CN104667855A - Heat-conducting oil transport system for reaction kettle - Google Patents
Heat-conducting oil transport system for reaction kettle Download PDFInfo
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- CN104667855A CN104667855A CN201510027286.7A CN201510027286A CN104667855A CN 104667855 A CN104667855 A CN 104667855A CN 201510027286 A CN201510027286 A CN 201510027286A CN 104667855 A CN104667855 A CN 104667855A
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Abstract
The invention discloses a heat-conducting oil transport system for a reaction kettle. The heat-conducting oil transport system comprises the reaction kettle 9, a hot oil kettle 4 and an oil filling tank 7 which are connected by a pipeline valve and a heat-conducting oil pump 5 sequentially to form a heat-conducting oil transport device for the reaction kettle; heat-conducting oil in the hot oil kettle is conveyed into a reaction kettle jacket 13 by the heat-conducting oil pump 5; oil of the oil filling tank enters the hot oil kettle 4; a jacket of the hot oil kettle 4 is fully filled with the heat-conducting oil; the heat-conducting oil is used for heating materials in the reaction kettle jacket 13 in cycle; after reaction is ended, the cycle is stopped; the heat-conducting oil in the reaction kettle jacket 13 is discharged into the oil filling tank 7; and steam and cooling water enter the reaction kettle to cool the materials through a coil pipe. The reaction kettle jacket is supplied with the oil through the hot oil pump; uniform temperature rise is ensured; rapid cooling can also be carried out; product quality is improved; and dry combustion of the hot oil kettle and overheating of the heat-conducting oil can be prevented. The heat-conducting oil transport system is simple in structure and low in investment; the economic benefits can be increased; and the heat-conducting oil transport system has the relatively high promotional value.
Description
Technical field
The present invention relates to the production equipment of emulsifying agent, particularly a kind of reactor conduction oil induction system system, is a kind of improved system.
Background technology
In process of production, conduction oil in deep fat still is entered reactor by pipeline by Heat-transfer Oil Pump, and in deep fat still, the liquid level of conduction oil declines, heater meeting dry combustion method; Conduction oil temperature often exceeds technological temperature, bad control; After having reacted due to high temperature heat conductive oil in reacting kettle jacketing, material cooling velocity is slow, efficiency is low, and affects emulsifying agent and normally produce and product quality.
Summary of the invention
The object of the invention is in emulsifying agent production process, adopt the heater in deep fat still to heat conduction oil.The conduction oil of intensification is thrown in reacting kettle jacketing and is evenly heated up to material by recycling hot oil pump, the temperature of conduction oil is by temperature digital display transmitter, temperature signal is fed back on Central Control Room computer, when temperature exceeds technological temperature, several groups of heaters closed automatically by computer, allow conduction oil constant temperature at technological temperature; High temperature heat conductive oil after reacting completely in emptying reacting kettle jacketing, logical steam and cold water carry out fast cooling to emulsifying agent successively.
Solve the technical scheme of the technology of the present invention problem: a kind of reactor conduction oil conveying device, comprise reactor, deep fat still, repairing tank, reactor conduction oil conveying device is connected to form successively by pipeline, valve, Heat-transfer Oil Pump, reactor is connected with deep fat still by its oil-out pipeline, deep fat still is connected with repairing tank through conduction oil repairing pipe, deep fat still is connected with reactor bottom through Heat-transfer Oil Pump, reactor heat conductive oil inlet pipeline, is connected bottom reactor with repairing tank top.Side, described reactor top is provided with conduction oil outlet and steam, cooling water inlet; Described reactor bottom is provided with its heat conductive oil inlet pipeline, steam and cooling water outlet, heat conductive oil inlet and conduction oil drain, in described reactor, be provided with reacting kettle jacketing.Described deep fat still top is provided with deep fat still evacuation port and deep fat still oil-in, in deep fat still, is provided with deep fat kettle heater, is provided with deep fat still oil-out in deep fat still lower side.Described repairing tank 7 is provided with repairing tank oil-collecting hole above, has benefit tank nozzle, be provided with the oil-feed of repairing tank and evacuation port in repairing tank upper right side on the left of repairing tank.Conduction oil after intensification in deep fat still is delivered in reacting kettle jacketing by Heat-transfer Oil Pump, and the conduction oil in repairing tank flow into deep fat still, supplements deep fat still conduction oil and enters reacting kettle jacketing part, return deep fat still, circulating-heating emulsifying agent after being full of chuck; After reaction terminates, the high temperature heat conductive oil in emptying reacting kettle jacketing, passes into steam by coil pipe under vacuum conditions, cooling water comes to cool emulsifying agent fast successively, lower the temperature.
