CN104611107A - Excellent-performance wiredrawing fluid added with nanometer graphite, and preparation method for wiredrawing fluid - Google Patents
Excellent-performance wiredrawing fluid added with nanometer graphite, and preparation method for wiredrawing fluid Download PDFInfo
- Publication number
- CN104611107A CN104611107A CN201510011059.5A CN201510011059A CN104611107A CN 104611107 A CN104611107 A CN 104611107A CN 201510011059 A CN201510011059 A CN 201510011059A CN 104611107 A CN104611107 A CN 104611107A
- Authority
- CN
- China
- Prior art keywords
- parts
- nano
- graphite
- wiredrawing
- auxiliary agent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Lubricants (AREA)
Abstract
The invention discloses an excellent-performance wiredrawing fluid added with nanometer graphite. The wiredrawing fluid is characterized by being prepared from the following raw materials in parts by weight: 6-9 parts of nanometer graphite, 2-4 parts of monoethaneamine benzoate, 3.5-4.5 parts of glycerin, 1-2 parts of tetramerization castor oil plant grease, 1.5-2.5 parts of methylbenzotriazole, 3-5 parts of OP-10, 2-3 parts of triethanolamine borate, 2-4 parts of chlorcosane, 8-10 parts of nanometer bentonite, 5-7 parts of an addition agent, and 900-950 parts of deionized water. According to the method, the nanometer graphite, the nanometer bentonite and a surfactant are mixed in a grinding manner, and the wiredrawing fluid has favorable lubricating performance and wear resistance, and protects wiredrawing molds; the addition agent is added, so that the wiredrawing fluid has favorable wear resistance, dispersibility, lubrication and filming performance. The wiredrawing fluid disclosed by the invention has good properties, can reduce the working temperature of wiredrawing machines, and is suitable for high-speed wiredrawing machines.
Description
Technical field
The present invention relates to wire-drawing technology field, particularly a kind ofly add wire drawing liquid of the excellent performance of nano-graphite and preparation method thereof.
Background technology
Being determined by the processing characteristics of metal itself, metal wire-drawing processing is very high to the requirement of wire drawing liquid.First require that the oilness of wire drawing liquid is very high, only have oilness to meet processing request, the wire pulled out smoothly could not have cut, could carry out the processing of postorder to wire; Its two, wire, after Uniform Tension, through the flushing of high velocity flow, will be rinsed the wire drawing liquid of metallic surface well, in order to carrying out the processing of next process, therefore, requires that wire drawing liquid has excellent cleaning; Certainly, for metal, etching problem no less important, this just requires that wire drawing liquid has excellent barrier propterty, even if still have good protection function to aluminium wire under high strength processing conditions.
Graphite has excellent resistance to abrasion and oilness, and nano-graphite adds in wire drawing liquid by the present invention's design, makes wire drawing liquid possess good oilness, and protection wortle is not damaged.
Summary of the invention
The object of this invention is to provide and a kind ofly add wire drawing liquid of the excellent performance of nano-graphite and preparation method thereof.
In order to realize object of the present invention, the present invention is by following scheme implementation:
Add a wire drawing liquid for the excellent performance of nano-graphite, be made up of the raw material of following weight part: nano-graphite 6-9, monoethanolamine benzoate 2-4, glycerine 3.5-4.5, four poly-castor-oil plant fat 1-2, methyl benzotriazazole 1.5-2.5, OP-10 3-5, triethanolamine borate 2-3, clorafin 2-4, nano-bentonite 8-10, auxiliary agent 5-7, deionized water 900-950;
Described auxiliary agent is made up of the raw material of following weight part: granular graphite 2-4, nano diatomite 2.5-3.5, bisphenol a dimethacrylate 1-2, sulfuration Oleum Gossypii semen 2-2.5, Lauryl Alcohol ester 2-3, anilinomethyl triethoxysilane 1-1.5, Oleum Bupleuri 1-2, pull open powder 3-4, water 90-94; Preparation method be first by granular graphite, nano diatomite, Oleum Bupleuri, pull open powder and add in the water of half amount, grinding 1-2 hour, then slowly adds all the other remaining components, is slowly heated to 70 DEG C-80 DEG C, stirring reaction 30-50 minute under 300-500 rev/min of condition, is cooled to room temperature and get final product.
