色环保、安全健康;木瓜提取物、九里香和柚子皮提取物、仙人掌粘液多糖、黄秋葵果胶和蜂王浆的同时使用在改善皮肤皱纹、增加皮肤弹性、清除自由基、淡化色斑、分解黑色素方面显示出良好的协同作用和优异的功效远远大于单独使用其中一种的效果。 1. The present invention is a plant extract formula derived from pure natural plants, which is green, environmentally friendly, safe and healthy; the simultaneous use of papaya extract, mulberry and pomelo peel extract, cactus mucus polysaccharide, okra pectin and royal jelly can improve skin wrinkles, It shows a good synergistic effect and excellent efficacy in increasing skin elasticity, scavenging free radicals, lightening spots, and decomposing melanin, which is far greater than the effect of using one of them alone.

2.本发明配方中含有的木瓜提取物和九里香提取物具有一定的防腐杀菌作用,该提取物的加入使该产品具有很好的抗菌防腐作用,保证了微生物指标符合化妆品生产的要求;本发明配方中含有的柚子皮提取物和黄秋葵果胶提取物中含有黄酮类成分,属于天然抗氧剂,无需额外添加抗氧剂就能发挥对自由基的清除作用。 2. The papaya extract and mulberry extract contained in the formula of the present invention have a certain antiseptic and bactericidal effect, and the addition of the extract makes the product have a good antibacterial and antiseptic effect, ensuring that the microbial indicators meet the requirements of cosmetic production; The grapefruit peel extract and okra pectin extract contained in the inventive formula contain flavonoids, which are natural antioxidants, and can scavenge free radicals without adding additional antioxidants.

3.本发明中对木瓜、九里香和柚子皮采用室温破碎提取法提取,即利用高速旋转的特殊刀具将原料破碎剪切至细微颗粒,通过高速搅拌、振动、混合、渗透、浸渍、均质化的结合作用,使药材内部的有效成分快速达到溶出平衡;该提取方法实现了原料粉碎和提取过程的同时完成,省去了药材单独粉碎的过程,破碎提取时间极短,一次提取仅需几分钟,同时提取过程无需加热,避免不耐热成分受热破坏的可能性,最大限度地保留了原有的营养及功效成分,具有提取快速、完全、高效节能,操作简便、工作效率高的优势;获得提取液采用真空薄膜浓缩装置进行闪蒸浓缩具有浓缩液受热温度低,受热时间极短,有效保护热敏性成分不被破坏,溶剂的回收率高,浓缩速度快、效率高,操作简单、使用方便、节能环保等优势。 3. In the present invention, the papaya, mulberry and pomelo peels are extracted by crushing and extracting at room temperature, that is, the raw materials are crushed and sheared into fine particles by using a special cutter rotating at high speed, and then stirred, vibrated, mixed, infiltrated, impregnated, and homogenized The combined effect of chemicalization makes the active ingredients inside the medicinal material quickly reach the dissolution equilibrium; this extraction method realizes the simultaneous completion of the raw material crushing and extraction process, eliminating the need for a separate crushing process of the medicinal material, and the crushing and extraction time is extremely short. At the same time, the extraction process does not require heating, avoiding the possibility of heat-resistant components being damaged by heat, and retaining the original nutrients and functional components to the greatest extent. It has the advantages of fast, complete, high-efficiency and energy-saving extraction, easy operation, and high work efficiency; The extract is obtained by using a vacuum thin film concentration device for flash concentration. The concentrated liquid has a low heating temperature and a very short heating time, which can effectively protect the heat-sensitive components from being destroyed. The recovery rate of the solvent is high, the concentration speed is fast, the efficiency is high, and the operation is simple and convenient. , energy saving and environmental protection and other advantages.

本专利申请中涉及的百分含量除另有说明的外,其余的均为有效成分的纯物质的重量百分含量。 Unless otherwise specified, the percentages involved in this patent application are the weight percentages of pure substances of active ingredients.

具体实施方式 Detailed ways

以下结合具体实施例对本发明作进一步说明。 The present invention will be further described below in conjunction with specific examples.

实施例1 Example 1

该护肤类化妆品由木瓜提取物、九里香和柚子皮提取物、仙人掌粘液多糖、黄秋葵果胶、蜂王浆按照重量比10 : 40 :20 : 20 : 10的比例制成; The skin care cosmetics are made of papaya extract, mulberry and pomelo peel extracts, cactus mucus polysaccharide, okra pectin, and royal jelly in a weight ratio of 10: 40: 20: 20: 10;

木瓜提取物的制备:将木瓜切片后低温烘干,将干燥后的木瓜片置破碎提取器的容器中,加入折合原料重量比8倍量70%含水乙醇进行破碎提取2次,每次提取时间为2分钟,将提取液抽滤,弃去滤渣,合并得到的提取液在70℃以下采用真空薄膜浓缩装置进行闪蒸浓缩至原体积的1/8,继续将浓缩液真空干燥成干粉,用研钵研细后得到木瓜提取物干粉,木瓜提取物收率达到25.9%; Preparation of papaya extract: Slice the papaya and dry it at low temperature, place the dried papaya slices in the container of the crushing extractor, add 70% hydrous ethanol equivalent to 8 times the weight ratio of the raw materials to carry out crushing and extraction twice, each extraction time For 2 minutes, the extract was suction-filtered, and the filter residue was discarded. The combined extract was flash-concentrated to 1/8 of the original volume using a vacuum thin-film concentrator below 70°C, and the concentrate was vacuum-dried to a dry powder. Papaya extract dry powder is obtained after grinding in a mortar, and the yield of papaya extract reaches 25.9%;

九里香和柚子皮提取物的制备:取干燥的九里香叶和干燥的柚子果皮,按照重量比1:1混合,然后置破碎提取器的容器中,加入折合混合原料重量比7倍量95%乙醇进行破碎提取2次,每次提取时间为2分钟,将提取液抽滤,弃去滤渣,合并得到的提取液在60℃以下采用真空薄膜浓缩装置进行闪蒸浓缩至原体积的1/6,继续将浓缩液进行真空干燥成干粉,用研钵研细后得九里香和柚子皮提取物干粉,提取物收率达到18.4%。 Preparation of Jiulixiang and grapefruit peel extract: take dried Jiulixiang leaves and dried grapefruit peel, mix them according to the weight ratio of 1:1, then put them in the container of the broken extractor, add 95% of the amount equivalent to 7 times the weight ratio of the mixed raw materials The ethanol is crushed and extracted twice, each extraction time is 2 minutes, the extract is filtered with suction, the filter residue is discarded, and the combined extract is flashed and concentrated to 1/6 of the original volume by using a vacuum thin film concentration device below 60°C , continue vacuum-drying the concentrated solution into a dry powder, and grind it finely with a mortar to obtain a dry powder of the extract of Murata and pomelo peel, and the yield of the extract reaches 18.4%.