This technological improvement effectively solves that uneven, the local temperature of emulsifying agent heating is too high causes the problems such as the easy carbonization of conduction oil, easily decomposition, make reaction temperature accurate, adjustable, not only increase the reaction efficiency of esterification, and this mode of heating can ensure conduction oil constant temperature, extend the service life of conduction oil greatly; By the quick cooling of cooling water, effectively solve the problem that product oxidation color deepens, structure of the present invention is simple, small investment.After installing this device, can raise labour efficiency, product quality reaches requirement, and increases.
Accompanying drawing explanation
Fig. 1 is assembling front view of the present invention
Fig. 2 is the front view of reactor of the present invention
Fig. 3 is deep fat still front view of the present invention
Fig. 4 is repairing tank front view of the present invention
In figure: 1 reactor conduction oil outlet, 2 conduction oil repairing pipes, 3 deep fat still evacuated tube, 4 deep fat stills, 5 Heat-transfer Oil Pump, 6 reactor conduction oil oil inlet pipes, 7 repairing tanks, 8 oil-feed of repairing tank and evacuated tube, 9 reactors, 10 reactor temperature digital display transmitters, 11 reactor conduction oil outlets, 12 steam and cooling water inlet, 13 reacting kettle jacketings, 14 steam and cooling water outlet, 15 reactor heat conductive oil inlets, 16 reactor conduction oil drains, 17 deep fat still temperature digital display transmitters, 18 deep fat kettle heaters, 19 deep fat still evacuation ports, 20 deep fat still oil-outs, 21 deep fat still oil-ins, 22 repairing tank oil-collecting holes, 23 mend tank nozzle, 24 oil-feed of repairing tank and evacuation ports.
Detailed description of the invention
With reference to accompanying drawing 1-4: a kind of reactor heat conduction induction system, comprise reactor 9, deep fat still 4, repairing tank 7, reactor conduction oil conveying device is connected to form successively by pipeline valve Heat-transfer Oil Pump 5, described reactor 9 is connected with deep fat still 4 by its oil-out 1 pipeline, deep fat still 4 is connected with repairing tank 7 through conduction oil repairing pipe 2, deep fat still 4 is connected with reactor 4 bottom through Heat-transfer Oil Pump 5 reactor conduction oil oil inlet pipe 6, is connected bottom reactor 9 with repairing tank 7 top.Side, described reactor 9 top is provided with reactor temperature digital display transmitter 10, conduction oil outlet 11 and steam cooling water inlet 12; Described reactor 9 bottom is provided with its conduction oil oil inlet pipe 6, steam and cooling water outlet 14, reactor heat conductive oil inlet 15 and reactor conduction oil drain 16, in described reactor 9, be provided with reacting kettle jacketing 13.Described deep fat still 4 top is provided with deep fat still temperature digital display transmitter 17, and deep fat still evacuation port 19 and deep fat still oil-in 21, be provided with deep fat kettle heater 18 in deep fat still, is provided with deep fat still oil-out 20 in deep fat still lower side.Described repairing tank 7 is provided with repairing tank oil-collecting hole 22 above, has and mends tank nozzle 23, be provided with the oil-feed of repairing tank and evacuation port 24 in repairing tank upper right side on the left of repairing tank.
Conduction oil in deep fat still is delivered in reacting kettle jacketing 13 by Heat-transfer Oil Pump 5, and at this moment the oil of repairing tank enters into deep fat still 4, and ensure that conduction oil is full of deep fat still 4 all the time, conduction oil is at reacting kettle jacketing 13 Inner eycle heated material.React complete, stop circulation, the conduction oil in reacting kettle jacketing 13 is put to repairing tank 7, then steam, cooling water are entered in reactor by coil pipe and material is cooled.
Claims (4)
1. a reactor conduction oil induction system, comprise reactor (9), deep fat still (4), repairing tank (7), pass through pipeline, valve, Heat-transfer Oil Pump (5) connects to form reactor conduction oil conveying device successively, it is characterized in that: described reactor (9) is connected with deep fat still (4) by its oil-out (1) pipeline, deep fat still (4) is connected with repairing tank (7) through conduction oil repairing pipe (2), deep fat still (4) is through Heat-transfer Oil Pump (5), reactor conduction oil inflow pipeline (6) is connected with reactor (4) bottom, reactor (9) bottom is connected with repairing tank (7) top, . described reactor (9) side, top is provided with conduction oil outlet (11) and steam cooling water inlet (12), described reactor (9) bottom is provided with its conduction oil oil inlet pipe (6), steam and cooling water outlet (14), reactor heat conductive oil inlet (15) and reactor conduction oil drain (16).
2. a kind of reactor conduction oil induction system as claimed in claim 1, is characterized in that: in described reactor (9), be provided with reactor temperature digital display transmitter (10), reacting kettle jacketing (13).