A kind of wire drawing liquid adding the excellent performance of nano-graphite of the present invention, be made up of following concrete steps:
(1) nano-graphite, nano-bentonite, OP-10 are mixed, add appropriate deionized water, be heated to 30 DEG C-35 DEG C, grinding 30-40 minute, obtain mixing A material;
(2) all the other remaining components except auxiliary agent are joined in reactor, be uniformly mixed, be slowly heated to 55 DEG C-65 DEG C, insulation 1-1.5 hour, obtain mixing B material;
(3) slowly joined while stirring in mixing A material by the mixing B of insulation material, add auxiliary agent after fully stirring, 600-800 rev/min of lower stirring reaction 40-60 minute, is cooled to room temperature and get final product.
Excellent effect of the present invention is: nano-graphite, nano-bentonite are mixed with tensio-active agent by lapping mode by the present invention, there is good oilness and wear resistance, protect wortle, add auxiliary agent, there is good wear-resistant, dispersion, lubrication, film-forming properties; Properties of the present invention is all excellent, and this product can reduce drawing wire machine working temperature, is applicable to high speed wiredrawing bench.
Embodiment
Below by specific examples, the present invention is described in detail.
Add a wire drawing liquid for the excellent performance of nano-graphite, be made up of the raw material of following weight part (kilogram): nano-graphite 6, monoethanolamine benzoate 2, glycerine 3.5, four poly-castor-oil plant fat 1, methyl benzotriazazole 1.5, OP-10 3, triethanolamine borate 2, clorafin 2, nano-bentonite 8, auxiliary agent 5, deionized water 900;
Described auxiliary agent is made up of the raw material of following weight part (kilogram): granular graphite 2, nano diatomite 2.5, bisphenol a dimethacrylate 1, sulfuration Oleum Gossypii semen 2, Lauryl Alcohol ester 2, anilinomethyl triethoxysilane 1, Oleum Bupleuri 1, pull open powder 3, water 90; Preparation method be first by granular graphite, nano diatomite, Oleum Bupleuri, pull open powder and add in the water of half amount, grinding 1-2 hour, then slowly adds all the other remaining components, is slowly heated to 70 DEG C-80 DEG C, stirring reaction 30-50 minute under 300-500 rev/min of condition, is cooled to room temperature and get final product.
A kind of wire drawing liquid adding the excellent performance of nano-graphite of the present invention, be made up of following concrete steps:
(1) nano-graphite, nano-bentonite, OP-10 are mixed, add appropriate deionized water, be heated to 30 DEG C-35 DEG C, grinding 30-40 minute, obtain mixing A material;
(2) all the other remaining components except auxiliary agent are joined in reactor, be uniformly mixed, be slowly heated to 55 DEG C-65 DEG C, insulation 1-1.5 hour, obtain mixing B material;
(3) slowly joined while stirring in mixing A material by the mixing B of insulation material, add auxiliary agent after fully stirring, 600-800 rev/min of lower stirring reaction 40-60 minute, is cooled to room temperature and get final product.
Use the present embodiment wire drawing liquid, the highest drawing speed can reach 18m/sec.Concentrate the oil sump drain period to be 3 years, the unit oil sump drain period is 8 months, decreases liquid waste disposal and discharge, protects environment.
Claims (2)
1. one kind is added the wire drawing liquid of the excellent performance of nano-graphite, it is characterized in that, be made up of the raw material of following weight part: nano-graphite 6-9, monoethanolamine benzoate 2-4, glycerine 3.5-4.5, four poly-castor-oil plant fat 1-2, methyl benzotriazazole 1.5-2.5, OP-10 3-5, triethanolamine borate 2-3, clorafin 2-4, nano-bentonite 8-10, auxiliary agent 5-7, deionized water 900-950;
Described auxiliary agent is made up of the raw material of following weight part: granular graphite 2-4, nano diatomite 2.5-3.5, bisphenol a dimethacrylate 1-2, sulfuration Oleum Gossypii semen 2-2.5, Lauryl Alcohol ester 2-3, anilinomethyl triethoxysilane 1-1.5, Oleum Bupleuri 1-2, pull open powder 3-4, water 90-94; Preparation method be first by granular graphite, nano diatomite, Oleum Bupleuri, pull open powder and add in the water of half amount, grinding 1-2 hour, then slowly adds all the other remaining components, is slowly heated to 70 DEG C-80 DEG C, stirring reaction 30-50 minute under 300-500 rev/min of condition, is cooled to room temperature and get final product.