仙人掌粘液多糖的制备:取新鲜的仙人掌洗净,除刺去皮,切成小块,称重,置破碎提取器的容器中,加入仙人掌鲜重6倍量的蒸馏水,进行高速搅拌破碎3分钟,将破碎后的仙人掌粘浆转移出,进行高速离心分离,取上清液。将上清液进行减压浓缩至原体积的1/6,加入无水乙醇,边加边搅拌,4℃以下静止醇析,高速离心分离,弃去上清液,沉淀物低温干燥后,得到仙人掌粘液多糖,仙人掌粘液多糖的收率达到29.6%。 Preparation of cactus mucus polysaccharide: take fresh cactus, wash them, remove thorns and peel, cut into small pieces, weigh them, put them in the container of the broken extractor, add distilled water of 6 times the fresh weight of cactus, and carry out high-speed stirring and crushing for 3 minutes , transfer the crushed cactus slime, perform high-speed centrifugation, and take the supernatant. Concentrate the supernatant under reduced pressure to 1/6 of the original volume, add absolute ethanol, stir while adding, static alcohol analysis below 4°C, high-speed centrifugation, discard the supernatant, and dry the precipitate at low temperature to obtain Cactus mucus polysaccharide, the yield of cactus mucus polysaccharide reaches 29.6%.

黄秋葵果胶的制备:取洗净晾干的黄秋葵嫩果,以横段面切片后低温烘干。将烘干后的黄秋葵果实置于提取容器中,加入蒸馏水煎煮提取3,每次60分钟,按照原料重量为1kg则蒸馏水的用量为8升的比例。进行高速离心分离,取上清液,得到的上清液在70℃条件下采用真空薄膜浓缩装置进行闪蒸浓缩至原体积的1/8,然后向浓缩液中加入95%的乙醇,使得含醇量达到80%,4℃以下静止醇析,出现大量的沉淀,高速离心分离,弃去上清液,收集沉淀物,40℃-50℃烘干,得到黄秋葵果胶,黄秋葵果胶的收率达到33.5%。 Preparation of okra pectin: take washed and dried tender okra fruit, cut into slices and dry at low temperature. Place the dried okra fruit in an extraction container, add distilled water to decoct and extract 3, each time for 60 minutes, according to the proportion of 8 liters of distilled water when the weight of the raw material is 1 kg. Carry out high-speed centrifugation, take the supernatant, and use a vacuum thin-film concentration device to flash-concentrate the obtained supernatant to 1/8 of the original volume at 70°C, and then add 95% ethanol to the concentrated solution to make it contain Alcohol content reaches 80%, static alcohol analysis below 4°C, a large amount of precipitation appears, high-speed centrifugation, discard the supernatant, collect the precipitate, dry at 40°C-50°C, and obtain okra pectin, the harvest of okra pectin The rate reached 33.5%.

实施例2 Example 2

该护肤类化妆品由木瓜提取物、九里香和柚子皮提取物、仙人掌粘液多糖、黄秋葵果胶、蜂王浆按照重量比15 :35:20 : 15 : 15的比例制成; The skin care cosmetics are made of papaya extract, mulberry and pomelo peel extracts, cactus mucus polysaccharide, okra pectin, and royal jelly in a weight ratio of 15:35:20:15:15;

木瓜提取物的制备:将木瓜切片后低温烘干。将干燥后的木瓜片置破碎提取器的容器中,加入折合原料重量比5倍量60%含水乙醇进行破碎提取2次,每次提取时间为3分钟,将提取液抽滤,弃去滤渣,合并得到的提取液在70℃以下采用真空薄膜浓缩装置进行闪蒸浓缩至原体积的1/6,继续将浓缩液真空干燥成干粉,用研钵研细后得到木瓜提取物干粉,木瓜提取物收率达到18.4%。 Preparation of papaya extract: Slice papaya and dry it at low temperature. Put the dried papaya slices in the container of the crushing extractor, add 60% hydrous ethanol equivalent to 5 times the weight ratio of raw materials and carry out crushing and extraction for 2 times, each extraction time is 3 minutes, the extract is suction filtered, and the filter residue is discarded. The combined extracts are flash-concentrated to 1/6 of the original volume using a vacuum thin-film concentration device below 70°C, and the concentrated solution is vacuum-dried into a dry powder, and then finely ground with a mortar to obtain a dry powder of papaya extract, papaya extract The yield reached 18.4%.

九里香和柚子皮提取物的制备:取干燥的九里香叶和干燥的柚子果皮,按照重量比1:1混合,然后置破碎提取器的容器中,加入折合混合原料重量比8倍量90%乙醇进行破碎提取3次,每次提取时间为1分钟。将提取液抽滤,弃去滤渣,合并得到的提取液在60℃以下采用真空薄膜浓缩装置进行闪蒸浓缩至原体积的1/8,继续将浓缩液进行真空干燥成干粉,用研钵研细后得九里香和柚子皮提取物干粉,提取物收率达到20.3%。 Preparation of Jiulixiang and grapefruit peel extract: take dried Jiulixiang leaves and dried grapefruit peel, mix them according to the weight ratio of 1:1, then put them into the container of the broken extractor, add 90% of the amount equivalent to 8 times the weight ratio of the mixed raw materials The ethanol was crushed and extracted 3 times, and the extraction time was 1 minute each time. Suction-filter the extract, discard the filter residue, and flash-concentrate the combined extract to 1/8 of the original volume using a vacuum thin-film concentrator below 60°C, and continue vacuum-drying the concentrate to dry powder, and grind it with a mortar and pestle. The dry powder of Jiulixiang and pomelo peel extracts can be obtained after being finely divided, and the yield of the extract can reach 20.3%.