3. a kind of reactor conduction oil induction system as claimed in claim 2, is characterized in that: described deep fat still (4) top is provided with deep fat still temperature digital display transmitter (17) deep fat still evacuation port (19) and deep fat still oil-in (21); Deep fat kettle heater (18) is provided with in deep fat still; Deep fat still oil-out (20) is provided with in deep fat still lower side.
4. a kind of reactor conduction oil induction system as claimed in claim 3, it is characterized in that: described repairing tank (7) is provided with repairing tank oil-collecting hole (22) above, have on the left of repairing tank and mend tank nozzle (23), be provided with the oil-feed of repairing tank and evacuation port (24) in repairing tank upper right side.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510027286.7A CN104667855A (en) | 2015-01-20 | 2015-01-20 | Heat-conducting oil transport system for reaction kettle |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510027286.7A CN104667855A (en) | 2015-01-20 | 2015-01-20 | Heat-conducting oil transport system for reaction kettle |
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| CN104667855A true CN104667855A (en) | 2015-06-03 |
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| CN201510027286.7A Pending CN104667855A (en) | 2015-01-20 | 2015-01-20 | Heat-conducting oil transport system for reaction kettle |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105498655A (en) * | 2015-12-15 | 2016-04-20 | 天津市鹏翔科技有限公司 | Heating system suitable for in-situ characterization |
| CN107303472A (en) * | 2016-04-18 | 2017-10-31 | 嘉峪关索通炭材料有限公司 | A kind of carbon paste cooling device |
| CN107537413A (en) * | 2016-06-29 | 2018-01-05 | 中国石油化工股份有限公司 | Olefin polymerization combined type method for controlling reaction temperature and device |
| CN113181868A (en) * | 2021-04-29 | 2021-07-30 | 新地能源工程技术有限公司 | Solid-phase tackifying reaction kettle and method |
| CN113639511A (en) * | 2021-08-25 | 2021-11-12 | 常州化工设计院有限公司 | Emergency cooling device for heat-conducting oil heating reaction kettle |
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| CN101480599A (en) * | 2008-12-30 | 2009-07-15 | 吕德斌 | Technique for heating and cooling material in reactor by heat carrier through jacket |
| CN203075951U (en) * | 2012-12-31 | 2013-07-24 | 中山市科田电子材料有限公司 | A kind of reaction kettle for preparing epoxy acrylate |
| CN203737191U (en) * | 2014-03-04 | 2014-07-30 | 上海旭创高分子材料有限公司 | Heat conduction oil anti-carbonization device for kneading machine |
| CN203990582U (en) * | 2014-01-02 | 2014-12-10 | 北京宝沃石油技术有限责任公司 | A kind of controllable temperature heating reactor |
| CN204084857U (en) * | 2014-07-31 | 2015-01-07 | 广东万木新材料科技有限公司 | A kind of conduction oil temperature-controlling system |
| CN204429279U (en) * | 2015-01-20 | 2015-07-01 | 湖南省南岭化工集团有限责任公司 | A kind of reactor conduction oil induction system |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101480599A (en) * | 2008-12-30 | 2009-07-15 | 吕德斌 | Technique for heating and cooling material in reactor by heat carrier through jacket |
| CN203075951U (en) * | 2012-12-31 | 2013-07-24 | 中山市科田电子材料有限公司 | A kind of reaction kettle for preparing epoxy acrylate |
| CN203990582U (en) * | 2014-01-02 | 2014-12-10 | 北京宝沃石油技术有限责任公司 | A kind of controllable temperature heating reactor |
| CN203737191U (en) * | 2014-03-04 | 2014-07-30 | 上海旭创高分子材料有限公司 | Heat conduction oil anti-carbonization device for kneading machine |
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| CN204429279U (en) * | 2015-01-20 | 2015-07-01 | 湖南省南岭化工集团有限责任公司 | A kind of reactor conduction oil induction system |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105498655A (en) * | 2015-12-15 | 2016-04-20 | 天津市鹏翔科技有限公司 | Heating system suitable for in-situ characterization |
| CN107303472A (en) * | 2016-04-18 | 2017-10-31 | 嘉峪关索通炭材料有限公司 | A kind of carbon paste cooling device |
| CN107537413A (en) * | 2016-06-29 | 2018-01-05 | 中国石油化工股份有限公司 | Olefin polymerization combined type method for controlling reaction temperature and device |
| CN107537413B (en) * | 2016-06-29 | 2019-07-30 | 中国石油化工股份有限公司 | Olefin polymerization combined type method for controlling reaction temperature and device |
| CN113181868A (en) * | 2021-04-29 | 2021-07-30 | 新地能源工程技术有限公司 | Solid-phase tackifying reaction kettle and method |
| CN113639511A (en) * | 2021-08-25 | 2021-11-12 | 常州化工设计院有限公司 | Emergency cooling device for heat-conducting oil heating reaction kettle |
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