2. a kind of wire drawing liquid adding the excellent performance of nano-graphite according to claim 1, is characterized in that, be made up of following concrete steps:
(1) nano-graphite, nano-bentonite, OP-10 are mixed, add appropriate deionized water, be heated to 30 DEG C-35 DEG C, grinding 30-40 minute, obtain mixing A material;
(2) all the other remaining components except auxiliary agent are joined in reactor, be uniformly mixed, be slowly heated to 55 DEG C-65 DEG C, insulation 1-1.5 hour, obtain mixing B material;
(3) slowly joined while stirring in mixing A material by the mixing B of insulation material, add auxiliary agent after fully stirring, 600-800 rev/min of lower stirring reaction 40-60 minute, is cooled to room temperature and get final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510011059.5A CN104611107A (en) | 2015-01-10 | 2015-01-10 | Excellent-performance wiredrawing fluid added with nanometer graphite, and preparation method for wiredrawing fluid |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510011059.5A CN104611107A (en) | 2015-01-10 | 2015-01-10 | Excellent-performance wiredrawing fluid added with nanometer graphite, and preparation method for wiredrawing fluid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104611107A true CN104611107A (en) | 2015-05-13 |
Family
ID=53145761
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510011059.5A Pending CN104611107A (en) | 2015-01-10 | 2015-01-10 | Excellent-performance wiredrawing fluid added with nanometer graphite, and preparation method for wiredrawing fluid |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104611107A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105482887A (en) * | 2015-11-30 | 2016-04-13 | 安徽创奇乐智能游乐设备有限公司 | Water-based nanometer tungsten disulfide isothermal die forging lubricant for high load and preparation method thereof |
| CN106883913A (en) * | 2017-02-07 | 2017-06-23 | 河北纳泰化工有限公司 | A kind of nano modification metal wire-drawing powder and preparation method thereof |
| CN110756996A (en) * | 2019-10-29 | 2020-02-07 | 宁波四维尔工业有限责任公司 | Wire drawing process for automobile label |
| CN116925839A (en) * | 2023-07-28 | 2023-10-24 | 浙江创特新材科技有限公司 | A method for preparing drawing graphite emulsion for high-strength fine tungsten wire |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103614203A (en) * | 2013-10-21 | 2014-03-05 | 全威（铜陵）铜业科技有限公司 | Aluminium drawing fluid and preparation method thereof |
| CN104263486A (en) * | 2014-09-09 | 2015-01-07 | 安徽旺达铜业发展有限公司 | Water-based metal wire drawing liquid with good lubricating effect and preparation method thereof |
| CN104263484A (en) * | 2014-09-09 | 2015-01-07 | 安徽旺达铜业发展有限公司 | High-cooling-property environment-friendly metal wire drawing solution and preparation method thereof |
| CN104263485A (en) * | 2014-09-09 | 2015-01-07 | 安徽旺达铜业发展有限公司 | Antiwear-additive-added aluminum wire drawing solution with bactericidal action and preparation method thereof |
-
2015
- 2015-01-10 CN CN201510011059.5A patent/CN104611107A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103614203A (en) * | 2013-10-21 | 2014-03-05 | 全威（铜陵）铜业科技有限公司 | Aluminium drawing fluid and preparation method thereof |
| CN104263486A (en) * | 2014-09-09 | 2015-01-07 | 安徽旺达铜业发展有限公司 | Water-based metal wire drawing liquid with good lubricating effect and preparation method thereof |
| CN104263484A (en) * | 2014-09-09 | 2015-01-07 | 安徽旺达铜业发展有限公司 | High-cooling-property environment-friendly metal wire drawing solution and preparation method thereof |
| CN104263485A (en) * | 2014-09-09 | 2015-01-07 | 安徽旺达铜业发展有限公司 | Antiwear-additive-added aluminum wire drawing solution with bactericidal action and preparation method thereof |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105482887A (en) * | 2015-11-30 | 2016-04-13 | 安徽创奇乐智能游乐设备有限公司 | Water-based nanometer tungsten disulfide isothermal die forging lubricant for high load and preparation method thereof |