仙人掌粘液多糖的制备:取新鲜的仙人掌洗净,除刺去皮,切成小块,称重,置破碎提取器的容器中,加入仙人掌鲜重7倍量的蒸馏水,进行高速搅拌破碎2分钟,将破碎后的仙人掌粘浆转移出,进行高速离心分离,取上清液,将上清液进行减压浓缩至原体积的1/7,加入无水乙醇,边加边搅拌,4℃以下静止醇析,高速离心分离,弃去上清液,沉淀物低温干燥后,得到仙人掌粘液多糖,仙人掌粘液多糖的收率达到28.4%-37.8%。 Preparation of cactus mucus polysaccharide: take fresh cactus, wash them, remove thorns and peel them, cut them into small pieces, weigh them, put them in the container of the crushing extractor, add distilled water of 7 times the fresh weight of cactus, and carry out high-speed stirring and crushing for 2 minutes , transfer the crushed cactus slime, perform high-speed centrifugation, take the supernatant, concentrate the supernatant under reduced pressure to 1/7 of the original volume, add absolute ethanol, and stir while adding, below 4°C Static alcohol analysis, high-speed centrifugation, discarding the supernatant, and drying the precipitate at low temperature to obtain the cactus mucus polysaccharide, the yield of the cactus mucus polysaccharide reaches 28.4%-37.8%.

黄秋葵果胶的制备:取洗净晾干的黄秋葵嫩果,以横段面切片后低温烘干。将烘干后的黄秋葵果实置于提取容器中,加入蒸馏水煎煮提取2次,每次90分钟,按照原料重量为1kg则蒸馏水的用量为10升的比例,进行高速离心分离,取上清液,得到的上清液在70℃条件下采用真空薄膜浓缩装置进行闪蒸浓缩至原体积的1/10,然后向浓缩液中加入95%的乙醇,使得含醇量达到80%,4℃以下静止醇析,出现大量的沉淀,高速离心分离,弃去上清液,收集沉淀物,40℃-50℃烘干,得到黄秋葵果胶,黄秋葵果胶的收率达到38.4%。 Preparation of okra pectin: take washed and dried tender okra fruit, cut into slices and dry at low temperature. Put the dried okra fruit in an extraction container, add distilled water to decoct and extract twice, each time for 90 minutes, carry out high-speed centrifugation according to the proportion that the weight of the raw material is 1 kg and the amount of distilled water is 10 liters, and take the supernatant , the obtained supernatant is flash-concentrated to 1/10 of the original volume by using a vacuum thin-film concentration device at 70°C, and then 95% ethanol is added to the concentrated solution to make the alcohol content reach 80%, and the concentration is below 4°C Static ethanol analysis, a large amount of precipitation occurs, high-speed centrifugation, discarding the supernatant, collecting the precipitate, drying at 40°C-50°C to obtain okra pectin, and the yield of okra pectin reaches 38.4%.

实施例3 Example 3

该护肤类化妆品由木瓜提取物、九里香和柚子皮提取物、仙人掌粘液多糖、黄秋葵果胶、蜂王浆按照重量比20 :30:30 : 10 : 10的比例制成; The skin care cosmetics are made of papaya extract, mulberry and pomelo peel extracts, cactus mucus polysaccharide, okra pectin, and royal jelly in a weight ratio of 20:30:30:10:10;

木瓜提取物的制备:将木瓜切片后低温烘干。将干燥后的木瓜片置破碎提取器的容器中,加入折合原料重量比6倍量75%含水乙醇进行破碎提取2次,每次提取时间为3分钟,将提取液抽滤,弃去滤渣,合并得到的提取液在70℃以下采用真空薄膜浓缩装置进行闪蒸浓缩至原体积的1/7,继续将浓缩液真空干燥成干粉,用研钵研细后得到木瓜提取物干粉,木瓜提取物收率达到23.7%。 Preparation of papaya extract: Slice papaya and dry it at low temperature. Put the dried papaya slices in the container of the crushing extractor, add 75% hydrous ethanol equivalent to 6 times the weight of the raw materials and carry out crushing and extraction for 2 times, each extraction time is 3 minutes, the extract is suction filtered, and the filter residue is discarded. The combined extracts are flash-concentrated to 1/7 of the original volume using a vacuum thin-film concentration device below 70°C, and the concentrated solution is vacuum-dried into a dry powder, and then finely ground with a mortar to obtain a dry powder of papaya extract, papaya extract The yield reaches 23.7%.

九里香和柚子皮提取物的制备:取干燥的九里香叶和干燥的柚子果皮,按照重量比1:1混合,然后置破碎提取器的容器中,加入折合混合原料重量比6倍量100%乙醇进行破碎提取2次,每次提取时间为3分钟,将提取液抽滤,弃去滤渣,合并得到的提取液在60℃以下采用真空薄膜浓缩装置进行闪蒸浓缩至原体积的1/7,继续将浓缩液进行真空干燥成干粉,用研钵研细后得九里香和柚子皮提取物干粉,提取物收率达到17.4%。 Preparation of Jiulixiang and grapefruit peel extract: take dried Jiulixiang leaves and dried grapefruit peel, mix them according to the weight ratio of 1:1, then put them in the container of the broken extractor, add 100% of the amount equivalent to 6 times the weight ratio of the mixed raw materials The ethanol is crushed and extracted twice, each extraction time is 3 minutes, the extract is filtered with suction, the filter residue is discarded, and the combined extract is flashed and concentrated to 1/7 of the original volume by using a vacuum thin film concentration device below 60°C , continue vacuum-drying the concentrated solution into a dry powder, and use a mortar to grind finely to obtain a dry powder of the extract of Murata and pomelo peel, and the yield of the extract reaches 17.4%.

仙人掌粘液多糖的制备:取新鲜的仙人掌洗净,除刺去皮,切成小块,称重,置破碎提取器的容器中,加入仙人掌鲜重5倍量的蒸馏水,进行高速搅拌破碎3分钟,将破碎后的仙人掌粘浆转移出,进行高速离心分离,取上清液。将上清液进行减压浓缩至原体积的1/5,加入无水乙醇,边加边搅拌,4℃以下静止醇析。高速离心分离,弃去上清液,沉淀物低温干燥后,得到仙人掌粘液多糖,仙人掌粘液多糖的收率达到30.4%。 Preparation of cactus mucus polysaccharide: wash fresh cactus, remove thorns and peel, cut into small pieces, weigh, put in the container of broken extractor, add distilled water of 5 times the fresh weight of cactus, carry out high-speed stirring and crushing for 3 minutes , transfer the crushed cactus slime, perform high-speed centrifugation, and take the supernatant. Concentrate the supernatant under reduced pressure to 1/5 of the original volume, add absolute ethanol, stir while adding, static alcohol analysis below 4°C. High-speed centrifugation, discarding the supernatant, and drying the precipitate at low temperature to obtain the cactus mucus polysaccharide, and the yield of the cactus mucus polysaccharide reaches 30.4%.

黄秋葵果胶的制备:取洗净晾干的黄秋葵嫩果,以横段面切片后低温烘干。将烘干后的黄秋葵果实置于提取容器中,加入蒸馏水煎煮提取3次,每次70分钟,按照原料重量为1kg则蒸馏水的用量为9升的比例。进行高速离心分离,取上清液,得到的上清液在70℃条件下采用真空薄膜浓缩装置进行闪蒸浓缩至原体积的1/9,然后向浓缩液中加入95%的乙醇,使得含醇量达到80%,4℃以下静止醇析,出现大量的沉淀,高速离心分离,弃去上清液,收集沉淀物,40℃-50℃烘干,得到黄秋葵果胶,黄秋葵果胶的收率达到34.2%。 Preparation of okra pectin: take washed and dried tender okra fruit, cut into slices and dry at low temperature. Place the dried okra fruit in an extraction container, add distilled water to decoct and extract 3 times, each time for 70 minutes, according to the proportion of 9 liters of distilled water when the weight of the raw material is 1 kg. Carry out high-speed centrifugation, take the supernatant, and use a vacuum thin-film concentration device to flash-concentrate the obtained supernatant to 1/9 of the original volume at 70°C, and then add 95% ethanol to the concentrated solution to make it contain Alcohol content reaches 80%, static alcohol analysis below 4°C, a large amount of precipitation appears, high-speed centrifugation, discard the supernatant, collect the precipitate, dry at 40°C-50°C, and obtain okra pectin, the harvest of okra pectin The rate reached 34.2%.

实施例4 Example 4

该护肤类化妆品由木瓜提取物、九里香和柚子皮提取物、仙人掌粘液多糖、黄秋葵果胶、蜂王浆按照重量比15 :30:20 : 25 : 10的比例制成; The skin care cosmetics are made of papaya extract, mulberry and pomelo peel extracts, cactus mucus polysaccharide, okra pectin, and royal jelly in a weight ratio of 15:30:20:25:10;

木瓜提取物的制备:将木瓜切片后低温烘干,将干燥后的木瓜片置破碎提取器的容器中,加入折合原料重量比7倍量80%含水乙醇进行破碎提取2次,每次提取时间为1分钟,将提取液抽滤,弃去滤渣,合并得到的提取液在70℃以下采用真空薄膜浓缩装置进行闪蒸浓缩至原体积的1/7,继续将浓缩液真空干燥成干粉,用研钵研细后得到木瓜提取物干粉,木瓜提取物收率达到24.1%。 Preparation of papaya extract: Slice the papaya and dry it at low temperature, place the dried papaya slices in the container of the crushing extractor, add 80% hydrous ethanol equivalent to 7 times the weight ratio of the raw materials, and carry out crushing and extraction twice, each extraction time For 1 minute, the extract was suction-filtered, and the filter residue was discarded. The combined extract was flash-concentrated to 1/7 of the original volume using a vacuum thin-film concentration device below 70°C, and the concentrated solution was vacuum-dried to a dry powder. The papaya extract dry powder is obtained after grinding in a mortar, and the yield of the papaya extract reaches 24.1%.

九里香和柚子皮提取物的制备:取干燥的九里香叶和干燥的柚子果皮,按照重量比1:1混合,然后置破碎提取器的容器中,加入折合混合原料重量比6倍量80%乙醇进行破碎提取2次,每次提取时间为2分钟,将提取液抽滤,弃去滤渣,合并得到的提取液在60℃以下采用真空薄膜浓缩装置进行闪蒸浓缩至原体积的1/7,继续将浓缩液进行真空干燥成干粉,用研钵研细后得九里香和柚子皮提取物干粉,提取物收率达到20.3%。 The preparation of the extract of Jiulixiang and grapefruit peel: take dried Jiulixiang leaves and dried grapefruit peel, mix them according to the weight ratio of 1:1, then put them in the container of the broken extractor, add 80% of the amount equivalent to 6 times the weight ratio of the mixed raw materials The ethanol is crushed and extracted twice, each extraction time is 2 minutes, the extract is filtered with suction, the filter residue is discarded, and the combined extract is flashed and concentrated to 1/7 of the original volume by using a vacuum thin film concentration device below 60 °C , continue vacuum-drying the concentrated solution into a dry powder, and grind it finely with a mortar to obtain a dry powder of the extract of Murata and pomelo peel, and the yield of the extract reaches 20.3%.

仙人掌粘液多糖的制备:取新鲜的仙人掌洗净,除刺去皮,切成小块,称重,置破碎提取器的容器中,加入仙人掌鲜重8倍量的蒸馏水,进行高速搅拌破碎2分钟,将破碎后的仙人掌粘浆转移出,进行高速离心分离,取上清液。将上清液进行减压浓缩至原体积的1/5,加入无水乙醇,边加边搅拌,4℃以下静止醇析。高速离心分离,弃去上清液,沉淀物低温干燥后,得到仙人掌粘液多糖,仙人掌粘液多糖的收率达到32.1%。 Preparation of cactus mucus polysaccharide: wash fresh cactus, remove thorns and peel, cut into small pieces, weigh, put in the container of broken extractor, add distilled water of 8 times the fresh weight of cactus, carry out high-speed stirring and crushing for 2 minutes , transfer the crushed cactus slime, perform high-speed centrifugation, and take the supernatant. Concentrate the supernatant under reduced pressure to 1/5 of the original volume, add absolute ethanol, stir while adding, static alcohol analysis below 4°C. High-speed centrifugation, discarding the supernatant, and drying the precipitate at low temperature to obtain the cactus mucus polysaccharide, and the yield of the cactus mucus polysaccharide reaches 32.1%.

黄秋葵果胶的制备:取洗净晾干的黄秋葵嫩果,以横段面切片后低温烘干,将烘干后的黄秋葵果实置于提取容器中,加入蒸馏水煎煮提取3次,每次30分钟,按照原料重量为1kg则蒸馏水的用量为6升的比例。进行高速离心分离,取上清液。得到的上清液在70℃条件下采用真空薄膜浓缩装置进行闪蒸浓缩至原体积的1/6,然后向浓缩液中加入95%的乙醇,使得含醇量达到80%,4℃以下静止醇析,出现大量的沉淀,高速离心分离,弃去上清液,收集沉淀物,40℃-50℃烘干,得到黄秋葵果胶,黄秋葵果胶的收率达到28.7%。 Preparation of okra pectin: Take the washed and dried tender okra fruit, cut it into slices and dry it at low temperature, place the dried okra fruit in an extraction container, add distilled water and decoct it for 3 times, each time 30 Minutes, according to the raw material weight is 1kg then the consumption of distilled water is the ratio of 6 liters. Perform high-speed centrifugation and take the supernatant. The obtained supernatant was flash-concentrated to 1/6 of the original volume using a vacuum thin-film concentration device at 70°C, and then 95% ethanol was added to the concentrated liquid to make the alcohol content reach 80%, and it was static below 4°C Alcohol analysis, a large amount of precipitation occurs, high-speed centrifugation, discarding the supernatant, collecting the precipitate, drying at 40°C-50°C to obtain okra pectin, and the yield of okra pectin reaches 28.7%.