| CN106883913A (en) * | 2017-02-07 | 2017-06-23 | 河北纳泰化工有限公司 | A kind of nano modification metal wire-drawing powder and preparation method thereof |
| CN110756996A (en) * | 2019-10-29 | 2020-02-07 | 宁波四维尔工业有限责任公司 | Wire drawing process for automobile label |
| CN116925839A (en) * | 2023-07-28 | 2023-10-24 | 浙江创特新材科技有限公司 | A method for preparing drawing graphite emulsion for high-strength fine tungsten wire |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104120010B (en) | A kind of excellent performance intermetallic composite coating aqueous cutting fluid and preparation method thereof | |
| CN103865622B (en) | Complete synthesis water-based stainless steel coolant, preparation method and using method thereof | |
| CN104611107A (en) | Excellent-performance wiredrawing fluid added with nanometer graphite, and preparation method for wiredrawing fluid | |
| CN104263484A (en) | High-cooling-property environment-friendly metal wire drawing solution and preparation method thereof | |
| CN104120015B (en) | Cutting fluid that a kind of antirust, anti-corrosive lubricity cooling is good and preparation method thereof | |
| CN104120006A (en) | Excellent-antiwear-effect water-based cutting fluid and preparation method thereof | |
| CN104120009A (en) | Waterborne cutting liquid suitable for various metals and preparation method of cutting liquid | |
| CN103614186A (en) | Wire drawing liquid specially used for metal wires and preparation method of the liquid | |
| CN104327929A (en) | High-abrasion resistance water-based cutting fluid and preparation method thereof | |
| CN104263486A (en) | Water-based metal wire drawing liquid with good lubricating effect and preparation method thereof | |
| CN104263483A (en) | Efficient environment-friendly water-based copper wire-drawing liquor and preparation method thereof | |
| CN103614203A (en) | Aluminium drawing fluid and preparation method thereof | |
| CN105602694A (en) | Copper rod complete-synthesis coarse-drawing lubricating fluid and preparation method as well as use method thereof | |
| CN104120002B (en) | A kind of cutting fluid with antibacterial and mouldproof effect and preparation method thereof | |
| CN104293454A (en) | Nano aluminium nitride-added copper wire drawing liquid and preparation method thereof | |
| CN104611105A (en) | Aluminum wiredrawing fluid with nanometer titanium dioxide, and preparation method for aluminum wiredrawing fluid | |
| CN104263485A (en) | Antiwear-additive-added aluminum wire drawing solution with bactericidal action and preparation method thereof | |
| CN104725843A (en) | Environment-friendly connecting piece | |
| CN104611104A (en) | Stainless steel wiredrawing fluid with excellent properties, and preparation method of stainless steel wiredrawing fluid | |
| CN104293456A (en) | Molybdenum disulfide-added stainless steel wire drawing liquid with good lubricity and preparation method thereof | |
| CN104109577A (en) | Metal cutting fluid having excellent antiwear and lubrication performances and preparation method thereof | |
| CN104212622A (en) | Special wire-drawing liquid for metal wire with good anti-rust effect and preparation method thereof | |
| CN104263487A (en) | Water-based aluminum product wire drawing solution with bactericidal action and preparation method thereof | |
| CN104120016B (en) | A kind of metalworking fluid with sterilizing and anti-foul effect and preparation method thereof | |
| CN104120012A (en) | Novel multifunctional cutting fluid with good performance and preparation method of novel multifunctional cutting fluid |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20150513 |
|
| RJ01 | Rejection of invention patent application after publication |