本发明的化妆品组合物中除含有以上植物提取物外,还包括助剂及载体,含有的化妆品助剂和载体可以包括防腐剂、抗氧剂、增稠剂、稳定剂、香味剂、成型剂、、乳化剂、醇类与酯类溶剂、油类、聚合物水等;具体助剂和载体可以是聚乙二醇、聚山梨醇酯、硬脂酸、环糊精、十二烷基硫酸钠、羟乙基纤维素、乙酸乙酯、苯甲酸苄酯、乙醇、丙二醇、二甲基硅油、甘油,蓖麻油等,本发明的化妆品组合物可以制作成的制剂,包括面乳、润肤露、嫩肤膏、护肤霜、面膜等,具体的制备工艺属于常规技术。 In addition to containing the above plant extracts, the cosmetic composition of the present invention also includes auxiliary agents and carriers. The cosmetic auxiliary agents and carriers contained may include preservatives, antioxidants, thickeners, stabilizers, flavoring agents, forming agents ,, emulsifiers, alcohol and ester solvents, oils, polymer water, etc.; specific additives and carriers can be polyethylene glycol, polysorbate, stearic acid, cyclodextrin, lauryl sulfate Sodium, hydroxyethyl cellulose, ethyl acetate, benzyl benzoate, ethanol, propylene glycol, simethicone, glycerin, castor oil, etc., the cosmetic composition of the present invention can be made into preparations, including facial milk, moisturizer Lotion, skin rejuvenation cream, skin cream, facial mask, etc., the specific preparation process belongs to conventional technology.

本发明涉及的一种护肤类化妆品的生产工艺是,先按照实施例中的配方的重量百分比例称取各组分,得到混合物料,然后将各种助剂和载体混合,在70-80℃左右的加热下进行磁力搅拌、混合、匀质化及乳化,然后将温度降至50℃-60℃,加入配制好的物料继续搅拌混合、匀质化及乳化,确保添加相完全溶解,使得乳化液无气泡出现为准,停止加热搅拌,放置至室温即得到成品。 The production process of a kind of skin care cosmetics involved in the present invention is to first weigh each component according to the weight percentage of the formula in the embodiment to obtain a mixed material, and then mix various auxiliary agents and carriers, Carry out magnetic stirring, mixing, homogenization and emulsification under left and right heating, then lower the temperature to 50°C-60°C, add the prepared materials and continue stirring, mixing, homogenization and emulsification to ensure that the added phase is completely dissolved and emulsified When the liquid has no bubbles, stop heating and stirring, and leave it to room temperature to obtain the finished product.

以下结合相应的试验数据进一步说明本发明的有益效果。 The beneficial effects of the present invention are further illustrated below in conjunction with corresponding test data.

试验1:增加皮肤弹性的润肤效果试验 Test 1: Emollient effect test for increasing skin elasticity

为证明其对面部皮肤的润肤效果,使用实施例1-4进行润肤效果试验。涂抹部位为面部,试验对象为50-60岁,皮肤弹性较差、皮肤干燥的女性。每次洁面后,每天在面部早晚两次进行涂抹,同时用手进行轻柔,坚持试用1个月,随访试验对象面部的润肤效果。 In order to prove its emollient effect on facial skin, the emollient effect test was carried out using Examples 1-4. The application site is the face, and the test subjects are 50-60-year-old women with poor skin elasticity and dry skin. After cleansing each time, apply it on the face twice a day in the morning and evening, and at the same time gently massage it with your hands. Try it for 1 month, and follow up the moisturizing effect on the face of the test subjects.

实施例1-4增加皮肤弹性的润肤效果试验 Embodiment 1-4 increases the emollient effect test of skin elasticity

实施例Example 受试人数Number of subjects 明显有效Obviously effective 有效efficient 无效invalid 有效率Efficient 实施例1Example 1 88 44 44 00 100%100% 实施例2Example 2 88 55 33 00 100%100% 实施例3Example 3 88 33 55 00 100%100% 实施例4Example 4 88 44 44 00 100%100%

试验2:改善皮肤皱纹的防皱效果试验 Test 2: Anti-wrinkle effect test for improving skin wrinkles

为证明其改善面部皮肤皱纹的效果,使用实施例1-4进行改善皮肤皱纹的防皱效果试验。涂抹部位为面部,试验对象为50-60岁,皮肤皱纹较多的女性。每次洁面后,在面部及眼睛的四周边缘每天早晚两次进行涂抹,同时用手进行轻柔与按摩,按摩时间3-4分钟,坚持试用2个月,随访试验对象面部及眼部皮肤皱纹的改善情况。 In order to prove its effect of improving facial skin wrinkles, the anti-wrinkle effect test of improving skin wrinkles was carried out using Examples 1-4. The application site is the face, and the test subjects are 50-60-year-old women with many skin wrinkles. After cleansing each time, apply it on the face and around the eyes twice a day, morning and evening, and at the same time gently massage with your hands for 3-4 minutes, keep trying it for 2 months, and follow up the test subjects for facial and eye skin wrinkles. improve the situation.

实施例1-4改善皮肤皱纹的防皱效果试验 Embodiment 1-4 Improves the anti-wrinkle effect test of skin wrinkles

实施例Example 受试人数Number of subjects 明显有效Obviously effective 有效efficient 无效invalid 有效率Efficient 实施例1Example 1 1010 44 55 11 90%90% 实施例2Example 2 1010 33 66 11 90%90% 实施例3Example 3 1212 55 55 22 83.3%83.3% 实施例4Example 4 1212 44 66 22 83.3%83.3%

试验3:抗氧化防辐射的防晒效果试验 Experiment 3: Sunscreen effect test for anti-oxidation and radiation protection

为证明其抗氧化、清除自由基的防晒效果,使用实施例1-4进行抗氧化防辐射的防晒效果试验。涂抹部位为面部,试验对象为20-40岁的女性。每次洁面后,在面部每天早进行涂抹,试用1个月,随访试验对象试用后抗辐射、防晒的应用效果。 In order to prove its sunscreen effect of anti-oxidation and scavenging free radicals, the sunscreen effect test of anti-oxidation and radiation protection was carried out using Examples 1-4. The application site is the face, and the test subjects are women aged 20-40. After cleansing the face each time, apply it on the face every morning for a trial period of 1 month, and follow up the application effects of anti-radiation and sunscreen on the test subjects after trial.

实施例1-4  抗氧化防辐射的防晒效果试验 Example 1-4 Sunscreen effect test of anti-oxidation and radiation protection

实施例Example 受试人数Number of subjects 明显有效Obviously effective 有效efficient 无效invalid 有效率Efficient 实施例1Example 1 66 33 33 00 100%100% 实施例2Example 2 66 33 33 00 100%100% 实施例3Example 3 66 22 33 11 83.3%83.3% 实施例4Example 4 66 22 33 11 83.3%83.3%

试验4:淡化色斑、分解黑色素的祛斑效果试验 Test 4: Freckle removal effect test of lightening spots and decomposing melanin

为证明其淡化面部色斑、分解黑色素的祛斑效果,使用实施例1-4进行淡化色斑、分解黑色素的祛斑效果试验。涂抹部位为面部,试验对象为30-45岁、面部有色斑的女性。每次洁面后,在整个面部每天早晚两次进行涂抹,同时对有色斑部位重点涂抹轻柔,坚持试用2个月,随访试验对象试用后祛斑效果。 In order to prove its freckle-removing effect of lightening facial spots and decomposing melanin, the freckle-removing effect test of lightening spots and decomposing melanin was carried out using Examples 1-4. The application site is the face, and the test subjects are 30-45-year-old women with pigmented spots on the face. After cleansing each time, apply it on the entire face twice a day in the morning and evening, and at the same time, apply it gently on the spots with spots. Keep trying it for 2 months, and follow up the test subjects for their freckle removal effect.

实施例1-4淡化色斑、分解黑色素的祛斑效果试验 Example 1-4 Lighten spots and decompose melanin's speckle-removing effect test

实施例Example 受试人数Number of subjects 明显有效Obviously effective 有效efficient 无效invalid 有效率Efficient 实施例1Example 1 1010 33 66 11 90%90% 实施例2Example 2 1010 44 55 11 90%90% 实施例3Example 3 1010 44 44 22 80%80% 实施例4Example 4 1010 33 55 22 80%80%

Claims (7)

1. 一种护肤类化妆品,其特征在于由木瓜提取物、九里香和柚子皮提取物、仙人掌粘液多糖、黄秋葵果胶、蜂王浆按照重量比10-20 : 20-40 : 10-40 : 10-30 : 10-20的比例制成; 1. A skin care cosmetic, characterized in that it consists of papaya extract, mulberry and pomelo peel extracts, cactus mucus polysaccharide, okra pectin, and royal jelly in a weight ratio of 10-20 : 20-40 : 10-40 : 10- 30: 10-20 ratio made; 所述的木瓜提取物采用以下方法制备:将木瓜切片后低温烘干,将干燥后的木瓜片置破碎提取器的容器中,按照木瓜重量1kg则含水乙醇5-8升的比例加入60%-80%含水乙醇进行破碎提取1-2次,每次提取时间为1-3分钟,将提取液抽滤,弃去滤渣,合并得到的提取液在70℃以下采用真空薄膜浓缩装置进行闪蒸浓缩至原体积的1/6-1/10,继续将浓缩液进行真空干燥成干粉,用研钵研细后得到木瓜提取物干粉; The papaya extract is prepared by the following method: slice the papaya and dry it at low temperature, place the dried papaya slices in a container of a crushing extractor, add 60%- 80% water-containing ethanol is crushed and extracted 1-2 times, each extraction time is 1-3 minutes, the extract is filtered with suction, the filter residue is discarded, and the combined extract is flashed and concentrated below 70°C using a vacuum thin film concentration device To 1/6-1/10 of the original volume, continue to vacuum-dry the concentrated solution into a dry powder, and grind it with a mortar to obtain a dry powder of papaya extract; 所述的九里香和柚子皮提取物采用以下方法制备:取干燥的九里香叶和干燥的柚子果皮,按照重量比1:1-2混合,然后置破碎提取器的容器中,按照原料重量1kg则含水乙醇6-8升的比例加入70%-100%乙醇进行破碎提取2-3次,每次提取时间为1-4分钟,将提取液抽滤,弃去滤渣,合并得到的提取液在60℃以下采用真空薄膜浓缩装置进行闪蒸浓缩至原体积的1/7-1/9,继续将浓缩液进行真空干燥成干粉,用研钵研细后得九里香和柚子皮提取物干粉; The described extract of mulberry and pomelo peel is prepared by the following method: take dried mulberry leaves and dried pomelo peel, mix them according to the weight ratio of 1:1-2, and then put them in the container of the crushing extractor, and mix them according to the weight of raw materials 1kg Then add 70%-100% ethanol to the ratio of 6-8 liters of aqueous ethanol to carry out crushing and extraction 2-3 times, each extraction time is 1-4 minutes, the extract is filtered with suction, the filter residue is discarded, and the combined extract is obtained in Below 60°C, use a vacuum thin film concentration device to flash concentrate to 1/7-1/9 of the original volume, continue to vacuum-dry the concentrated solution into a dry powder, and use a mortar to grind it finely to obtain a dry powder of Murata and pomelo peel extract; 所述的仙人掌粘液多糖采用以下方法制备:取新鲜的仙人掌洗净,除刺去皮,切成小块,称重,置破碎提取器的容器中,加入仙人掌鲜重4-8倍量的蒸馏水,进行高速搅拌破碎1-3分钟,将破碎后的仙人掌粘浆转移出,进行高速离心分离,取上清液,将上清液进行减压浓缩至原体积的1/3-1/6,加入无水乙醇,边加边搅拌,1-4℃下静止醇析,高速离心分离,弃去上清液,沉淀物低温干燥后,得到仙人掌粘液多糖; The described cactus mucus polysaccharide is prepared by the following method: take fresh cactus, wash, remove thorns and peel, cut into small pieces, weigh them, put them in a container of a broken extractor, and add distilled water of 4-8 times the fresh weight of the cactus , perform high-speed stirring and crushing for 1-3 minutes, transfer the crushed cactus slime, perform high-speed centrifugation, take the supernatant, and concentrate the supernatant under reduced pressure to 1/3-1/6 of the original volume, Add absolute ethanol, stir while adding, static alcohol analysis at 1-4°C, high-speed centrifugation, discard the supernatant, and dry the precipitate at low temperature to obtain cactus mucus polysaccharide; 所述的黄秋葵果胶采用以下方法制备:取洗净晾干的黄秋葵嫩果,以横段面切片后低温烘干,将烘干后的黄秋葵果实置于提取容器中,按照原料重量为1kg则蒸馏水的用量为6-10升的比例加入蒸馏水煎煮提取2-3次,每次30-90分钟,进行高速离心分离,取上清液;得到的上清液在60-70℃条件下采用真空薄膜浓缩装置进行闪蒸浓缩至原体积的1/6-1/10,然后向浓缩液中加入92-95%的乙醇,使得含醇量达到80%,1-4℃以下静止醇析,出现大量的沉淀,高速离心分离,弃去上清液,收集沉淀物,40℃-50℃烘干,得到黄秋葵果胶。 The described okra pectin is prepared by the following method: take the tender okra fruit that has been washed and dried, slice it in cross-section and then dry it at low temperature, place the dried okra fruit in an extraction container, and take the okra fruit according to the weight of the raw material as 1kg. The amount of distilled water is 6-10 liters, add distilled water to decoct and extract 2-3 times, each time for 30-90 minutes, carry out high-speed centrifugation, and take the supernatant; the obtained supernatant is used at 60-70°C The vacuum thin film concentrating device performs flash evaporation and concentration to 1/6-1/10 of the original volume, and then adds 92-95% ethanol to the concentrated solution to make the alcohol content reach 80%, and static alcohol analysis below 1-4°C, When a large amount of precipitation occurs, it is centrifuged at a high speed, the supernatant is discarded, the precipitate is collected, and dried at 40° C. to 50° C. to obtain okra pectin. 2. 如权利要求1所述的一种护肤类化妆品,其特征在于木瓜提取物、九里香和柚子皮提取物、仙人掌粘液多糖、黄秋葵果胶、蜂王浆的重量比为12-18 : 25-35 : 15-35 : 15-25 : 12-18。 2. A kind of skin care cosmetic as claimed in claim 1, characterized in that the weight ratio of papaya extract, mulberry and pomelo peel extract, cactus mucus polysaccharide, okra pectin, and royal jelly is 12-18: 25-35 : 15-35 : 15-25 : 12-18. 3. 如权利要求1所述的一种护肤类化妆品,其特征在于木瓜提取物、九里香和柚子皮提取物、仙人掌粘液多糖、黄秋葵果胶、蜂王浆的重量比为14-16 : 28-32 : 18-30 : 18-22 : 15-16。 3. A kind of skin care cosmetics as claimed in claim 1, characterized in that the weight ratio of papaya extract, mulberry and pomelo peel extract, cactus mucus polysaccharide, okra pectin, and royal jelly is 14-16: 28-32 : 18-30 : 18-22 : 15-16. 4. 如权利要求1所述的一种护肤类化妆品,其特征在于所述木瓜提取物的制备方法中:按照木瓜重量1kg则含水乙醇6-7升的比例加入65%-75%含水乙醇进行破碎提取1次,每次提取时间为2分钟,闪蒸浓缩至原体积的1/7-1/9。 4. A kind of skin care cosmetics as claimed in claim 1, characterized in that in the preparation method of the papaya extract: add 65%-75% hydrous ethanol according to the ratio of 6-7 liters of hydrous ethanol according to the weight of papaya 1kg Crushed and extracted once, each extraction time is 2 minutes, and flash concentrated to 1/7-1/9 of the original volume. 5. 如权利要求1所述的一种护肤类化妆品,其特征在于所述九里香和柚子皮提取物提取物的制备方法中:九里香叶和干燥的柚子果皮的重量比1:1.5混合,按照原料重量1kg则含水乙醇7升的比例加入80%-90%乙醇进行破碎提取,每次提取时间为2-3分钟,提取液闪蒸浓缩至原体积的1/8。 5. A kind of skin care cosmetics as claimed in claim 1, characterized in that in the preparation method of the extract of Murata and pomelo peel extract: the weight ratio of the leaves and dried grapefruit peel is mixed at 1:1.5, 80%-90% ethanol is added according to the ratio of 7 liters of water-containing ethanol according to the weight of the raw material for crushing and extraction. The extraction time is 2-3 minutes each time, and the extract is concentrated to 1/8 of the original volume by flash evaporation. 6. 如权利要求1所述的一种护肤类化妆品,其特征在于所述仙人掌粘液多糖的制备方法中:加入仙人掌鲜重5-7倍量的蒸馏水,进行高速搅拌破碎2分钟,将上清液进行减压浓缩至原体积的1/4-1/5。 6. A kind of skin care cosmetics as claimed in claim 1, characterized in that in the preparation method of the cactus mucus polysaccharide: add distilled water of 5-7 times the fresh weight of the cactus, carry out high-speed stirring and crushing for 2 minutes, and dissolve the supernatant The solution was concentrated under reduced pressure to 1/4-1/5 of the original volume. 7. 如权利要求1所述的一种护肤类化妆品,其特征在于所述黄秋葵果胶的制备方法中:按照原料重量为1kg则蒸馏水的用量为7-9升的比例加入蒸馏水煎煮提取,每次50-60分钟,上清液闪蒸浓缩至原体积的1/7-1/9,42℃-45℃烘干,得到黄秋葵果胶。 7. A kind of skin care cosmetics as claimed in claim 1, it is characterized in that in the preparation method of described okra pectin: add distilled water to decoct and extract according to the ratio that the consumption of distilled water is 7-9 liters according to raw material weight is 1kg, Each time for 50-60 minutes, the supernatant is concentrated by flash evaporation to 1/7-1/9 of the original volume, and dried at 42°C-45°C to obtain okra pectin.
CN201510146755.7A 2015-03-31 2015-03-31 skin care cosmetics Expired - Fee Related CN104721121B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201510146755.7A CN104721121B (en) 2015-03-31 2015-03-31 skin care cosmetics

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201510146755.7A CN104721121B (en) 2015-03-31 2015-03-31 skin care cosmetics

Publications (2)

Publication Number Publication Date
CN104721121A true CN104721121A (en) 2015-06-24
CN104721121B CN104721121B (en) 2018-06-15

Family

ID=53445924

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201510146755.7A Expired - Fee Related CN104721121B (en) 2015-03-31 2015-03-31 skin care cosmetics

Country Status (1)

Country Link
CN (1) CN104721121B (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105055299A (en) * 2015-09-27 2015-11-18 龚灿锋 Whitening and skin protecting emulsion
CN109700724A (en) * 2019-03-05 2019-05-03 陈伟伟 A kind of cosmetic face cream and preparation method thereof added with camellia flower extract
CN110538113A (en) * 2019-09-27 2019-12-06 广州环亚化妆品科技有限公司 Traditional Chinese medicine composition with moisturizing and hydrating effects and preparation method and application thereof
CN115038426A (en) * 2020-02-03 2022-09-09 加特弗斯股份公司 Murraya koenigii extract and application thereof in cosmetics

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102727630A (en) * 2012-06-29 2012-10-17 河南中医学院 Plant extract dripping pill
CN104042538A (en) * 2014-05-31 2014-09-17 青岛博泓海洋生物技术有限公司 Whitening and firming mask
CN104288061A (en) * 2014-11-09 2015-01-21 陈佩诗 A skin-beautifying and health-care massage liquid
CN104435240A (en) * 2014-05-19 2015-03-25 南京正亮医药科技有限公司 Kamuning massaging emulsion
CN104434617A (en) * 2014-07-22 2015-03-25 程远韶 Pawpaw nutritional mask

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102727630A (en) * 2012-06-29 2012-10-17 河南中医学院 Plant extract dripping pill
CN104435240A (en) * 2014-05-19 2015-03-25 南京正亮医药科技有限公司 Kamuning massaging emulsion
CN104042538A (en) * 2014-05-31 2014-09-17 青岛博泓海洋生物技术有限公司 Whitening and firming mask
CN104434617A (en) * 2014-07-22 2015-03-25 程远韶 Pawpaw nutritional mask
CN104288061A (en) * 2014-11-09 2015-01-21 陈佩诗 A skin-beautifying and health-care massage liquid

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105055299A (en) * 2015-09-27 2015-11-18 龚灿锋 Whitening and skin protecting emulsion
CN109700724A (en) * 2019-03-05 2019-05-03 陈伟伟 A kind of cosmetic face cream and preparation method thereof added with camellia flower extract
CN110538113A (en) * 2019-09-27 2019-12-06 广州环亚化妆品科技有限公司 Traditional Chinese medicine composition with moisturizing and hydrating effects and preparation method and application thereof
CN115038426A (en) * 2020-02-03 2022-09-09 加特弗斯股份公司 Murraya koenigii extract and application thereof in cosmetics
CN115038426B (en) * 2020-02-03 2024-04-26 加特弗斯股份公司 Murraya koenigii extract and its application in cosmetics

Also Published As

Publication number Publication date
CN104721121B (en) 2018-06-15

Similar Documents

Publication Publication Date Title
KR101373636B1 (en) Composition for improving condition of skin and scalp containing fermented extracts of herb mixture
CN104825351B (en) A kind of Lignum Aquilariae Resinatum whitening cleansing facial milk containing and preparation method thereof
CN102113987B (en) Cosmetic containing natural plant extractives and preparation method thereof
CN106667837A (en) Camellia oleifera component based body lotion and preparation method thereof
KR101054378B1 (en) Herbal soap composition and its manufacturing method
CN107937176A (en) A kind of high-efficiency antioxidant anti-acne handmade soap
CN105997827A (en) Compound camellia oil moisturizing liquid and preparation method thereof
CN105125466A (en) Freckle removing night cream and preparing method thereof
CN104473805A (en) Tea oil hair conditioner
CN104721121B (en) skin care cosmetics
KR20120060296A (en) Cosmetic Composition
KR101065799B1 (en) Manufacturing method of bath salt using sun salt
CN101637440A (en) Traditional Chinese medicine antidandruff and antipruritic shampoo and preparation method thereof
CN103462855B (en) Cosmetic containing American ginseng and longan and preparation method thereof
KR101606381B1 (en) Manufacture method of complex beauty Salt using solar salt processing environmentally friendly
CN104887603A (en) Skin moisturizer containing jasmine essential oil
CN107898749A (en) A kind of topical composition with skin-care effect and preparation method thereof
CN102188690B (en) Hair growth lotion and preparation method thereof
CN104398426A (en) Mask for treating common acne
CN106902062A (en) Eclipta arbor-vitae dark hair shampoo
CN107441340B (en) Hand and foot chap cream for relieving swelling, pain and itching and nourishing skin and preparation method thereof
CN105441230A (en) Camellia oil cold processed soap
KR20110119358A (en) Cosmetic composition for whitening containing Dong-a extract, preparation method thereof and cosmetics using this composition
CN104013555A (en) Herbal shampoo and preparation method thereof
CN107805559A (en) A kind of preparation method of high-efficiency antioxidant anti-acne handmade soap

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
CB03 Change of inventor or designer information

Inventor after: Cai Rongrong

Inventor after: Yuan Ke

Inventor after: Wang Guanghua

Inventor after: Yang Zhonghan

Inventor after: Niu Yingpeng

Inventor after: Jia Panpan

Inventor before: Yuan Ke

Inventor before: Wang Guanghua

Inventor before: Yang Zhonghan

Inventor before: Niu Yingpeng

Inventor before: Jia Panpan

CB03 Change of inventor or designer information
GR01 Patent grant
GR01 Patent grant
TR01 Transfer of patent right

Effective date of registration: 20190718

Address after: Building No. 1899 Shangshu Road, Fengxian District, Shanghai, 201414

Patentee after: Shanghai Aiying Health Technology Co.,Ltd.

Address before: 311800, No. 77, Puyang Road, Zhuji, Zhejiang, Shaoxing

Patentee before: JIYANG COLLEGE OF ZHEJIANG A&F UNIVERSITY

TR01 Transfer of patent right
PE01 Entry into force of the registration of the contract for pledge of patent right

Denomination of invention: A kind of skin care cosmetics

Effective date of registration: 20210323

Granted publication date: 20180615

Pledgee: Pacific Anxin Agricultural Insurance Co.,Ltd. Shanghai Fengxian Branch

Pledgor: Shanghai Aiying Health Technology Co.,Ltd.

Registration number: Y2021310000018

PE01 Entry into force of the registration of the contract for pledge of patent right
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20180615

CF01 Termination of patent right due to non-payment of annual fee